CN107700236A - A kind of preparation method of acanthaceous indigo blade of grass powder print paste - Google Patents
A kind of preparation method of acanthaceous indigo blade of grass powder print paste Download PDFInfo
- Publication number
- CN107700236A CN107700236A CN201711142177.5A CN201711142177A CN107700236A CN 107700236 A CN107700236 A CN 107700236A CN 201711142177 A CN201711142177 A CN 201711142177A CN 107700236 A CN107700236 A CN 107700236A
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- China
- Prior art keywords
- blade
- print paste
- acanthaceous indigo
- grass powder
- indigo
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The present invention relates to a kind of preparation method of acanthaceous indigo blade of grass powder print paste, belong to technical field of textile printing.The present invention substitutes conventional pigment using acanthaceous indigo blade of grass powder and prepares print paste, the ratio that acanthaceous indigo blade of grass powder, adhesive UDT, thickener that particle diameter is 100 200nm are respectively 9 13%, 95 91.5%, 0.5 2% by mass percentage is mixed, after mixing under conditions of environment temperature is 29 31 DEG C, 11 21min are first stirred with 190 290r/min rotating speed in mixer, it is stirred for uniformly, 25 45min are stirred with 950 1150r/min rotating speed again, stood, form print paste.The present invention prepares print paste using source nature, safe and non-toxic acanthaceous indigo blade of grass powder, and required equipment is few, and operating method is simple, and production cost is low, and manufactured print paste has the medicinal efficacy of acanthaceous indigo.Stamp is carried out to fabric using acanthaceous indigo blade of grass powder print paste prepared by the present invention, the pattern contour of printing is clear, and printing fastness is good, and solves the pollution problem caused by pigment use.
Description
Technical field
The present invention relates to a kind of preparation method of acanthaceous indigo blade of grass powder print paste, belong to technical field of textile printing.
Background technology
Stamp is one of textile dyeing method, typically prepares print paste using synthetic dyestuff, adhesive and thickener,
Such as Chinese public publication《Printing and dyeing》, at 2005 publication date, article name is " pigment printing of cotton fabric ", and the document describes
Pigment printing technology, filters out part coatings print paste and auxiliary aid product, wherein auxiliary aid product include adhesive,
Thickener and ammoniacal liquor, the product good hand touch printed using these pigment printing pastes and auxiliary aid, fastness are good, weak point be with
Environmental Protection Situation is increasingly serious, the preparation of synthetic dyestuff and using can cause certain environmental pollution.
Acanthaceous indigo blade of grass is the leaf of Acanthaceae acanthaceous indigo platymiscium acanthaceous indigo grass, has good medical value, is commonly used for Chinese medicine
To treat influenza, meningococal meningitis, Japanese Type-B encephalitis, viral pneumonia, parotitis and atypical
Pneumonia etc..In addition, the leaf of acanthaceous indigo grass plant can be used for producing bipseudoindoxyl dye, such as Chinese patent publication No.
CN104341793A, date of publication 2015 year 02 month 11 days, entitled " a kind of vegetalitas blue dyes of cotton " of innovation and creation,
This application case is disclosed using alcohol-pickled acanthaceous indigo and indigo plant, through centrifuging, filtering, distilling, is added blue vitriol, after being well mixed, is obtained
Blue dyes is obtained, dyed bafta adhesive force is strong, rubbed and washing nondiscoloration.Chinese patent publication No.
CN105178061A, date of publication on December 23rd, 2015, innovation and creation it is entitled " a kind of vegetable indigo dye dyeing wool bar
Process ", this application case, which discloses, is soaked to the granulated slag of acanthaceous indigo leaf plant using the mixed solution of second alcohol and water, is ultrasonic
After ripple processing, vegetable indigo extract solution is obtained.Extract solution obtains vegetable indigo powder through centrifuging, being concentrated in vacuo drying.Above-mentioned two
Kind technology is disadvantageous in that extracts pigment using organic solvent, and the pigment content of extract solution is not high, while extraction process is not
Cause waste and the problem of environmental pollution of resource with can avoiding,
The content of the invention
For above-mentioned problem, traditional face is substituted using acanthaceous indigo blade of grass powder it is an object of the invention to provide one kind
The method that material prepares print paste.To achieve the above object, the technical scheme is that：
A kind of preparation method of acanthaceous indigo blade of grass powder print paste, by acanthaceous indigo blade of grass powder that particle diameter is 100-200nm, viscous
Mixture UDT, thickener are respectively 9-13%, 95-91.5%, 0.5-2% ratio mixing by mass percentage, in ring after mixing
Under conditions of border temperature is 29-31 DEG C, 11-21min is first stirred with 190-290r/min rotating speed in mixer, is stirred for
Uniformly, then with 950-1150r/min rotating speed 25-45min is stirred, stood, form print paste.
As a result of above technical scheme, because the acanthaceous indigo blade of grass powder used is the superfine powder of Nano grade, its grain
Footpath replaces pigment with acanthaceous indigo blade of grass powder, mixed with adhesive UDT and thickener, prepare acanthaceous indigo blade of grass powder close to pigment
Print paste.Meanwhile acanthaceous indigo blade of grass powder still has certain medical value, print paste can be made to have medicinal efficacy concurrently.This hair
It is bright to prepare print paste using acanthaceous indigo blade of grass powder, the efficient utilization of acanthaceous indigo natural resources is realized, and solve pigment to make
The pollution problem caused by.
It is in the range of 21-23 DEG C in environment temperature, acanthaceous indigo blade of grass powder, adhesive UDT and thickening is made by stirring at low speed
Sufficiently mixing is realized in agent, and after three kinds of material mixings are uniform, high-speed stirred makes acanthaceous indigo blade of grass powder and the water in adhesive UDT
Molecule combines, and occurs the swelling of appropriate degree, and volume becomes big, makes between acanthaceous indigo blade of grass powder granule dispersedly more fully, to glue
Mixture UDT is easier to be coated in binder film.In addition, acanthaceous indigo blade of grass powder belongs to the granular material containing cellulose components
Material, has more reactive groups with conventional pigment particle compared with, and the hydroxyl in strand can be chemical with adhesive UDT generations
Reaction, enhances the active force between acanthaceous indigo blade of grass powder granule and adhesive.The present invention is natural, safe and non-toxic using source
Acanthaceous indigo blade of grass powder prepares print paste, and required equipment is few, and operating method is simple, and production cost is low, manufactured print paste tool
There is the medicinal efficacy of acanthaceous indigo.Stamp, the figure of printing are carried out to fabric using acanthaceous indigo blade of grass powder print paste prepared by the present invention
Case is clear-cut, and printing fastness is good.
Embodiment
With reference to specific embodiment, the present invention is described in further detail：
A kind of preparation method of acanthaceous indigo blade of grass powder print paste, is added dry acanthaceous indigo using superfine powder process equipment
Acanthaceous indigo blade of grass powder of the work into particle diameter for 100-200nm, by acanthaceous indigo blade of grass powder, adhesive UDT, thickener by mass percentage
Respectively 9-13%, 95-91.5%, 0.5-2% ratio mixing, after mixing under conditions of environment temperature is 29-31 DEG C,
11-21min is first stirred with 190-290r/min rotating speed in mixer, is stirred for uniformly, then is turned with 950-1150r/min
Speed stirring 25-45min, stands, forms print paste.With the print paste prepared, stamp, re-test print on pure cotton fabric
Pattern depth and dry, fastness to wet rubbing.Specific embodiment
Embodiment 1
By particle diameter be 100nm acanthaceous indigo blade of grass powder, adhesive UDT, thickener be respectively 9% by mass percentage,
91.5%th, 0.5% ratio mixing, after mixing under conditions of environment temperature is 29 DEG C, first with 190r/min in mixer
Rotating speed stirring 21min, be stirred for uniformly, then 45min is stirred with 950r/min rotating speed, stand, form print paste.
Embodiment 2
By particle diameter be 150nm acanthaceous indigo blade of grass powder, adhesive UDT, thickener be respectively 11% by mass percentage,
88%th, 1% ratio mixing, after mixing under conditions of environment temperature is 30 DEG C, first turned in mixer with 240r/min
Speed stirring 16min, is stirred for uniformly, then stirs 35min with 1050r/min rotating speed, stands, forms print paste.
Embodiment 3
By particle diameter be 200nm acanthaceous indigo blade of grass powder, adhesive UDT, thickener be respectively 13% by mass percentage,
85%th, 2% ratio mixing, after mixing under conditions of environment temperature is 31 DEG C, first turned in mixer with 290r/min
Speed stirring 11min, is stirred for uniformly, then stirs 25min with 1150r/min rotating speed, stands, forms print paste.
The Apparent Depth and fastness of the PRINTED FABRIC of table 1
As shown in Table 1, synthetic dyestuff is substituted using coloured acanthaceous indigo blade of grass powder, it is full PRINTED FABRIC can be assigned
Color, and there is no any pollution to environment.With the increase of acanthaceous indigo blade of grass powder quality percentage in print paste, stamp is knitted
The Apparent Depth of thing gradually increases, do, wet fastness of rubbing it is good, more than 3 grades.
Claims (1)
- A kind of 1. preparation method of acanthaceous indigo blade of grass powder print paste, it is characterised in that：Described preparation method refers to particle diameter For 100-200nm acanthaceous indigo blade of grass powder, adhesive UDT, thickener by mass percentage be respectively 9-13%, 95-91.5%, 0.5-2% ratio mixing, after mixing under conditions of environment temperature is 29-31 DEG C, first with 190-290r/ in mixer Min rotating speed stirring 11-21min, is stirred for uniformly, then stirs 25-45min with 950-1150r/min rotating speed, stands, Form print paste.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142177.5A CN107700236A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of acanthaceous indigo blade of grass powder print paste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711142177.5A CN107700236A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of acanthaceous indigo blade of grass powder print paste |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107700236A true CN107700236A (en) | 2018-02-16 |
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ID=61180240
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711142177.5A Pending CN107700236A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of acanthaceous indigo blade of grass powder print paste |
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| Country | Link |
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| CN (1) | CN107700236A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
-
2017
- 2017-11-17 CN CN201711142177.5A patent/CN107700236A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127868A (en) * | 2010-12-07 | 2011-07-20 | 江南大学 | Preparation method of ultraviolet-fluorescence-visible printing color paste for fabric |
| CN102978975A (en) * | 2012-12-07 | 2013-03-20 | 绍兴市天基印刷材料厂 | Printing paste preparation and printing process thereof |
| CN105350355A (en) * | 2015-11-30 | 2016-02-24 | 无锡新德印染制品有限公司 | Preparation method of printing color paste |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180216 |
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| RJ01 | Rejection of invention patent application after publication |