CN107881011A - A kind of preparation method of compound fruit medicinal extract - Google Patents
A kind of preparation method of compound fruit medicinal extract Download PDFInfo
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- CN107881011A CN107881011A CN201711318408.3A CN201711318408A CN107881011A CN 107881011 A CN107881011 A CN 107881011A CN 201711318408 A CN201711318408 A CN 201711318408A CN 107881011 A CN107881011 A CN 107881011A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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Abstract
The invention discloses a kind of preparation method of compound fruit medicinal extract, step includes：(1) fresh mulberries and indigo fruit are shredded and boils pretreatment in gallic acid heated in water solution, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；(2) by solid phase filtrate multiplex-enzyme extraction；(3) liquid mixes after the filtered fluid after enzyme deactivation and processing, is concentrated under reduced pressure, to concentration after add hydrogen peroxide in liquid, filter off and the compound extracted solution that room temperature obtains mulberries and indigo fruit except sediment, be cooled to after heating；(4) fresh Nanking cherry is shredded and ultrasound adverse current is extracted in the ethanol solution containing third nonalactone, extract solution, which is concentrated under reduced pressure, obtains Nanking cherry extract solution；(5) by mulberries and the well mixed compound fruit medicinal extract of acquisition of indigo fruit compound extracted solution and Nanking cherry extract solution.After the present invention mixes Nanking cherry extract solution with the compound extracted solution of mulberries/indigo fruit, hence it is evident that the miscellaneous gas and excitant of flue gas, the more rich exquisiteness of gained medicinal extract fragrance can be coordinated, cigarette odor-absorbing is improved.
Description
Technical field
The invention belongs to tobacco aromaticss technical field, more particularly to a kind of preparation method of compound fruit medicinal extract.
Background technology
Mulberry fruit（Latin name：Fructus Mori）It is the fruit of Moraceae Morus perennial woody plant mulberry tree, ellipse is long
1~3 centimetre, uneven surface.It is green during prematurity, gradually grows up and be changed into white, red, is aubergine or purple black after maturation
Color, sweet and sour.《Book on Chinese herbal medicine is newly organized》There is the record of " purple person is first, and red person takes second place, blue or green then unavailable ".Contain a variety of work(in mulberry fruit
Energy property composition, such as rutin, anthocyanidin, RV, there is the effect such as good anti-cancer, anti-aging, antiulcer, antiviral.
The oval bluish violet berry of indigo fruit is as Agate, taste sweet and sour taste.Berry contains 7 kinds of amino acid and vitamin C, can give birth to
Food, can provide pigment, can also make wine, cook beverage and jam again.Bud, fruit, flower are nectar source again.Except the high edibility of tool
Outside, there is high medical value also containing abundant vP active materials, rutin, anthocyanin etc. in fruit.Fruit is not
The effect of only clearing heat and detoxicating, and to decompression, blood cell number is improved, treatment baby anorexia has certain curative effect.Spray can enter
Medicine is clearing heat and detoxicating.
In tobacco product, the fragrance and suction taste of tobacco are vital, and addition spices is the key in cigarette process
Link, and improve product style and improve one of effective means of cigarette flavor quality, it is fragrant that some can be provided to consumer
Gas and the cigarette products for inhaling taste satisfaction.Tobacco extract refers to extract the tobacco aromaticss obtained by spice berry organ with organic solvent
Product.Conventional tobacco extract has Mao Xiang medicinal extract, Lysimachia sikokiana medicinal extract, Peru's medicinal extract, Tolu concrete, maple extract, chicory concrete etc..By
There is pleasant fragrance and sweet mouthfeel in most fruits, therefore it is tobacco processing to extract medicinal extract as raw material by the use of fruit
The focus of industry research, for example, patent CN104017647A, CN103740465A, CN101455442A, CN101455441A,
CN103146485A etc. is extracted tobacco aromaticss using different fruit, there is different degrees of improvement to cigarette smoke.But
Improvement direction and mode of the existing fruits medicinal extract to flue gas are single, or fragrant aroma is strong, the excitant of flue gas is changed
It is kindhearted good, but the tobacco flavor deficiency of cigarette script, inaccurate coordination, pleasant impression deficiency, it is difficult to reach the mouthfeel of smoking tobaccos；It is fragrant
Gas and flue gas harmony are preferable, but fragrance is excessively gentle, and flavouring essence quality deficiency, miscellaneous gas is more, and excitant is big.Therefore how to select
Suitable fruit is selected as raw material, how to optimize the extracting method of fruit so that the perfume (or spice) composition processed extracted in fruit can and cigarette
Gas is coordinated well, while will not cover the smoke of flue gas script and suck pleasant impression, is heavy to closing in development perfuming cigarette technology
The problem of wanting, and the priority and difficulty of development tobacco extract technology.
The content of the invention
Based on above-mentioned technical problem, the invention provides a kind of preparation method of compound fruit medicinal extract, preparation process includes：
(1) fresh mulberries and indigo fruit are shredded and mixed, mixture is immersed in gallic acid heated in water solution and boils pre- place
Reason, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in into water bath with thermostatic control in multiplex-enzyme extraction liquid to extract, filtered after the completion of extraction, incited somebody to action
Filtrate high temperature destroy the enzyme treatment；
(3) liquid mixes after the filtered fluid after enzyme deactivation and the processing, then is concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide added in liquid and stir more than 10min, then filter off except the sediment in solution, solution heating
To 85~90 DEG C of 6~8min of insulation, the compound extracted solution that room temperature obtains mulberries and indigo fruit is cooled to；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands certain time, it is quiet
After the completion of putting carry out ultrasound adverse current extract, after extraction separation of solid and liquid obtain extract solution, be concentrated under reduced pressure into extracting liquid volume 0.2~
0.4 times, that is, obtain Nanking cherry extract solution；
(5) mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution are well mixed, that is, obtain the compound fruit
Medicinal extract.
Further, in the step (1), the mixing quality ratio of mulberries and indigo fruit is mulberries:Indigo fruit=1:1~8,
The addition weight of the gallic acid aqueous solution is mulberries and indigo fruit chopping more than 4 times of total weight of the mixture, the gallic acid
The concentration of solute is 10~50g/L in the aqueous solution, and heating boiling time is 5~15min.
Further, in the step (2), the multiplex-enzyme extraction liquid is water-soluble for the mixing of cellulase and pectase
Each component quality compares cellulase in liquid, wherein multiplex-enzyme extraction liquid：Pectase：Sterilized water=7~10:7~10:1000, it is described
The material of solid phase filtrate and multiplex-enzyme extraction liquid/liquid mass ratio is 1:2~5.
Further, the water bath with thermostatic control temperature is 45~50 DEG C, and water bath with thermostatic control extraction time is 2~3h, the high temperature
Destroy the enzyme treatment temperature is 85~95 DEG C, and the enzyme deactivation time is 20~25min.
Further, in the step (3), concentration of hydrogen peroxide is 35% in the hydrogen peroxide, the addition of hydrogen peroxide
For：
The quality of hydrogen peroxide：Quality=0.5~1 of liquid after being concentrated under reduced pressure:10.
Further, in the step (4), in the ethanol solution containing third nonalactone, third nonalactone/ethanol of volume ratio
=4~5:10, the feed liquid mass ratio of Nanking cherry small pieces and the ethanol solution containing third nonalactone is 1:3~7, supersonic frequency 50
~100KHz, adverse current extraction time are 0.5~1h.
Further, in the step (5), mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:
1 mixing.
The invention also discloses application of the compound fruit medicinal extract in cigarette made from the above method, the compound fruit leaching
Cream is added in cigarette shreds in a manner of feeding, and the addition of medicinal extract is the 0.05 ~ 0.1% of pipe tobacco weight.
As can be seen from the above technical solutions, it is an advantage of the invention that：
1. the present invention prepares tobacco aromaticss using mulberries and indigo fruit compound collecting first.Experiment is found, using common pure water
Mulberries and indigo fruit compound extracted solution after extraction or ethanol extraction no matter are single use or and Nanking cherry extract solution compounding
Use, the improvement to cigarette smoke is bad, especially undesirable to miscellaneous gas in flue gas and irritating improvement, does not reach cigarette use
Effect needed for spices.
After 2. Nanking cherry extract solution mixes with the nutgall acid solution extract solution of mulberries/indigo fruit, hence it is evident that flue gas can be coordinated
Miscellaneous gas and excitant, the more rich exquisiteness of gained medicinal extract fragrance, cigarette odor-absorbing be improved.
3. being mixed into third nonalactone in Nanking cherry extract solution, the harmony of spices fragrance and flue gas can be balanced, is increased
Cigarette smoking pleasant impression.
Embodiment
It is described in detail with reference to embodiment：
Embodiment 1
A kind of preparation method of compound fruit medicinal extract, preparation process include：
(1) by fresh mulberries and indigo fruit in mass ratio 1:1 shreds and mixes, and the concentration that mixture is immersed in solute is 10g/L
Gallic acid heated in water solution boil pretreatment, the addition weight of the gallic acid aqueous solution is that mulberries and indigo fruit chopping are mixed
5 times of compound gross weight, boiling time 5min, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in 45~50 DEG C of thermostatted waters in the multiplex-enzyme extraction liquid of cellulase and pectase
Bath extraction 2h, wherein each component quality compares cellulase in multiplex-enzyme extraction liquid：Pectase：Sterilized water=7:7:1000, solid phase mistake
The material of screening and multiplex-enzyme extraction liquid/liquid mass ratio is 1:2, filtered after the completion of extraction, by filtered fluid under 85~95 DEG C of environment
Enzyme deactivation 20min；
(3) filtered fluid after enzyme deactivation and mixed with liquid after the processing, then be concentrated under reduced pressure into 0.2 times of mixed liquor original volume, to
The hydrogen peroxide that concentration of hydrogen peroxide is 35% is added after concentration in liquid and stirs 10min, the addition of hydrogen peroxide is：Hydrogen peroxide
Quality=1 of liquid after quality/be concentrated under reduced pressure:10, filtered off after the completion of stirring except the sediment in solution, solution is heated to 85~
90 DEG C of insulation 6min, are cooled to the compound extracted solution that room temperature obtains mulberries and indigo fruit；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands 30min, wherein containing
In the ethanol solution of third nonalactone, third nonalactone/ethanol=4 of volume ratio:10, Nanking cherry small pieces and containing third nonalactone
The feed liquid mass ratio of ethanol solution is 1:3.Ultrasound adverse current is carried out after the completion of standing to extract, and supersonic frequency 100KHz, is countercurrently carried
It is 0.5h to take the time.Separation of solid and liquid obtains extract solution after extraction, is concentrated under reduced pressure into 0.2 times of extracting liquid volume, that is, obtains hair cherry
Peach extract solution；
(5) by the mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 is well mixed, that is, obtains
The compound fruit medicinal extract.
Embodiment 2
A kind of preparation method of compound fruit medicinal extract, preparation process include：
(1) by fresh mulberries and indigo fruit in mass ratio 1:3 shred and mix, and the concentration that mixture is immersed in solute is 20g/L
Gallic acid heated in water solution boil pretreatment, the addition weight of the gallic acid aqueous solution is that mulberries and indigo fruit chopping are mixed
5 times of compound gross weight, boiling time 5min, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in 45~50 DEG C of thermostatted waters in the multiplex-enzyme extraction liquid of cellulase and pectase
Bath extraction 2h, wherein each component quality compares cellulase in multiplex-enzyme extraction liquid：Pectase：Sterilized water=7:7:1000, solid phase mistake
The material of screening and multiplex-enzyme extraction liquid/liquid mass ratio is 1:3, filtered after the completion of extraction, by filtered fluid under 85~95 DEG C of environment
Enzyme deactivation 20min；
(3) filtered fluid after enzyme deactivation and mixed with liquid after the processing, then be concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide that concentration of hydrogen peroxide is 35% added in liquid and stir more than 10min, the addition of hydrogen peroxide is：
Quality=0.7 of liquid after the quality of hydrogen peroxide/be concentrated under reduced pressure:10, filtered off after the completion of stirring except the sediment in solution, solution
85~90 DEG C of insulation 6min are heated to, are cooled to the compound extracted solution that room temperature obtains mulberries and indigo fruit；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands 30min, wherein containing
In the ethanol solution of third nonalactone, third nonalactone/ethanol=4 of volume ratio:10, Nanking cherry small pieces and containing third nonalactone
The feed liquid mass ratio of ethanol solution is 1:5.Carry out ultrasound adverse current after the completion of standing to extract, supersonic frequency 80KHz, adverse current is extracted
Time is 0.5h.Separation of solid and liquid obtains extract solution after extraction, is concentrated under reduced pressure into 0.2 times of extracting liquid volume, that is, obtains Nanking cherry
Extract solution；
(5) by the mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 is well mixed, that is, obtains
The compound fruit medicinal extract.
Embodiment 3
A kind of preparation method of compound fruit medicinal extract, preparation process include：
(1) by fresh mulberries and indigo fruit in mass ratio 1:4 shred and mix, and the concentration that mixture is immersed in solute is 40g/L
Gallic acid heated in water solution boil pretreatment, the addition weight of the gallic acid aqueous solution is that mulberries and indigo fruit chopping are mixed
5 times of compound gross weight, boiling time 10min, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in 45~50 DEG C of thermostatted waters in the multiplex-enzyme extraction liquid of cellulase and pectase
Bath extraction 2.5h, wherein each component quality compares cellulase in multiplex-enzyme extraction liquid：Pectase：Sterilized water=8:10:1000, Gu
The material of phase filtrate and multiplex-enzyme extraction liquid/liquid mass ratio is 1:4, filtered after the completion of extraction, by filtered fluid in 85~95 DEG C of rings
Enzyme deactivation 25min under border；
(3) filtered fluid after enzyme deactivation and mixed with liquid after the processing, then be concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide that concentration of hydrogen peroxide is 35% added in liquid and stir more than 10min, the addition of hydrogen peroxide is：
Quality=1 of liquid after the quality of hydrogen peroxide/be concentrated under reduced pressure:10, filtered off after the completion of stirring except the sediment in solution, solution add
Heat is cooled to the compound extracted solution that room temperature obtains mulberries and indigo fruit to 85~90 DEG C of insulation 8min；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands 50min, wherein containing
In the ethanol solution of third nonalactone, third nonalactone/ethanol=5 of volume ratio:10, Nanking cherry small pieces and containing third nonalactone
The feed liquid mass ratio of ethanol solution is 1:5.Carry out ultrasound adverse current after the completion of standing to extract, supersonic frequency 50KHz, adverse current is extracted
Time is 1h.Separation of solid and liquid obtains extract solution after extraction, is concentrated under reduced pressure into 0.4 times of extracting liquid volume, that is, obtains Nanking cherry and carry
Take liquid；
(5) by the mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 is well mixed, that is, obtains
The compound fruit medicinal extract.
Embodiment 4
A kind of preparation method of compound fruit medicinal extract, preparation process include：
(1) by fresh mulberries and indigo fruit in mass ratio 1:6 shred and mix, and the concentration that mixture is immersed in solute is 40g/L
Gallic acid heated in water solution boil pretreatment, the addition weight of the gallic acid aqueous solution is that mulberries and indigo fruit chopping are mixed
5 times of compound gross weight, boiling time 15min, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in 45~50 DEG C of thermostatted waters in the multiplex-enzyme extraction liquid of cellulase and pectase
Bath extraction 3h, wherein each component quality compares cellulase in multiplex-enzyme extraction liquid：Pectase：Sterilized water=10:7:1000, solid phase
The material of filtrate and multiplex-enzyme extraction liquid/liquid mass ratio is 1:5, filtered after the completion of extraction, by filtered fluid in 85~95 DEG C of environment
Lower enzyme deactivation 25min；
(3) filtered fluid after enzyme deactivation and mixed with liquid after the processing, then be concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide that concentration of hydrogen peroxide is 35% added in liquid and stir more than 10min, the addition of hydrogen peroxide is：
Quality=0.8 of liquid after the quality of hydrogen peroxide/be concentrated under reduced pressure:10, filtered off after the completion of stirring except the sediment in solution, solution
85~90 DEG C of insulation 6min are heated to, are cooled to the compound extracted solution that room temperature obtains mulberries and indigo fruit；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands 30min, wherein containing
In the ethanol solution of third nonalactone, third nonalactone/ethanol=5 of volume ratio:10, Nanking cherry small pieces and containing third nonalactone
The feed liquid mass ratio of ethanol solution is 1:7.Carry out ultrasound adverse current after the completion of standing to extract, supersonic frequency 80KHz, adverse current is extracted
Time is 0.5h.Separation of solid and liquid obtains extract solution after extraction, is concentrated under reduced pressure into 0.2 times of extracting liquid volume, that is, obtains Nanking cherry
Extract solution；
(5) by the mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 is well mixed, that is, obtains
The compound fruit medicinal extract.
Embodiment 5
A kind of preparation method of compound fruit medicinal extract, preparation process include：
(1) by fresh mulberries and indigo fruit in mass ratio 1:8 shred and mix, and the concentration that mixture is immersed in solute is 50g/L
Gallic acid heated in water solution boil pretreatment, the addition weight of the gallic acid aqueous solution is that mulberries and indigo fruit chopping are mixed
5 times of compound gross weight, boiling time 15min, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in 45~50 DEG C of thermostatted waters in the multiplex-enzyme extraction liquid of cellulase and pectase
Bath extraction 2h, wherein each component quality compares cellulase in multiplex-enzyme extraction liquid：Pectase：Sterilized water=8:7:1000, solid phase mistake
The material of screening and multiplex-enzyme extraction liquid/liquid mass ratio is 1:3, filtered after the completion of extraction, by filtered fluid under 85~95 DEG C of environment
Enzyme deactivation 20min；
(3) filtered fluid after enzyme deactivation and mixed with liquid after the processing, then be concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide that concentration of hydrogen peroxide is 35% added in liquid and stir more than 10min, the addition of hydrogen peroxide is：
Quality=0.5 of liquid after the quality of hydrogen peroxide/be concentrated under reduced pressure:10, filtered off after the completion of stirring except the sediment in solution, solution
85~90 DEG C of insulation 6min are heated to, are cooled to the compound extracted solution that room temperature obtains mulberries and indigo fruit；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands 30min, wherein containing
In the ethanol solution of third nonalactone, third nonalactone/ethanol=4 of volume ratio:10, Nanking cherry small pieces and containing third nonalactone
The feed liquid mass ratio of ethanol solution is 1:6.Ultrasound adverse current is carried out after the completion of standing to extract, and supersonic frequency 100KHz, is countercurrently carried
It is 0.5h to take the time.Separation of solid and liquid obtains extract solution after extraction, is concentrated under reduced pressure into 0.2 times of extracting liquid volume, that is, obtains hair cherry
Peach extract solution；
(5) by the mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 is well mixed, that is, obtains
The compound fruit medicinal extract.
Comparative example 1
A kind of preparation method of compound fruit medicinal extract, its method and step are only existed using the step described in embodiment 3, its difference
In：Pretreatment is boiled in heating in deionized water for mulberries and the immersion of indigo fruit small pieces mixture in step (1), deionized water
Addition is identical with the addition of the gallic acid aqueous solution described in embodiment 3, and boiling temps are also identical.Other step methods and
Parameter is identical with embodiment 3, and compound fruit medicinal extract is finally made.
Comparative example 2
A kind of preparation method of compound fruit medicinal extract, its method and step are only existed using the step described in embodiment 3, its difference
In：Mulberries and indigo fruit small pieces mixture in step (1) are immersed in heating in ethanol solution and boil pretreatment, ethanol solution
Addition is identical with the addition of the gallic acid aqueous solution described in embodiment 3, and boiling temps are also identical.Other step methods and
Parameter is identical with embodiment 3, and compound fruit medicinal extract is finally made.
Comparative example 3
A kind of preparation method of compound fruit medicinal extract, its method and step are only existed using the step described in embodiment 3, its difference
In：Nanking cherry extract solution is not included in fruit medicinal extract, i.e., not comprising the step (4), directly by the mulberries and indigo fruit of acquisition
Compound extracted solution as fruit medicinal extract.
Comparative example 4
A kind of preparation method of compound fruit medicinal extract, its method and step are only existed using the step described in embodiment 3, its difference
In：Pacified in the step (4) using with the straight alcohol of the ethanol solution equivalent containing third nonalactone replacement for soaking Nanking cherry
Moral, and do not include third nonalactone.Other step methods and parameter are identical with embodiment 3, and compound fruit leaching is finally made
Cream.
Embodiment 6
Fruit medicinal extract made from the present embodiment 1~5 and comparative example 1~4 is added in cigarette shreds in a manner of feeding, every group
The addition of medicinal extract is the 0.1% of pipe tobacco weight.Cigarette is made in each group pipe tobacco after the completion of addition, cigarette finished product is by smokeing panel test specially
Group of family presses《GB5606.4-2005 cigarette sense organ technical requirements》Regulation carry out cigarette sense organ, its smoking result such as institute of table 1
Show.
Using same series-produced any spices cigarette shreds do not added cigarette is made as blank control group, blank control group
Cigarette also oil smoke panel test panel of expert by《GB5606.4-2005 cigarette sense organ technical requirements》Regulation carry out cigarette sense organ, it is commented
It is as shown in table 1 to inhale result.
The evaluation result of table 1
As shown in table 1, from embodiment 1~5, in the method for the invention step and parameter area, what is obtained is compound
Fruit medicinal extract, which is added in cigarette shreds, is made cigarette, can be obviously improved the sucking quality of flue gas.Pass through the He of comparative example 3
Comparative example 1, comparative example 2 understand, using common Aqua pure extract or ethanol extraction after mulberries and indigo fruit compound extracted solution and
After medicinal extract is made in Nanking cherry extract solution compounding use, it is added into pipe tobacco and cigarette is made, the improvement to cigarette smoke is not substantially not as
Infanticide acid solution extracts manufactured medicinal extract after mulberries and indigo fruit, especially the miscellaneous gas of flue gas is removed and excitant improve on not
It is good, do not reach the extraction effect of nutgall acid solution.By comparative example 3 and comparative example 3, individually mulberries and indigo are used
Fruit compound extracted solution is used for tobacco perfuming as medicinal extract, and the harmony and fragrance to pipe tobacco improve deficiency, are extracted using Nanking cherry
After liquid compounds mulberries and indigo fruit compound extracted solution, hence it is evident that the miscellaneous gas and excitant of flue gas can be coordinated, gained medicinal extract fragrance is more
Abundant exquisiteness, cigarette odor-absorbing are improved.By comparative example 3 and comparative example 4, third is mixed into Nanking cherry extract solution
Position nonalactone, can balance the harmony of spices fragrance and flue gas, increase cigarette smoking pleasant impression, show as harmony and pleasant impression
Improve.
Technical scheme provided by the present invention is described in detail above, for those of ordinary skill in the art,
According to the thought of the embodiment of the present invention, there will be changes in specific embodiments and applications, in summary, this theory
Bright book content should not be construed as limiting the invention.
Claims (8)
1. a kind of preparation method of compound fruit medicinal extract, it is characterised in that preparation process includes：
(1) fresh mulberries and indigo fruit are shredded and mixed, mixture is immersed in gallic acid heated in water solution and boils pre- place
Reason, liquid and solid phase filtrate after separation of solid and liquid is handled after pretreatment；
(2) the solid phase filtrate is immersed in into water bath with thermostatic control in multiplex-enzyme extraction liquid to extract, filtered after the completion of extraction, incited somebody to action
Filtrate high temperature destroy the enzyme treatment；
(3) liquid mixes after the filtered fluid after enzyme deactivation and the processing, then is concentrated under reduced pressure into the 0.2~0.4 of mixed liquor original volume
Times, to concentration after hydrogen peroxide added in liquid and stir more than 10min, then filter off except the sediment in solution, solution heating
To 85~90 DEG C of 6~8min of insulation, the compound extracted solution that room temperature obtains mulberries and indigo fruit is cooled to；
(4) fresh Nanking cherry is shredded, is immersed in after chopping in the ethanol solution containing third nonalactone and stands certain time, it is quiet
After the completion of putting carry out ultrasound adverse current extract, after extraction separation of solid and liquid obtain extract solution, be concentrated under reduced pressure into extracting liquid volume 0.2~
0.4 times, that is, obtain Nanking cherry extract solution；
(5) mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution are well mixed, that is, obtain the compound fruit
Medicinal extract.
A kind of 2. preparation method of compound fruit medicinal extract according to claim 1, it is characterised in that in the step (1),
The mixing quality of mulberries and indigo fruit ratio is mulberries:Indigo fruit=1:1~8, the addition weight of the gallic acid aqueous solution be mulberries and
Indigo fruit chopping more than 4 times of total weight of the mixture, the concentration of solute is 10~50g/L in the gallic acid aqueous solution, is added
Hot boiling time is 5~15min.
A kind of 3. preparation method of compound fruit medicinal extract according to claim 1, it is characterised in that in the step (2),
The multiplex-enzyme extraction liquid is the mixed aqueous solution of cellulase and pectase, wherein each component mass ratio in multiplex-enzyme extraction liquid
Cellulase：Pectase：Sterilized water=7~10:7~10:1000, material/liquid matter of the solid phase filtrate and multiplex-enzyme extraction liquid
Amount is than being 1:2~5.
A kind of 4. preparation method of compound fruit medicinal extract according to claim 1 or 3, it is characterised in that the thermostatted water
Bath temperature is 45~50 DEG C, and water bath with thermostatic control extraction time is 2~3h, and the high temperature destroy the enzyme treatment temperature is 85~95 DEG C, enzyme deactivation
Time is 20~25min.
A kind of 5. preparation method of compound fruit medicinal extract according to claim 1, it is characterised in that in the step (3),
Concentration of hydrogen peroxide is 35% in the hydrogen peroxide, and the addition of hydrogen peroxide is：
The quality of hydrogen peroxide：Quality=0.5~1 of liquid after being concentrated under reduced pressure:10.
A kind of 6. preparation method of compound fruit medicinal extract according to claim 1, it is characterised in that in the step (4),
In ethanol solution containing third nonalactone, third nonalactone/ethanol=4~5 of volume ratio:10, Nanking cherry small pieces and containing in third nonyl
The feed liquid mass ratio of the ethanol solution of ester is 1:3~7, supersonic frequency is 50~100KHz, and adverse current extraction time is 0.5~1h.
A kind of 7. preparation method of compound fruit medicinal extract according to claim 1, it is characterised in that in the step (5),
Mulberries and indigo fruit compound extracted solution and Nanking cherry extract solution in mass ratio 1:1 mixing.
8. application of the compound fruit medicinal extract in cigarette as made from any one of claim 1~7 methods described, its feature exist
In, the compound fruit medicinal extract is added in cigarette shreds in a manner of feeding, the addition of medicinal extract for pipe tobacco weight 0.05 ~
0.1%。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711318408.3A CN107881011B (en) | 2017-12-12 | 2017-12-12 | Preparation method of composite fruit extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110279631A (en) * | 2019-07-27 | 2019-09-27 | 吴辉军 | Black cream rinse |
| WO2020227422A1 (en) * | 2019-05-06 | 2020-11-12 | Greenology Products, Llc | Plant extract compositions |
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| CN110279631A (en) * | 2019-07-27 | 2019-09-27 | 吴辉军 | Black cream rinse |
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