CN107904696A - One kind manufacture wig sensitization discoloration fiber and preparation method thereof - Google Patents
One kind manufacture wig sensitization discoloration fiber and preparation method thereof Download PDFInfo
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- CN107904696A CN107904696A CN201710999704.8A CN201710999704A CN107904696A CN 107904696 A CN107904696 A CN 107904696A CN 201710999704 A CN201710999704 A CN 201710999704A CN 107904696 A CN107904696 A CN 107904696A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D13/00—Complete machines for producing artificial threads
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- Chemical & Material Sciences (AREA)
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Abstract
The present invention relates to one kind to manufacture wig sensitization discoloration fiber and preparation method thereof, and fiber is prepared from the following raw materials in parts by weight：0.1 5 parts of 100 parts of base material, 1 10 parts of microcapsules sensitization discoloration powder, 1 10 parts of additive, 0.1 10 parts of pigment and dispersing wax, the PBT polyester section that the PTT polyester slices and 5 50% inherent viscosity that PET polyester slices that base material is 0.8 by 10 90% inherent viscosity, 5 50% inherent viscosity are 1.0 are 1.0 forms, and preparation method comprises the following steps：A, raw material removal moisture drying；B, Single screw extrusion；C, as-spun fibre cools down；D, oiling treatment；E, thermal finalization, finally packs.Sensitization discoloration fiber produced by the present invention can change color automatically according to the change of light environment, prepared wig product can more show the stylishness of wig, and the color shown by wig would know that the intensity of ultraviolet, remind people from injury of the intensive ultraviolet to human body.
Description
Technical field
The present invention relates to synthetic wig fiber technical field, and in particular to one kind manufacture wig with sensitization discoloration fiber and its
Preparation method.
Background technology
With economic level development and the raising of living standards of the people, wig has become fashion decorations important in the modern life
Product, the whole world is per annual consumption at 150,000 tons or so.With going from strength to strength for hair product industry, human hair material rate is increasingly
Few, domestic and international human hair resource is gradually reduced.Therefore, artificial hair product industry need find a kind of new human hair substitution of resources product.It is false
Hair is generally divided into animal ceratin fiber hair and artificial synthesized wig, animal ceratin wig generally comprise human hair, horse hair, horse
Hair on the neck, yak hair, oxtail etc., animal ceratin wig simulation quality is preferable, but animal ceratin fiber production is low, price is high and raw
Long period is longer, far can not meet the wilderness demand in market；Synthesizing macromolecule has cheap, and processing is simple, and synthesis is fine
For dimension except the general superior function with chemical fibre, such as intensity is high, light, quick-drying washable, elasticity is good, is not afraid of mould moth spy
Point, brings great convenience to human lives, and application in production is also extremely wide.
It is inflexible without expression activitiy but traditional wig fiber color is single, produced without true man's hair under light more
Become color effects, the wig that color can change according to the change of light environment not yet occur, based on this, design a kind of system
Fraud hair sensitization discoloration fiber and preparation method thereof, to make up blank of the market on the wig that changes colour, fills up international
Cosplayer animations market is directed to the novel demand of fashion.
The content of the invention
The purpose of the present invention is the deficiency for solution above-mentioned technical problem, there is provided one kind manufacture wig sensitization discoloration fiber
And preparation method thereof, obtained sensitization discoloration wig fiber can change color automatically according to the change of light environment.
To solve the deficiency of above-mentioned technical problem, used technical solution is the present invention：One kind manufacture wig is with photosensitive
Chameleon fibre, is prepared from the following raw materials in parts by weight：100 parts of base material, 1-10 parts of microcapsules sensitization discoloration powder, additive 1-10
0.1-5 parts of part, 0.1-10 parts of pigment and dispersing wax, the base material are cut by the PET polyester that the inherent viscosity of 10-90% is 0.8
The PBT polyester section group that the inherent viscosity of piece, the PTT polyester slices that the inherent viscosity of 5-50% is 1.0 and 5-50% is 1.0
Into.
As a kind of further optimization for manufacturing wig with sensitization discoloration fiber of the present invention：The additive for calcium carbonate,
One kind or any mixture in talcum powder, titanium dioxide, silica, diatomite, silicon powder, glass microballoon and mica powder.
As a kind of further optimization for manufacturing wig with sensitization discoloration fiber of the present invention：The particle diameter of the silicon powder is
3000 mesh, the particle diameter of silica is 4000 mesh.
As a kind of further optimization for manufacturing wig with sensitization discoloration fiber of the present invention：The microcapsules sensitization discoloration powder
For high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C.
As a kind of further optimization for manufacturing wig with sensitization discoloration fiber of the present invention：The addition of the dispersing wax is
2 parts, the molecular weight of dispersing wax is 2000-5000.
The above-mentioned manufacture wig preparation method of sensitization discoloration fiber, comprises the following steps：
A, raw material are taken according to parts by weight, the removal moisture drying at a temperature of 80-150 DEG C respectively by raw material, filters particle surface
Metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair
As-spun fibre is cooled down；
D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and is drawn
Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300-
1000m/min；
Or drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae
Finish is added to oil to fiber；
E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel
Filament in sink is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine
It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
As a kind of further optimization for manufacturing wig with the preparation method of sensitization discoloration fiber of the present invention：The step b
Spinneret melting extrusion of the middle as-spun fibre by spinneret orifice for 0.1-1.4mm.
As a kind of further optimization for manufacturing wig with the preparation method of sensitization discoloration fiber of the present invention：The step d
In the oil finish that uses for one kind in polyethers based compound, fatty acid ester based compound and organic amine salt based compound or appoint
Meaning mixture.
As a kind of further optimization for manufacturing wig with the preparation method of sensitization discoloration fiber of the present invention：The step e
Draw ratio during middle stretching is controlled in 1.5-8.0.
Beneficial effect
First, sensitization discoloration fiber of the invention can change color, prepared wig automatically according to the change of light environment
Product can more show the animation wide market such as the stylishness of wig, Europe, China and Japan, fill up the world
Cosplayer animations market is directed to the novel demand of fashion；
2nd, according to the intensity of ultraviolet color can occur for the prepared wig product of sensitization discoloration fiber of the invention
Change, enables the color that the user of wig is shown by wig to know the intensity of ultraviolet, reminds people from strong ultraviolet
Injury of the line to human body；
3rd, sensitization discoloration fiber of the invention selects the PTT that PET polyester slices, inherent viscosity that inherent viscosity is 0.8 are 1.0
Polyester slice and the PBT polyester section that inherent viscosity is 1.0 are used as base material, and obtained fiber flexibility is good, cardability, heatproof
Property, shaping persistence and the excellent protrusion of elasticity, and the elongation at break of fiber is big, using made of the wig fiber of the present invention
Wig product easily combs in use, and molding effect is lasting；
4th, a certain proportion of additive and dispersing wax are added in sensitization discoloration fiber of the invention, is 0.8 with inherent viscosity
The PBT polyester section that the PTT polyester slices and inherent viscosity that PET polyester slices, inherent viscosity are 1.0 are 1.0 cooperates,
Obtained wig fibre matting degree and smoothness are preferable, and there is manufactured wig product good shaded effect and vision to imitate
Fruit, can effectively protect human body from uv damage and strengthen the aesthetic feeling of wig product.
5th, the present invention is in the preparation process of sensitization discoloration fiber, for base material and additive and the characteristic of dispersing wax,
Drying temperature, single-screw extrusion temperature, cooling temperature and draft temperature to raw material are particularly limited to, a series of
At a temperature of handled, obtained photosensitive wig fibre strength is high, and elasticity is good, and resistance to elevated temperatures is preferable.
Embodiment
Further technical scheme is illustrated below in conjunction with embodiment.
Embodiment 1
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 20 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 40 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 40 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh to add agent）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned original
The material removal moisture drying at a temperature of 100 DEG C respectively, filters particle surface metallic dust and impurity, makes the water content control of raw material
In 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 15 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound）, the nascent fibre after oiling treatment
Dimension silk is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature that drawing-off is controlled in drawing process is
100 DEG C, rotating speed 600m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 10m/min, is finally packed.
Embodiment 2：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 10 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 45 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 45 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
2 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silica that particle diameter is 4000 mesh to add agent）, 0.5 part of 0.5 part of pigment and dispersing wax（Dispersing wax selects molecular weight to exist
The Tissuemat E of 2000-5000）, by the removal moisture drying at a temperature of 8 DEG C respectively of above-mentioned raw material, filter particle surface metallic dust
And impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is fatty acid ester based compound）, it is first after oiling treatment
Raw filament is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 60 DEG C DEG C, rotating speed 300m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 120 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 3m/min, is finally packed.
Embodiment 3：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 30 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 20 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 50 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
8 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh and the silica that particle diameter is 4000 mesh to add agent, both ratios are 1:1）, 5 parts of pigment with
And 5 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, by above-mentioned raw material respectively in 150 DEG C of temperature
The lower removal moisture drying of degree, filters particle surface metallic dust and impurity, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 25 DEG C；
D, oiled by oiling roller to as-spun fibre（Finish is organic amine salt based compound）Processing, it is first after oiling treatment
Raw filament is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 130 DEG C, rotating speed 1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 210 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 30m/min, is finally packed.
Embodiment 4：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 40 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 50 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 10 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is calcium carbonate, talcum powder and titanium dioxide to add agent, and the ratio of three is 1:1:1）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax
Molecular weight is selected in the Tissuemat E of 2000-5000）, by the removal moisture drying at a temperature of 90 DEG C respectively of above-mentioned raw material, filtering
Grain surface metal dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 220 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 20 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 80 DEG C, rotating speed is
800m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 180 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 15m/min, is finally packed.
Embodiment 5：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 50 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 15 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 35 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is silica, diatomite, silicon powder, glass microballoon and mica powder to add agent, and five ratio is 1:1:1:1:1）, 2 parts of pigment
And 2 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, by above-mentioned raw material respectively at 100 DEG C
At a temperature of removal moisture drying, filter particle surface metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 6：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 60 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 30 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 10 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is calcium carbonate, talcum powder, titanium dioxide, silica and diatomite to add agent, and five ratio is 1:1:1:1:1）, 2 parts of pigment
And 2 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, by above-mentioned raw material respectively at 100 DEG C
At a temperature of removal moisture drying, filter particle surface metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 7
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 70 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 10 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 20 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh to add agent）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned original
The material removal moisture drying at a temperature of 100 DEG C respectively, filters particle surface metallic dust and impurity, makes the water content control of raw material
In 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60 DEG C, drafting multiple 1.5, and oil is added in hot water storgae
Agent oils fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
The ratio of person is 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 120 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 3m/min, is finally packed.
Embodiment 8：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 80 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 10 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 10 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
2 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silica that particle diameter is 4000 mesh to add agent）, 0.5 part of 0.5 part of pigment and dispersing wax（Dispersing wax selects molecular weight to exist
The Tissuemat E of 2000-5000）, by the removal moisture drying at a temperature of 8 DEG C respectively of above-mentioned raw material, filter particle surface metallic dust
And impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 80 DEG C, drafting multiple 4, and finish is added in hot water storgae
Oil to fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 160 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 3-30m/min, is finally packed.
Embodiment 9：
A kind of manufacture wig its preparation method of sensitization discoloration fiber, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 90 parts of PET polyester slices（Optional particle shape also may be used
Select powder morphology）, inherent viscosity be 1.0 5 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 5 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
8 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh and the silica that particle diameter is 4000 mesh to add agent, both ratios are 1:1）, 5 parts of pigment with
And 5 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, by above-mentioned raw material respectively in 150 DEG C of temperature
The lower removal moisture drying of degree, filters particle surface metallic dust and impurity, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 100 DEG C, drafting multiple 6, and finish is added in hot water storgae
Oil to fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 210 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 30m/min, is finally packed.
The above described is only a preferred embodiment of the present invention, not make limitation in any form to the present invention, though
So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, without departing from the scope of the present invention, when the technology contents using the disclosure above make out a little change or repair
The equivalent embodiment for equivalent variations is adornd, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content
Any simple modification, equivalent change and modification made to above example, in the range of still falling within technical solution of the present invention.
Claims (9)
1. one kind manufacture wig sensitization discoloration fiber, it is characterised in that：It is prepared from the following raw materials in parts by weight：Base material 100
Part, 1-10 parts of microcapsules sensitization discoloration powder, 1-10 parts of additive, 0.1-10 parts of pigment and 0.1-5 parts of dispersing wax, the base material
The PTT polyester slices and 5- that the PET polyester slices for being 0.8 by the inherent viscosity of 10-90%, the inherent viscosity of 5-50% are 1.0
The PBT polyester section composition that 50% inherent viscosity is 1.0.
A kind of 2. manufacture wig sensitization discoloration fiber as claimed in claim 1, it is characterised in that：The additive is carbonic acid
One kind or any mixing in calcium, talcum powder, titanium dioxide, silica, diatomite, silicon powder, glass microballoon and mica powder
Thing.
A kind of 3. manufacture wig sensitization discoloration fiber as claimed in claim 2, it is characterised in that：The particle diameter of the silicon powder is
3000 mesh, the particle diameter of silica is 4000 mesh.
A kind of 4. manufacture wig sensitization discoloration fiber as claimed in claim 1, it is characterised in that：The microcapsules sensitization discoloration
Powder is high temperature resistant sensitization discoloration powder, its temperature resistant range is 160-230 DEG C.
A kind of 5. manufacture wig sensitization discoloration fiber as claimed in claim 1, it is characterised in that：The addition of the dispersing wax
For 2 parts, the molecular weight of dispersing wax is 2000-5000.
A kind of 6. preparation method for manufacturing wig sensitization discoloration fiber as claimed in claim 1, it is characterised in that：Including following
Step：
A, raw material are taken according to parts by weight, the removal moisture drying at a temperature of 80-150 DEG C respectively by raw material, filters particle surface
Metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair
As-spun fibre is cooled down；
D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and is drawn
Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300-
1000m/min；
Or drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae
Finish is added to oil to fiber；
E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel
Filament in sink is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine
It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
A kind of 7. preparation method for manufacturing wig sensitization discoloration fiber as claimed in claim 6, it is characterised in that：The step
Spinneret melting extrusion of the as-spun fibre by spinneret orifice for 0.1-1.4mm in b.
A kind of 8. preparation method for manufacturing wig sensitization discoloration fiber as claimed in claim 6, it is characterised in that：The step
Oil in d the finish that uses for one kind in polyethers based compound, fatty acid ester based compound and organic amine salt based compound or
Any mixture.
A kind of 9. preparation method for manufacturing wig sensitization discoloration fiber as claimed in claim 6, it is characterised in that：The step
Draw ratio when being stretched in d by drafting machine is controlled in 1.5-8.0.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710999704.8A CN107904696A (en) | 2017-10-24 | 2017-10-24 | One kind manufacture wig sensitization discoloration fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710999704.8A CN107904696A (en) | 2017-10-24 | 2017-10-24 | One kind manufacture wig sensitization discoloration fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107904696A true CN107904696A (en) | 2018-04-13 |
Family
ID=61841599
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710999704.8A Withdrawn CN107904696A (en) | 2017-10-24 | 2017-10-24 | One kind manufacture wig sensitization discoloration fiber and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107904696A (en) |
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Cited By (4)
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| CN110656397A (en) * | 2019-11-22 | 2020-01-07 | 湖州隆之源纺织科技有限公司 | Preparation method of photochromic modified polyester fiber |
| CN111593422A (en) * | 2020-05-14 | 2020-08-28 | 许昌鸿洋生化实业发展有限公司 | PETG (polyethylene terephthalate glycol) -based rapid-forming wig fiber and preparation process thereof |
| CN111593422B (en) * | 2020-05-14 | 2021-06-29 | 许昌鸿洋生化实业发展有限公司 | PETG (polyethylene terephthalate glycol) -based rapid-forming wig fiber and preparation process thereof |
| WO2021227852A1 (en) * | 2020-05-14 | 2021-11-18 | 许昌鸿洋生化实业发展有限公司 | Petg-based rapidly-formed wig fiber and preparation process therefor |
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