CN107881808A - A kind of preparation method of wormwood leaf powder print paste - Google Patents
A kind of preparation method of wormwood leaf powder print paste Download PDFInfo
- Publication number
- CN107881808A CN107881808A CN201711142217.6A CN201711142217A CN107881808A CN 107881808 A CN107881808 A CN 107881808A CN 201711142217 A CN201711142217 A CN 201711142217A CN 107881808 A CN107881808 A CN 107881808A
- Authority
- CN
- China
- Prior art keywords
- leaf powder
- wormwood leaf
- print paste
- wormwood
- stirred
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
Abstract
The present invention relates to a kind of preparation method of wormwood leaf powder print paste, belong to technical field of textile printing.The present invention substitutes conventional pigment using wormwood leaf powder and prepares print paste, the ratio that wormwood leaf powder, adhesive UDT, thickener that particle diameter is 100 200nm are respectively 2 6%, 92 97.5%, 0.5 2% by mass percentage is mixed, after mixing under conditions of environment temperature is 20 22 DEG C, 20 30min are first stirred with 100 200r/min rotating speed in mixer, it is stirred for uniformly, 70 90min are stirred with 500 700r/min rotating speed again, stood, form print paste.The present invention prepares print paste using wormwood leaf powder, and preparation method is simple, and production cost is low, and the wormwood leaf powder in mill base maintains certain slow release characteristic.Stamp is carried out to fabric using wormwood leaf powder print paste prepared by the present invention, the pattern contour of printing is clear, and printing fastness is good, and solves the pollution problem caused by pigment use.
Description
Technical field
The present invention relates to a kind of preparation method of wormwood leaf powder print paste, belong to technical field of textile printing.
Background technology
Stamp is one of textile dyeing method, typically prepares print paste using synthetic dyestuff, adhesive and thickener,
Such as Chinese public publication《Printing and dyeing》, at 2005 publication date, article name is " pigment printing of cotton fabric ", and the document describes
Pigment printing technology, filters out part coatings print paste and auxiliary aid product, wherein auxiliary aid product include adhesive,
Thickener and ammoniacal liquor, the product good hand touch printed using these pigment printing pastes and auxiliary aid, fastness are good, weak point be with
Environmental Protection Situation is increasingly serious, the preparation of synthetic dyestuff and using can cause certain environmental pollution.
Wormwood belongs to composite family class herbaceous plant for many years, containing the volatilization compound such as class and flavonoids, has good sustained release
Performance, a kind of unique smell can be discharged, play expelling mosquito and it is antibacterial the effect of, wormwood, which also has, relievings asthma, antibechic, dispels
Phlegm, hemostasis, anticoagulation, calmness, antiallergy, protect liver cholagogic etc. act on.In addition, wormwood can extract natural dye, such as China is open
Publication《Silk》, publication date in August, 2011, article name is " alkalescence condition extracts wormwood natural dye and its silk broadcloth
Dyeing ", the document describes to be contaminated silk broadcloth with the technique of natural dye and extract solution in sodium hydrate aqueous solution extraction wormwood
The technique of color, dyeing of real silk silk fabric are denseer than the color of water extraction natural dye dying silk broadcloth.Chinese public publication《Spin in Shandong
Knit science and technology》, in January, 2016 publication date, article name is " bafta cation-modified and argy wormwood natural pigment dyeing ", this article
The pigment for describing and being extracted and being dried in wormwood powder with absolute ethyl alcohol is offered, and then cationic modified cotton is knitted using pigment extract
Thing is dyed, to have good affinity existing for anionic form between wormwood pigment and cation-modified bafta,
The directly upper dye of wormwood natural dye can be made to arrive fabric, fastness to rubbing and soaping fastness reach the general textile standardses of country.
Above two technology is disadvantageous in that the extraction process of wormwood natural dye is complex, using substantial amounts of in extraction process
Chemical reagent, a certain degree of environmental pollution is caused, higher Extracting temperature and longer extraction time cause the serious of the energy
Loss, while the extraction of wormwood pigment destroys the original structure of wormwood, so as to lose the slow-release function of wormwood.
The content of the invention
For above-mentioned problem, conventional pigment is substituted using wormwood leaf powder it is an object of the invention to provide one kind
The method for preparing print paste.To achieve the above object, the technical scheme is that：
A kind of preparation method of wormwood leaf powder print paste, by wormwood leaf powder, the adhesive that particle diameter is 100-200nm
UDT, thickener are respectively 2-6%, 92-97.5%, 0.5-2% ratio mixing by mass percentage, in environment temperature after mixing
Spend under conditions of 20-22 DEG C, first 20-30min is stirred with 100-200r/min rotating speed in mixer, be stirred for
It is even, then 70-90min is stirred with 500-700r/min rotating speed, stand, form print paste.
As a result of above technical scheme, because the wormwood leaf powder used is Nano grade, internal reservoir has wormwood
Volatilize oil substances, can keep certain slow-release function, and the color of wormwood leaf powder itself institute band then assigns mill base color.This hair
The bright fine wormwood leaf powder using Nano grade, instead of traditional granules of pigments, after being mixed with adhesive UDT and thickener
Wormwood leaf powder print paste is prepared, realizes the efficient recycling of natural resources, also solving pigment use from source makes
Into pollution problem.
It is that stirring at low speed makes wormwood leaf powder, adhesive UDT and thickener abundant in the range of 20-22 DEG C in environment temperature
Mixing, wormwood leaf powder and thickener are relatively evenly dispersed into adhesive, and high-speed stirred makes wormwood leaf powder and adhesive
Water molecules in UDT, occur the swelling of appropriate degree, and volume becomes big, make between wormwood leaf powder granule dispersedly more
Fully, adhesive UDT is easier to be coated in binder film.In addition, wormwood leaf powder belongs to containing cellulose components
Granular materials, has more reactive groups compared with conventional pigment particle, and the hydroxyl in strand can be sent out with adhesive UDT
Biochemical reaction, enhance the active force between wormwood leaf powder granule and adhesive.The present invention is prepared using wormwood leaf powder
Print paste, preparation method is simple, and production cost is low.Fabric is carried out using wormwood leaf powder print paste prepared by the present invention
Stamp, the pattern contour of printing is clear, and printing fastness is good.
Embodiment
With reference to specific embodiment, the present invention is described in further detail：
A kind of preparation method of wormwood leaf powder print paste, is added dry wormwood using fine powder process equipment
Work distinguishes wormwood leaf powder, adhesive UDT, thickener into the wormwood leaf powder that particle diameter is 100-200nm by mass percentage
Mix for 2-6%, 92-97.5%, 0.5-2% ratio, after mixing under conditions of environment temperature is 20-22 DEG C, stirring
20-30min is first stirred with 100-200r/min rotating speed in machine, is stirred for uniformly, then stirred with 500-700r/min rotating speed
70-90min is mixed, is stood, forms print paste.With the print paste prepared on pure cotton fabric stamp, re-test stamp color
Deep and dry, fastness to wet rubbing.Specific embodiment
Embodiment 1
By particle diameter be 100nm wormwood leaf powder, adhesive UDT, thickener be respectively 2% by mass percentage,
97.5%th, 0.5% ratio mixing, after mixing under conditions of environment temperature is 20 DEG C, first with 100r/min in mixer
Rotating speed stirring 30min, be stirred for uniformly, then 90min is stirred with 500r/min rotating speed, stand, form print paste.Will
A kind of wormwood leaf powder print paste prepared by the above method, carries out stamp on pure cotton fabric.
Embodiment 2
By particle diameter be 150nm wormwood leaf powder, adhesive UDT, thickener be respectively 4% by mass percentage, 95%,
1% ratio mixing, after mixing under conditions of environment temperature is 21 DEG C, is first stirred in mixer with 150r/min rotating speed
25min, it is stirred for uniformly, then 80min is stirred with 600r/min rotating speed, stand, forms print paste.By above method system
A kind of standby wormwood leaf powder print paste, carries out stamp on pure cotton fabric.
Embodiment 3
By particle diameter be 200nm wormwood leaf powder, adhesive UDT, thickener be respectively 6% by mass percentage, 92%,
2% ratio mixing, after mixing under conditions of environment temperature is 22 DEG C, is first stirred in mixer with 200r/min rotating speed
20min, it is stirred for uniformly, then 70min is stirred with 700r/min rotating speed, stand, forms print paste.By above method system
A kind of standby wormwood leaf powder print paste, carries out stamp on pure cotton fabric.
The Apparent Depth and fastness of the PRINTED FABRIC of table 1
As shown in Table 1, synthetic dyestuff is substituted using coloured wormwood leaf powder, can assigns PRINTED FABRIC full face
Color, and there is no any pollution to environment.With the increase of wormwood leaf powder quality percentage in print paste, PRINTED FABRIC
Apparent Depth gradually increases, do, wet fastness of rubbing it is good, more than 3 grades.
Claims (1)
- A kind of 1. preparation method of wormwood leaf powder print paste, it is characterised in that：Described preparation method refers to 100-200nm wormwood leaf powder, adhesive UDT, thickener is respectively 2-6%, 92-97.5%, 0.5- by mass percentage 2% ratio mixing, after mixing under conditions of environment temperature is 20-22 DEG C, first with 100-200r/min's in mixer Rotating speed stirs 20-30min, is stirred for uniformly, then stirs 70-90min with 500-700r/min rotating speed, stands, and forms print Pattern is starched.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142217.6A CN107881808A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of wormwood leaf powder print paste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142217.6A CN107881808A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of wormwood leaf powder print paste |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107881808A true CN107881808A (en) | 2018-04-06 |
Family
ID=61777749
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711142217.6A Pending CN107881808A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of wormwood leaf powder print paste |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107881808A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111979762A (en) * | 2020-08-26 | 2020-11-24 | 常熟市亿盛日用品有限公司 | Preparation method of bamboo fiber antibacterial cleaning cloth |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
-
2017
- 2017-11-17 CN CN201711142217.6A patent/CN107881808A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111979762A (en) * | 2020-08-26 | 2020-11-24 | 常熟市亿盛日用品有限公司 | Preparation method of bamboo fiber antibacterial cleaning cloth |
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Application publication date: 20180406 |