CN107894344A - A kind of circulating sampler of industrial reaction container - Google Patents
A kind of circulating sampler of industrial reaction container Download PDFInfo
- Publication number
- CN107894344A CN107894344A CN201711132064.7A CN201711132064A CN107894344A CN 107894344 A CN107894344 A CN 107894344A CN 201711132064 A CN201711132064 A CN 201711132064A CN 107894344 A CN107894344 A CN 107894344A
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- China
- Prior art keywords
- push switch
- surge drum
- reaction container
- chassis
- electric pushrod
- Prior art date
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/04—Devices for withdrawing samples in the solid state, e.g. by cutting
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The present invention provides a kind of circulating sampler of industrial reaction container.The circulating sampler of the industrial reaction container, including base；Baffle plate, the baffle plate are fixed on the base sidepiece；Rotating mechanism, the rotating mechanism include disk, chassis and motor；Include groove, electromagnet, the second push switch and the second electric pushrod inside the disk；First push switch, first push switch are located at the sidepiece on the chassis；First electric pushrod, first electric pushrod are fixed between the disk and the chassis；Sampling container, the sampling container include surge drum, rubber stopper and iron block；Probe tube, the probe tube are placed in the top of the sampling container.The circulating sampler of industrial reaction container provided by the invention, being sampled to inside reactor for circulation can be effectively realized, security performance is high, simple to operate flexible, reduces labour.
Description
Technical field
The present invention relates to technical field of industrial equipment, more particularly to a kind of circulating sampler of industrial reaction container.
Background technology
Industrial reaction container be chemically reacted, the container of physical reactions, industrial reaction container has rapid, the resistance to height of heating
Warm, corrosion-resistant, hygienic, non-environmental-pollution, the features such as not needing boiler automatic heating, be easy to use, it is widely used in oil, changes
Work, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying, hydrogenating, hydrocarbonylation, polymerization, the technical process such as condensation.
Being sampled to reaction vessel interior for timing, existing reactor sampler are needed in order to detect reaction process
Manual sampling is used mostly, manual sampling security performance is low, it is necessary to which timing sampling, labor intensive, error are big.
Therefore, it is necessary to the circulating sampler for providing a kind of new industrial reaction container solves above-mentioned technical problem.
The content of the invention
Present invention solves the technical problem that it is to provide a kind of automatic sampling that can effectively realize circulation, and efficiency high, operation
The circulating sampler of simple industrial reaction container.
In order to solve the above technical problems, the circulating sampler of industrial reaction container provided by the invention, including：Bottom
Seat；Baffle plate, the baffle plate are fixed on the base sidepiece；Rotating mechanism, the rotating mechanism include disk, chassis and motor；
The motor is provided with the inside of the base, and chassis described in the motor connection；The top on the chassis is provided with the disk；
Include groove, electromagnet, the second push switch and the second electric pushrod inside the disk, and the groove is located at the circle
The surface of disk；The inner side of the groove is provided with the electromagnet, and second electric pushrod is fixed in the bottom of the electromagnet；
The sidepiece of second electric pushrod is provided with second push switch, and described in second push switch electric connection
Second electric pushrod and the electromagnet；First push switch, first push switch are located at the sidepiece on the chassis,
And first push switch is electrically connected with second electric pushrod and the electromagnet；First electric pushrod, described
One electric pushrod is fixed between the disk and the chassis, and first electric pushrod is electrically connected with first pressing
Formula switchs and second push switch；Sampling container, the sampling container include surge drum, rubber stopper and iron block, and institute
State the inside that surge drum is placed in the groove；The inside of the surge drum is from top to bottom provided with the rubber stopper and the iron block；
Probe tube, the probe tube are placed in the top of the sampling container.
Preferably, the probe tube runs through reacting tank body, and side shield is fixed in the both sides of the reacting tank body.
Preferably, the inside of the reacting tank body is provided with collecting pipe, and the collecting pipe be from top to bottom equally spaced it is some
Individual through hole；The through hole connects the probe tube.
Preferably, the sampling container also includes sideboard, and the sideboard is rotationally connected with the surge drum；
The anglec of rotation between the surge drum and the sideboard is 0 ° -90 °.
Preferably, the chassis uses the structure of central concave, and the surrounding on the chassis is equally spaced four described the
One push switch.
Preferably, the top surface of the disk be provided with the same number of groove of first push switch, and
The sidepiece of each disk is equipped with first push switch.
Preferably, the top of the surge drum is provided with opening, and the open top diameter of the surge drum and the sampling
Pipe diameter is identical.
Preferably, the use disc-shaped structure of the electromagnet, and the diameter of the electromagnet is less than the straight of the groove
Footpath；The electromagnet is with second push switch on a horizontal line.
Preferably, the basal surface of the surge drum is provided with opening, and the opening diameter of the surge drum basal surface is less than institute
State diameter at the center of surge drum；The interior diameter of the surge drum and the rubber stopper, the iron block diameter it is identical.
Compared with correlation technique, the circulating sampler of industrial reaction container provided by the invention is with following beneficial
Effect：
The present invention provides a kind of circulating sampler of industrial reaction container, and the sampling is driven using the rotation on the chassis
The rotation of container, when the sampling container rotates to the bottom of the probe tube, pressed using the spacing opening of the baffle plate
Formula switch makes the sampling container be connected with the probe tube in a manner of electric pushrod, while is carried out in a manner of negative pressure pull
Sampling, without manual operation, sampling is convenient, while the rotation that automatically reset after sampling carries out secondary sample, when realization obtains different
The sample of the interior reacting tank body, it is easy to observe and detect reaction process, automation mechanized operation is safe, flexible.
Brief description of the drawings
Fig. 1 is that a kind of structure of preferred embodiment of the circulating sampler of industrial reaction container provided by the invention is shown
It is intended to；
Fig. 2 is the reacting tank body internal structure schematic diagram shown in Fig. 1；
Fig. 3 is the probe tube and sampling container attachment structure schematic diagram shown in Fig. 1；
Fig. 4 is the disk internal structure schematic diagram shown in Fig. 1；
Fig. 5 is the sampling container structural representation shown in Fig. 1；
Fig. 6 is the workflow diagram of the control method of the circulating sampler of industrial reaction container provided by the invention.
Label in figure：1st, reacting tank body, 2, side shield, 3, probe tube, the 4, first push switch, 5, sampling container, 51,
Sideboard, 52, surge drum, 53, rubber stopper, 54, iron block, 6, rotating mechanism, 61, disk, 611, groove, 612, electromagnet,
613rd, the second push switch, the 614, second electric pushrod, 62, chassis, 63, motor, 7, baffle plate, 8, base, 9, collecting pipe,
91st, through hole, 9a, the first electric pushrod.
Embodiment
The invention will be further described with embodiment below in conjunction with the accompanying drawings.
Fig. 1, Fig. 2, Fig. 3, Fig. 4 and Fig. 5 are please referred to, wherein, Fig. 1 is industrial reaction container provided by the invention
A kind of structural representation of preferred embodiment of circulating sampler；Fig. 2 is the reacting tank body internal structure signal shown in Fig. 1
Figure；Fig. 3 is the probe tube and sampling container attachment structure schematic diagram shown in Fig. 1；Fig. 4 is that the disk internal structure shown in Fig. 1 is shown
It is intended to；Fig. 5 is the sampling container structural representation shown in Fig. 1；The circulating sampler of industrial reaction container includes：Base 8；
Baffle plate 7, the baffle plate 7 are fixed on the sidepiece of base 8；Rotating mechanism 6, the rotating mechanism 6 include disk 61, the and of chassis 62
Motor 63；The motor 63 is provided with the inside of the base 8, and the motor 63 connects the chassis 62；The chassis 62
Top is provided with the disk 61；The inside of the disk 61 includes groove 611, electromagnet 612, the second push switch 613 and the
Two electric pushrods 614, and the groove 611 is located at the surface of the disk 61；The inner side of the groove 611 is provided with the electromagnetism
Iron 612, and second electric pushrod 614 is fixed in the bottom of the electromagnet 612；The sidepiece of second electric pushrod 614
Provided with second push switch 613, and second push switch 613 is electrically connected with second electric pushrod 614
With the electromagnet 612；First push switch 4, first push switch 4 are located at the sidepiece on the chassis 62, and institute
State the first push switch 4 and be electrically connected with second electric pushrod 614 and the electromagnet 612；First electric pushrod 9a, institute
State the first electric pushrod 9a to be fixed between the disk 61 and the chassis 62, and the first electric pushrod 9a is electrically connected with
First push switch 4 and second push switch 613；Sampling container 5, the sampling container 5 include surge drum
52nd, rubber stopper 53 and iron block 54, and the surge drum 52 is placed in the inside of the groove 611；The inside of the surge drum 52 by
Above have the rubber stopper 53 and the iron block 54；Probe tube 3, the probe tube 3 are placed in the top of the sampling container 5
Portion.
For fast sampling, the probe tube 3 runs through reacting tank body 1, and side shield is fixed in the both sides of the reacting tank body 1
2。
In order that the sample obtained is representative, the inside of the reacting tank body 1 is provided with collecting pipe 9, and the collection
Pipe 9 is from top to bottom equally spaced several through holes 91；The through hole 91 connects the probe tube 3.
In order to be packaged to the sample of acquirement, the sampling container 5 also includes sideboard 51, and the sideboard
51 are rotationally connected with the surge drum 52；The anglec of rotation between the surge drum 52 and the sideboard 51 is 0 ° -90 °.
In order to realize that the lifting to the disk 61 is controlled, the chassis 62 uses the structure of central concave, and institute
The surrounding for stating chassis 62 is equally spaced four first push switch 4.
For the ease of obtaining the sample of multiple different times, the top surface of the disk 61 is provided with and first push type
4 the same number of grooves 611 are switched, and the sidepiece of each disk 61 is equipped with first push switch 4.
In order to avoid sample is spilt, the top of the surge drum 52 is provided with opening, and the open top of the surge drum 52
Diameter is identical with the diameter of probe tube 3.
For the ease of carrying out taking out detection after acquirement sample, the electromagnet 612 uses disc-shaped structure, and the electricity
The diameter of magnet 612 is less than the diameter of the groove 611；The electromagnet 612 is with second push switch 613 at one
On horizontal line.
In order to avoid pull excessively causes the waste of sample, the basal surface of the surge drum 52 is provided with opening, and the receipts
The opening diameter for collecting the basal surface of cylinder 52 is less than diameter at the center of the surge drum 52；The interior diameter of the surge drum 52 with it is described
Rubber stopper 53, the diameter of the iron block 54 are identical.
Fig. 6 is the workflow diagram of the control method of the circulating sampler of industrial reaction container provided by the invention.
The control method of the circulating sampler of the industrial reaction container comprises the following steps：
S1：Sampler is put into；
Specifically, the sampling container 5 is sequentially placed into the inside of the groove 611.
S2：Connect sampler；
S21：The rotation of sampling mechanism；
Specifically, opening the motor 63, the motor 63 is set to drive the chassis 62 to rotate.
S22：The connection of probe tube and surge drum；
Specifically, when first push switch 4 rotates to the bottom of the baffle plate 7, the quilt of the first push switch 4
Open, start the first electric pushrod 9a, the disk 61, which rises, connects the surge drum 52 and the probe tube 3
It is logical.
S3：Sampling below atmospheric pressure；
S31：It is sampled；
It is powered specifically, first push switch 4 can make the electromagnet 612 switch on power after being opened, it is right
The iron block 54 is attracted, and second electric pushrod 614 is i.e. recyclable, pulls the iron block 54 and the rubber stopper 53
Make to form negative pressure in the surge drum 52, to being sampled inside the reacting tank body 1.
S32：Sampler disconnects；
Specifically, second push switch 613, driving described first are pressed after second electric pushrod 614 decline
Electric pushrod 9a resets the power supply for the electromagnet 612 for simultaneously switching off relevant position, makes the surge drum 52 and the sampling
Pipe 3 disconnects.
S33：Cycle sampling；
Specifically, the motor 63 continues to rotate, next first push switch 4 is pressed progress next round and take
Sample, complete circulating sampling.
S4：Sampler is removed；
Specifically, close the motor 63, deenergization, it is ensured that it is nonmagnetic between the electromagnet 612 and the iron block 54, just
The surge drum 52 can be removed to be checked.
Compared with correlation technique, the circulating sampler of industrial reaction container provided by the invention is with following beneficial
Effect：
The present invention provides a kind of circulating sampler of industrial reaction container, is taken using described in the rotation drive on the chassis 62
The rotation of sample container 5, when the sampling container 5 rotates to the bottom of the probe tube 3, beaten using the spacing of baffle plate 7
Open push switch makes the sampling container 5 be connected with the probe tube 3 in a manner of electric pushrod, while with negative pressure pull
Mode is sampled, and without manual operation, sampling is convenient, while the rotation that automatically reset after sampling carries out secondary sample, and realization takes
The sample of the reacting tank body 1 in different time is obtained, is easy to observe and detect reaction process, automation mechanized operation is safe, flexible.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
The equivalent structure or equivalent flow conversion that bright specification and accompanying drawing content are made, or directly or indirectly it is used in other related skills
Art field, is included within the scope of the present invention.
Claims (9)
- A kind of 1. circulating sampler of industrial reaction container, it is characterised in that including：Base；Baffle plate, the baffle plate are fixed on the base sidepiece；Rotating mechanism, the rotating mechanism include disk, chassis and motor；The motor is provided with the inside of the base, and institute State chassis described in motor connection；The top on the chassis is provided with the disk；Include groove, electromagnet, the inside the disk Two push switch and the second electric pushrod, and the groove is located at the surface of the disk；The inner side of the groove is provided with institute Electromagnet is stated, and second electric pushrod is fixed in the bottom of the electromagnet；The sidepiece of second electric pushrod is provided with institute The second push switch is stated, and second push switch is electrically connected with second electric pushrod and the electromagnet；First push switch, first push switch are located at the sidepiece on the chassis, and first push switch It is electrically connected with second electric pushrod and the electromagnet；First electric pushrod, first electric pushrod are fixed between the disk and the chassis, and described first electronic Push rod is electrically connected with first push switch and second push switch；Sampling container, the sampling container includes surge drum, rubber stopper and iron block, and the surge drum is placed in the interior of the groove Portion；The inside of the surge drum is from top to bottom provided with the rubber stopper and the iron block；Probe tube, the probe tube are placed in the top of the sampling container.
- 2. the circulating sampler of industrial reaction container according to claim 1, it is characterised in that the probe tube passes through Reacting tank body is worn, and side shield is fixed in the both sides of the reacting tank body.
- 3. the circulating sampler of industrial reaction container according to claim 2, it is characterised in that the reacting tank body Inside be provided with collecting pipe, and the collecting pipe is from top to bottom equally spaced several through holes；The through hole connects the sampling Pipe.
- 4. the circulating sampler of industrial reaction container according to claim 1, it is characterised in that the sampling container Also include sideboard, and the sideboard is rotationally connected with the surge drum；The surge drum and the sideboard it Between the anglec of rotation be 0 ° -90 °.
- 5. the circulating sampler of industrial reaction container according to claim 1, it is characterised in that the chassis uses The structure of central concave, and the surrounding on the chassis is equally spaced four first push switch.
- 6. the circulating sampler of industrial reaction container according to claim 1, it is characterised in that the top of the disk Surface be provided with the same number of groove of first push switch, and the sidepiece of each disk be equipped with it is described First push switch.
- 7. the circulating sampler of industrial reaction container according to claim 4, it is characterised in that the surge drum Top is provided with opening, and the open top diameter of the surge drum is identical with the sampling pipe diameter.
- 8. the circulating sampler of industrial reaction container according to claim 1, it is characterised in that the electromagnet Using disc-shaped structure, and the diameter of the electromagnet is less than the diameter of the groove；The electromagnet and the described second pressing Formula is switched on a horizontal line.
- 9. the circulating sampler of industrial reaction container according to claim 7, it is characterised in that the surge drum Basal surface is provided with opening, and the opening diameter of the surge drum basal surface is less than diameter at the center of the surge drum；The receipts Collect interior diameter and the rubber stopper of cylinder, the iron block diameter it is identical.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711132064.7A CN107894344B (en) | 2017-11-15 | 2017-11-15 | Circulating sampling device of industrial reaction vessel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711132064.7A CN107894344B (en) | 2017-11-15 | 2017-11-15 | Circulating sampling device of industrial reaction vessel |
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| Publication Number | Publication Date |
|---|---|
| CN107894344A true CN107894344A (en) | 2018-04-10 |
| CN107894344B CN107894344B (en) | 2021-11-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711132064.7A Active CN107894344B (en) | 2017-11-15 | 2017-11-15 | Circulating sampling device of industrial reaction vessel |
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| CN (1) | CN107894344B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108593350A (en) * | 2018-06-04 | 2018-09-28 | 天津中德应用技术大学 | Automatic sampling system |
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| CN203490110U (en) * | 2013-10-18 | 2014-03-19 | 鲁泰纺织股份有限公司 | Automatic water sample collecting device |
| CN105806663A (en) * | 2016-06-01 | 2016-07-27 | 王保锋 | Water quality sampler for fisheries and aquaculture |
| CN105929185A (en) * | 2016-06-21 | 2016-09-07 | 鹿钦宇 | Full-automatic biochemical instrument and reagent adding method thereof |
| CN205785933U (en) * | 2016-05-23 | 2016-12-07 | 中国环境科学研究院 | A kind of lake water quality different water levels Turbidity measurement sampler |
| CN206035486U (en) * | 2016-09-13 | 2017-03-22 | 魏海 | Producing well continuous sampling device |
| CN206416727U (en) * | 2016-11-16 | 2017-08-18 | 邱卓然 | A kind of automatic ink suction pen |
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2017
- 2017-11-15 CN CN201711132064.7A patent/CN107894344B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86207448U (en) * | 1986-10-21 | 1987-11-18 | 煤炭工业部煤炭科学研究院煤化学研究所 | Ionometer with functios of automatic selection and feed of standard solution |
| CN203490110U (en) * | 2013-10-18 | 2014-03-19 | 鲁泰纺织股份有限公司 | Automatic water sample collecting device |
| CN205785933U (en) * | 2016-05-23 | 2016-12-07 | 中国环境科学研究院 | A kind of lake water quality different water levels Turbidity measurement sampler |
| CN105806663A (en) * | 2016-06-01 | 2016-07-27 | 王保锋 | Water quality sampler for fisheries and aquaculture |
| CN105929185A (en) * | 2016-06-21 | 2016-09-07 | 鹿钦宇 | Full-automatic biochemical instrument and reagent adding method thereof |
| CN206035486U (en) * | 2016-09-13 | 2017-03-22 | 魏海 | Producing well continuous sampling device |
| CN206416727U (en) * | 2016-11-16 | 2017-08-18 | 邱卓然 | A kind of automatic ink suction pen |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108593350A (en) * | 2018-06-04 | 2018-09-28 | 天津中德应用技术大学 | Automatic sampling system |
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| Publication number | Publication date |
|---|---|
| CN107894344B (en) | 2021-11-02 |
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Effective date of registration: 20211018 Address after: 330319 Spark Industrial Park, Yongxiu County, Jiujiang City, Jiangxi Province Applicant after: Jiangxi Spark Space New Materials Co.,Ltd. Address before: 210000 No.10 Fenghuang street, Jiangpu street, Pukou District, Nanjing City, Jiangsu Province - qc007 Applicant before: Nanjing think half day Technology Co.,Ltd. |
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