CN107858058A - A kind of Compound waterborne acrylate outer wall heat-insulating coating and preparation method thereof - Google Patents
A kind of Compound waterborne acrylate outer wall heat-insulating coating and preparation method thereof Download PDFInfo
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- CN107858058A CN107858058A CN201711142487.7A CN201711142487A CN107858058A CN 107858058 A CN107858058 A CN 107858058A CN 201711142487 A CN201711142487 A CN 201711142487A CN 107858058 A CN107858058 A CN 107858058A
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
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Abstract
The present invention provides a kind of Compound waterborne acrylate outer wall heat-insulating coating, and its raw material includes following components by weight：20 40 parts of aqueous acroleic acid resin, 25 parts of hollow glass bead, 8 15 parts of diatomite, 5 10 parts of nano titanium oxide, 6 10 parts of ceramic hollow microballon, 36 parts of nano far infrared ceramic powder, 46 parts of infra-red radiation powder, 15 25 parts of titanium dioxide, 8 12 parts of nano titanium oxide, 13 parts of alumina powder, 0.3 0.9 parts of PH conditioning agents, 0.5 1.0 parts of dispersant, 0.2 0.5 parts of defoamer, 1.0 2.5 parts of coalescents, 0.5 0.8 parts of thickener, 0.5 0.8 parts of antifreezing agent, 0.1 0.3 parts of wetting agent, 30 50 parts of deionized water.The present invention also provides its preparation method, and the coating has good compatibility, dispersiveness and stability, the advantages such as heat insulation property, the feature of environmental protection, outdoor weathe resistance, thermal conductivity factor are low, meets the development trend of building external paint low-carbon energy-saving environmental protection.
Description
Technical field
The present invention relates to a kind of outer wall heat-insulating coating, and in particular to a kind of Compound waterborne acrylate outer wall heat-insulating coating
And preparation method thereof.
Background technology
Insulating moulding coating can be divided into 3 kinds of isolation-type, reflection-type and radial pattern, the wherein heat-insulated painting of isolation-type according to insulating mechanism
Material belongs to thick matter traditional coating, and its insulating mechanism is impedance heat transfer, technology relative maturity；Radiation Heat-insulated Paint is to pass through
The form of radiation, which is transmitted into the sunshine light heat that building absorbs in air with certain wavelength, reaches heat insulation and heat control；Reflection
The insulating mechanism of type insulating moulding coating is reflected sunlight.
Construction wall heat insulation thermal insulation coatings, it is a kind of adiabatic coating, belongs to functional coating.Conducted according to heat, convection current
With three kinds of modes of radiation, construction wall heat insulation thermal insulation coatings are accordingly divided into isolation-type construction wall heat insulation thermal insulation coatings, anti-
Emitting construction wall heat insulation thermal insulation coatings, radial pattern construction wall thermal insulation coatings three major types, the Insulating mechanism of this three classes coating is not
Together, using also having nothing in common with each other.
Isolation-type heat insualting building heat insulating coating material for wall is based on adiabatic aggregate, is a kind of " adiabatic mortar "；Reflection-type
Heat insualting building heat insulating coating material for wall is the reflex by coating, and the infra-red radiation in daylight is reflexed into exterior space, from
And avoid because absorbing radiation-induced temperature rise.
Reflection type thermal insulation construction wall thermal insulation coatings can effectively prevent the inflow of outside heat；Isolation-type heat insualting building wall
Body thermal insulation coatings are effectively to prevent flowing in and out for heat with adiabatic aggregate.This two kinds of heat insulating coatings are all that building is outer
The effective ways of wall heat-insulation and heat-preservation, but some defects are equally existed as various thermal isolation techniques during exclusive use, should
It is unavoidable insufficient in.
The content of the invention
A kind of existing existing issue of the purpose of the present invention aiming at single type coating, there is provided Compound waterborne propylene
Acid esters outer wall heat-insulating coating, this kind of Compound waterborne acrylate outer wall heat-insulating coating is using aqueous acroleic acid resin emulsion as film forming
Material, it is the hollow glass bead of addition, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, red
The compound heat-insulated face such as external radiation powder, titanium dioxide, nano titanium oxide, alumina powder, filler, and add part of auxiliary and go
Ionized water, a kind of Compound waterborne acrylate outer wall heat-insulating coating being prepared.Outside this kind of Compound waterborne acrylate
Wall insulating moulding coating not only has good compatibility, dispersiveness and stability, and with the good transparency, insulation
Property, the advantage such as the feature of environmental protection, outdoor weathe resistance, thermal conductivity factor be low, meet the development trend of building external paint low-carbon energy-saving environmental protection.
It is a further object of the present invention to provide the preparation method of this kind of Compound waterborne acrylate outer wall heat-insulating coating.
To realize above-mentioned purpose of the present invention, a kind of Compound waterborne acrylate outer wall heat-insulating coating of the present invention is using following
Technical scheme：A kind of Compound waterborne acrylate outer wall heat-insulating coating, its raw material include following components by weight：Water-based third
Olefin(e) acid resin 20-40 parts, hollow glass bead 2-5 parts, diatomite 8-15 parts, nano titanium oxide 5-10 parts, ceramic hollow
Microballon 6-10 parts, nano far infrared ceramic powder 3-6 parts, infra-red radiation powder 4-6 parts, titanium dioxide 15-25 parts, nano titanium oxide
8-12 parts, alumina powder 1-3 parts, PH conditioning agent 0.3-0.9 parts, dispersant 0.5-1.0 parts, defoamer 0.2-0.5 parts, into
Film auxiliary agent 1.0-2.5 parts, thickener 0.5-0.8 parts, antifreezing agent 0.5-0.8 parts, wetting agent 0.1-0.3 parts, deionized water
30-50 parts.
Further, described ceramic hollow microballon is the hollow beads of 10~100 μm of particle diameter.
Further, described hollow glass bead is the hollow beads of 50~150 μm of particle diameter.
Further, described nano titanium oxide is 15~60nm of particle diameter rutile type nano titanic oxide.
Further, described infra-red radiation powder is in matrix Al2O3 powders, adds 15-20% mass fractions
MnO2 and 10-15% mass fraction TiO2 powders, are sieved after sufficiently mixing, then powder is put into high alumina ceramic crucible,
1~4 hour is incubated at 1100~1300 DEG C, synthetic product is after attrition grinding, the infra-red radiation powder of acquisition.
Further, described wetting agent is non-ionic wetting agent；Described dispersant is non-ionic dispersing agent；Institute
One or both of defoamer organic silicon defoamer, organic silicon modified by polyether and mineral oil antifoam agent for stating；Described thickening
Agent is：One or both of hydroxyethyl cellulose, hydroxypropyl cellulose, polyurethanes thickener or alkali swelling type thickener with
On；The coalescents are ethylene glycol or ethylene glycol diether.
Further, its preparation method comprises the following steps：
S10, according to formula ratio dispersant, wetting agent, antifreezing agent, 1/2-3/5 defoamers are added in deionized water, 300~
5-10min is stirred under 500r/min rotating speed to be sufficiently mixed；
The glass hollow for being slowly added to formula ratio in S11, the mixture obtained to step S10 by density order big after first small is micro-
Pearl, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, infra-red radiation powder, titanium dioxide, nanometer two
Titanium oxide, alumina powder while appropriate defoamer is according to circumstances added, be then slowly added into coalescents, part thickener
Disperse 25-50min under 1000~2000r/min rotating speed and obtain the mixed system that fineness is 60 μm；
S12, under 300~600r/min rotating speeds, water-based the third of formula ratio is sequentially added in the mixed system obtained to step S11
Olefin(e) acid resin, remaining defoamer, thickener, 30-40min is stirred, adjust viscosity and PH, stop stirring, stood, filtering, obtained
Compound waterborne acrylate outer wall heat-insulating coating.
It is compared with the prior art, the invention has the advantages that：
1st, it is strong that the effect of nano titanium oxide shielding ultraviolet rays is added in the present invention, the infringement of ultraviolet is prevented, improves coating
Service life.Meanwhile its higher hardness, density, dielectric constant and refractive index, be favorably improved coating covering power and
Color power, and have good reflex to the heat radiation in sunlight；
2nd, ceramic hollow microballon, hollow glass bead, diatomite are with the addition of in the present invention, low thermal conductivity, guarantor can be played to building
The heat-insulated effect of temperature, when play the role of thermal source close to when can play heat-insulated, effectively raise the ignition temperature of film, extend
The fire resistance period of film, prevents fire from occurring rapidly；
3rd, the nano far infrared ceramic powder that adds not only heat-insulation and heat-preservation in the present invention, in sunshine（Especially ultraviolet）Under irradiation
OH- is generated, can effectively remove benzene, formaldehyde, sulfide, ammonia and the stink substance of indoor and outdoor, and there is sterilizing function, is green ring
Friendly coating；
4th, the infra-red radiation powder with high radiant rate is used in a kind of Compound waterborne acrylate outer wall heat-insulating coating of the present invention
Reach the purpose of high radiation.Thus combine traditional heat-insulated effect of tiny balloon, form with high reflection and it is high radiate based on,
Novel aqueous insulating moulding coating supplemented by tradition is heat-insulated, has reached optimal heat insulation and preservation effect；
5th, a kind of Compound waterborne acrylate outer wall heat-insulating coating of the present invention not only has good compatibility, dispersiveness and steady
It is qualitative, and with the advantage such as the good transparency, heat insulation property, the feature of environmental protection, outdoor weathe resistance, thermal conductivity factor be low, meet
The development trend of building external paint low-carbon energy-saving environmental protection.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.The specific embodiments described herein are merely illustrative of the present invention, is not used to limit
The present invention.
Embodiment 1
A kind of Compound waterborne acrylate outer wall heat-insulating coating, its raw material include following components by weight：Water soluble acrylic acid
20 parts of resin, 2 parts of hollow glass bead, 8 parts of diatomite, 5 parts of nano titanium oxide, 6 parts of ceramic hollow microballon, nano-far-infrared
3 parts of ceramic powder, 4 parts of infra-red radiation powder, 15 parts of titanium dioxide, 8 parts of nano titanium oxide, 1 part of alumina powder, PH conditioning agents 0.3
Part, 0.5 part of dispersant, 0.2 part of defoamer, 1.0 parts of coalescents, 0.5 part of thickener, 0.5 part of antifreezing agent, 0.1 part of wetting agent,
30 parts of deionized water.
Described ceramic hollow microballon is the hollow beads of 10 μm of particle diameter.
Described hollow glass bead is the hollow beads of 50 μm of particle diameter.
Described nano titanium oxide is the nm of particle diameter 15 rutile type nano titanic oxide.
Described infra-red radiation powder is the MnO2 and 10% mass that 15% mass fraction is added in matrix Al2O3 powders
Fraction TiO2 powders, are sieved after sufficiently mixing, then powder is put into high alumina ceramic crucible, and 1 hour is incubated at 1100 DEG C, are closed
Into product after attrition grinding, the infra-red radiation powder of acquisition.
Described wetting agent is non-ionic wetting agent；Described dispersant is non-ionic dispersing agent；Described defoaming
Agent organic silicon defoamer；Described thickener is：Hydroxyethyl cellulose；The coalescents are ethylene glycol.
Its preparation method comprises the following steps：
S10, according to formula ratio by dispersant, wetting agent, antifreezing agent, 1/2-3/5 defoamers add deionized water in, in 300r/
5min is stirred under min rotating speed to be sufficiently mixed；
The glass hollow for being slowly added to formula ratio in S11, the mixture obtained to step S10 by density order big after first small is micro-
Pearl, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, infra-red radiation powder, titanium dioxide, nanometer two
Titanium oxide, alumina powder while appropriate defoamer is according to circumstances added, be then slowly added into coalescents, part thickener
Disperse 25min under 1000r/min rotating speed and obtain the mixed system that fineness is 60 μm；
S12, under 300r/min rotating speeds, the water soluble acrylic acid of formula ratio is sequentially added in the mixed system obtained to step S11
Resin, remaining defoamer, thickener, 30min is stirred, adjust viscosity and PH, stop stirring, stood, filtering, obtain composite water
Property acrylate outer wall heat-insulating coating.
Embodiment 2
A kind of Compound waterborne acrylate outer wall heat-insulating coating, its raw material include following components by weight：Water soluble acrylic acid
40 parts of resin, 5 parts of hollow glass bead, 15 parts of diatomite, 10 parts of nano titanium oxide, ceramic hollow microballon 10 part, nanometer
6 parts of far-infared ceramic powder, 6 parts of infra-red radiation powder, 25 parts of titanium dioxide, 12 parts of nano titanium oxide, 3 parts of alumina powder, PH are adjusted
Save 0.9 part of agent, 1.0 parts of dispersant, 0.5 part of defoamer, 2.5 parts of coalescents, 0.8 part of thickener, antifreezing agent 0.8
Part, 0.3 part of wetting agent, 50 parts of deionized water.
Described ceramic hollow microballon is the hollow beads of 100 μm of particle diameter.
Described hollow glass bead is the hollow beads of 150 μm of particle diameter.
Described nano titanium oxide is particle diameter 60nm rutile type nano titanic oxide.
Described infra-red radiation powder is the MnO2 and 15% mass that 20% mass fraction is added in matrix Al2O3 powders
Fraction TiO2 powders, are sieved after sufficiently mixing, then powder is put into high alumina ceramic crucible, and 4 hours are incubated at 1300 DEG C, are closed
Into product after attrition grinding, the infra-red radiation powder of acquisition.
Described wetting agent is non-ionic wetting agent；Described dispersant is non-ionic dispersing agent；Described defoaming
Agent organic silicon modified by polyether；Described thickener is：Hydroxypropyl cellulose；The coalescents are ethylene glycol diether.
Its preparation method comprises the following steps：
S10, according to formula ratio by dispersant, wetting agent, antifreezing agent, 1/2-3/5 defoamers add deionized water in, in 500r/
10min is stirred under min rotating speed to be sufficiently mixed；
The glass hollow for being slowly added to formula ratio in S11, the mixture obtained to step S10 by density order big after first small is micro-
Pearl, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, infra-red radiation powder, titanium dioxide, nanometer two
Titanium oxide, alumina powder while appropriate defoamer is according to circumstances added, be then slowly added into coalescents, part thickener
Disperse 50min under 2000r/min rotating speed and obtain the mixed system that fineness is 60 μm；
S12, under 600r/min rotating speeds, the water soluble acrylic acid of formula ratio is sequentially added in the mixed system obtained to step S11
Resin, remaining defoamer, thickener, 40min is stirred, adjust viscosity and PH, stop stirring, stood, filtering, obtain composite water
Property acrylate outer wall heat-insulating coating.
Embodiment 3
A kind of Compound waterborne acrylate outer wall heat-insulating coating, its raw material include following components by weight：Water soluble acrylic acid
35 parts of resin, 4 parts of hollow glass bead, 12 parts of diatomite, 8 parts of nano titanium oxide, ceramic hollow microballon 8 part, nanometer are remote red
Outer 5 parts of ceramic powder, 5 parts of infra-red radiation powder, 18 parts of titanium dioxide, 9 parts of nano titanium oxide, 2 parts of alumina powder, PH conditioning agents
0.6 part, 0.7 part of dispersant, 0.4 part of defoamer, 1.5 parts of coalescents, 0.6 part of thickener, 0.6 part of antifreezing agent, wetting agent
0.2 part, 35 parts of deionized water.
Described ceramic hollow microballon is the hollow beads of 80 μm of particle diameter.
Described hollow glass bead is the hollow beads of 70 μm of particle diameter.
Described nano titanium oxide is particle diameter 40nm rutile type nano titanic oxide.
Described infra-red radiation powder is the MnO2 and 12% mass that 18% mass fraction is added in matrix Al2O3 powders
Fraction TiO2 powders, are sieved after sufficiently mixing, then powder is put into high alumina ceramic crucible, and 3 hours are incubated at 1200 DEG C, are closed
Into product after attrition grinding, the infra-red radiation powder of acquisition.
Described wetting agent is non-ionic wetting agent；Described dispersant is non-ionic dispersing agent；Described defoaming
Two kinds of agent organic silicon defoamer, organic silicon modified by polyether combinations arbitrarily matched；Described thickener is：Polyurethanes thickener
It is two or more；The coalescents are ethylene glycol diether.
Its preparation method comprises the following steps：
S10, according to formula ratio by dispersant, wetting agent, antifreezing agent, 1/2-3/5 defoamers add deionized water in, in 400r/
6min is stirred under min rotating speed to be sufficiently mixed；
The glass hollow for being slowly added to formula ratio in S11, the mixture obtained to step S10 by density order big after first small is micro-
Pearl, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, infra-red radiation powder, titanium dioxide, nanometer two
Titanium oxide, alumina powder while appropriate defoamer is according to circumstances added, be then slowly added into coalescents, part thickener
Disperse 40min under 1800r/min rotating speed and obtain the mixed system that fineness is 60 μm；
S12, under 500r/min rotating speeds, the water soluble acrylic acid of formula ratio is sequentially added in the mixed system obtained to step S11
Resin, remaining defoamer, thickener, 35min is stirred, adjust viscosity and PH, stop stirring, stood, filtering, obtain composite water
Property acrylate outer wall heat-insulating coating.
Claims (7)
1. a kind of Compound waterborne acrylate outer wall heat-insulating coating, it is characterised in that its raw material includes with the following group by weight
Point：Aqueous acroleic acid resin 20-40 parts, hollow glass bead 2-5 parts, diatomite 8-15 parts, nano titanium oxide 5-10 parts,
Ceramic hollow microballon 6-10 parts, nano far infrared ceramic powder 3-6 parts, infra-red radiation powder 4-6 parts, titanium dioxide 15-25 parts, nanometer
Titanium dioxide 8-12 parts, alumina powder 1-3 parts, PH conditioning agent 0.3-0.9 parts, dispersant 0.5-1.0 parts, defoamer 0.2-
0.5 part, coalescents 1.0-2.5 parts, thickener 0.5-0.8 parts, antifreezing agent 0.5-0.8 parts, wetting agent 0.1-0.3 parts,
Deionized water 30-50 parts.
A kind of 2. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is described
Ceramic hollow microballon be 10~100 μm of particle diameter hollow beads.
A kind of 3. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is described
Hollow glass bead be 50~150 μm of particle diameter hollow beads.
A kind of 4. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is described
Nano titanium oxide be 15~60nm of particle diameter rutile type nano titanic oxide.
A kind of 5. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is described
Infra-red radiation powder be in matrix Al2O3 powders, add 15-20% mass fractions MnO2 and 10-15% mass fractions
TiO2 powders, are sieved after sufficiently mixing, then powder is put into high alumina ceramic crucible, and it is small that 1~4 is incubated at 1100~1300 DEG C
When, synthetic product is after attrition grinding, the infra-red radiation powder of acquisition.
A kind of 6. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is described
Wetting agent be non-ionic wetting agent；Described dispersant is non-ionic dispersing agent；Described defoamer organosilicon defoaming
One or both of agent, organic silicon modified by polyether and mineral oil antifoam agent；Described thickener is：Hydroxyethyl cellulose, hydroxyl
It is more than one or both of propyl cellulose, polyurethanes thickener or alkali swelling type thickener；The coalescents are second
Glycol or ethylene glycol diether.
A kind of 7. Compound waterborne acrylate outer wall heat-insulating coating according to claim 1, it is characterised in that：It is made
Preparation Method comprises the following steps：
S10, according to formula ratio dispersant, wetting agent, antifreezing agent, 1/2-3/5 defoamers are added in deionized water, 300~
5-10min is stirred under 500r/min rotating speed to be sufficiently mixed；
The glass hollow for being slowly added to formula ratio in S11, the mixture obtained to step S10 by density order big after first small is micro-
Pearl, diatomite, nano titanium oxide, ceramic hollow microballon, nano far infrared ceramic powder, infra-red radiation powder, titanium dioxide, nanometer two
Titanium oxide, alumina powder while appropriate defoamer is according to circumstances added, be then slowly added into coalescents, part thickener
Disperse 25-50min under 1000~2000r/min rotating speed and obtain the mixed system that fineness is 60 μm；
S12, under 300~600r/min rotating speeds, water-based the third of formula ratio is sequentially added in the mixed system obtained to step S11
Olefin(e) acid resin, remaining defoamer, thickener, 30-40min is stirred, adjust viscosity and PH, stop stirring, stood, filtering, obtained
Compound waterborne acrylate outer wall heat-insulating coating.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711142487.7A CN107858058A (en) | 2017-11-17 | 2017-11-17 | A kind of Compound waterborne acrylate outer wall heat-insulating coating and preparation method thereof |
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| CN201711142487.7A CN107858058A (en) | 2017-11-17 | 2017-11-17 | A kind of Compound waterborne acrylate outer wall heat-insulating coating and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108587366A (en) * | 2018-04-16 | 2018-09-28 | 合肥天沃能源科技有限公司 | A kind of insulating mould coating exposed wall of building and preparation method thereof |
| CN108912778A (en) * | 2018-07-18 | 2018-11-30 | 合肥帧讯低温科技有限公司 | Heat-insulating coating for heat-insulating wall and preparation method thereof |
| CN109577701A (en) * | 2018-11-30 | 2019-04-05 | 国网河南省电力公司商丘供电公司 | One kind is based on substation's protection exterior wall |
| CN109852175A (en) * | 2018-12-19 | 2019-06-07 | 南京红枫环保材料有限公司 | A kind of reflective insulation exterior wall paint and preparation method thereof |
| CN109913056A (en) * | 2019-04-03 | 2019-06-21 | 星空男孩(杭州)科技有限公司 | Aqueous thick-slurry type insulating moulding coating and its preparation process |
| CN110218499A (en) * | 2019-06-28 | 2019-09-10 | 苏州凯康化工科技有限公司 | A kind of heat-reflecting heat-insulating water-repellent paint and preparation method thereof for external surface of buildings |
| CN110294608A (en) * | 2019-06-29 | 2019-10-01 | 扬州市海纳源科技服务有限责任公司 | A kind of compound insulating refractory engineering material and preparation method |
| CN116041995A (en) * | 2022-12-23 | 2023-05-02 | 杭州明敏涂料有限公司 | Reflective heat-insulating diatom inorganic heat-insulating coating and preparation process thereof |
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2017
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108587366A (en) * | 2018-04-16 | 2018-09-28 | 合肥天沃能源科技有限公司 | A kind of insulating mould coating exposed wall of building and preparation method thereof |
| CN108912778A (en) * | 2018-07-18 | 2018-11-30 | 合肥帧讯低温科技有限公司 | Heat-insulating coating for heat-insulating wall and preparation method thereof |
| CN109577701A (en) * | 2018-11-30 | 2019-04-05 | 国网河南省电力公司商丘供电公司 | One kind is based on substation's protection exterior wall |
| CN109577701B (en) * | 2018-11-30 | 2020-11-17 | 国网河南省电力公司商丘供电公司 | Protection outer wall for transformer substation |
| CN109852175A (en) * | 2018-12-19 | 2019-06-07 | 南京红枫环保材料有限公司 | A kind of reflective insulation exterior wall paint and preparation method thereof |
| CN109913056A (en) * | 2019-04-03 | 2019-06-21 | 星空男孩(杭州)科技有限公司 | Aqueous thick-slurry type insulating moulding coating and its preparation process |
| CN110218499A (en) * | 2019-06-28 | 2019-09-10 | 苏州凯康化工科技有限公司 | A kind of heat-reflecting heat-insulating water-repellent paint and preparation method thereof for external surface of buildings |
| CN110294608A (en) * | 2019-06-29 | 2019-10-01 | 扬州市海纳源科技服务有限责任公司 | A kind of compound insulating refractory engineering material and preparation method |
| CN116041995A (en) * | 2022-12-23 | 2023-05-02 | 杭州明敏涂料有限公司 | Reflective heat-insulating diatom inorganic heat-insulating coating and preparation process thereof |
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