CN107897674A - A kind of water chestnut cake and preparation method thereof - Google Patents
A kind of water chestnut cake and preparation method thereof Download PDFInfo
- Publication number
- CN107897674A CN107897674A CN201711186639.3A CN201711186639A CN107897674A CN 107897674 A CN107897674 A CN 107897674A CN 201711186639 A CN201711186639 A CN 201711186639A CN 107897674 A CN107897674 A CN 107897674A
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- extract
- water chestnut
- water
- cake
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- A—HUMAN NECESSITIES
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Abstract
The invention belongs to food technology field.Specifically disclose a kind of water chestnut cake and preparation method thereof, 25% 35% water of water chestnut cake, 10% 15% water chestnut starches, 10% 15% wheat flours, 10% 15% mung bean flours, 5% 10% traditional Chinese drug inspissation things, 5% 10% flavor enhancements, 10% 15% green tea powders, 1% 5% tea oils；The traditional Chinese drug inspissation thing is made according to percent by weight of following raw material：+ 20 30% Bitter Melon P.E of+15 25% carambola root extract of 15 25% mulberry bark extract+15 25% lucid asparagus extract of+10 20% Yeradetajo extract.The technical solution close association of the application does not separate out the not stratified effect of water after reaching cooling, and this product is not only delicious and has the good shelf-life, suppresses rotten spot significant effect by detection.
Description
Technical field
The present invention relates to planting technology field, more particularly to a kind of water chestnut cake and preparation method thereof.
Background technology
Water chestnut cake is kind typical in Cantonese dim sum, and the whole nation " Chinese famous snacks " assert in the first batch it
One, it be with syrup mix have the function of tonifying lung cool liver, eliminate indigestion and phlegm, the water chestnut starch of fall fire is steamed and formed, its color tea is yellow, in half
It is transparent, it can roll over without splitting, stick up and continuous, soft, sliding, refreshing, tough to have both, taste is extremely fragrant and sweet, suitable for four seasons.The main original of water chestnut cake at present
Material is water chestnut starch, its taste, nutritive effect are all more single.In order to which the present our factory of the progress in the epoch of catering to develops a kind of water chestnut cake
Have the function that hypoglycemic.
The content of the invention
The goal of the invention of the present invention is：A kind of water chestnut cake and preparation method thereof is provided, it is not only delicious and with certain
Hypoglycemic effect, and there is the good shelf-life, suppress rotten spot significant effect by detection.
In order to realize foregoing invention purpose, the technical solution adopted by the present invention is as follows：
A kind of water chestnut cake, is made according to percent by weight of following raw material：25%-35% water, 10%-15% horseshoes
Powder, 10%-15% wheat flours, 10%-15% mung bean flours, 5%-10% traditional Chinese drug inspissations thing, 5%-10% flavor enhancements, 10%-
15% green tea powder, 1%-5% tea oils；The traditional Chinese drug inspissation thing is made according to percent by weight of following raw material：15-25%
Mulberry bark extract+10-20% Yeradetajo extract+15-25% lucid asparagus extract+15-25% carambola roots extract+
20-30% Bitter Melon P.Es.
Further illustrate, the flavor enhancement is xylitol or oligoisomaltose.
Further illustrate, the mulberry bark extract is prepared by following methods：Picking is taken to be produced July in Guangzhou
The root bark of white mulberry crushed after cross 50 mesh sieves, precision weighs 100g, puts in boiling flask, and it is 75-80%'s to add mass concentration
Ethanol solution 500mL, carries out alcohol extracting, also using ultrasonic power be 100W in alcohol extracting, frequency be 40 hertz of assisted extraction 20-25
Minute, take out and stand to room temperature, filter to take 1.01 times that filtrate then carries out being concentrated under reduced pressure into original volume.Obtained material
In the content containing glycoprotein be 5.86mg/g-8.02mg/g.
Further illustrate, the Yeradetajo extract is prepared by following methods：After eclipta herb is crushed, add
Complex enzyme for hydrolyzing 10-20 minutes, carries out 3500-4000r/min using centrifuge and centrifuges 5-10 minutes, take supernatant, add
Sevag reagents take off albumen 2-3 times, each 5-8 minutes, then carry out after being concentrated in vacuo to 1.12 times of original volume, add quality
Fraction carries out alcohol precipitation for the ethanol solution of 70-80% at 5-8 DEG C and stays overnight, and then carries out 3000-4000r/min using centrifuge
Centrifugation 1-3 minutes, takes out precipitation, extract is obtained after steam drying after standing；The Sevag reagents are according to volume ratio trichlorine
Methane-n-butanol 3-4: 1 is mixed to get；The content containing dietary fiber is 9.59mg/g-12.06mg/g in obtained material.
Further illustrate, the lucid asparagus extract is prepared by following methods：After lucid asparagus root tuber is cleaned, crush
100 mesh sieves are crossed, 200g powder is weighed and adds in conical flask, add the volume fraction 40-50% ethanol solutions of 500mL, then add
The mass concentration for entering 10mL is the ammonium sulfate of 0.3-0.4g/m L, and vibration stands 20-25 minutes after 1 minute, in temperature 40-
50 DEG C, extract 30min under the ultrasound condition of power 50-60W, filter, solution moved into stratification in separatory funnel.Take upper strata
Solution, can obtain lucid asparagus extract after being spray-dried.The content containing steroidal is 18.26mg/ in obtained material
g-30.00mg/g。
Further illustrate, the carambola root extract is prepared by following methods：After carambola root rhizome is crushed
Take 100g to add in triangular flask, the acetic acid methanol solution of the 1-3% of cumulative volume is added, at 35-40 DEG C, under microwave power 500W
The reaction of 20-25 minutes is carried out, is then centrifuged and takes solution, carambola root extract is can obtain after spray drying.
Contain flavonoids 5.36mg/g-13.25mg/g, phenols 7.69mg/g-12.63mg/g, alkaloid 3.96mg/ in obtained material
G-12.96mg/g, terpene 2.69mg/g-10.02mg/g, saponin 3.20mg/g-11.31mg/g.
Further illustrate, the Bitter Melon P.E is prepared by following methods：After balsam pear remove seed is smashed to pieces, quality is added
Fraction 40-50% ethanol solutions carry out refluxing extraction, and the condition of refluxing extraction is to repeat extraction 2-3 times, 20-30 minutes each,
The temperature of extraction is 50-60 DEG C, and be concentrated under reduced pressure into original volume after the filtrate for repeating extraction is merged 1.12 times can obtain
To Bitter Melon P.E；The volume ratio of balsam pear and ethanol solution is 1:20-30.Contain terpene 2.69mg/g- in obtained material
8.21mg/g, steroidal 2.69mg/g-5.96mg/g.
The preparation method of water chestnut cake as described above, specifically includes following steps：
Step 1：Mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, balsam pear are carried
Take thing to match combination according to percetage by weight after being extracted and obtain traditional Chinese drug inspissation thing,
Step 2：Stirred evenly after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
To agranular mixed serum；
Step 3：Moderate heat boils mixed serum constant temperature to 30-40 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea are poured into when boiling
Tree oil, stirring to slurries becomes thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 5-8min, turns moderate heat 15- after water is boiled
18min is transparent to cake body, that is, water chestnut cake is made.
In conclusion by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
1. one layer of constant water chestnut cake can be improved as one of raw material present invention uses green tea powder, traditional Chinese drug inspissation thing
Taste, by obtaining active ingredient after Chinese medicine material to be carried out to different extractions, can also reduce the bitter taste of Chinese medicine in itself,
The additional proportioning for using green tea powder certain with tea oil is combined so that overall water chestnut cake has effects that fall fire；Using green
Tea powder and the pure natural raw material of mung bean flour to carry light green color during water chestnut cake is transparent, improves the appearance of water chestnut cake；Addition
Traditional Chinese drug inspissation thing causes water chestnut cake to have the function that certain hypoglycemic, water chestnut cake designed for the patient with diabetes,
So that the patient with diabetes can also trust it is edible.
2. our factory is directed to the change in the epoch of chasing, many food all have healthcare function, as research is found with sugar
The inside of patient ten is urinated with regard to the phenomenon of one, in order to which the sales volume opened up markets is in order to causing patient also to eat delicious food
Water chestnut cake, our factory is found by constantly research, and the Chinese traditional medicine composition reasonably matched is with the addition of on the formula for making water chestnut cake
Active material, has effect hypoglycemic well, reaches and eats delicious water chestnut cake while can reach treatment diabetes
Double action.
The effect of Chinese medicine active compound：The root bark of white mulberry is cold in nature, sweet in flavor.It is distributed in lung channel.Removing heat from lung and relieving asthma, inducing diuresis for removing edema.Belong to damp-clearing drug
The edema-alleviating diuretic of subordinate's classification.Eclipta is cold in nature, sweet in flavor, sour.Return kidney channel, Liver Channel.It is nourishing liver and kidney, cooling blood and hemostasis.Lucid asparagus
It is cold in nature, it is sweet in flavor, sour.Return kidney channel, Liver Channel.It is nourishing liver and kidney, cooling blood and hemostasis.Carambola root slight bitter, puckery, temperature.Promoting blood circulation and stopping pain, relaxing muscles and tendons are lived
Network, enriching yin and nourishing kidney, hemostasis by invigorating QI.Balsam pear is cold in nature, bitter.Thoughts of returning home warp, the spleen channel, lung channel.Heat, improving eyesight, removing toxic substances are washed in driving away summer heat.
Embodiment
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine in any way.This specification (including any accessory claim, summary)
Disclosed in any feature, unless specifically stated, can be replaced by other alternative features that are equivalent or have similar purpose.
I.e., unless specifically stated, each feature is an example in a series of equivalent or similar characteristics.
Embodiment 1
A kind of water chestnut cake, is made according to percent by weight of following raw material：25% water, 14% water chestnut starch, 13% wheat
Flour, 14% mung bean flour, 9% traditional Chinese drug inspissation thing, 9% flavor enhancement, 12% green tea powder, 4% tea oil；The traditional Chinese drug inspissation thing is pressed
It is made according to percent by weight of following raw material：+ 25% lucid asparagus of+20% Yeradetajo extract of 15% mulberry bark extract is extracted
+ 20% Bitter Melon P.E of the carambola root of thing+20% extract.
Further illustrate, the flavor enhancement is xylitol or oligoisomaltose.
Further illustrate, the mulberry bark extract is prepared by following methods：Picking is taken to be produced July in Guangzhou
The root bark of white mulberry crushed after cross 50 mesh sieves, precision weighs 100g, puts in boiling flask, adds the ethanol that mass concentration is 75%
Solution 500mL, carries out alcohol extracting, also using ultrasonic power be 100W in alcohol extracting, frequency be 40 hertz of assisted extractions 20 minutes, take
Go out to stand to room temperature, filter to take 1.01 times that filtrate then carries out being concentrated under reduced pressure into original volume.Contain in obtained material
The content of glycoprotein is 5.86mg/g.
Further illustrate, the Yeradetajo extract is prepared by following methods：After eclipta herb is crushed, add
Complex enzyme for hydrolyzing 10 minutes, carries out 3500r/min using centrifuge and centrifuges 5 minutes, take supernatant, add Sevag reagents and take off egg
White 2 times, 5 minutes every time, then carry out after being concentrated in vacuo to 1.12 times of original volume, it is molten to add the ethanol that mass fraction is 70%
Liquid carries out alcohol precipitation at 5 DEG C and stays overnight, and then carrying out 3000r/min using centrifuge centrifuges 1 minute, and precipitation is taken out after standing, is steamed
Extract is obtained after vapour drying；The Sevag reagents are mixed to get according to volume ratio chloroform-n-butanol 3: 1；Obtain
The content containing dietary fiber is 9.59mg/g in material.
Further illustrate, the lucid asparagus extract is prepared by following methods：After lucid asparagus root tuber is cleaned, crush
100 mesh sieves are crossed, 200g powder is weighed and adds in conical flask, add 40% ethanol solution of volume fraction of 500mL, be subsequently added into
The mass concentration of 10mL is the ammonium sulfate of 0.3g/m L, and vibration stands 20 minutes after 1 minute, in 40 DEG C of temperature, power 50W
Ultrasound condition under extract 30min, filter, by solution move into separatory funnel in stratification.Upper solution is taken, it is dry to carry out spraying
Lucid asparagus extract is can obtain after dry.The content containing steroidal is 18.26mg/g in obtained material.
Further illustrate, the carambola root extract is prepared by following methods：After carambola root rhizome is crushed
Take 100g to add in triangular flask, add 1% acetic acid methanol solution of cumulative volume, carried out at 35 DEG C, under microwave power 500W
The reaction of 20 minutes, is then centrifuged and takes solution, and carambola root extract is can obtain after spray drying.Obtained thing
Contain flavonoids 5.36mg/g, phenols 7.69mg/g, alkaloid 3.96mg/g, terpene 2.69mg/g, saponin 3.20mg/g in matter.
Further illustrate, the Bitter Melon P.E is prepared by following methods：After balsam pear remove seed is smashed to pieces, quality is added
40% ethanol solution of fraction carries out refluxing extraction, and the condition of refluxing extraction is to repeat extraction 2 times, 20 minutes every time, the temperature of extraction
Spend for 50 DEG C, carry out being concentrated under reduced pressure into original volume after the filtrate for repeating extraction is merged 1.12 times can obtain balsam pear extraction
Thing；The volume ratio of balsam pear and ethanol solution is 1:20.Contain terpene 2.69mg/g, steroidal 2.69mg/g in obtained material.
The preparation method of water chestnut cake as described above, specifically includes following steps：
Step 1：Mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, balsam pear are carried
Take thing to match combination according to percetage by weight after being extracted and obtain traditional Chinese drug inspissation thing,
Step 2：Stirred evenly after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
To agranular mixed serum；
Step 3：Moderate heat boils mixed serum constant temperature to 30 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea tree are poured into when boiling
Oil, stirring to slurries becomes thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 5min, turns moderate heat 15min to cake after water is boiled
Body is transparent, that is, water chestnut cake is made.
Embodiment 2
A kind of water chestnut cake, is made according to percent by weight of following raw material：29% water, 15% water chestnut starch, 15% wheat
Flour, 15% mung bean flour, 10% traditional Chinese drug inspissation thing, 5% flavor enhancement, 10% green tea powder, 1% tea oil；The traditional Chinese drug inspissation thing
It is made according to percent by weight of following raw material：+ 15% lucid asparagus of+10% Yeradetajo extract of 25% mulberry bark extract carries
Take+25% Bitter Melon P.E of the carambola root of thing+25% extract.
Further illustrate, the flavor enhancement is xylitol or oligoisomaltose.
Further illustrate, the mulberry bark extract is prepared by following methods：Picking is taken to be produced July in Guangzhou
The root bark of white mulberry crushed after cross 50 mesh sieves, precision weighs 100g, puts in boiling flask, adds the ethanol that mass concentration is 76%
Solution 500mL, carries out alcohol extracting, also using ultrasonic power be 100W in alcohol extracting, frequency be 40 hertz of assisted extractions 21 minutes, take
Go out to stand to room temperature, filter to take 1.01 times that filtrate then carries out being concentrated under reduced pressure into original volume.Contain in obtained material
The content of glycoprotein is 6.21mg/g.
Further illustrate, the Yeradetajo extract is prepared by following methods：After eclipta herb is crushed, add
Complex enzyme for hydrolyzing 13 minutes, carries out 3600r/min using centrifuge and centrifuges 6 minutes, take supernatant, add Sevag reagents and take off egg
White 3 times, 6 minutes every time, then carry out after being concentrated in vacuo to 1.12 times of original volume, it is molten to add the ethanol that mass fraction is 72%
Liquid carries out alcohol precipitation at 6 DEG C and stays overnight, and then carrying out 3250r/min using centrifuge centrifuges 2 minutes, and precipitation is taken out after standing, is steamed
Extract is obtained after vapour drying；The Sevag reagents are mixed to get according to volume ratio chloroform-n-butanol 3: 1；Obtain
The content containing dietary fiber is 10.21mg/g in material.
Further illustrate, the lucid asparagus extract is prepared by following methods：After lucid asparagus root tuber is cleaned, crush
100 mesh sieves are crossed, 200g powder is weighed and adds in conical flask, add 43% ethanol solution of volume fraction of 500mL, be subsequently added into
The mass concentration of 10mL is the ammonium sulfate of 0.32g/m L, and vibration stands 22 minutes after 1 minute, in 42 DEG C of temperature, power
30min is extracted under the ultrasound condition of 52W, is filtered, solution is moved into stratification in separatory funnel.Upper solution is taken, is sprayed
Lucid asparagus extract is can obtain after mist drying.The content containing steroidal is 19.96mg/g in obtained material.
Further illustrate, the carambola root extract is prepared by following methods：After carambola root rhizome is crushed
Take 100g to add in triangular flask, add 2% acetic acid methanol solution of cumulative volume, carried out at 36 DEG C, under microwave power 500W
The reaction of 22 minutes, is then centrifuged and takes solution, and carambola root extract is can obtain after spray drying.Obtained thing
Contain flavonoids 7.20mg/g, phenols 8.57mg/g, alkaloid 4.95mg/g, terpene 5.21mg/g, saponin 4.21mg/g in matter.
Further illustrate, the Bitter Melon P.E is prepared by following methods：After balsam pear remove seed is smashed to pieces, quality is added
42% ethanol solution of fraction carries out refluxing extraction, and the condition of refluxing extraction is to repeat extraction 2 times, 22 minutes every time, the temperature of extraction
Spend for 52 DEG C, carry out being concentrated under reduced pressure into original volume after the filtrate for repeating extraction is merged 1.12 times can obtain balsam pear extraction
Thing；The volume ratio of balsam pear and ethanol solution is 1:22.Contain terpene 5.17mg/g, steroidal 3.05mg/g in obtained material.
The preparation method of water chestnut cake as described above, specifically includes following steps：
Step 1：Mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, balsam pear are carried
Take thing to match combination according to percetage by weight after being extracted and obtain traditional Chinese drug inspissation thing,
Step 2：Stirred evenly after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
To agranular mixed serum；
Step 3：Moderate heat boils mixed serum constant temperature to 35 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea tree are poured into when boiling
Oil, stirring to slurries becomes thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 6min, turns moderate heat 16min to cake after water is boiled
Body is transparent, that is, water chestnut cake is made.
Embodiment 3
A kind of water chestnut cake, is made according to percent by weight of following raw material：32% water, 13% water chestnut starch, 12% wheat
Flour, 11% mung bean flour, 8% traditional Chinese drug inspissation thing, 7% flavor enhancement, 14% green tea powder, 3% tea oil；The traditional Chinese drug inspissation thing is pressed
It is made according to percent by weight of following raw material：+ 20% lucid asparagus of+15% Yeradetajo extract of 20% mulberry bark extract is extracted
+ 30% Bitter Melon P.E of the carambola root of thing+15% extract.
Further illustrate, the flavor enhancement is xylitol or oligoisomaltose.
Further illustrate, the mulberry bark extract is prepared by following methods：Picking is taken to be produced July in Guangzhou
The root bark of white mulberry crushed after cross 50 mesh sieves, precision weighs 100g, puts in boiling flask, adds the ethanol that mass concentration is 77%
Solution 500mL, carries out alcohol extracting, also using ultrasonic power be 100W in alcohol extracting, frequency be 40 hertz of assisted extractions 23 minutes, take
Go out to stand to room temperature, filter to take 1.01 times that filtrate then carries out being concentrated under reduced pressure into original volume.Contain in obtained material
The content of glycoprotein is 7.27mg/g.
Further illustrate, the Yeradetajo extract is prepared by following methods：After eclipta herb is crushed, add
Complex enzyme for hydrolyzing 14 minutes, carries out 3700r/min using centrifuge and centrifuges 7 minutes, take supernatant, add Sevag reagents and take off egg
White time, 7 minutes every time, then carry out after being concentrated in vacuo to 1.12 times of original volume, it is molten to add the ethanol that mass fraction is 76%
Liquid carries out alcohol precipitation at 7 DEG C and stays overnight, and then carrying out 3500r/min using centrifuge centrifuges 2 minutes, and precipitation is taken out after standing, is steamed
Extract is obtained after vapour drying；The Sevag reagents are mixed to get according to volume ratio chloroform-n-butanol 3: 1；Obtain
The content containing dietary fiber is 12.06mg/g in material.
Further illustrate, the lucid asparagus extract is prepared by following methods：After lucid asparagus root tuber is cleaned, crush
100 mesh sieves are crossed, 200g powder is weighed and adds in conical flask, add 46% ethanol solution of volume fraction of 500mL, be subsequently added into
The mass concentration of 10mL is the ammonium sulfate of 0.35/m L, and vibration stands 23 minutes after 1 minute, in 46 DEG C of temperature, power 57W
Ultrasound condition under extract 30min, filter, by solution move into separatory funnel in stratification.Upper solution is taken, it is dry to carry out spraying
Lucid asparagus extract is can obtain after dry.The content containing steroidal is 30.00mg/g in obtained material.
Further illustrate, the carambola root extract is prepared by following methods：After carambola root rhizome is crushed
Take 100g to add in triangular flask, add 1.5% acetic acid methanol solution of cumulative volume, at 37 DEG C, under microwave power 500W into
The row reaction of 23 minutes, is then centrifuged and takes solution, and carambola root extract is can obtain after spray drying.Obtain
Contain flavonoids 13.25mg/g, phenols 12.63mg/g, alkaloid 12.96mg/g, terpene 10.02mg/g, saponin in material
11.31mg/g。
Further illustrate, the Bitter Melon P.E is prepared by following methods：After balsam pear remove seed is smashed to pieces, quality is added
47% ethanol solution of fraction carries out refluxing extraction, and the condition of refluxing extraction is to repeat extraction 2 times, 27 minutes every time, the temperature of extraction
Spend for 56 DEG C, carry out being concentrated under reduced pressure into original volume after the filtrate for repeating extraction is merged 1.12 times can obtain balsam pear extraction
Thing；The volume ratio of balsam pear and ethanol solution is 1:26.Contain terpene 8.21mg/g, steroidal 5.96mg/g in obtained material.
The preparation method of water chestnut cake as described above, specifically includes following steps：
Step 1：Mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, balsam pear are carried
Take thing to match combination according to percetage by weight after being extracted and obtain traditional Chinese drug inspissation thing,
Step 2：Stirred evenly after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
To agranular mixed serum；
Step 3：Moderate heat boils mixed serum constant temperature to 36 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea tree are poured into when boiling
Oil, stirring to slurries becomes thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 7min, turns moderate heat 17min to cake after water is boiled
Body is transparent, that is, water chestnut cake is made.
Embodiment 4
A kind of water chestnut cake, is made according to percent by weight of following raw material：35% water, 10% water chestnut starch, 10% wheat
Flour, 10% mung bean flour, 5% traditional Chinese drug inspissation thing, 10% flavor enhancement, 15% green tea powder, 5% tea oil；The traditional Chinese drug inspissation thing
It is made according to percent by weight of following raw material：+ 22% lucid asparagus of+18% Yeradetajo extract of 18% mulberry bark extract carries
Take+20% Bitter Melon P.E of the carambola root of thing+22% extract.
Further illustrate, the flavor enhancement is xylitol or oligoisomaltose.
Further illustrate, the mulberry bark extract is prepared by following methods：Picking is taken to be produced July in Guangzhou
The root bark of white mulberry crushed after cross 50 mesh sieves, precision weighs 100g, puts in boiling flask, adds the ethanol that mass concentration is 80%
Solution 500mL, carries out alcohol extracting, also using ultrasonic power be 100W in alcohol extracting, frequency be 40 hertz of assisted extractions 25 minutes, take
Go out to stand to room temperature, filter to take 1.01 times that filtrate then carries out being concentrated under reduced pressure into original volume.Contain in obtained material
The content of glycoprotein is 7.42mg/g.
Further illustrate, the Yeradetajo extract is prepared by following methods：After eclipta herb is crushed, add
Complex enzyme for hydrolyzing 20 minutes, carries out 4000r/min using centrifuge and centrifuges 10 minutes, take supernatant, add Sevag reagents and take off egg
White 3 times, 8 minutes every time, then carry out after being concentrated in vacuo to 1.12 times of original volume, it is molten to add the ethanol that mass fraction is 80%
Liquid carries out alcohol precipitation at 8 DEG C and stays overnight, and then carrying out 4000r/min using centrifuge centrifuges 3 minutes, and precipitation is taken out after standing, is steamed
Extract is obtained after vapour drying；The Sevag reagents are mixed to get according to volume ratio chloroform-n-butanol 4: 1；Obtain
The content containing dietary fiber is 12.06mg/g in material.
Further illustrate, the lucid asparagus extract is prepared by following methods：After lucid asparagus root tuber is cleaned, crush
100 mesh sieves are crossed, 200g powder is weighed and adds in conical flask, add 50% ethanol solution of volume fraction of 500mL, be subsequently added into
The mass concentration of 10mL is the ammonium sulfate of 0.4g/m L, and vibration stands 25 minutes after 1 minute, in temperature 50 C, power 60W
Ultrasound condition under extract 30min, filter, by solution move into separatory funnel in stratification.Upper solution is taken, it is dry to carry out spraying
Lucid asparagus extract is can obtain after dry.The content containing steroidal is 30.00mg/g in obtained material.
Further illustrate, the carambola root extract is prepared by following methods：After carambola root rhizome is crushed
Take 100g to add in triangular flask, add 3% acetic acid methanol solution of cumulative volume, carried out at 40 DEG C, under microwave power 500W
The reaction of 25 minutes, is then centrifuged and takes solution, and carambola root extract is can obtain after spray drying.Obtained thing
Contain flavonoids 13.25mg/g, phenols 12.63mg/g, alkaloid 12.96mg/g, terpene 10.02mg/g, saponin in matter
11.31mg/g。
Further illustrate, the Bitter Melon P.E is prepared by following methods：After balsam pear remove seed is smashed to pieces, quality is added
50% ethanol solution of fraction carries out refluxing extraction, and the condition of refluxing extraction is to repeat extraction 3 times, 30 minutes every time, the temperature of extraction
Spend for 60 DEG C, carry out being concentrated under reduced pressure into original volume after the filtrate for repeating extraction is merged 1.12 times can obtain balsam pear extraction
Thing；The volume ratio of balsam pear and ethanol solution is 1:30.Contain terpene 8.21mg/g, steroidal 5.96mg/g in obtained material.
The preparation method of water chestnut cake as described above, specifically includes following steps：
Step 1：Mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, balsam pear are carried
Take thing to match combination according to percetage by weight after being extracted and obtain traditional Chinese drug inspissation thing,
Step 2：Stirred evenly after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
To agranular mixed serum；
Step 3：Moderate heat boils mixed serum constant temperature to 39 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea tree are poured into when boiling
Oil, stirring to slurries becomes thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 6min, turns moderate heat 17min to cake after water is boiled
Body is transparent, that is, water chestnut cake is made.
Experiment one：
Water chestnut cake that 1-4 of the embodiment of the present invention, comparative example 1-3 are prepared carries out ocular estimate, gel strength and cold
But there are the situation that evaporated condensation water separates out, record such as table 1 below afterwards.
Comparative example 1：It is essentially identical with the water chestnut cake formula of embodiment 3, common side is used unlike in preparation method
Method will all raw materials mix after directly polish and place steaming plate and steam and form.
Comparative example 2：Essentially identical with the water chestnut cake formula of embodiment 3, step 3 does not have the stream that moderate heat boils in preparation method
Journey, directly with entering step 3 after traditional Chinese drug inspissation thing, flavor enhancement, tea oil stirring.
Comparative example 3：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is to be not added with green tea powder in formula.
Comparative example 4：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is that to be not added with Chinese medicine dense in formula
Contracting thing.
Table 1
| Appearance | Gel strength (g/cm2) | There is evaporated condensation water precipitation after cooling | |
| Embodiment 1 | Surface is smooth, without layering, nattierblue | 312 | Nothing |
| Embodiment 2 | Surface is smooth, without layering, nattierblue | 322 | Nothing |
| Embodiment 3 | Surface is smooth, without layering, nattierblue | 351 | Nothing |
| Embodiment 4 | Surface is smooth, without layering, nattierblue | 324 | Nothing |
| Comparative example 1 | Surface is smooth, has layering, nattierblue | 220 | Have |
| Comparative example 2 | Surface is smooth, has layering, nattierblue | 200 | Have |
| Comparative example 3 | Surface is smooth, has layering, is faint yellow | 234 | Have |
| Comparative example 4 | Surface is smooth, has layering, nattierblue | 221 | Have |
It is advantageous in appearance using comparative example 1-4 as seen from the above table, and processing step difference can influence water chestnut cake
, there is lamination in quality, and gel strength can also decrease；And by varying the composition on raw material, it can also influence to coagulate
There is the phenomenon that evaporated condensation water separates out after glue intensity and appearance cooling, turned out by comparative example 3-4, illustrate green tea powder and Chinese medicine
Concentrate has significant impact to the physical qualities of water chestnut cake.
Experiment two：
After embodiment 1-4 and comparative example the 1-6 water chestnut cake being prepared are packed, random selection 3 carries out such as
Under experiment：
With reference to GB/T 4789.2 (2003) food hygiene Micro biological Tests-total plate count method for measuring.First use hammer
Water chestnut cake is ground across vacuum packaging bag.Under sterile environment, vacuum bag is cut off, with transfer needle picking 5g samples to containing
In the triangular flask of 45ml aqua sterilisas, cloth plug beyond the Great Wall.Triangular flask is placed in shake well about 3min on eddy mixer, obtains 1:10
Uniform bacteria suspension.
1ml 1 is pipetted respectively with the pipette of 1ml:100、1:103With 1:104Bacteria suspension in sterilized culture dish,
After 37 DEG C of nutrient agar culture 24h, by colonometer, the clump count of each culture dish is counted.Sanitary index
Quote GB799 (2003) cake, bread sanitary standard --- total plate count is dispatched from the factory≤750, sale≤1000.
Comparative example 1：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is：The root bark of white mulberry is not added with formula
Extract.
Comparative example 2：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is：Eclipta is not added with formula
Extract.
Comparative example 3：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is：Lucid asparagus is not added with formula
Extract.
Comparative example 4：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is：Fine hair wood is not added with formula
Blue extract.
Comparative example 5：Essentially identical with the water chestnut cake preparation method of embodiment 3, difference is：Balsam pear is not added with formula to carry
Take thing.
Comparative example 6：Water chestnut cake difference with embodiment 3 is：The root bark of white mulberry, eclipta, lucid asparagus, fine hair are used in formula
Traditional Chinese drug inspissation thing is replaced in mixing after wooden blue, balsam pear is crushed.
2 colony count unit (a) of table
| 1 day | 2 days | 3 days | 5 days | 7 days | 9 days | |
| Embodiment 1 | 14 | 92 | 126 | 354 | 2651 | 45632 |
| Embodiment 2 | 16 | 89 | 119 | 346 | 2598 | 44265 |
| Embodiment 3 | 10 | 86 | 112 | 326 | 2459 | 42585 |
| Embodiment 4 | 15 | 90 | 120 | 349 | 2596 | 44897 |
| Comparative example 1 | 25 | 115 | 295 | 952 | 8521 | - |
| Comparative example 2 | 26 | 126 | 300 | 958 | 8561 | - |
| Comparative example 3 | 24 | 120 | 294 | 968 | 8412 | - |
| Comparative example 4 | 28 | 119 | 289 | 972 | 8597 | - |
| Comparative example 5 | 23 | 123 | 305 | 1011 | 8602 | - |
| Comparative example 6 | 18 | 124 | 312 | 869 | 5695 | 78562 |
Remarks："-" represents countless.
As seen from the above table, being added to one of raw material using the formula combination of the traditional Chinese drug inspissation thing of the application has significant resist
Bacterium ability, has the function that synergy compared to more single combination antibacterial effect；Also had using the Chinese traditional medicine composition of active compound compared to relatively direct
There is significant difference, it was demonstrated that the combination of the active material of traditional Chinese drug inspissation thing can play the role of synergy and notable antibacterial.
Experiment three：
1 toxicological test：
Acute toxicity test：Mouse, rat limosis gavage traditional Chinese drug inspissation thing of the present invention, are observed 7 days, male and female mouse and rat
It is showed no poisoning symptom, no death, traditional Chinese drug inspissation thing male and female mouse of the present invention and rat peroral acute toxicity experiment MTD>
10.0g/kg.BW, the true nontoxic level in border.
With the traditional Chinese drug inspissation thing of embodiment in the application 3 to mouse, rat limosis gavage, thing is dead after observing 14 days, right
Male and female mouse and rat are showed no poisoning symptom, no death, and animal subject is not put to death and carries out dissection inspection by the observation period, liver, board,
The main organs such as kidney, stomach, intestines, the heart, lung, show no obvious abnormalities change.Traditional Chinese drug inspissation thing male and female mouse of the present invention and rat oral
Acute toxicity test MTD>10.0g/kg.BW according to《Health food is examined and assessment technique specification)) urgency in (version in 2003)
Property toxicity grading standard, belongs to nontoxic level.
Traditional Chinese drug inspissation thing Salmonella reversion test of the present invention, mouse marrow cell micro nuclear test and mouse sperm distortion test result are equal
For feminine gender, traditional Chinese drug inspissation thing safety of the present invention is prompted.
In the present invention during 30 days feeding trials of medicine concentrate, the activity of animal, ingest, the ordinary circumstance such as defecation has no
It is obvious abnormal, and the weight to animal, food-intake, routine blood indexes, organ weights have no significant effect, in the high agent of female male rat
Items Testing index does not observe anomalous variation when amount group is 20.00g/kg.BW (equivalent to 500 times of human body recommended amounts).2
Clinical test
Quench one's thirst to the present invention treatment deficiency of both qi and yin disease patient the effect of carry out clinical observation, pass through and contrast that medication is front and rear to suffer from
Person uses the amount analysis of insulin hypoglycemic effect of the invention.
3 inclusive criterias
All have that polydipsia, the paddy that disappears are easily hungry, urine is more and sweet tea, body are gradually shown in that patient of becoming thin can be diagnosed as diabete
(diabetes)；All lassitude hypodynamias, the lazy speech of spontaneous sweating, shortness of breath, thirst and liking drink, dysphoria in chestpalms-soles, palpitation and insomnia, urinate red constipation, tongue
HongShaoJin(SIC), tongue body fat big, tongue are thin or flower is shelled, small and wiry pulse or number person, are Qi and Yin deficiency diabetes mellitus；There is diabetic symptom, appoint
When between blood glucose ＞ 11.1mmol/L or fasting blood-glucose ＞ 7.0mmol/L；Diabetes B is had been determined as, long-term use of diformazan is double
The patient of guanidine or the patient of long term injections insulin；All patients meet 1 or more than 1 in above-mentioned 4.
4 case selections
It is all while meet above-mentioned doctor trained in Western medicine criteria for classification, TCM syndrome diagnostic criteria patient；Age 18-65 year person；It is ready to connect
By 2 weeks curers；Signature enters clinical research informed consent form person.
4 medicines
The water chestnut cake prepared by 3 method of embodiment；
Regular iletin：Jiangsu Wanbang Biological Pharmaceutical Co., Ltd., lot number：1007217.
5 clinical tests are grouped
Comparative example group：Insulin
Test example group：Embodiment 3+ insulin
6 observation indexs：Observe the situation of change of main clinic symptoms and sign, on an empty stomach and it is postprandial 2 it is small when blood sugar test；Pancreas
The decrement of island element dosage.
7 treatment methods：
7.1 start to check that blood glucose mean is fasting blood-glucose ＞ 7.0mmol/L before being administered for continuous 3 times, and postprandial blood sugar is
＞ 11.1mmol/L；Other any hypoglycemics must be disabled before meeting 100 clothes for patients development clinical test of inclusion criteria
Chinese and Western medicine.
100 patients of 7.2 comparative example groups continue to use insulin；The horseshoe of 100 clothes for patients embodiments 3 of test example group
Cake water chestnut cake, each 100g, 3 times a day, 30 minutes before meals oral, and 2 weeks are 1 course for the treatment of, and therapeutic process is used cooperatively insulin
Blood glucose is controlled in critical field.
7.3 therapeutic processes strictly carry out dietetic treatment.
7.4 result：Test group patient is gradually reduced in 2 weeks or so blood glucose of taking medicine, and insulin usage amount gradually reduces, hypoglycemic
Effect is steady, and the observation to safety indexes shows, medicine of the present invention has no adverse reaction.Insulin dosage is seen below after clinical treatment
Table.
Insulin dosage (x ± s) (n=100) after table 3 is treated
| Group | Insulin dosage |
| Experimental group | 19±1.2U |
| Contrast groups | 49±2.6U |
Test example group is compared with comparative example group, P<0.01.
The result shows that：With the use of the dosage of insulin while treatment using the present invention, controlled with insulin is used alone
Dosage during treatment is compared, and has pole significant difference (P<0.01), illustrate that Chinese medicine composition of the present invention suffers from type of deficiency of both QI and YIN diabetes
Person has notable hypoglycemic effect, its insulin dosage is substantially reduced to insulin-dependent patient.
And two courses for the treatment of are carried out to 100 water chestnut cake for taking embodiment 3 patients and take rear physical examination, result of the test shows,
After taking two courses for the treatment of, type of deficiency of both QI and YIN diabetes patient clinical symptom can be obviously improved, reduces fasting blood-glucose and postprandial 2h blood
Sugar (P<0.05)；Blood, urine, stool and hepatic and renal function items Testing index prompt embodiment 3 in normal range (NR) before and after test-meal
Water chestnut cake, without obvious infringement, has treatment diabetes effect to tested patients' health.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, equal change or the modification change completed under the technical spirit suggested by all present invention, should all belong to
Cover the scope of the claims in the present invention.
Claims (8)
1. a kind of water chestnut cake, it is characterised in that be made according to percent by weight of following raw material：25%-35% water, 10%-
15% water chestnut starch, 10%-15% wheat flours, 10%-15% mung bean flours, 5%-10% traditional Chinese drug inspissations thing, 5%-10% seasonings
Agent, 10%-15% green tea powders, 1%-5% tea oils；The traditional Chinese drug inspissation thing is according to percent by weight by following raw material system
Into：15-25% mulberry bark extract+10-20% Yeradetajo extract+15-25% lucid asparagus extract+15-25% fine hair wood
Blue extract+20-30% Bitter Melon P.Es.
2. water chestnut cake according to claim 1, it is characterised in that the flavor enhancement is xylitol or oligoisomaltose.
3. water chestnut cake according to claim 1, it is characterised in that the mulberry bark extract is prepared into by following methods
Arrive：Take picking to be produced July and 50 mesh sieves are crossed after the root bark of white mulberry in Guangzhou is crushed, precision weighs 100g, puts boiling flask
In, the ethanol solution 500mL that mass concentration is 75-80% is added, alcohol extracting is carried out, is also using ultrasonic power in alcohol extracting
100W, frequency are 40 hertz of assisted extractions 20-25 minute, take out standing to room temperature, filter to take filtrate and be then concentrated under reduced pressure
To 1.01 times of original volume.
4. water chestnut cake according to claim 1, it is characterised in that the Yeradetajo extract is prepared into by following methods
Arrive：
After eclipta herb is crushed, add complex enzyme for hydrolyzing 10-20 minute, using centrifuge progress 3500-4000r/min from
Heart 5-10 minutes, takes supernatant, adds Sevag reagents and takes off albumen 2-3 times, each 5-8 minutes, then carries out being concentrated in vacuo to original
After 1.12 times of volume, addition mass fraction carries out alcohol precipitation for the ethanol solution of 70-80% at 5-8 DEG C and stays overnight, and then uses
Centrifuge carries out 3000-4000r/min and centrifuges 1-3 minutes, and precipitation is taken out after standing, extract is obtained after steam drying；It is described
Sevag reagents are mixed to get according to volume ratio chloroform-n-butanol 3-4: 1.
5. water chestnut cake according to claim 1, it is characterised in that the lucid asparagus extract is prepared into by following methods
Arrive：After lucid asparagus root tuber is cleaned, 100 mesh sieves are crushed, 200g powder is weighed and adds in conical flask, add the volume of 500mL
Fraction 40-50% ethanol solutions, the mass concentration for being subsequently added into 10mL is the ammonium sulfate of 0.3-0.4g/m L, vibrates 1 point
Stand 20-25 minutes after clock, 40-50 DEG C of temperature, power 50-60W ultrasound condition under extract 30min, filter, solution is moved
Enter stratification in separatory funnel.Upper solution is taken, lucid asparagus extract is can obtain after being spray-dried.
6. water chestnut cake according to claim 1, it is characterised in that the carambola root extract is prepared into by following methods
Arrive：Take 100g to add in triangular flask after carambola root rhizome is crushed, add the acetic acid methanol solution of the 1-3% of cumulative volume,
The reaction of 20-25 minutes is carried out at 35-40 DEG C, under microwave power 500W, is then centrifuged and takes solution, after spray drying
It can obtain carambola root extract.
7. water chestnut cake according to claim 1, it is characterised in that the Bitter Melon P.E is prepared by following methods：
After balsam pear remove seed is smashed to pieces, add mass fraction 40-50% ethanol solutions and carry out refluxing extraction, the condition of refluxing extraction is to repeat
Extraction 2-3 times, 20-30 minutes each, the temperature of extraction is 50-60 DEG C, after the filtrate for repeating extraction is merged depressurize dense
Be reduced to original volume 1.12 times can obtain Bitter Melon P.E；The volume ratio of balsam pear and ethanol solution is 1:20-30.
8. the preparation method of the water chestnut cake according to claim 1-7 any one, it is characterised in that specifically include following step
Suddenly：
Step 1：By mulberry bark extract, Yeradetajo extract, lucid asparagus extract, carambola root extract, Bitter Melon P.E
Traditional Chinese drug inspissation thing is obtained according to percetage by weight proportioning combination after being extracted,
Step 2：Nothing is evenly stirred until after water, water chestnut starch, wheat flour, mung bean flour, green tea powder are mixed according to percentage by weight
The mixed serum of particle；
Step 3：Moderate heat boils mixed serum constant temperature to 30-40 DEG C, and traditional Chinese drug inspissation thing, flavor enhancement, tea oil are poured into when boiling,
Stirring to slurries become thick-pasty cake；
Step 4：Paste cake is poured into steaming plate and is smoothed out, water proof big fire steaming 5-8min, turns moderate heat 15-18min extremely after water is boiled
Cake body is transparent, that is, water chestnut cake is made.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103461846A (en) * | 2013-09-22 | 2013-12-25 | 李燕 | Grain water chestnut cake and preparation method thereof |
| CN104187489A (en) * | 2014-07-31 | 2014-12-10 | 周晓兰 | Smoked plum and water chestnut cake and preparing method thereof |
| CN105285291A (en) * | 2015-10-27 | 2016-02-03 | 安徽科技学院 | Pagodatree flower and water chestnut cakes and making method thereof |
-
2017
- 2017-11-24 CN CN201711186639.3A patent/CN107897674A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103461846A (en) * | 2013-09-22 | 2013-12-25 | 李燕 | Grain water chestnut cake and preparation method thereof |
| CN104187489A (en) * | 2014-07-31 | 2014-12-10 | 周晓兰 | Smoked plum and water chestnut cake and preparing method thereof |
| CN105285291A (en) * | 2015-10-27 | 2016-02-03 | 安徽科技学院 | Pagodatree flower and water chestnut cakes and making method thereof |
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Application publication date: 20180413 |