CN107903086A - A kind of ceramic tile that can produce low-light dry granular effect and preparation method thereof - Google Patents
A kind of ceramic tile that can produce low-light dry granular effect and preparation method thereof Download PDFInfo
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- CN107903086A CN107903086A CN201711080457.8A CN201711080457A CN107903086A CN 107903086 A CN107903086 A CN 107903086A CN 201711080457 A CN201711080457 A CN 201711080457A CN 107903086 A CN107903086 A CN 107903086A
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- Prior art keywords
- dry granular
- preparation
- glaze slip
- glaze
- light
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
Abstract
The present invention relates to a kind of ceramic tile that can produce low-light dry granular effect and preparation method thereof, which comprises the following steps:Dry granular glaze slip is sprayed to brick face using spraying equipment, to form uniform dry granular on brick face;And burn till gained adobe, essence throwing, obtain producing the ceramic tile of low-light dry granular effect;Wherein, the formula of the dry granular glaze slip is:By mass, dry granular 26~28%, glue roller squeegee oil 22~24%, levelling agent 7~9%, dumb light glaze slip 43~45%.
Description
Technical field
The present invention relates to architectural pottery field, and in particular to a kind of ceramic tile that can produce low-light dry granular effect and its preparation
Method.
Background technology
With the continuous improvement of people's living standards, the demand with personalized high-end ceramic brick product is also increasingly
It is more.The low-light stereoeffect on the surface of ceramic tile increasingly causes the extensive concern of society, prepares with low-light stereoeffect
Ceramic tile is one of hot spot prepared by current ceramic tile.For this reason, ceramic brick surface can add dry granular now.
Chinese patent application 201310349396.6 discloses a kind of manufacture method of wear-resistant antiskid dry-particle ceramic tile, uses
Dry granular distributing device charity dry granular, this method need the higher dry granular particle of specific dry granular equipment and cost, and during cloth
Dry granular skewness.
Chinese patent application 200810220436.6, which discloses a kind of surface, has the production of stereo sandrock effect Ceramic Tiles
Technique, is got ready by getting cabinet ready, glaze is applied on brick face with imitating the effect of dry granular, ceramic tile dry granular particle made from this method
It is larger, surface low-light effect can not be formed.
Chinese patent application 201410114999.2 discloses a kind of manufacturing process of candy effect Ceramic Tiles, on base substrate
Charity overglaze, by slip shower charity candy dry granular glaze after charity overglaze, is fired afterwards, and post processing obtains candy effect ceramics
Brick.But slip shower charity candy dry granular glaze, it is full sized brick cloth candy dry granular, dry granular material utilization amount is big, can not be formed soft micro-
Light effect.
Chinese patent application 201510533823.5 discloses a kind of cement ceramic tile, it passes through the charity face on cement base substrate
Glaze, by glaze spraying cabinet spray drying grain glaze after charity overglaze, is fired, post processing forms afterwards.But by glaze spraying cabinet spray drying grain glaze,
For full sized brick charity dry granular, dry granular material utilization amount is big, can not form soft low-light effect.
The content of the invention
In view of the above-mentioned problems, it is an object of the invention to provide a kind of ceramic tile and its system that can produce low-light dry granular effect
Preparation Method.
On the one hand, the present invention provides a kind of preparation method for the ceramic tile that can produce low-light dry granular effect, including following step
Suddenly:
Dry granular glaze slip is sprayed to brick face using spraying equipment, to form uniform dry granular on brick face;And
Gained adobe is burnt till, essence throwing, obtain producing the ceramic tile of low-light dry granular effect;
Wherein, the formula of the dry granular glaze slip is:By mass, dry granular 26~28%, glue roller squeegee oil 22~24%, levelling agent 7
~9%, dumb light glaze slip 43~45%.
According to the present invention, dry granular glaze slip is sprayed using spraying equipment and applies dry granular, the dry granular glaze slip good fluidity and glued
Degree is big, and dry granular particle is not easy to precipitate, glaze spraying excellent performance, cooperates with spraying equipment, can be in plane or concave-convex brick
The very thin dry granular of last layer is uniformly applied on face, rear fine grained is burnt till and is densely distributed in adobe surface, then thrown and formed using essence
Soft low-light effect.
It is preferred that the spraying equipment is spray gun, it is preferably that high pressure pumps knife machine spray gun.
It is preferred that the nozzle bore of the spraying equipment is 0.65~0.72mm, injection pressure is 4.5~5 jin.
It is preferred that the dry granular is crushed sieving by frit and is obtained, it is preferable that the particle diameter of the dry granular is 150~180 mesh.
It is preferred that the flow velocity of the glue roller squeegee oil is 10~12 seconds, the flow velocity of the dumb light glaze slip is 60~100 seconds, institute
The flow velocity for stating levelling agent is 60~100 seconds.
It is preferred that the levelling agent is made into by alkylphenol polyoxyethylene ether and hydrophobic silica.
It is preferred that the flow velocity of the dry granular glaze slip is 35~45 seconds, glaze spraying weight is 260~270 grams/m.
It is preferred that the brick face is overglaze, the overglaze contains:By mass, SiO259~61%, Al2O325~
28%th, CaO 0.1~0.3%, MgO 0.1~0.4%, K2O 2.8~3.1%, Na2O 1.5~1.8%.
It is preferred that essence is combined to using the abrading block of 3~5 group of 1500 mesh, 3~5 group of 2000 mesh, 4~6 group of 3000 mesh
Throw.
On the other hand, the present invention is provided can produce low-light dry granular effect by prepared by any one above-mentioned preparation method
Ceramic tile.
Brief description of the drawings
Fig. 1 is the photo of the ceramic tile that can produce low-light dry granular effect of an embodiment of the present invention.
Embodiment
Hereinafter, the present invention is further illustrated with reference to following embodiments, it should be appreciated that following embodiments are merely to illustrate this
Invention, is not intended to limit the present invention.In following formula, unless otherwise instructed, the content of each component refers both to mass percent.
In an embodiment of the present invention, dry granular glaze slip is sprayed to brick face using spraying equipment, it is uniform to be formed on brick face
Dry granular;Then gained adobe is burnt till, essence throwing, obtains producing the ceramic tile of low-light dry granular effect." low-light dry granular effect "
Refer to that the dumb light dry granular effect for being sprayed on product surface is very tiny, after the abrading block by high mesh number half is thrown, in the protuberance of dry granular
Point formed some uniformly tiny shining points, it is necessary to survey light could be visible.Hereinafter, the preparation method of the ceramic tile is illustrated.
First, adobe is prepared.It can be prepared according to a conventional method by known ceramic raw material, such as carry out blank ball successively
Grind, granulation of dusting, pressed compact drying, obtain dry base.
Preferably, overglaze is applied in adobe.Charity dry granular glaze can make dry granular glaze and the adhesion in brick face more on overglaze
It is high.In addition, applying overglaze can also play a part of to cover base substrate and easy to color development.In order to ensure tiny dry granular is kept on overglaze
Sharp keen sense will not be melt flat, and overglaze is preferably provided with suitable formula and sintering temperature.For example, compared with general common overglaze,
It main in overglaze formula can increase the content of silicon (Si), aluminium (Al), and reduce the elements such as calcium (Ca), magnesium (Mg), sodium (Na)
Content.In one example, overglaze includes following component:By mass, SiO259~61%, Al2O325~28%, CaO
0.1~0.3%, MgO 0.1~0.4%, K2O 2.8~3.1%, Na2O 1.5~1.8%.The overglaze sintering temperature of the system
High (such as sintering temperature is 1150~1170 DEG C), can allow particle to be stood after burning till on surface.
Apply overglaze mode and include but not limited to glaze spraying, leaching glaze etc..The fineness of overglaze glaze slip can be 0.7~0.9 (325 mesh).
The proportion of overglaze glaze slip can be 1.80~1.85.The flow velocity of overglaze glaze slip can be 15~29 seconds.In the present invention, flow velocity refers to flow
Fast cup expires determinand, opens aperture below flow velocity cup, by determinand from starting to flowing to end after time be denoted as the stream of determinand
Speed.The overglaze weight that unit area is applied can be 320~350g/m2。
The charity dry granular on brick face.Brick face can be plane or male and fomale(M&F).In an embodiment of the present invention, adopt
With spraying equipment dry granular glaze slip is sprayed to brick face.Spraying equipment may be, for example, spray gun.Preferably, the spraying equipment is high pressure spray
Penetrate, such as injection pressure can be 4.5~5 jin.Preferably, the spraying equipment has larger nozzle bore, such as nozzle bore
Footpath can be 0.65~0.72mm.Using such high pressure and/or large aperture nozzle spraying equipment, can equably be applied on brick face
The very thin dry granular of last layer, and its nozzle will not be blocked by dry granular glaze slip.In one example, the spraying equipment is high-pressure pump
Water knife machine spray gun.
Polishing is thrown so as to essence to make after spray drying grain glaze to be formed compacted grains in brick face and forms low-light effect, in the present invention, is done
Grain is preferably high temperature and particle is tiny.The particle diameter fineness of dry granular can be 150~180 mesh.In one example, the firing temperature of dry granular
Scope can be 1155~1170 DEG C.In one example, high temperature frit is crushed into sieving, it is 150~180 purposes to sub-elect fineness
Grain, as dry granular.
Due to applying dry granular using glaze spraying mode by spraying equipment, it is therefore desirable to dry granular is configured to glaze slip and possesses glaze spraying
Performance.Preferably, dry granular glaze slip has suspension, the caking property of dry granular and brick face and the flowing of slurry of good dry granular
Property.For example, the flow velocity of dry granular glaze slip is preferably 30~40 seconds.Dry granular glaze slip with the flow velocity with good glaze spraying performance,
It can cause the dry granular being sprayed on brick face evenly.It is highly preferred that the flow velocity of dry granular glaze slip is 35~45 seconds.
In one example, roller stamp-pad ink (or glue roller squeegee oil) and matting glaze glaze slip (or dumb light glaze slip) is selected to make dry granular
Suspension is got up, then is incorporated a small amount of levelling agent to adjust the flow velocity of slurry." roller stamp-pad ink " is that a kind of have splendid rheological behavior
The printed medium of ceramic tile roller printing, suspension is good, good dispersion, good fluidity.The flow velocity of roller stamp-pad ink can be 10~12
Second." matting glaze glaze slip " refers to that glossiness protects glaze than relatively low dumb light after burning till, and main rise suspends and allow in the present invention
The effect that dry granular is preferably fused together.In one example, dumb light glaze slip contains:By mass, SiO249~52%,
Al2O318~21%, CaO 4.8~5.3%, MgO 3.9~4.6%, K2O 0.2~0.4%, Na2O 5.7~6.6%, CaO
(and/or BaO) 11~13%, ZnO 2.6~3.0%.Matting glaze glaze slip flow velocity can be between 60~100 seconds.The present invention's is dry
Contain roller stamp-pad ink and matting glaze glaze slip at the same time in grain glaze slip, good suspendability can be possessed at the same time and burn till meltbility
Energy.Levelling agent can be made into by alkylphenol polyoxyethylene ether and hydrophobic silica.Wherein, the percentage of alkylphenol polyoxyethylene ether contains
Amount can be 70~80%, and the percentage composition of hydrophobic silica can be 20~30%.The flow velocity of levelling agent can be 60~100 seconds it
Between.
In one example, the formula of dry granular glaze slip is:By mass, dry granular 26~28%, glue roller squeegee oil 22~24%, stream
Flat agent 7~9%, dumb light glaze slip 43~45%.The dry granular glaze slip dry granular glaze slip good fluidity and viscosity of the formula are big, dry granular grain
Son is not easy to precipitate.Its flow velocity is 35~45 seconds.In one preferred example, the formula of dry granular glaze slip is:By mass, do
Grain 27%, glue roller squeegee oil 23%, levelling agent 8%, dumb light glaze slip 42%.
During using spraying equipment to brick face injection dry granular glaze slip, glaze spraying weight can be 260~270 grams/m.Using spray
After jet device sprays dry granular glaze slip to brick face, one layer of very thin uniform dry granular is formed on brick face, thickness is about 0.3~0.4mm.
Then burnt till.Firing temperature can be 1150~1175 DEG C.Firing time can be 60~65 minutes.Done after burning till
Grain is dispersed in ceramic tile surface automatically.
Then it is polished, forms one of soft low-light effect.Polishing mode can be half throwing.Half throwing refers to dry granular
Tip jettisoning sub-fraction slightly, has retained the major part of dry granular particle.It is preferred that carried out using the smart polishing chip of high mesh number light
Throw, to form softer low-light effect.Polishing thickness can be 0.1~0.15mm.In one example, using 4 group of 1500 mesh, 4
2000 mesh of group, the abrading block of 5 group of 3000 mesh are combined to polish.
In addition, it should be understood that above-mentioned steps are only examples, the present invention is not limited thereto, for example, can also be first before dry granular is applied
The stamp on brick face, such as use ink jet printing device spray printing pattern.
According to an embodiment of the present invention, dry granular, energy are applied by the way of high pressure pumps the large aperture nozzle glaze spraying of knife machine
It is enough uniformly to apply the very thin dry granular of last layer in plane or concave-convex brick face, after high temperature firing fine grained it is intensive respectively in brick
Base surface, then soft low-light effect is formed using the smart polishing chip polishing gently of high mesh number.Due to using spray gun glaze spraying side
Formula applies dry granular, and in order to which dry granular is configured to glaze slip and possesses glaze spraying performance, present invention uses glue roller squeegee oil and levelling agent to make
For dry granular carrier, after being made into dry granular glaze slip according to a certain percentage, the good fluidity and viscosity of glaze slip are big, and dry granular particle is not easy
Precipitation.After pumping knife machine glaze spraying with high pressure, one layer of very thin uniform dry granular, the dry granular after high temperature firing are formed in product surface
Automatically ceramic tile surface is dispersed in, one of soft low-light effect is formed after essence is thrown.The porcelain for having used the present invention to make
Brick surface particles effect has more tiny particle and softer low-light surface tactile sensation for half throwing product is got ready.
Embodiment is enumerated further below so that the present invention will be described in detail.It will similarly be understood that following embodiments are served only for this
Invention is further described, it is impossible to is interpreted as limiting the scope of the invention, those skilled in the art is according to this hair
Some nonessential modifications and adaptations that bright the above is made belong to protection scope of the present invention.Following examples are specific
Technological parameter etc. is also only an example in OK range, i.e. those skilled in the art can be done properly by the explanation of this paper
In the range of select, and do not really want to be defined in hereafter exemplary concrete numerical value.
Embodiment 1
1) adobe is prepared;
2) overglaze is applied in adobe, overglaze main components in percentage by weight is as shown in table 1:
Table 1
SiO2 | Al2O3 | CaO | MgO | K2O | Na2O |
60.54 | 26.32 | 0.11 | 0.19 | 2.97 | 1.63 |
The fineness of overglaze glaze slip is 0.7~0.9 (325 mesh), proportion can be that 1.80~1.85, flow velocity can be 15~29 seconds, glazing
Weight can be 320~350g/m2;
3) dry granular glaze slip is prepared
Purchase is selected from special 150~180 mesh dry granular TDJ5606 only thought;
With dry granular 27%, glue roller squeegee oil (spy only thinks TW268) 23%, levelling agent (by 80% alkylphenol polyoxyethylene ether and 20%
Hydrophobic silica is made into) 8%, dumb light glaze slip (its chemical composition:By mass, SiO250.6%th, Al2O319%th, CaO
5.29%th, MgO 4.21%, K2O0.255%, Na2O 6.14%, BaO 12.3%, ZnO2.88%) 42% mass ratio prepare
Into dry granular glaze slip, the flow velocity of the dry granular glaze slip is 40 seconds;
4) knife machine spray gun spray drying grain glaze slip on overglaze is pumped using high pressure, the nozzle bore that high pressure pumps knife machine spray gun is
0.65mm, pressure are 4.5 jin, and glaze spraying weight is 260~270 grams/m;
5) burn till:Fired 63 minutes in 1170 DEG C in roller kilns;
6) polish:It is combined to polish using the abrading block of 4 group of 1500 mesh, 4 group of 2000 mesh, 5 group of 3000 mesh.
Fig. 1 is the surface picture of the ceramic tile obtained by the present embodiment, it can be seen that the ceramic tile has soft low-light effect.
Claims (11)
1. a kind of preparation method for the ceramic tile that can produce low-light dry granular effect, it is characterised in that comprise the following steps:
Dry granular glaze slip is sprayed to brick face using spraying equipment, to form uniform dry granular on brick face;And
Gained adobe is burnt till, essence throwing, obtain producing the ceramic tile of low-light dry granular effect;
Wherein, the formula of the dry granular glaze slip is:By mass, dry granular 26~28%, glue roller squeegee oil 22~24%, levelling agent 7~
9%th, dumb light glaze slip 43~45%.
2. preparation method according to claim 1, it is characterised in that the spraying equipment is spray gun, is preferably high-pressure pump
Water knife machine spray gun.
3. preparation method according to claim 1 or 2, it is characterised in that the nozzle bore of the spraying equipment is 0.65
~0.72mm, injection pressure are 4.5~5 jin.
4. preparation method according to any one of claim 1 to 3, it is characterised in that the dry granular was crushed by frit
Sieve and obtain, it is preferable that the particle diameter of the dry granular is 150~180 mesh.
5. preparation method according to any one of claim 1 to 4, it is characterised in that the flow velocity of the glue roller squeegee oil is
10~12 seconds, the flow velocity of the dumb light glaze slip was 60~100 seconds, and the flow velocity of the levelling agent is 60~100 seconds.
6. preparation method according to any one of claim 1 to 5, it is characterised in that the levelling agent is gathered by alkyl phenol
Ethylene oxide ether is made into hydrophobic silica.
7. preparation method according to any one of claim 1 to 6, it is characterised in that the flow velocity of the dry granular glaze slip is
30~40 seconds, glaze spraying weight was 260~270 Ke ∕ square metre.
8. preparation method according to any one of claim 1 to 7, it is characterised in that the brick face is overglaze, the face
Glaze contains:By mass, SiO2 59~61%, Al2O3 25~28%, CaO 0.1~0.3%, MgO 0.1~0.4%, K2O 2.8
~3.1%, Na2O 1.5~1.8%.
9. preparation method according to any one of claim 1 to 8, it is characterised in that the dumb light glaze slip contains:By matter
Gauge, SiO2 49~52%, Al2O318~21%, CaO 4.8~5.3%, MgO 3.9~4.6%, K2O 0.2~0.4%, Na2O
5.7~6.6%, CaO 11~13%, ZnO 2.6~3.0%.
10. preparation method according to any one of claim 1 to 9, it is characterised in that using 3~5 group of 1500 mesh, 3~
5 group of 2000 mesh, the abrading block of 4~6 group of 3000 mesh are combined to smart throwing.
11. prepared by a kind of preparation method as any one of claims 1 to 10 can produce low-light dry granular effect
Ceramic tile.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108911701A (en) * | 2018-08-27 | 2018-11-30 | 佛山石湾鹰牌陶瓷有限公司 | Dumb light dry granular glazed tile and preparation method thereof |
CN109369220A (en) * | 2018-05-30 | 2019-02-22 | 佛山唯思创意产品策划股份有限公司 | A kind of soft polishing ceramic tile production technology of dry granular |
CN110372209A (en) * | 2019-07-31 | 2019-10-25 | 佛山欧神诺陶瓷有限公司 | A kind of Polished crystal tile and preparation method thereof with babysbreath effect |
CN111116235A (en) * | 2019-12-30 | 2020-05-08 | 肇庆乐华陶瓷洁具有限公司 | Fine dry particle ceramic tile, preparation method thereof and fine dry particle glaze |
CN114262208A (en) * | 2022-01-17 | 2022-04-01 | 江西富利高新材料有限公司 | Large-particle dry particle superposed matte glaze ceramic plate and preparation method thereof |
CN115215548A (en) * | 2022-08-08 | 2022-10-21 | 佛山市典石釉科技有限公司 | Dry grain glaze for ceramic tiles and preparation method thereof, ceramic tiles and preparation method thereof |
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CN201971749U (en) * | 2010-12-31 | 2011-09-14 | 广东新明珠陶瓷集团有限公司 | Templet glaze blocking printing equipment |
CN103224736A (en) * | 2013-04-08 | 2013-07-31 | 佛山市道氏科技有限公司 | Matte glaze ink for ceramic jet printing and preparation method thereof |
CN104016728A (en) * | 2014-06-03 | 2014-09-03 | 广东蒙娜丽莎新型材料集团有限公司 | Ceramic tile with bulged particle effect and preparation method of ceramic tile |
CN106746651A (en) * | 2017-01-16 | 2017-05-31 | 佛山市道氏科技有限公司 | A kind of dry granular glaze with diamond luster effect |
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EP1070687B1 (en) * | 1999-07-21 | 2003-09-10 | Institut Français du Pétrole | Monolithic honeycomb structure made of porous ceramic material, and use as filter for particulates |
CN201971749U (en) * | 2010-12-31 | 2011-09-14 | 广东新明珠陶瓷集团有限公司 | Templet glaze blocking printing equipment |
CN103224736A (en) * | 2013-04-08 | 2013-07-31 | 佛山市道氏科技有限公司 | Matte glaze ink for ceramic jet printing and preparation method thereof |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109369220A (en) * | 2018-05-30 | 2019-02-22 | 佛山唯思创意产品策划股份有限公司 | A kind of soft polishing ceramic tile production technology of dry granular |
CN108911701A (en) * | 2018-08-27 | 2018-11-30 | 佛山石湾鹰牌陶瓷有限公司 | Dumb light dry granular glazed tile and preparation method thereof |
CN108911701B (en) * | 2018-08-27 | 2021-04-27 | 佛山石湾鹰牌陶瓷有限公司 | Matte dry particle glazed tile and preparation method thereof |
CN110372209A (en) * | 2019-07-31 | 2019-10-25 | 佛山欧神诺陶瓷有限公司 | A kind of Polished crystal tile and preparation method thereof with babysbreath effect |
CN110372209B (en) * | 2019-07-31 | 2022-08-16 | 佛山欧神诺陶瓷有限公司 | Polished crystal brick with starry sky effect and preparation method thereof |
CN111116235A (en) * | 2019-12-30 | 2020-05-08 | 肇庆乐华陶瓷洁具有限公司 | Fine dry particle ceramic tile, preparation method thereof and fine dry particle glaze |
CN114262208A (en) * | 2022-01-17 | 2022-04-01 | 江西富利高新材料有限公司 | Large-particle dry particle superposed matte glaze ceramic plate and preparation method thereof |
CN115215548A (en) * | 2022-08-08 | 2022-10-21 | 佛山市典石釉科技有限公司 | Dry grain glaze for ceramic tiles and preparation method thereof, ceramic tiles and preparation method thereof |
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