CN107903114A - Rich in nitro organic composite fertilizer slurry-spraying pelletizing technique - Google Patents
Rich in nitro organic composite fertilizer slurry-spraying pelletizing technique Download PDFInfo
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- CN107903114A CN107903114A CN201711201869.2A CN201711201869A CN107903114A CN 107903114 A CN107903114 A CN 107903114A CN 201711201869 A CN201711201869 A CN 201711201869A CN 107903114 A CN107903114 A CN 107903114A
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- Prior art keywords
- slurry
- composite fertilizer
- rich
- nitro
- fertilizer slurry
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
Abstract
The present invention relates to technical field of fertilizers, and in particular to one kind is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique.By potassium chloride：Hydrochloric acid=100g:40 ~ 50ml, which is added under the conditions of reactive tank is heated to 120 130 DEG C, reacts 10min generation nitre potassium hydrogen phthalates, then forms nitration mixture after being mixed with isometric dilute phosphoric acid solution, and it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.6 ~ 0.9 ratio is after tubular reactor reacts generation compound fertilizer slurry; compound fertilizer slurry adds 10 ~ 20% organic matters, 5 ~ 10% plant ash control its water content 25 ~ 40%; composite fertilizer's granulation slurry is obtained, then sprays into generation Inorganic whisker fat particles in rotary drum granulator.The present invention not only obtains the nitro-compound fertilizer of low concentration, also achieves the recycling of production discarded object, economic and environment-friendly, and nutrient is complete, promoting root growth strong sprout, activating soil.
Description
Technical field
The present invention relates to spray granulation field, and in particular to one kind is rich in nitro organic composite fertilizer slurry-spraying pelletizing work
Skill.
Background technology
The moisture (the liquid general name that can be vaporized) in slurry (mixture, solution and solute), by being ejected into an equipment
In, with heating, the method for taking out pressure, after vaporizing the moisture content in slurry and separating, retention will not gasify (under certain condition)
Solid form granular process and claim slurry-spraying pelletizing.Such as the final manufacturing process of phosphorus ammonium granulated fertilizer.Urea whitewashing is urea
Spray reaches in compound fertilizer granulating device after melting, reduces urea and crushes link.
Color, granularity are uneven to be reflected in slurry-spraying pelletizing fertilizer production to liquid flow rate of slurry and temperature to a certain extent
There is the big problem of high low head in control.As temperature fall certainly will cause greatly grain graininess size degree drop to fall with carbonization problem greatly
It is poor big；The high color of carbonation rate is corresponding deeply, dissolution velocity is slow；The small color of carbonation rate is accordingly shallow, dissolution velocity is very fast.With amino acid
Organic fertilizer is topic（All it is the whitewashing organic fertilizer with amino acid fermentation mostly currently on the market）, it is not single liquid agent, rich
Containing protein, amino acid material, nitrogenous material, other materials containing organic matter etc., thus in face of same high temperature, same section
In section, the slurry-spraying pelletizing technical process of same time, its material corruption amount of cure, humification degree, activation degree etc. differ
Cause, thus grain color, granularity non-uniform phenomenon occur, but do not influence fertilizer content quality problems.Low concentration in order to obtain
Nitro-compound fertilizer, the method for having producer to use physical mixed, nitro-compound fertilizer material adds part mixes after making material, to reduce
Concentration.But this method, due to that cannot carry out organic composite with nitro-compound fertilizer, can not really solve the above above problem.
But the technology has Fertilizer nutrient component low etc., the use of earth material so that effective fertility reduces in fertilizer, cost of transportation
Rise, is unfavorable for playing the efficient fertility of composite fertilizer.
The content of the invention
It is an object of the invention to reference to actual conditions, overcome the deficiencies of the prior art and provide a kind of answering containing organic matter
Slurry-spraying pelletizing technique is expected in Hefei, and the fertilizer which obtains not only realizes nitro low concentration, and fertilizer rate of release delays
Slowly, it is and neat rich in number Ten microelements, nutrients such as the organic carbons and boron, zinc, copper included in plant organic matter, plant ash
Entirely, fertilizer is balanced, plays an important roll to promoting root growth strong sprout, activating soil, increasing of quality and production.
To achieve these goals, present invention employs following technical scheme：
One kind is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique, by potassium chloride：Nitric acid=100g:40 ~ 50ml adds reactive tank
10min generation potassium nitrate is reacted under the conditions of being heated to 120-130 DEG C, then nitration mixture is formed after being mixed with isometric dilute phosphoric acid solution,
It is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.6 ~ 0.9 ratio tubular reactor react generation compound fertilizer slurry after, and
Slurry is concentrated into 90% ~ 95%, rotary drum granulator is sprayed into after concentration, compound fertilizer slurry add 10 ~ 20% Litter-fall matrix, 10 ~
20% organic matter, 5 ~ 10% plant ash control its water content 25 ~ 40%, obtain composite fertilizer's granulation slurry, then spray into rotary drum granulator
Middle generation Inorganic whisker fat particles.
The further restriction bright as we, the phosphoric acid,diluted is that phosphorus acid content is 2 ~ 10%.
The further restriction bright as we, the Litter-fall matrix is the Litter-fall of shrub vegetation, its withered fallen leaf contains
Amount >=60%, its water content≤15%.
The further restriction bright as we, the organic matter particle particle diameter is 5-15 mesh, and organic composition is fiber
Property stalk thing, vinasse, creeping oxalis composition, fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in composition:2:1.Institute
It is any of rice bran, bagasse, tea bran, wheat bran, peanut press pulp or their mixture to state fibre-bearing stalk thing.
We are bright to realize technical principle：Production technology is granulated using nitrification, secondary dechlorination, potassium chloride and nitric acid are added
Reactive tank is heated and reacted under certain condition, and certain density hydrochloric acid can be made in the HCL gases of effusion after water absorbs, generation
Potassium nitrate mixed with phosphoric acid,diluted after form nitration mixture.The nitration mixture is reacted into generation compound fertilizer in tubular reactor in proportion with synthesis ammonia
Slurry, adds certain proportion plant source organic matter, stirs evenly, and control water content is 25 ~ 40%, then sprays into rotary drum granulator
Middle generation nitrogen, phosphorus, a certain proportion of organic compound fertilizer granules containing nitro of potassium.The composite fertilizer that this technique obtains, which has, to be granulated
Even, bright in color, stable quality, nutrient be sufficient, soluble and the features such as be absorbed by crops, and particularly makees that seed manure is opposite to seed to pacify
Entirely.The multiple kinds of crops such as suitable all kinds of soil and wheat, corn, melon and fruit, peanut, vegetables, beans, flowers, fruit tree and economic work
Thing, is applied suitable for base manure, seed manure, top dressing, seed manure, punching.
The present invention obtains good technique effect through the above scheme：
For nitro inorganic nutrients content between 30 ~ 40%, nitro content is relatively traditional in the bright obtained Inorganic whisker fertilizer of we
Fertilizer reduces, and obtains the reduction of fertilizer rate of release, and crops can obtain sufficiently absorbing fertilizer nutrient, avoid conventional fertilizers
The problem of Nutrient Absorption is not caused to waste, is lost in entirely occurs, and improves resource utilization；The bright obtained composite fertilizer's nitro of we is low dense
Degree, and rich in the number Ten microelements such as plant organic matter, humic acid, organic carbon and boron, zinc, copper, it is fully sharp to organic matter
With making compound fertilizer nutrient complete, fertilizer is balanced, plays an important roll to promoting root growth strong sprout, activating soil, increasing of quality and production.
Embodiment
In order to which the technological means for realizing the present invention is apparent to, the present invention is done further with reference to specific embodiment
Illustrate.
Embodiment 1
The present embodiment organic matter particle particle diameter is 15 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, group for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in compound:2:1.The fibre-bearing stalk thing is rice bran, bagasse
1:1 mixture.The Litter-fall matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content≤
15%。
By potassium chloride：Nitric acid=100g:50ml, which is added under the conditions of reactive tank is heated to 125 DEG C, reacts 10min generation nitric acid
Potassium, then nitration mixture is formed after being mixed with isometric dilute phosphoric acid solution, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.6 ratio
After tubular reactor reacts generation compound fertilizer slurry, and slurry is concentrated into 95%, rotary drum granulator is sprayed into after concentration, in compound fertilizer
Slurry adds 10% Litter-fall matrix, 10% organic matter, 10% plant ash and controls its water content 30%, obtains composite fertilizer's granulation material
Slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fat particles nitro that the present embodiment obtains
Inorganic nutrients content is 35% or so.
Embodiment 2
The present embodiment organic matter particle particle diameter is 5 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, combination for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in thing:2:1.The fibre-bearing stalk thing is wheat bran, peanut press pulp 1:
1 mixture.The Litter-fall matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content≤15%.
By potassium chloride：Nitric acid=100g:45ml, which is added under the conditions of reactive tank is heated to 120 DEG C, reacts 10min generation nitric acid
Potassium, then with isometric dilute phosphoric acid solution（2%）Nitration mixture is formed after mixing, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.6
Slurry is concentrated into 90% by ratio after tubular reactor reacts generation compound fertilizer slurry, and rotary drum granulator is sprayed into after concentration,
Compound fertilizer slurry adds 20% Litter-fall matrix, 15% organic matter, 10% plant ash and controls its water content to obtain composite fertilizer's system 40%
Granule material slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fat particles that the present embodiment obtains
Nitro inorganic nutrients content is 40% or so.
Embodiment 3
The present embodiment organic matter particle particle diameter is 10 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, group for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in compound:2:1.The fibre-bearing stalk thing is rice bran, sugarcane
Slag, tea bran, wheat bran, peanut press pulp 1：1：1：1：1 mixture.The Litter-fall matrix is the Litter-fall of shrub vegetation, its is withered
Fallen leaves content >=60%, its water content≤15%.
By potassium chloride：Nitric acid=100g:45ml, which is added under the conditions of reactive tank heats 130 DEG C, reacts 10min generation potassium nitrate,
Again with isometric dilute phosphoric acid solution（10%）Nitration mixture is formed after mixing, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.7 ratio
Slurry is concentrated into 95% by example after tubular reactor reacts generation compound fertilizer slurry, and rotary drum granulator is sprayed into after concentration, multiple
Fertilizer slurry adds 15% Litter-fall matrix, 18% organic matter, 8% plant ash and controls its water content 30%, obtains composite fertilizer's granulation
Slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fat particles nitre that the present embodiment obtains
Base inorganic nutrients content is 38% or so.
Embodiment 4
The present embodiment organic matter particle particle diameter is 12 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, group for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in compound:2:1.The fibre-bearing stalk thing is wheat bran, peanut press pulp
1:1 mixture.The Litter-fall matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content≤
15%。
By potassium chloride：Nitric acid=100g:50ml, which is added under the conditions of reactive tank is heated to 120 DEG C, reacts 10min generation nitric acid
Potassium, then with isometric dilute phosphoric acid solution（5%）Nitration mixture is formed after mixing, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.8
Slurry is concentrated into 92% by ratio after tubular reactor reacts generation compound fertilizer slurry, and rotary drum granulator is sprayed into after concentration,
Compound fertilizer slurry adds 17% Litter-fall matrix, 20% organic matter, 5% plant ash and controls its water content to obtain composite fertilizer's system 40%
Granule material slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fat particles that the present embodiment obtains
Nitro inorganic nutrients content is 36.6%.
Embodiment 5
The present embodiment organic matter particle particle diameter is 8 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, combination for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in thing:2:1.The fibre-bearing stalk thing is rice bran, tea bran, wheat
Bran 1:1:1 mixture.The Litter-fall matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content
≤15%。
By potassium chloride：Nitric acid=100g:42ml, which is added under the conditions of reactive tank is heated to 130 DEG C, reacts 10min generation nitric acid
Potassium, then with isometric dilute phosphoric acid solution（6%）Nitration mixture is formed after mixing, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.9
Slurry is concentrated into 95% by ratio after tubular reactor reacts generation compound fertilizer slurry, and rotary drum granulator is sprayed into after concentration,
Compound fertilizer slurry adds 16% Litter-fall matrix, 20% organic matter, 5% plant ash and controls its water content to obtain composite fertilizer's system 30%
Granule material slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fat particles that the present embodiment obtains
Nitro inorganic nutrients content is between 38.5%.
Embodiment 6
The present embodiment organic matter particle particle diameter is 9 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition, combination for fibroid
Fibroid stalk thing, vinasse, creeping oxalis three mass ratio are 5 in thing:2:1.The fibre-bearing stalk thing is rice bran, peanut press pulp 1:
1 mixture.The Litter-fall matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content≤15%.
By potassium chloride：Nitric acid=100g:40ml, which is added under the conditions of reactive tank is heated to 130 DEG C, reacts 10min generation nitric acid
Potassium, then with isometric dilute phosphoric acid solution（8%）Nitration mixture is formed after mixing, it is 1 by volume that nitration mixture is synthesized ammonia with liquid： 0.9
Ratio after tubular reactor reacts generation compound fertilizer slurry, and slurry is concentrated into 95%, rotary drum granulator is sprayed into after concentration,
Adding 15% Litter-fall matrix, 15% organic matter, 10% plant ash in compound fertilizer slurry controls its water content to obtain composite fertilizer 25%
Granulation slurry, then spray into generation Inorganic whisker fat particles in rotary drum granulator.The Inorganic whisker fertilizer that the present embodiment obtains
Grain nitro inorganic nutrients content is 32.5%.
Application Example
The compound fat particles of the gained of embodiment 1 ~ 6 are administered to No. 1 corn of the summer corn of the same race of field 3 and survey production, field 2 is to use common inorganic
Fertilizer, field 1 are the low concentration nitro inorganic composite fertilizer without nutrients such as organic matter, plant ash, Litter-falls, and result of the test is as follows：
Production result is surveyed in 1 corn average yield per mu of table
Result of the test shows：Increased production using corn after the bright Inorganic whisker fertilizer of we, and the plant quantity of lesion occur
Relative to the reduction in field 1 and field 2,40 ~ 50% are reduced, realizes that nutrient is complete, fertilizer is balanced, being capable of promoting root growth strong sprout, activated soil
Earth, increasing of quality and production, and per mu yield 873.7kg, compared with per mu yield 765.2kg, 757.5kg in field 1, field 2, rate of growth is up to 12 ~
17%。
Embodiment of above is merely illustrative of the technical solution of the present invention and unrestricted, and those skilled in the art should manage
Solution, is not departing from the purpose and scope of the invention, can be to technical scheme technical scheme is modified or replaced equivalently, its is equal
It should cover within the scope of the present invention.
Claims (5)
1. one kind is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique, it is characterised in that by potassium chloride：Nitric acid=100g:40~
50ml, which is added under the conditions of reactive tank is heated to 120-130 DEG C, reacts 10min generation potassium nitrate, then is mixed with isometric dilute phosphoric acid solution
Nitration mixture is formed after conjunction, it is 1 by volume that nitration mixture is synthesized ammonia with liquid：0.6 ~ 0.9 ratio is reacted in tubular reactor to be generated
After compound fertilizer slurry, and slurry is concentrated into 90% ~ 95%, sprays into rotary drum granulator after concentration, 10 ~ 20% are added in compound fertilizer slurry
Litter-fall matrix, 10 ~ 20% organic matters, 5 ~ 10% plant ash control its water content 25 ~ 40%, obtain composite fertilizer's granulation slurry, then
Spray into and Inorganic whisker fat particles are generated in rotary drum granulator.
2. it is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique as claimed in claim 1, it is characterised in that dilute phosphorus
Acid is that phosphorus acid content is 2 ~ 10%.
3. it is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique as claimed in claim 1, it is characterised in that the Litter-fall
Matrix be shrub vegetation Litter-fall, its withered fallen leaf content >=60%, its water content≤15%.
4. it is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique as claimed in claim 1, it is characterised in that described is organic
Matter grain diameter is 5-15 mesh, and organic composition obstructs thing, vinasse, creeping oxalis composition for fibroid, and fibroid is obstructed in composition
Thing, vinasse, creeping oxalis three mass ratio are 5:2:1.
5. it is rich in nitro organic composite fertilizer slurry-spraying pelletizing technique as claimed in claim 4, it is characterised in that the fibre-bearing
Property stalk thing be any of rice bran, bagasse, tea bran, wheat bran, peanut press pulp or their mixture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711201869.2A CN107903114A (en) | 2017-11-27 | 2017-11-27 | Rich in nitro organic composite fertilizer slurry-spraying pelletizing technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711201869.2A CN107903114A (en) | 2017-11-27 | 2017-11-27 | Rich in nitro organic composite fertilizer slurry-spraying pelletizing technique |
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| Publication Number | Publication Date |
|---|---|
| CN107903114A true CN107903114A (en) | 2018-04-13 |
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ID=61848761
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711201869.2A Withdrawn CN107903114A (en) | 2017-11-27 | 2017-11-27 | Rich in nitro organic composite fertilizer slurry-spraying pelletizing technique |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108947729A (en) * | 2018-08-02 | 2018-12-07 | 张居政 | A kind of preparation method of the legal compound fertilizer of carbon |
-
2017
- 2017-11-27 CN CN201711201869.2A patent/CN107903114A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108947729A (en) * | 2018-08-02 | 2018-12-07 | 张居政 | A kind of preparation method of the legal compound fertilizer of carbon |
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Application publication date: 20180413 |