CN107904695A - A kind of artificial nylon wig fiber of high temperature resistant and preparation method thereof - Google Patents
A kind of artificial nylon wig fiber of high temperature resistant and preparation method thereof Download PDFInfo
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- CN107904695A CN107904695A CN201710999686.3A CN201710999686A CN107904695A CN 107904695 A CN107904695 A CN 107904695A CN 201710999686 A CN201710999686 A CN 201710999686A CN 107904695 A CN107904695 A CN 107904695A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/12—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyamide as constituent
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
- D01D5/088—Cooling filaments, threads or the like, leaving the spinnerettes
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
- D01D5/14—Stretch-spinning methods with flowing liquid or gaseous stretching media, e.g. solution-blowing
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/06—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
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Abstract
The present invention relates to artificial nylon wig fiber of a kind of high temperature resistant and preparation method thereof, fiber is prepared from the following raw materials in parts by weight：Inherent viscosity is 2.55 0.1 5 parts of 100 parts of PA nylon chips, 0.5 part of titanium dioxide, 6 parts of talcum powder, 0.1 10 parts of pigment and dispersing wax, and preparation method comprises the following steps：A, raw material removal moisture drying；B, Single screw extrusion；C, as-spun fibre cools down；D, oiling treatment；E, thermal finalization, finally packs.Fibre fire resistant produced by the present invention, has good smoothness, excellent hydrofuge gas permeability and true man's hair natural gloss of uniqueness, and free from environmental pollution in preparation process, does not produce waste water and discarded object.
Description
Technical field
The present invention relates to synthetic wig fiber technical field, and in particular to a kind of artificial nylon wig fiber of high temperature resistant and its
Preparation method.
Background technology
With economic level development and the raising of living standards of the people, wig has become fashion decorations important in the modern life
Product, the whole world is per annual consumption at 150,000 tons or so.With going from strength to strength for hair product industry, human hair material rate is increasingly
Few, domestic and international human hair resource is gradually reduced.Therefore, artificial hair product industry need find a kind of new human hair substitution of resources product.It is false
Hair is generally divided into animal ceratin fiber hair and artificial synthesized wig, animal ceratin wig generally comprise human hair, horse hair, horse
Hair on the neck, yak hair, oxtail etc., animal ceratin wig simulation quality is preferable, but animal ceratin fiber production is low, price is high and raw
Long period is longer, far can not meet the wilderness demand in market, and with the rapid increase of domestic and international hair products demand, generation
Reinforcement of the various countries of boundary to environmental protection consciousness, the processing technique of natural human hair cause seriously to pollute to environment and water source, people
It is the final trend of hair products raw material that imitation hair fibe, which is made, as human hair substitute.
The content of the invention
The purpose of the present invention is to solve deficiency of the prior art, there is provided a kind of artificial nylon wig fiber of high temperature resistant and
Its preparation method, obtained fiber can have the true of good smoothness, excellent hydrofuge gas permeability and uniqueness with high temperature resistant
Human hair natural gloss, and it is free from environmental pollution in preparation process, do not produce waste water and discarded object.
To solve the deficiency of above-mentioned technical problem, used technical solution is the present invention：A kind of artificial nylon of high temperature resistant
Wig fiber, is prepared from the following raw materials in parts by weight：100 parts of PA nylon chips, the titanium dioxide 0.5 that inherent viscosity is 2.55
Part, 6 parts of talcum powder, 0.1-10 parts of pigment and 0.1-5 parts of dispersing wax, the temperature resistant range of the pigment is 180-350 DEG C.
Further optimization as a kind of artificial nylon wig fiber of high temperature resistant of the present invention：The titanium dioxide is chemical fiber grade
Titanium dioxide.
Further optimization as a kind of artificial nylon wig fiber of high temperature resistant of the present invention：The addition of the dispersing wax is
2 parts, the molecular weight of dispersing wax is 2000-5000.
Further optimization as a kind of artificial nylon wig fiber of high temperature resistant of the present invention：The particle size range of the talcum powder
For 1-5 μm.
The preparation method of the above-mentioned artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, the removal moisture drying at a temperature of 80-150 DEG C respectively by raw material, filters particle surface
Metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair
As-spun fibre is cooled down；
D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and is drawn
Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300-
1000m/min；
Or drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae
Finish is added to oil to fiber；
E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel
Filament in sink is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine
It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
Further optimization as a kind of preparation method of the artificial nylon wig fiber of high temperature resistant of the present invention：The step b
Spinneret melting extrusion of the middle as-spun fibre by spinneret orifice for 0.1-1.4mm.
Further optimization as a kind of preparation method of the artificial nylon wig fiber of high temperature resistant of the present invention：The step d
In the oil finish that uses for one kind in polyethers based compound, fatty acid ester based compound and organic amine salt based compound or appoint
Meaning mixture.
Further optimization as a kind of preparation method of the artificial nylon wig fiber of high temperature resistant of the present invention：The step e
Draw ratio during middle stretching is controlled in 1.5-8.0.
Beneficial effect
First, artificial nylon wig fiber of the invention can with high temperature resistant, have good smoothness, excellent hydrofuge gas permeability with
And unique true man send out natural gloss, and raw material are recyclable in preparation process reuses, free from environmental pollution, do not produce useless
Water and discarded object, can substitute true man's hair completely；
2nd, artificial nylon wig fibre abrasion of the invention is higher than other fibers, 10 times higher than cotton wearability, is sent out than true man
20 times high, when being stretched to 3-6%, elastic recovery rate is amenable to up to ten thousand foldings and scratches and not broken, can obviously improve up to 100%
Or avoid wearing the entanglement during use, long periods of wear is not easy the unrest of fold hair.
3rd, the PA nylon chips that wig fiber of the invention selection inherent viscosity is 2.55 are as base material, obtained fiber
Pliability is preferable, and the elongation at break of fiber is big, easy in use using wig product made of the wig fiber of the present invention
Comb, and molding effect is lasting；
4th, a certain proportion of titanium dioxide, talcum powder and dispersing wax are added in wig fiber of the invention, is with inherent viscosity
2.55 PA nylon chips cooperate, and obtained wig fiber is smoothness and hydrofuge gas permeability is preferable, and compares true man
Hair has good moth-resistant, corrosion resistance.
5th, the present invention is in the preparation process of wig fiber, for base material and titanium dioxide, talcum powder and dispersing wax
Characteristic, drying temperature, single-screw extrusion temperature, cooling temperature and draft temperature to raw material are particularly limited to,
Handled at a series of temperature, obtained photosensitive wig fibrous elasticity and elastic recovery are fabulous.
Embodiment
Further technical scheme is illustrated below in conjunction with embodiment.
Embodiment 1
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 2 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 2 parts of dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned raw material respectively 100
Removal moisture drying at a temperature of DEG C, filters particle surface metallic dust and impurity, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 15 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound）, the nascent fibre after oiling treatment
Dimension silk is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature that drawing-off is controlled in drawing process is
100 DEG C, rotating speed 600m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 10m/min, is finally packed.
Embodiment 2：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 0.5 part of pigment（Face
The temperature resistant range of material is 180-350 DEG C）And 0.5 part of dispersing wax（Dispersing wax selects molecular weight in the polyethylene of 2000-5000
Wax）, by the removal moisture drying at a temperature of 8 DEG C respectively of above-mentioned raw material, particle surface metallic dust and impurity are filtered, makes raw material
Water content control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is fatty acid ester based compound）, it is first after oiling treatment
Raw filament is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 60 DEG C DEG C, rotating speed 300m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 120 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 3m/min, is finally packed.
Embodiment 3：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 5 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 5 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, will
The removal moisture drying at a temperature of 150 DEG C respectively of above-mentioned raw material, filters particle surface metallic dust and impurity, makes the aqueous of raw material
Amount control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 25 DEG C；
D, oiled by oiling roller to as-spun fibre（Finish is organic amine salt based compound）Processing, it is first after oiling treatment
Raw filament is sent into drafting machine and is stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 130 DEG C, rotating speed 1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 210 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 30m/min, is finally packed.
Embodiment 4：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 2 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 2 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, will
The removal moisture drying at a temperature of 90 DEG C respectively of above-mentioned raw material, filters particle surface metallic dust and impurity, makes the aqueous of raw material
Amount control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 220 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 20 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 80 DEG C, rotating speed is
800m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 180 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 15m/min, is finally packed.
Embodiment 5：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 2 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 2 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, will
The removal moisture drying at a temperature of 100 DEG C respectively of above-mentioned raw material, filters particle surface metallic dust and impurity, makes the aqueous of raw material
Amount control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 6：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 2 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 2 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, will
The removal moisture drying at a temperature of 100 DEG C respectively of above-mentioned raw material, filters particle surface metallic dust and impurity, makes the aqueous of raw material
Amount control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and has
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 7
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 2 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 2 parts of dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned raw material respectively 100
Removal moisture drying at a temperature of DEG C, filters particle surface metallic dust and impurity, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60 DEG C, drafting multiple 1.5, and oil is added in hot water storgae
Agent oils fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
The ratio of person is 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 120 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 3m/min, is finally packed.
Embodiment 8：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 0.5 part of pigment（Face
The temperature resistant range of material is 180-350 DEG C）And 0.5 part of dispersing wax（Dispersing wax selects molecular weight in the polyethylene of 2000-5000
Wax）, by the removal moisture drying at a temperature of 8 DEG C respectively of above-mentioned raw material, particle surface metallic dust and impurity are filtered, makes raw material
Water content control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 80 DEG C, drafting multiple 4, and finish is added in hot water storgae
Oil to fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 160 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 3-30m/min, is finally packed.
Embodiment 9：
A kind of its preparation method of the artificial nylon wig fiber of high temperature resistant, comprises the following steps：
A, raw material are taken according to parts by weight, inherent viscosity is 2.55 100 parts of PA nylon chips（Optional particle shape also may be used
Select powder morphology）, 6 parts of talcum powder, 0.5 part of titanium dioxide（Titanium dioxide is chemical-fiber-grade titanium dioxide）, 5 parts of pigment（Pigment
Temperature resistant range be 180-350 DEG C）And 5 parts of dispersing wax（Dispersing wax selects molecular weight in the Tissuemat E of 2000-5000）, will
The removal moisture drying at a temperature of 150 DEG C respectively of above-mentioned raw material, filters particle surface metallic dust and impurity, makes the aqueous of raw material
Amount control is in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 100 DEG C, drafting multiple 6, and finish is added in hot water storgae
Oil to fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 210 DEG C by automaticity device for filtering water and carries out thermal finalization,
Speed of the control fiber tow in thermal finalization cabinet is 30m/min, is finally packed.
The above described is only a preferred embodiment of the present invention, not make limitation in any form to the present invention, though
So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, without departing from the scope of the present invention, when the technology contents using the disclosure above make out a little change or repair
The equivalent embodiment for equivalent variations is adornd, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content
Any simple modification, equivalent change and modification made to above example, in the range of still falling within technical solution of the present invention.
Claims (8)
- A kind of 1. artificial nylon wig fiber of high temperature resistant, it is characterised in that：It is prepared from the following raw materials in parts by weight：Inherent viscosity For 2.55 100 parts of PA nylon chips, 0.5 part of titanium dioxide, 6 parts of talcum powder, 0.1-10 parts of pigment and dispersing wax 0.1-5 Part, the temperature resistant range of the pigment is 180-350 DEG C.
- A kind of 2. artificial nylon wig fiber of high temperature resistant as claimed in claim 1, it is characterised in that：The titanium dioxide is chemical fibre Grade titanium dioxide.
- A kind of 3. artificial nylon wig fiber of high temperature resistant as claimed in claim 1, it is characterised in that：The addition of the dispersing wax For 0.3 part, the molecular weight of dispersing wax is 2000-5000.
- A kind of 4. artificial nylon wig fiber of high temperature resistant as claimed in claim 1, it is characterised in that：The particle diameter model of the talcum powder Enclose for 1-5 μm.
- A kind of 5. preparation method of the artificial nylon wig fiber of high temperature resistant as claimed in claim 1, it is characterised in that：Including following Step：A, raw material are taken according to parts by weight, the removal moisture drying at a temperature of 80-150 DEG C respectively by raw material, filters particle surface Metallic dust and impurity, make the water content control of raw material in 30-100ppm；B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair As-spun fibre is cooled down；D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and is drawn Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300- 1000m/min；Or drawing-off carries out as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae Finish is added to oil to fiber；E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel Filament in sink is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
- A kind of 6. preparation method of the artificial nylon wig fiber of high temperature resistant as claimed in claim 5, it is characterised in that：The step Spinneret melting extrusion of the as-spun fibre by spinneret orifice for 0.1-1.4mm in b.
- A kind of 7. preparation method of the artificial nylon wig fiber of high temperature resistant as claimed in claim 5, it is characterised in that：The step Oil in d the finish that uses for one kind in polyethers based compound, fatty acid ester based compound and organic amine salt based compound or Any mixture.
- A kind of 8. preparation method of the artificial nylon wig fiber of high temperature resistant as claimed in claim 5, it is characterised in that：The step Draw ratio when being stretched in d by drafting machine is controlled in 1.5-8.0.
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| CN201710999686.3A CN107904695A (en) | 2017-10-24 | 2017-10-24 | A kind of artificial nylon wig fiber of high temperature resistant and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710999686.3A CN107904695A (en) | 2017-10-24 | 2017-10-24 | A kind of artificial nylon wig fiber of high temperature resistant and preparation method thereof |
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| CN107904695A true CN107904695A (en) | 2018-04-13 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020073628A1 (en) * | 2018-10-12 | 2020-04-16 | 河南瑞贝卡发制品股份有限公司 | High-temperature-resistant polyamide fiber for high-quality artificial human hair wig and preparation method therefor |
| WO2020170921A1 (en) * | 2019-02-19 | 2020-08-27 | デンカ株式会社 | Artificial hair fiber |
| CN114381934A (en) * | 2022-02-16 | 2022-04-22 | 邵阳市美丽湘龙发制品有限公司 | Low-temperature processed wavy curly hair and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011246843A (en) * | 2010-05-27 | 2011-12-08 | Denki Kagaku Kogyo Kk | Fiber for artificial hair |
| CN102766962A (en) * | 2012-06-28 | 2012-11-07 | 吴江亚太化纺有限公司 | Anti-ultraviolet nylon fiber spinning process |
| CN102926024A (en) * | 2012-10-23 | 2013-02-13 | 许昌鸿洋生化实业发展有限公司 | Degradable polylactic acid fiber for wig and production process for polylactic acid fiber |
| CN104674366A (en) * | 2015-02-11 | 2015-06-03 | 浙江益南纤维科技有限公司 | Polyamide yarn production technology |
| CN105682497A (en) * | 2013-10-17 | 2016-06-15 | 电化株式会社 | Artificial hair fiber with shape memory function and shape restoring function, excellent flame retardance, and low gloss appearance |
-
2017
- 2017-10-24 CN CN201710999686.3A patent/CN107904695A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011246843A (en) * | 2010-05-27 | 2011-12-08 | Denki Kagaku Kogyo Kk | Fiber for artificial hair |
| CN102766962A (en) * | 2012-06-28 | 2012-11-07 | 吴江亚太化纺有限公司 | Anti-ultraviolet nylon fiber spinning process |
| CN102926024A (en) * | 2012-10-23 | 2013-02-13 | 许昌鸿洋生化实业发展有限公司 | Degradable polylactic acid fiber for wig and production process for polylactic acid fiber |
| CN105682497A (en) * | 2013-10-17 | 2016-06-15 | 电化株式会社 | Artificial hair fiber with shape memory function and shape restoring function, excellent flame retardance, and low gloss appearance |
| CN104674366A (en) * | 2015-02-11 | 2015-06-03 | 浙江益南纤维科技有限公司 | Polyamide yarn production technology |
Non-Patent Citations (2)
| Title |
|---|
| 李青山: "《着色配色技术手册》", 31 January 2016, 中国纺织出版社 * |
| 肖长发: "《化学纤维概论》", 30 June 2015, 中国纺织出版社 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020073628A1 (en) * | 2018-10-12 | 2020-04-16 | 河南瑞贝卡发制品股份有限公司 | High-temperature-resistant polyamide fiber for high-quality artificial human hair wig and preparation method therefor |
| WO2020170921A1 (en) * | 2019-02-19 | 2020-08-27 | デンカ株式会社 | Artificial hair fiber |
| JPWO2020170921A1 (en) * | 2019-02-19 | 2021-12-16 | デンカ株式会社 | Fiber for artificial hair |
| JP7344273B2 (en) | 2019-02-19 | 2023-09-13 | デンカ株式会社 | Fiber for artificial hair |
| CN114381934A (en) * | 2022-02-16 | 2022-04-22 | 邵阳市美丽湘龙发制品有限公司 | Low-temperature processed wavy curly hair and preparation method thereof |
| CN114381934B (en) * | 2022-02-16 | 2023-08-08 | 邵阳市美丽湘龙发制品有限公司 | Wave hair curler processed at low temperature and preparation method thereof |
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