CN107901546A - A kind of anlistatig two-sided cured film of anti-pollution and preparation method thereof - Google Patents
A kind of anlistatig two-sided cured film of anti-pollution and preparation method thereof Download PDFInfo
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- CN107901546A CN107901546A CN201711084181.0A CN201711084181A CN107901546A CN 107901546 A CN107901546 A CN 107901546A CN 201711084181 A CN201711084181 A CN 201711084181A CN 107901546 A CN107901546 A CN 107901546A
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- layer
- pollution
- cured film
- layers
- antistatic
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/32—Layered products comprising a layer of synthetic resin comprising polyolefins
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/36—Layered products comprising a layer of synthetic resin comprising polyesters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/0038—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding involving application of liquid to the layers prior to lamination, e.g. wet laminating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/26—Polymeric coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/28—Multiple coating on one surface
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/20—Properties of the layers or laminate having particular electrical or magnetic properties, e.g. piezoelectric
- B32B2307/21—Anti-static
Abstract
The present invention provides a kind of anlistatig two-sided cured film of anti-pollution, including cuticular layer, the first UV hardened layers, antistatic layer, substrate layer, the 2nd UV hardened layers, layer of silica gel and the stripping film contacted successively；In terms of mass ratio, the formula of the antistatic layer is:Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).The antistatic two-sided cured film of anti-pollution in the present invention has excellent anti-pollution and antistatic property, and after UV irradiation tests, the film surface of the two-sided cured film of the application does not change significantly, and illustrates that it has the function that good anti-UV irradiation.Present invention also offers a kind of preparation method of the anlistatig two-sided cured film of anti-pollution, the preparation method in the present invention is simple, is conducive to produce in enormous quantities.
Description
Technical field
The invention belongs to protect technical field of membrane, more particularly to a kind of anlistatig two-sided cured film of anti-pollution and its preparation side
Method.
Background technology
Two-sided cured film on the market is mainly used in machine form, display screen etc., does not all have anti-pollution antistatic effect,
In use, easily there is electrostatic hazard on machine, and two-sided cured film nonreactive UV irradiation behaviours on the market, irradiated by UV easy
Bubble is produced, influences using effect.
The content of the invention
It is an object of the invention to provide anlistatig two-sided cured film of a kind of anti-pollution and preparation method thereof, in the present invention
Two-sided cured film anti-pollution is antistatic, while resistance to UV is radiated.
The present invention provides a kind of anlistatig two-sided cured film of anti-pollution, including contact successively cuticular layer, anti-pollution hardened layer,
Antistatic layer, substrate layer, UV hardened layers, layer of silica gel and stripping film；
In terms of mass ratio, the formula of the antistatic layer is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(3~20).
Preferably, the thickness of the antistatic layer is 1~2 μm.
Preferably, in terms of mass ratio, the formula of the anti-pollution hardened layer is：It is acrylic resin modified：Solvent=(15~
30)：(11~25)；
The thickness of the anti-pollution hardened layer is 3~15 μm.
Preferably, the material of the UV hardened layers is acrylic resin；
The thickness of the UV hardened layers is 3~6 μm.
Preferably, the substrate layer for pet layer, PE layers, OPP layers, BOPET layers or BOPP layers；
The thickness of the substrate layer is 50~200 μm.
Preferably, the cuticular layer for pet layer, PE layers, OPP layers, BOPET layers or BOPP layers；
The thickness of the cuticular layer is 25~75 μm.
Preferably, the thickness of the stripping film is 15~150 μm.
Preferably, in terms of mass ratio, the formula of the layer of silica gel is：Organosilicon：Additive：Solvent=(30~40)：
(1~10)：(60~65)；
The thickness of the layer of silica gel is 15~50 μm.
The present invention provides a kind of preparation method of the anlistatig two-sided cured film of anti-pollution, comprises the following steps：
A) in the coated on one side antistatic solution of base material, drying, obtains antistatic layer；
B the first UV glue) is coated with the antistatic layer, protective film is covered with after curing；
C the 2nd UV glue) is coated with the another side of base material, silica gel is coated with after curing, covers stripping film, it is antistatic to obtain anti-pollution
Two-sided cured film；
In terms of mass ratio, the formula of the antistatic solution is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).
The present invention provides a kind of anlistatig two-sided cured film of anti-pollution, including the cuticular layer, the first UV that contact successively hard
Change layer, antistatic layer, substrate layer, the 2nd UV hardened layers, layer of silica gel and stripping film；In terms of mass ratio, the antistatic layer
It is formulated and is:Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).Anti-pollution in the present invention is antistatic
Two-sided cured film has excellent anti-pollution and antistatic property, and after UV irradiation tests, the two-sided cured film of the application
Film surface does not change significantly, and illustrates that it has the function that good anti-UV irradiation.
Present invention also offers a kind of preparation method of the anlistatig two-sided cured film of anti-pollution, the preparation method in the present invention
Simply, be conducive to produce in enormous quantities.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
There is attached drawing needed in technology description to be briefly described, it should be apparent that, drawings in the following description are only this
The embodiment of invention, for those of ordinary skill in the art, without creative efforts, can also basis
The attached drawing of offer obtains other attached drawings.
Fig. 1 is the structure diagram of the anlistatig two-sided cured film of anti-pollution in the present invention, wherein, 1 is cuticular layer, and 2 be anti-
Dirty hardened layer, 3 be antistatic layer, and 4 be substrate layer, and 5 be UV hardened layers, and 6 be layer of silica gel, and 7 be stripping film.
Embodiment
The present invention provides a kind of anlistatig two-sided cured film of anti-pollution, including the cuticular layer, the anti-pollution that contact successively harden
Layer, antistatic layer, substrate layer, UV hardened layers, layer of silica gel and stripping film；
In terms of mass ratio, the formula of the antistatic layer is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).
In the present invention, the cuticular layer be preferably pet layer, PE layers, OPP layers, BOPET layers or BOPP layers；The cuticula
The thickness of layer is preferably 25~75 μm, more preferably 35~50 μm.
The formula of the anti-pollution hardened layer is preferably：It is acrylic resin modified：Solvent=(15~30)：(11~25)；More
Preferably (20~25)：(15~20)；The solvent is preferably one kind in ethyl acetate, malonic acid methyl ether acetate and butanone
It is or several.The thickness of the anti-pollution hardened layer is preferably 3~15 μm, more preferably 5~10 μm.
The formula of the antistatic layer is preferably polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(3~
20), more preferably (1~5)：(5~10)：(3~10)；Specifically, can be 1:5:5、2:5:3 or 2:7:9.It is described antistatic
The thickness of layer is preferably 1~2 μm.
The substrate layer be preferably pet layer, PE layers, OPP layers, BOPET layers or BOPP layers；The thickness of the substrate layer is preferred
For 50~200 μm, more preferably 100~150 μm.
The material of the UV hardened layers is preferably acrylic resin, and the thickness of the UV hardened layers is preferably 3~6 μm, more
Preferably 4~5 μm.
The formula of the layer of silica gel is preferably organosilicon：Additive：Solvent=(30~40)：(1~10)：(60~65),
In the present invention, the additive is preferably antioxidant or ultraviolet absorber, and the thickness of the layer of silica gel is preferably 15~50 μ
M, more preferably 25~45 μm, are most preferably 30~35 μm.
The stripping film is preferably the stripping film of PET materials, and the thickness of the stripping film is preferably 15~150 μm, more excellent
Elect 50~100 μm as.
Present invention also offers a kind of preparation method of the anlistatig two-sided cured film of anti-pollution, comprise the following steps：
A) in the coated on one side antistatic solution of base material, drying, obtains antistatic layer；
B anti-pollution glue) is coated with the antistatic layer, protective film is covered with after curing；
C) in the another side coating UV glue of base material, silica gel is coated with after curing, covers stripping film, it is anlistatig double to obtain anti-pollution
Face cured film；
In terms of mass ratio, the formula of the antistatic solution is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).
Specifically, it can be prepared according to following steps：
The first step：Apply aqueous antistatic liquid
Anilox roll coating is selected, by aqueous antistatic solution coating in PET base material, coating thickness is 1-2 μm, selected
PET base material is 50~200 μm, by 60~150 DEG C of bakings of oven；
Second step：UV glue applications
3~15 μm of UV glue is coated with the liquid antistatic of the first step, by oven (60~200 DEG C), UV lamp energy
(60~90%), 1~3min of time, curing obtain anti-pollution hardened layer, are covered with 50~75 μm of PE protective films on it；Wherein,
The UV glue formulas are acrylic resin modified：Solvent==(15~30)：(11~25)；
3~6 μm of UV glue is coated with base material another side, by oven (60~200 DEG C) and UV energy (60~90%)
Cure, obtain UV hardened layers；The UV glue is acrylic resin；
3rd step：Coating silica gel
The silica gel of 15~50 μ is coated with above-mentioned 3~6 μ UV hardening aspects, by (60-200 DEG C) drying of oven, covers stripping
Film
In the present invention, the component and consistency of thickness of the component of above layers and thickness and above each layer, herein no longer
Repeat.
It is anlistatig two-sided to a kind of anti-pollution provided by the invention with reference to embodiments in order to further illustrate the present invention
Cured film and preparation method thereof is described in detail, but cannot be understood as limiting the scope of the present invention.
Embodiment 1
1 μm of aqueous antistatic layer is first coated with using 110 mesh number nick rods in 100 μm of PET base material inner faces；It is described water-based anti-
Electrostatic layer is by polythiophene class compound：Alcohol：Water=1:5:5, obtained by 100 DEG C of heat cures, with hand-held sheet resistance
The impedance of instrument test surfaces is 106~109；
Then anti-pollution hardened layer is coated with using 120 mesh number nick rods on antistatic layer,；The anti-pollution hardened layer is special
It is acrylic resin modified：15 parts, ethyl acetate：25 parts, start shooting 6m/min, first passes through 60 DEG C of oven, and UV lamp energy 85% × 2 is solid
Wound after change.The anti-pollution hardened layer is streaked with oil pike, is polymerized to oil droplet, hardness test 500g, 3H rapidly.
Then 3 μm of UV hardened layers are coated with substrate backside, the UV hardened layers pass through 110 DEG C of oven for acrylic resin
UV mercury lamps are crossed afterwards, its energy 80% × 2, start shooting 8m/min, cures hardened layer, hardness test 500g, 2H.
25 μm of silica gel is coated with above-mentioned UV hardened layers, covers 50 μm of PET film；The silica gel is 42 parts of organosilicon, solvent
For 56 parts, 2 parts of ultraviolet absorber.By silica gel face paste in the tempered glass surface of specially treated, after UV irradiates test 92h,
Film surface is without significant change.
Embodiment 2
2 μm of aqueous antistatic layer is first coated with using 110 mesh number nick rods in 125 μm of PET base material inner faces；It is described water-based anti-
Electrostatic layer is by polythiophene class compound：Alcohol：Water=2:3:5, cure antistatic layer for 120 DEG C by heat cure, with hand-held
The impedance of formula sheet resistance instrument test surfaces is 106~109；
Then it is special using 120 mesh number nick rods coating anti-pollution hardened layer, the anti-pollution hardened layer on antistatic layer
It is acrylic resin modified：60 parts, malonic acid methyl ether acetate：40 parts, start shooting 10m/min, first passes through 120 DEG C of oven, UV lamp energy
Amount 80% × 2 is wound after curing.The anti-pollution hardened layer is streaked with oil pike, is polymerized to oil droplet rapidly, and hundred lattice of hardened layer have gently
Micro- degumming,
Then 5 μm of UV hardened layers, hardened layer mistake after 60 DEG C of oven for acrylic resin are coated with substrate backside
UV mercury lamps, its energy 80% × 2, start shooting 8m/min, cures hardened layer.
25 μ silica gel, overlay film 50PET films are coated with above-mentioned UV hardened layers；The silica gel is 30 parts of organosilicon, solvent 70
Part.By silica gel face paste in the tempered glass surface of specially treated, after UV irradiates test 72h, fitting glass surface has slightly
Bubble.
Embodiment 3
The aqueous antistatic layer of 1 μ is first coated with using 110 mesh number nick rods in 100 μ PET base materials inner faces；It is described water-based anti-quiet
Electric layer is by polythiophene class compound：Alcohol：Water=2:9:7, cure antistatic layer for 120 DEG C by heat cure, use hand-held
Sheet resistance instrument test surfaces impedance not 106-1010；
Then it is special using 120 mesh number nick rods coating anti-pollution hardened layer, the anti-pollution hardened layer on antistatic layer
It is acrylic resin modified：60 parts, butanone：40 parts, start shooting 8m/min, first passes through 100 DEG C of oven, and UV lamp energy 85% × 2 cures
After wound.The anti-pollution hardened layer is streaked with oil pike, is polymerized to oil droplet rapidly.
Then 4 μ UV hardened layers, hardened layer mistake after 100 DEG C of oven for acrylic resin are coated with substrate backside
UV mercury lamps, its energy 80% × 2, start shooting 10m/min, cures hardened layer, hardness test 500g, 2H.
30 μ silica gel, overlay film 50PET films are coated with above-mentioned UV hardened layers；The silica gel is 30 parts of organosilicon, solvent 60
Part, 10 parts of antioxidant.By silica gel face paste in the tempered glass surface of specially treated, after UV irradiates test 72h, glass is bonded
There is slight bubble on glass surface, but better than embodiment 2.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (9)
1. a kind of anlistatig two-sided cured film of anti-pollution, including cuticular layer, anti-pollution hardened layer, antistatic layer, the base contacted successively
Material layer, UV hardened layers, layer of silica gel and stripping film；
In terms of mass ratio, the formula of the antistatic layer is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(3~20).
2. two-sided cured film according to claim 1, it is characterised in that the thickness of the antistatic layer is 1~2 μm.
3. two-sided cured film according to claim 1, it is characterised in that in terms of mass ratio, the anti-pollution hardened layer
It is formulated and is：It is acrylic resin modified：Solvent=(15~30)：(11~25)；
The thickness of the anti-pollution hardened layer is 3~15 μm.
4. two-sided cured film according to claim 1, it is characterised in that the material of the UV hardened layers is acrylic acid tree
Fat；
The thickness of the UV hardened layers is 3~6 μm.
5. two-sided cured film according to claim 1, it is characterised in that the substrate layer for pet layer, PE layers, OPP layers,
BOPET layers or BOPP layers；
The thickness of the substrate layer is 50~200 μm.
6. two-sided cured film according to claim 1, it is characterised in that the cuticular layer for pet layer, PE layers, OPP layers,
BOPET layers or BOPP layers；
The thickness of the cuticular layer is 25~75 μm.
7. two-sided cured film according to claim 1, it is characterised in that the thickness of the stripping film is 15~150 μm.
8. two-sided cured film according to claim 1, it is characterised in that in terms of mass ratio, the formula of the layer of silica gel
For：Organosilicon：Additive：Solvent=(30~40)：(1~10)：(60~65)；
The thickness of the layer of silica gel is 15~50 μm.
9. a kind of preparation method of the anlistatig two-sided cured film of anti-pollution, comprises the following steps：
A) in the coated on one side antistatic solution of base material, drying, obtains antistatic layer；
B the first UV glue) is coated with the antistatic layer, protective film is covered with after curing；
C the 2nd UV glue) is coated with the another side of base material, silica gel is coated with after curing, covers stripping film, it is anlistatig double to obtain anti-pollution
Face cured film；
In terms of mass ratio, the formula of the antistatic solution is:
Polythiophene class compound：Water：Ethanol=(1~10)：(3~15:)：(5~20).
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| CN201711084181.0A CN107901546A (en) | 2017-11-07 | 2017-11-07 | A kind of anlistatig two-sided cured film of anti-pollution and preparation method thereof |
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| CN201711084181.0A CN107901546A (en) | 2017-11-07 | 2017-11-07 | A kind of anlistatig two-sided cured film of anti-pollution and preparation method thereof |
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| CN104194580A (en) * | 2014-08-20 | 2014-12-10 | 昆山博益鑫成高分子材料有限公司 | Antistatic scratch-resistant coating and coating method thereof |
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| CN204605051U (en) * | 2015-01-30 | 2015-09-02 | 东莞市纳利光学材料有限公司 | A kind of diaphragm with anti-blue light and anti-fingerprint function |
| CN204749425U (en) * | 2015-05-21 | 2015-11-11 | 东莞市尼的科技股份有限公司 | High transparent electron protection film |
| CN107090253A (en) * | 2017-04-28 | 2017-08-25 | 东莞市纳利光学材料有限公司 | A kind of antiultraviolet insulation film and its manufacture method |
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2017
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Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168402A (en) * | 1996-04-30 | 1997-12-24 | 录象色彩股份公司 | Anti-glare anti-static coating and method |
| CN101481589A (en) * | 2009-01-19 | 2009-07-15 | 石海兰 | Antistatic high temperature resistant pressure-sensitive adhesive tape and preparation thereof |
| CN103865364A (en) * | 2014-03-11 | 2014-06-18 | 苏州斯迪克新材料科技股份有限公司 | Polythiophene antistatic coating liquid and preparation method thereof |
| CN104194580A (en) * | 2014-08-20 | 2014-12-10 | 昆山博益鑫成高分子材料有限公司 | Antistatic scratch-resistant coating and coating method thereof |
| CN104673124A (en) * | 2014-12-19 | 2015-06-03 | 东莞市纳利光学材料有限公司 | High-hardness anti-blue-light anti-fingerprint optical protective film and preparation method thereof |
| CN204605051U (en) * | 2015-01-30 | 2015-09-02 | 东莞市纳利光学材料有限公司 | A kind of diaphragm with anti-blue light and anti-fingerprint function |
| CN204749425U (en) * | 2015-05-21 | 2015-11-11 | 东莞市尼的科技股份有限公司 | High transparent electron protection film |
| CN107090253A (en) * | 2017-04-28 | 2017-08-25 | 东莞市纳利光学材料有限公司 | A kind of antiultraviolet insulation film and its manufacture method |
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