CN107874324A - A kind of nicotine paper fiber element carrier and preparation method - Google Patents

A kind of nicotine paper fiber element carrier and preparation method Download PDF

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Publication number
CN107874324A
CN107874324A CN201810013031.9A CN201810013031A CN107874324A CN 107874324 A CN107874324 A CN 107874324A CN 201810013031 A CN201810013031 A CN 201810013031A CN 107874324 A CN107874324 A CN 107874324A
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CN
China
Prior art keywords
nicotine
paper fiber
fiber element
element carrier
carrier
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Pending
Application number
CN201810013031.9A
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Chinese (zh)
Inventor
张宇
曾灿中
金波
李贺
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Individual
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Individual
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Priority to CN201810013031.9A priority Critical patent/CN107874324A/en
Publication of CN107874324A publication Critical patent/CN107874324A/en
Pending legal-status Critical Current

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    • A24F47/008

Abstract

A kind of nicotine paper fiber element carrier, including the paper fiber element carrier for absorbing liquid nicotine, wherein cellulose carrier includes the paper fiber piece that wood pulp and/or string make, and liquid nicotine component is absorbed among the space of cellulose carrier;Every cellulose carrier adheres to 0.01 ~ 0.1mg pure nicotine component.The space aperture of paper fiber element carrier is 50 ~ 175 nanometers.Specifically, the space aperture of paper fiber element carrier is 90 ~ 110 nanometers.Nicotine paper fiber element carrier of the present invention is inserted on electronic cigarette heater strip or heating plate, it is heated to 300 ~ 350 DEG C, the composition such as nicotine component and sweetener, flavor additives useful slowly discharges, but there is no tar generation among this process, the burning-point of paper fiber element is unable to reach simultaneously, and paper fiber element, which can not burn, produces dust.

Description

A kind of nicotine paper fiber element carrier and preparation method
Technical field
The present invention relates to electronic cigarette technical field, especially provides the nicotine paper fiber element that electronic cigarette heater uses and carries Body and preparation method.
Background technology
China consumes big country as cigarette, and 2016 are only ramuscule cigarette retail sales up to 68,500,000,000.Work as in result of combustion of tobacco process In, not only nicotine and tar burning outwardly discharges pollution factor, and the burning of tobacco itself equally produces the pollutants such as flue dust, The microenvironment on periphery is impacted.
The content of the invention
The nicotine paper fiber element carrier used it is an object of the invention to provide a kind of electronic cigarette heater and making Method, nicotine is absorbed among paper fiber element, the purpose of the i.e. reachable nicotine volatilization intake of heating paper fiber element, Reduce result of combustion of tobacco influences to caused by environment.
The present invention specifically provides a kind of nicotine paper fiber element carrier, including for absorbing the papery of liquid nicotine Cellulose carrier, wherein cellulose carrier include the paper fiber piece that wood pulp and/or string make, liquid nicotine Ingredient draws are among the space of cellulose carrier;Every cellulose carrier adheres to 0.01 ~ 0.1mg pure nicotine component.
Nicotine is tobacco extract and/or artificial synthesized nicotine, pure nicotine mass fraction in liquid nicotine Content is 2 ~ 73%, and surplus is diluent and/or additive;
The space aperture of paper fiber element carrier is 50 ~ 175 nanometers.Specifically, the space aperture of paper fiber element carrier be 90 ~ 110 nanometers.
It is fine that the string that the present invention uses includes cotton, beet, wheat bran, orange peel, herbage, straw, bark, tealeaves, bamboo One of dimension or its combination.The cellulose extraction that the present invention uses is extensive, floristics is not limited to, especially with paper pulp Fiber, it can be beaten into using treated waste and old paper as fiber, realize reusing for resource.
For the present invention in order to reach preferable assimilation effect, every cellulose carrier adheres to 0.22 ~ 0.05mg pure Buddhist nun Gu Fourth composition.This metering uses pure nicotine equivalent.
In order to ensure that absorption process is quick, and cause nicotine paper fiber carrier that there is its in addition to nicotine His flavor, crowd's adaptability is lifted, increased diluent and/or additive are solvent, increased in nicotine paper fiber carrier Mould one of agent, NMF, adhesive, sweetener, spices or its combination.Additive in the present invention can also add antioxygen Agent.
Wherein:
Solvent is one of organic solvent, water, honey, inspissated juice or its combination.
Organic solvent includes but is not limited to:Propane diols, ethanol, glycerine, vegetable oil, partially hydrogenated vegetable oil, medium chain triglyceride Three esters, phthalic acid ester, polycarboxylate, hexylene glycol, butanediol, glyceride, vinyl alcohol, disaccharide iron agar, sugar alcohol, glycerine, One of sorbierite, xylitol, maltitol, hydroxyl isomaltulose, mannitol, polymer polyatomic alcohol, beverage wine or its combination.
Adhesive includes but is not limited to:Dextrin, cyclodextrine derivatives, starch, modified starch, carboxymethyl cellulose, hydroxypropyl Base cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, methylcellulose, konjaku flour, collagen, inulin, soybean protein, Lactalbumin, casein, gluten powder, carrageenan, sodium alginate, propylene glycol alginate, xanthans, Propiram are more Sugar, condense polysaccharide, be gellan gum, locust bean gum, sesbania gum, tara gum, tragacanth, pectin, agar, zeins, bright Glue, Chinese parasol tree extract, Semen Plantaginis extract, chitin, chitosan, Arabic gum, polyvinylpyrrolidone, PEO, It is polyvinyl alcohol, guar gum, xanthans, cellulose, maltodextrin, polyurethane, silicon-containing polymer, polyester, polyacrylate, poly- Ethene, hydrogenated styrene-butadiene block copolymer, SBS, the isoamyl of styrene one Diene-styrene copolymer, loquat extract, natural gum, butadiene-styrene rubber, butyl rubber, polyisobutene, glyceride, terpenes tree Fat, polyvinyl acetate, paraffin, microwax, hydrogenated vegetable oil, lecithin, glycerin monostearate, Heveatex, dragon spruce One of fat, frankincense gum or its combination.Adhesive can lift attachment degree of the nicotine on cellulose carrier.
NMF includes but is not limited to:One of Quillaia saponaria bark extract, 'alpha '-hydroxy acids, lactic acid, aloe gel, honey or It is combined.NMF prevents paper fiber element carrier from excessively drying phenomena such as being broken.
Sweetener includes but is not limited to:Polydextrose, glucose mixture, molasses element, corn sweetener, syrup, fructose, Fruit drops, lactose, milk sugar, maltose, mannitol, D-sorbite, D-sorbite, inspissated juice, saccharin, Aspartame, sugarcane One of sugared element, acesulfame potassium or its combination.Lift the experience property of user.
Spices includes but is not limited to:Honey, radix glycyrrhizae, peppermint, fruit flavor, sweet wine flavoring, spirits flavoring, peppermint are adjusted Taste substance, lavender flavoring, Chinese cassia tree flavoring, cardamom flavoring, cloves flavoring, santal flavoring, honey elite, rose One of oil, vanilla elite, lemon oil, orange oil, refined jasmine oil, capsicum oil, coffee flavoring, cocoa flavoring or its group Close.The experience property of user is lifted, is adapted to women or the user more sensitive to tobacco.
In order to lift rate of drying, organic solvent is preferred for propane diols, absolute ethyl alcohol, propane diols and aqueous mixtures, ethanol With one of aqueous mixtures or its combine.
Paper fiber element carrier grows 5 ~ 35mm, wide 2 ~ 6mm, 0.5 ~ 1.5mm of thickness;Paper fiber element carrier width direction is folding It is stacked.Cellulose carrier of the present invention is filament shape, and its main purpose is when in use, by tens of or over one hundred paper Matter cellulose carrier is involved among cigarette jointly, while paper fiber element carrier keeps appropriate spacing, prevent from heating or Person heats uneven.
The mass ratio of liquid nicotine and cellulose is 1:1000~50:1000.
A kind of method for making nicotine paper fiber element carrier, papery is made using wood pulp and/or string Cellulose carrier;Pure liquid nicotine and diluent and/or additive are well mixed, form nicotine mixed liquor, will Paper fiber element carrier is completely soaked among nicotine mixed liquor and moistened completely to cellulose carrier, takes out;In 25 ~ 50 DEG C of rings Under border, aeration-drying to paper fiber element carrier water content is under 5 ~ 15% states, takes out nicotine cellulose carrier, is used Polyvinyl chloride packs bag hermetic package.
Nicotine paper fiber element carrier of the present invention is inserted on electronic cigarette heater strip or heating plate, heated To 300 ~ 350 DEG C, the composition such as nicotine component and sweetener, flavor additives useful slowly discharges, but does not have among this process Tar produces, while is unable to reach the burning-point of paper fiber element, and paper fiber element, which can not burn, produces dust.
Embodiment
Embodiment 1
The purpose of the present embodiment is to provide nicotine paper fiber element carrier and the making side that a kind of electronic cigarette heater uses Method, nicotine is absorbed among paper fiber element, the purpose of the i.e. reachable nicotine volatilization intake of heating paper fiber element, subtracted Few result of combustion of tobacco influences to caused by environment.
The present embodiment specifically provides a kind of nicotine paper fiber element carrier, including for absorbing the paper of liquid nicotine Matter cellulose carrier, wherein cellulose carrier include the paper fiber piece that wood pulp and/or string make, and liquid Buddhist nun is ancient Fourth ingredient draws are among the space of cellulose carrier;Every cellulose carrier adhere to 0.01 ~ 0.1mg pure nicotine into Point.
Nicotine is tobacco extract and/or artificial synthesized nicotine, pure nicotine mass fraction in liquid nicotine Content is 2 ~ 73%, and surplus is diluent and/or additive;
The space aperture of paper fiber element carrier is 50 ~ 175 nanometers.Specifically, the space aperture of paper fiber element carrier be 90 ~ 110 nanometers.
The string that the present embodiment uses includes cotton, beet, wheat bran, orange peel, herbage, straw, bark, tealeaves, bamboo One of fiber or its combination.The cellulose extraction that the present embodiment uses is extensive, is not limited to floristics, especially with Paper pulp fiber, it can be beaten into using treated waste and old paper as fiber, realize reusing for resource.
For the present embodiment in order to reach preferable assimilation effect, every cellulose carrier adheres to 0.22 ~ 0.05mg pure Buddhist nun Ancient fourth composition.This metering uses pure nicotine equivalent.
In order to ensure that absorption process is quick, and cause nicotine paper fiber carrier that there is its in addition to nicotine His flavor, crowd's adaptability is lifted, increased diluent and/or additive are solvent, increased in nicotine paper fiber carrier Mould one of agent, NMF, adhesive, sweetener, spices or its combination.Additive in the present embodiment can also add anti- Oxidant.
Wherein:
Solvent is one of organic solvent, water, honey, inspissated juice or its combination.
Organic solvent includes but is not limited to:Propane diols, ethanol, glycerine, vegetable oil, partially hydrogenated vegetable oil, medium chain triglyceride Three esters, phthalic acid ester, polycarboxylate, hexylene glycol, butanediol, glyceride, vinyl alcohol, disaccharide iron agar, sugar alcohol, glycerine, One of sorbierite, xylitol, maltitol, hydroxyl isomaltulose, mannitol, polymer polyatomic alcohol, beverage wine or its combination.
Adhesive includes but is not limited to:Dextrin, cyclodextrine derivatives, starch, modified starch, carboxymethyl cellulose, hydroxypropyl Base cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, methylcellulose, konjaku flour, collagen, inulin, soybean protein, Lactalbumin, casein, gluten powder, carrageenan, sodium alginate, propylene glycol alginate, xanthans, Propiram are more Sugar, condense polysaccharide, be gellan gum, locust bean gum, sesbania gum, tara gum, tragacanth, pectin, agar, zeins, bright Glue, Chinese parasol tree extract, Semen Plantaginis extract, chitin, chitosan, Arabic gum, polyvinylpyrrolidone, PEO, It is polyvinyl alcohol, guar gum, xanthans, cellulose, maltodextrin, polyurethane, silicon-containing polymer, polyester, polyacrylate, poly- Ethene, hydrogenated styrene-butadiene block copolymer, SBS, the isoamyl of styrene one Diene-styrene copolymer, loquat extract, natural gum, butadiene-styrene rubber, butyl rubber, polyisobutene, glyceride, terpenes tree Fat, polyvinyl acetate, paraffin, microwax, hydrogenated vegetable oil, lecithin, glycerin monostearate, Heveatex, dragon spruce One of fat, frankincense gum or its combination.Adhesive can lift attachment degree of the nicotine on cellulose carrier.
NMF includes but is not limited to:One of Quillaia saponaria bark extract, 'alpha '-hydroxy acids, lactic acid, aloe gel, honey or It is combined.NMF prevents paper fiber element carrier from excessively drying phenomena such as being broken.
Sweetener includes but is not limited to:Polydextrose, glucose mixture, molasses element, corn sweetener, syrup, fructose, Fruit drops, lactose, milk sugar, maltose, mannitol, D-sorbite, D-sorbite, inspissated juice, saccharin, Aspartame, sugarcane One of sugared element, acesulfame potassium or its combination.Lift the experience property of user.
Spices includes but is not limited to:Honey, radix glycyrrhizae, peppermint, fruit flavor, sweet wine flavoring, spirits flavoring, peppermint are adjusted Taste substance, lavender flavoring, Chinese cassia tree flavoring, cardamom flavoring, cloves flavoring, santal flavoring, honey elite, rose One of oil, vanilla elite, lemon oil, orange oil, refined jasmine oil, capsicum oil, coffee flavoring, cocoa flavoring or its group Close.The experience property of user is lifted, is adapted to women or the user more sensitive to tobacco.
In order to lift rate of drying, organic solvent is preferred for propane diols, absolute ethyl alcohol, propane diols and aqueous mixtures, ethanol With one of aqueous mixtures or its combine.
Paper fiber element carrier grows 5 ~ 35mm, wide 2 ~ 6mm, 0.5 ~ 1.5mm of thickness;Paper fiber element carrier width direction is folding It is stacked.Cellulose carrier described in the present embodiment is filament shape, and its main purpose is when in use, by tens of or over one hundred Paper fiber element carrier is involved among cigarette jointly, while paper fiber element carrier keeps appropriate spacing, prevents from heating Or heating is uneven.
The mass ratio of liquid nicotine and cellulose is 1:1000~50:1000.
A kind of method for making nicotine paper fiber element carrier, papery is made using wood pulp and/or string Cellulose carrier;Pure liquid nicotine and diluent and/or additive are well mixed, form nicotine mixed liquor, will Paper fiber element carrier is completely soaked among nicotine mixed liquor and moistened completely to cellulose carrier, takes out;In 25 ~ 50 DEG C of rings Under border, aeration-drying to paper fiber element carrier water content is under 5 ~ 15% states, takes out nicotine cellulose carrier, is used Polyvinyl chloride packs bag hermetic package.
Nicotine paper fiber element carrier described in the present embodiment is inserted on electronic cigarette heater strip or heating plate, added To 300 ~ 350 DEG C, the composition such as nicotine component and sweetener, flavor additives useful slowly discharges heat, but does not have among this process There is tar generation, while be unable to reach the burning-point of paper fiber element, paper fiber element, which can not burn, produces dust.
Embodiment 2
Nicotine is tobacco extract in this implementation, and pure nicotine mass fraction content is in liquid nicotine mixed solution 50%, surplus is 50% propane diols(Volume ratio)And attar of rose, NMF use aloe gel.
The space aperture of cellulose is mostly 100 nanometers in 95 ~ 105 nanometer ranges;Every cellulose carrier attachment 0.02mg pure nicotine component.
Remaining embodiment and preparation method are same as Example 1.
Embodiment 3
Nicotine is artificial synthesized nicotine in this implementation, pure nicotine mass fraction content in liquid nicotine mixed solution For 70%, surplus is 60% ethanol(Volume ratio)And mint flavor, NMF use lactic acid.
The space aperture of cellulose is mostly 105 nanometers;Every cellulose carrier attachment 0.05mg pure nicotine component.
Remaining embodiment and preparation method are same as Example 1.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art Scholar can understand present disclosure and implement according to this, and it is not intended to limit the scope of the present invention.It is all according to the present invention The equivalent change or modification that Spirit Essence is made, it should all be included within the scope of the present invention.
In addition, there is omitted herein the description to known features and technology, to avoid unnecessarily obscuring idea of the invention.

Claims (10)

  1. A kind of 1. nicotine paper fiber element carrier, it is characterised in that:Including the paper fiber element for absorbing liquid nicotine Carrier, wherein cellulose carrier include the paper fiber piece that wood pulp and/or string make, and liquid nicotine component is inhaled It is received among the space of cellulose carrier;Every cellulose carrier adheres to 0.01 ~ 0.1mg pure nicotine component;
    Nicotine is tobacco extract and/or artificial synthesized nicotine, pure nicotine mass fraction content in liquid nicotine For 2 ~ 73%, surplus is diluent and/or additive;
    The space aperture of paper fiber element carrier is 50 ~ 175 nanometers.
  2. 2. according to the nicotine paper fiber element carrier described in claim 1, it is characterised in that:String includes cotton, sweet tea One of dish, wheat bran, orange peel, herbage, straw, bark, tealeaves, bamboo fibre or its combination.
  3. 3. according to described in claim 1, it is characterised in that:Every cellulose carrier adheres to 0.22 ~ 0.05mg pure nicotine Composition.
  4. 4. according to the nicotine paper fiber element carrier described in claim 1, it is characterised in that:Diluent and/or additive are One of solvent, plasticizer, NMF, adhesive, sweetener, spices or its combination.
  5. 5. according to the nicotine paper fiber element carrier described in claim 1, it is characterised in that:The space of paper fiber element carrier Aperture is 90 ~ 110 nanometers.
  6. 6. according to the nicotine paper fiber element carrier described in claim 4, it is characterised in that:Solvent is organic solvent, water, honeybee One of honey, inspissated juice or its combination.
  7. 7. according to the nicotine paper fiber element carrier described in claim 6, it is characterised in that:Organic solvent is propane diols, nothing One of water-ethanol, propane diols and aqueous mixtures, ethanol and aqueous mixtures or its combine.
  8. 8. according to the nicotine paper fiber element carrier described in claim 1, it is characterised in that:Paper fiber element carrier length 5 ~ 35mm, wide 2 ~ 6mm, 0.5 ~ 1.5mm of thickness;Paper fiber element carrier width direction is bending.
  9. 9. according to the nicotine paper fiber element carrier described in claim 1, it is characterised in that:Liquid nicotine and cellulose Mass ratio is 1:1000~50:1000.
  10. A kind of 10. method for making nicotine paper fiber element carrier described in claim 1, it is characterised in that:Use wood pulp fibre paper Slurry and/or string make paper fiber element carrier;Pure liquid nicotine and diluent and/or additive are mixed equal It is even, nicotine mixed liquor is formed, paper fiber element carrier is completely soaked among nicotine mixed liquor complete to cellulose carrier Full moistening, takes out;Under 25 ~ 50 DEG C of environment, aeration-drying to paper fiber element carrier water content is under 5 ~ 15% states, is taken Go out nicotine cellulose carrier, bag hermetic package is packed using polyvinyl chloride.
CN201810013031.9A 2018-01-07 2018-01-07 A kind of nicotine paper fiber element carrier and preparation method Pending CN107874324A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109371747A (en) * 2018-09-27 2019-02-22 安庆市恒原纸塑有限公司 A kind of disposable degradable paper disc and preparation method thereof
CN110720657A (en) * 2019-10-28 2020-01-24 武汉红金叶新材料科技有限公司 Rod-shaped body formed by rope made of paper sheets and manufacturing process thereof

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GB1033674A (en) * 1963-01-17 1966-06-22 Battelle Memorial Institute Improvements relating to inhaling devices
CN86103434A (en) * 1985-05-24 1986-11-26 高级烟草制品公司 The nicotine dispenser of band polymeric reservoir of nicotine
CN101158126A (en) * 2007-10-27 2008-04-09 广西大学 Pulping method for plant fibre raw material combined with biology
CN101302717A (en) * 2007-05-09 2008-11-12 孙新龙 Process for making plant fiber capable of absorbing nicotine
WO2008151777A2 (en) * 2007-06-11 2008-12-18 Bel Air International Corp. Nicotine depot, in particular for a smoke-free cigarette, and method for the production thereof
CN101528199A (en) * 2006-03-16 2009-09-09 尼科诺瓦姆股份公司 Improved snuff composition
CN105642016A (en) * 2016-01-13 2016-06-08 唐山立雄峰汇材料科技有限公司 Functional cigarette holder filter bag
US20160295926A1 (en) * 2013-12-05 2016-10-13 Philip Morris Products S.A. Non-tobacco nicotine containing article
WO2016184977A1 (en) * 2015-05-20 2016-11-24 British American Tobacco (Investments) Limited Aerosol generating material and devices including the same
US20170273347A1 (en) * 2014-09-30 2017-09-28 Philip Morris Products S.A. Homogenized tobacco material and method of production of homogenized tobacco material

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1033674A (en) * 1963-01-17 1966-06-22 Battelle Memorial Institute Improvements relating to inhaling devices
CN86103434A (en) * 1985-05-24 1986-11-26 高级烟草制品公司 The nicotine dispenser of band polymeric reservoir of nicotine
CN101528199A (en) * 2006-03-16 2009-09-09 尼科诺瓦姆股份公司 Improved snuff composition
CN101302717A (en) * 2007-05-09 2008-11-12 孙新龙 Process for making plant fiber capable of absorbing nicotine
WO2008151777A2 (en) * 2007-06-11 2008-12-18 Bel Air International Corp. Nicotine depot, in particular for a smoke-free cigarette, and method for the production thereof
CN101158126A (en) * 2007-10-27 2008-04-09 广西大学 Pulping method for plant fibre raw material combined with biology
US20160295926A1 (en) * 2013-12-05 2016-10-13 Philip Morris Products S.A. Non-tobacco nicotine containing article
US20170273347A1 (en) * 2014-09-30 2017-09-28 Philip Morris Products S.A. Homogenized tobacco material and method of production of homogenized tobacco material
WO2016184977A1 (en) * 2015-05-20 2016-11-24 British American Tobacco (Investments) Limited Aerosol generating material and devices including the same
CN105642016A (en) * 2016-01-13 2016-06-08 唐山立雄峰汇材料科技有限公司 Functional cigarette holder filter bag

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109371747A (en) * 2018-09-27 2019-02-22 安庆市恒原纸塑有限公司 A kind of disposable degradable paper disc and preparation method thereof
CN110720657A (en) * 2019-10-28 2020-01-24 武汉红金叶新材料科技有限公司 Rod-shaped body formed by rope made of paper sheets and manufacturing process thereof

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Application publication date: 20180406