CN107881582A - It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof - Google Patents
It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof Download PDFInfo
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- CN107881582A CN107881582A CN201710999256.1A CN201710999256A CN107881582A CN 107881582 A CN107881582 A CN 107881582A CN 201710999256 A CN201710999256 A CN 201710999256A CN 107881582 A CN107881582 A CN 107881582A
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- China
- Prior art keywords
- wig
- parts
- sensitization discoloration
- manufacture
- fiber
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G3/00—Wigs
- A41G3/0083—Filaments for making wigs
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/04—Pigments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
Abstract
The present invention relates to a kind of sensitization discoloration fiber for being used to manufacture wig and preparation method thereof, fiber is prepared from the following raw materials in parts by weight：0.1 5 parts of 100 parts of base material, 1 10 parts of microcapsules sensitization discoloration powder, 1 10 parts of additive, 0.1 10 parts of pigment and dispersing wax, preparation method comprises the following steps：A, raw material removal moisture drying；B, Single screw extrusion；C, as-spun fibre cools down；D, oiling treatment；E, thermal finalization, finally pack.Sensitization discoloration fiber produced by the present invention can change color automatically according to the change of photoenvironment, the stylishness of wig can more be shown by making obtained wig product, and the color shown by wig would know that the intensity of ultraviolet, remind people from injury of the intensive ultraviolet to human body.
Description
Technical field
The present invention relates to synthetic wig fiber technical field, and in particular to a kind of sensitization discoloration fiber for being used to manufacture wig
And preparation method thereof.
Background technology
With economic level development and the raising of living standards of the people, wig has turned into fashion decorations important in the modern life
Product, the whole world is per annual consumption at 150,000 tons or so.With going from strength to strength for hair product industry, human hair material rate is increasingly
Few, domestic and international human hair resource is gradually reduced.Therefore, artificial hair product industry need find a kind of new human hair substitution of resources product.It is false
Hair is generally divided into animal ceratin fiber hair and artificial synthesized wig, animal ceratin wig generally comprise human hair, horse hair, horse
Hair on the neck, yak hair, oxtail etc., animal ceratin wig simulation quality is preferable, but animal ceratin fiber production is low, price is high and raw
Long period is longer, far can not meet the wilderness demand in market；Synthesis macromolecule has cheap, and processing is simple, and synthesis is fine
For dimension except the general superior function with chemical fibre, such as intensity is high, light, quick-drying washable, elasticity is good, is not afraid of mould moth spy
Point, brings great convenience to human lives, and application in production is also extremely wide.
It is inflexible without expression activitiy but traditional wig fiber color is single, without true man's hair under light it is caused more
Become color effects, the wig that color can change according to the change of photoenvironment not yet occur, applicant is based on this, designed
It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof, to make up blank of the market on the wig that changes colour, fill up
International cosplayer animations market is for the novel demand of fashion.
The content of the invention
The purpose of the present invention is to solve the deficiency of above-mentioned technical problem, there is provided a kind of sensitization discoloration for being used to manufacture wig
Fiber and preparation method thereof, obtained sensitization discoloration wig fiber can change color automatically according to the change of photoenvironment.
To solve the deficiency of above-mentioned technical problem, used technical scheme is the present invention：It is a kind of to be used to manufacture wig
Sensitization discoloration fiber, is prepared from the following raw materials in parts by weight：100 parts of base material, microcapsules sensitization discoloration powder 1-10 parts, additive
1-10 parts, pigment 0.1-10 parts and dispersing wax 0.1-5 parts, the base material is polypropylene PP, PET polyester slice, PBT polyester is cut
The mixture of piece, PET polyester slices and both mixture, PET polyester slices and the PTT polyester slices of both PBT polyester sections
Or the mixture of the section of PET polyester slices, PBT polyester and PTT polyester slice threes.
As a kind of further optimization for being used to manufacture the sensitization discoloration fiber of wig of the present invention：The PET polyester slices
Inherent viscosity be 0.675-0.1, the inherent viscosity of PBT polyester section and PTT polyester slices is 0.8-1.2, polypropylene PP's
Melt index is 10-15g/10min.
As a kind of further optimization for being used to manufacture the sensitization discoloration fiber of wig of the present invention：The PET polyester slices
It is made up of with both mixtures of PBT polyester section the PBT polyester section of 20-80% PET polyester slices and 20-80%.
As a kind of further optimization for being used to manufacture the sensitization discoloration fiber of wig of the present invention：The PET polyester slices
It is made up of with the mixture of both PTT polyester slices 20-80% PET polyester slices and 20-80% PTT polyester slices.
As a kind of further optimization for being used to manufacture the sensitization discoloration fiber of wig of the present invention：The PET polyester slices,
PBT polyester is cut into slices and the mixture of PTT polyester slice threes is cut into slices by 10-90% PET polyester slices, 5-50% PBT polyester
Formed with 5-50% PTT polyester slices.
The above-mentioned preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps：
A, raw material are taken according to parts by weight, by the raw material removal moisture drying at a temperature of 80-150 DEG C respectively, filters particle surface
Metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair
As-spun fibre is cooled down；
D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and drawn
Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300-
1000m/min；
Or drawing-off is carried out to as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae
Finish is added to oil to fiber；
E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel
Filament in tank is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine
It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
As a kind of further optimization for being used to manufacture the preparation method of the sensitization discoloration fiber of wig of the present invention：The step
Spinneret melting extrusion of the as-spun fibre by spinneret orifice for 0.1-1.4mm in rapid b.
As a kind of further optimization for being used to manufacture the preparation method of the sensitization discoloration fiber of wig of the present invention：The step
The finish used is oiled as one kind in polyethers based compound, fatty acid ester based compound and organic amine salt based compound in rapid d
Or any mixture.
As a kind of further optimization for being used to manufacture the preparation method of the sensitization discoloration fiber of wig of the present invention：The step
Draw ratio when being stretched in rapid e is controlled in 1.5-8.0.
Beneficial effect
First, sensitization discoloration fiber of the invention can change color automatically according to the change of photoenvironment, make obtained wig
Product can more show the animation wide market such as the stylishness of wig, Europe, China and Japan, fill up the world
Cosplayer animations market is for the novel demand of fashion；
2nd, according to the intensity of ultraviolet color can occur for the wig product that sensitization discoloration fiber of the invention makes to obtain
Change, the color for enabling the user of wig to be shown by wig know the intensity of ultraviolet, remind people from strong ultraviolet
Injury of the line to human body；
3rd, the optional polypropylene PP of sensitization discoloration fiber of the invention, the PET polyester slices that inherent viscosity is 0.8, inherent viscosity
The PBT polyester section that PTT polyester slices and inherent viscosity for 1.0 are 1.0 is used as base material, and obtained fiber flexibility is good,
Cardability, temperature tolerance, shaping persistence and the excellent protrusion of elasticity, and the elongation at break of fiber is big, uses the vacation of the present invention
Wig product made of hair fiber easily combs in use, and molding effect is lasting；
4th, a certain proportion of additive and dispersing wax are added in sensitization discoloration fiber of the invention, obtained wig fiber disappears
Luminosity and smoothness are preferable, and manufactured wig product has good shaded effect and visual effect, can effectively protect people
Aesthetic feeling of the body from uv damage and enhancing wig product.
5th, the present invention is in the preparation process of sensitization discoloration fiber, for base material and additive and the characteristic of dispersing wax,
Drying temperature, single-screw extrusion temperature, chilling temperature and draft temperature to raw material are particularly limited to, a series of
At a temperature of handled, obtained photosensitive wig fibre strength is high, and elasticity is good, and resistance to elevated temperatures is preferable.
Embodiment
Further technical scheme is illustrated below in conjunction with embodiment.
Embodiment 1
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 20 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 40 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 40 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh to add agent）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned original
The material removal moisture drying at a temperature of 100 DEG C respectively, particle surface metallic dust and impurity are filtered, make the water content control of raw material
In 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 15 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound）, the nascent fibre after oiling treatment
Dimension silk is sent into drafting machine and stretched, and tow is collected by winder, and the temperature that drawing-off is controlled in drawing process is
100 DEG C, rotating speed 600m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 10m/min, is finally packed.
Embodiment 2：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 100 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, 2 parts of microcapsules sensitization discoloration powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its heatproof model
Enclose for 160-230 DEG C）, 5 parts of additive（Additive is the silica that particle diameter is 4000 mesh）, 0.5 part of pigment and dispersing wax
0.5 part（Dispersing wax selects molecular weight in 2000-5000 Tissuemat E）, above-mentioned raw material are dehumidified at a temperature of 8 DEG C respectively
Dry, filter particle surface metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is fatty acid ester based compound）, it is first after oiling treatment
Raw filament is sent into drafting machine and stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 60 DEG C DEG C, rotating speed 300m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 120 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 3m/min, is finally packed.
Embodiment 3：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 60 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 PBT polyester cut into slices 40 parts（Powder morphology also can be selected in optional particle shape）、
8 parts of microcapsules sensitization discoloration powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230
℃）, 5 parts of additive（Additive is the silicon powder that particle diameter is 3000 mesh and the silica that particle diameter is 4000 mesh, both ratios
For 1:1）, 5 parts of 5 parts of pigment and dispersing wax（Dispersing wax selects molecular weight in 2000-5000 Tissuemat E）, by above-mentioned former material
Expect the removal moisture drying at a temperature of 150 DEG C respectively, filter particle surface metallic dust and impurity, the water content control of raw material is existed
30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 25 DEG C；
D, as-spun fibre is oiled by oiling roller（Finish is organic amine salt based compound）Processing, it is first after oiling treatment
Raw filament is sent into drafting machine and stretched, and tow is collected by winder, and the temperature of drawing-off is controlled in drawing process
Spend for 130 DEG C, rotating speed 1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 210 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 30m/min, is finally packed.
Embodiment 4：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 60 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 40 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
5 parts of microcapsules sensitization discoloration powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230
℃）, 3 parts of additive（Additive is calcium carbonate, talcum powder and titanium dioxide, and the ratio of three is 1:1:1）, 2 parts of pigment and
2 parts of dispersing wax（Dispersing wax selects molecular weight in 2000-5000 Tissuemat E）, by above-mentioned raw material respectively at a temperature of 90 DEG C
Removal moisture drying, particle surface metallic dust and impurity are filtered, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 220 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 20 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and had
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 80 DEG C, rotating speed is
800m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 180 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 15m/min, is finally packed.
Embodiment 5：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, melt index is 12.8g/10min polypropylene PP100 parts, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is silica, diatomite, silicon powder, glass microballoon and mica powder to add agent, and five ratio is 1:1:1:1:1）, 2 parts of pigment
And 2 parts of dispersing wax（Dispersing wax selects molecular weight in 2000-5000 Tissuemat E）, by above-mentioned raw material respectively at 100 DEG C
At a temperature of removal moisture drying, filter particle surface metallic dust and impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and had
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 6：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, the PBT polyester that inherent viscosity is 1.0 is cut into slices 100 parts（Optional particle shape also may be used
From powder morphology）, 5 parts of microcapsules sensitization discoloration powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, its heatproof model
Enclose for 160-230 DEG C）, 3 parts of additive（Additive is calcium carbonate, talcum powder, titanium dioxide, silica and diatomite, five
Ratio be 1:1:1:1:1）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax selects molecular weight in 2000-5000 polyethylene
Wax）, by the removal moisture drying at a temperature of 100 DEG C respectively of above-mentioned raw material, particle surface metallic dust and impurity are filtered, makes raw material
Water content control in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 280 DEG C；
C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 22 DEG C；
D, oiling treatment is carried out to as-spun fibre by oiling roller（Finish is polyethers based compound, fatty acid ester based compound and had
The mixture of machine amine salt based compound, the ratio of three is 1:1:1）, the as-spun fibre silk feeding drafting machine after oiling treatment
Stretched, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 120 DEG C, rotating speed is
1000m/min；
E, the filament on roll dies is sent into the thermal finalization cabinet that temperature is 160 DEG C by creel and carries out thermal finalization, control fiber
Speed of the tow in thermal finalization cabinet is 20m/min, is finally packed.
Embodiment 7
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 70 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 10 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 20 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
5 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230 DEG C）, 3 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh to add agent）, 2 parts of 2 parts of pigment and dispersing wax（Dispersing wax selects Tissuemat E）, by above-mentioned original
The material removal moisture drying at a temperature of 100 DEG C respectively, particle surface metallic dust and impurity are filtered, make the water content control of raw material
In 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 250 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off is carried out to as-spun fibre silk by hot water storgae, water temperature is 60 DEG C, drafting multiple 1.5, and oil is added in hot water storgae
Agent oils to fiber（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
The ratio of person is 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 120 DEG C by automaticity device for filtering water and carries out thermal finalization,
It is 3m/min to control speed of the fibre bundle in thermal finalization cabinet, is finally packed.
Embodiment 8：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 80 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 10 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 10 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
2 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silica that particle diameter is 4000 mesh to add agent）, 0.5 part of 0.5 part of pigment and dispersing wax（Dispersing wax is existed from molecular weight
2000-5000 Tissuemat E）, by the removal moisture drying at a temperature of 8 DEG C respectively of above-mentioned raw material, filter particle surface metallic dust
And impurity, make the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 205 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off is carried out to as-spun fibre silk by hot water storgae, water temperature is 80 DEG C, drafting multiple 4, and finish is added in hot water storgae
Fiber is oiled（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 160 DEG C by automaticity device for filtering water and carries out thermal finalization,
It is 3-30m/min to control speed of the fibre bundle in thermal finalization cabinet, is finally packed.
Embodiment 9：
A kind of its preparation method for being used to manufacture the sensitization discoloration fiber of wig, comprises the following steps
A, raw material are taken according to parts by weight, inherent viscosity is 0.8 90 parts of PET polyester slices（Optional particle shape also may be used
From powder morphology）, inherent viscosity be 1.0 5 parts of PTT polyester slices（Powder morphology also can be selected in optional particle shape）、
The PBT polyester that inherent viscosity is 1.0 is cut into slices 5 parts（Powder morphology also can be selected in optional particle shape）, microcapsules sensitization discoloration
8 parts of powder（Microcapsules sensitization discoloration powder is high temperature resistant sensitization discoloration powder, and its temperature resistant range is 160-230 DEG C）, 5 parts of additive（Add
It is the silicon powder that particle diameter is 3000 mesh and the silica that particle diameter is 4000 mesh to add agent, and both ratios are 1:1）, 5 parts of pigment with
And 5 parts of dispersing wax（Dispersing wax selects molecular weight in 2000-5000 Tissuemat E）, by above-mentioned raw material respectively in 150 DEG C of temperature
The lower removal moisture drying of degree, filters particle surface metallic dust and impurity, makes the water content control of raw material in 30-100ppm；
B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret
Extrusion obtains as-spun fibre, and extruder temperature is 300 DEG C；
C, as-spun fibre is cooled down by bosh；
D, drawing-off is carried out to as-spun fibre silk by hot water storgae, water temperature is 100 DEG C, drafting multiple 6, and finish is added in hot water storgae
Fiber is oiled（Finish be polyethers based compound, fatty acid ester based compound and organic amine salt based compound mixture, three
Ratio be 1:1:1）；
E, the filament in hot water storgae is sent into the thermal finalization cabinet that temperature is 210 DEG C by automaticity device for filtering water and carries out thermal finalization,
It is 30m/min to control speed of the fibre bundle in thermal finalization cabinet, is finally packed.
The above described is only a preferred embodiment of the present invention, any formal limitation not is made to the present invention, though
So the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology people
Member, without departing from the scope of the present invention, when the technology contents using the disclosure above make out a little change or repair
The equivalent embodiment for equivalent variations is adornd, as long as being the technical spirit according to the present invention without departing from technical solution of the present invention content
Any simple modification, equivalent change and modification made to above example, in the range of still falling within technical solution of the present invention.
Claims (10)
- A kind of 1. sensitization discoloration fiber for being used to manufacture wig, it is characterised in that：It is prepared from the following raw materials in parts by weight：Base material 100 parts, microcapsules sensitization discoloration powder 1-10 parts, additive 1-10 parts, pigment 0.1-10 parts and dispersing wax 0.1-5 parts are described Base material be polypropylene PP, PET polyester slice, PBT polyester section, PET polyester slices and PBT polyester section both mixtures, The mixture or PET polyester slices of both PET polyester slices and PTT polyester slices, PBT polyester section and PTT polyester slices three The mixture of person.
- A kind of 2. sensitization discoloration fiber for being used to manufacture wig as claimed in claim 1, it is characterised in that：The PET polyester is cut The inherent viscosity of piece is 0.675-0.1, and PBT polyester section and the inherent viscosity of PTT polyester slices are 0.8-1.2, polypropylene PP Melt index be 10-15g/10min.
- A kind of 3. sensitization discoloration fiber for being used to manufacture wig as claimed in claim 1, it is characterised in that：The PET polyester is cut Piece is made up of with both mixtures of PBT polyester section the PBT polyester section of 20-80% PET polyester slices and 20-80%.
- A kind of 4. sensitization discoloration fiber for being used to manufacture wig as claimed in claim 1, it is characterised in that：The PET polyester is cut The mixture of piece and both PTT polyester slices is made up of 20-80% PET polyester slices and 20-80% PTT polyester slices.
- A kind of 5. sensitization discoloration fiber for being used to manufacture wig as claimed in claim 1, it is characterised in that：The PET polyester is cut The mixture of piece, PBT polyester section and PTT polyester slice threes is cut by 10-90% PET polyester slices, 5-50% PBT polyester Piece and 5-50% PTT polyester slices form.
- A kind of 6. sensitization discoloration fiber for being used to manufacture wig as claimed in claim 1, it is characterised in that：The additive is carbon One kind or any mixed in sour calcium, talcum powder, titanium dioxide, silica, diatomite, silicon powder, glass microballoon and mica powder Compound.
- A kind of 7. preparation method for being used to manufacture the sensitization discoloration fiber of wig as claimed in claim 1, it is characterised in that：Including Following steps：A, raw material are taken according to parts by weight, by the raw material removal moisture drying at a temperature of 80-150 DEG C respectively, filters particle surface Metallic dust and impurity, make the water content control of raw material in 30-100ppm；B, single screw extrusion machine is put into after the raw material after removal moisture drying are uniformly mixed, is melted through gear pump and spinneret Extrusion obtains as-spun fibre, and extruder temperature is 205-300 DEG C；C, by ring blowing or cross air blasting, as-spun fibre is cooled down, wind-warm syndrome is controlled at 5-25 DEG C；Or pass through bosh pair As-spun fibre is cooled down；D, oiling treatment is carried out to as-spun fibre by oiling roller, the as-spun fibre silk after oiling treatment is sent into drafting machine and drawn Stretch, and tow is collected by winder, the temperature that drawing-off is controlled in drawing process is 60 DEG C -130 DEG C, rotating speed 300- 1000m/min；Or drawing-off is carried out to as-spun fibre silk by hot water storgae, water temperature is 60-100 DEG C, drafting multiple 1.5-6, in hot water storgae Finish is added to oil to fiber；E, it is thermal finalization to be carried out in 120-210 DEG C of thermal finalization cabinet or by heat the filament on roll dies to be sent into temperature by creel Filament in tank is sent into the thermal finalization cabinet that temperature is 120-210 DEG C by automaticity device for filtering water carries out thermal finalization, and control is fine It is 3-30m/min to tie up speed of the tow in thermal finalization cabinet, is finally packed.
- A kind of 8. preparation method for being used to manufacture the sensitization discoloration fiber of wig as claimed in claim 7, it is characterised in that：It is described Spinneret melting extrusion of the as-spun fibre by spinneret orifice for 0.1-1.4mm in step b.
- A kind of 9. preparation method for being used to manufacture the sensitization discoloration fiber of wig as claimed in claim 7, it is characterised in that：It is described The finish used is oiled in step d as one in polyethers based compound, fatty acid ester based compound and organic amine salt based compound Kind or any mixture.
- A kind of 10. preparation method for being used to manufacture the sensitization discoloration fiber of wig as claimed in claim 7, it is characterised in that：Institute Draw ratio when stretching by drafting machine in step d is stated to control in 1.5-8.0.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710999256.1A CN107881582A (en) | 2017-10-24 | 2017-10-24 | It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710999256.1A CN107881582A (en) | 2017-10-24 | 2017-10-24 | It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107881582A true CN107881582A (en) | 2018-04-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710999256.1A Pending CN107881582A (en) | 2017-10-24 | 2017-10-24 | It is a kind of to be used to manufacture sensitization discoloration fiber of wig and preparation method thereof |
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| CN (1) | CN107881582A (en) |
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| CN109454960A (en) * | 2018-11-19 | 2019-03-12 | 浙江荣鑫纤维有限公司 | A kind of compound-type fabric of changeable colour |
| CN111676545A (en) * | 2020-06-19 | 2020-09-18 | 华中科技大学 | Thermotropic bionic color-changing fiber, yarn and fabric and preparation method thereof |
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| CN109454960A (en) * | 2018-11-19 | 2019-03-12 | 浙江荣鑫纤维有限公司 | A kind of compound-type fabric of changeable colour |
| CN111676545A (en) * | 2020-06-19 | 2020-09-18 | 华中科技大学 | Thermotropic bionic color-changing fiber, yarn and fabric and preparation method thereof |
| CN111676545B (en) * | 2020-06-19 | 2021-07-30 | 华中科技大学 | Thermotropic bionic color-changing fiber, yarn and fabric and preparation method thereof |
| CN114457456A (en) * | 2020-06-19 | 2022-05-10 | 华中科技大学 | Thermotropic bionic color-changing fiber, yarn and fabric and preparation method thereof |
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