CN107854414A - A kind of the effect of juice containing bear gall property topical composition - Google Patents

Abstract

The effect of providing a kind of juice containing bear gall property topical composition of the invention, is made up of following raw material：Rose, sanchi flower, biological carbohydrate gum 1, rose rhodobryum herb, glycerine, Jojoba wax, rhodiola root, testis et penis canitis, mulberry fruit, octadecyl alcolol, Morinda officinalis, lanolin, bear gall juice, niacinamide, Scleroglucan, compared with prior art, the present invention has following beneficial effect：By adding appropriate bear gall juice in cosmetic base; promote subcutaneous blood circulation; improve the metabolic capabilities of skin cell sebum; can it is effectively soft and moist, conditioning, protection skin; make skin naturally pure white; tender, wrinkle is reduced and high resilience, plays a part of delay skin aging.

Description

A kind of the effect of juice containing bear gall property topical composition

Technical field

A kind of the effect of present invention is juice containing bear gall property topical composition, belongs to cosmetic technical field.

Background technology

Human skin aging is the skin senescence phenomenon as caused by natural cause or non-natural factor.Skin group after people's birth Knit increasingly flourishing, function is gradually active, will start to degenerate when reaching certain age, this degeneration often in people unconsciously In slowly carry out.The growth stage of skin histology typically ends at 25 years old or so, is carried out simultaneously with aging from hereafter growth, skin bullet Power fiber is gradually thicker, and 25-28 the beginning of the year old phase, the aging of skin is slowly obvious, although degree of aging can vary with each individual.

The infringements such as certain skin senescence is the intrinsic physiological mechanism of human senility and the external world exposes to the weather, environmental pollution are common The result of effect, but can suppress the presenility excessively of skin by supplementing nutrient in good time.Skin senescence is generally embodied in skin Elasticity, wrinkle of skin and roughness, moisten the several respects such as intensity.Simple use moisturizer skin care is for prevention in daily life Skin senescence is clearly inadequate.

Bear gall is commonly used by people for treatment disease of being used as medicine for a long time as a kind of traditional natural biological medicinal material.There is research Person through for many years further study show that, bear gall can also effectively improve skin, and in the case of long-term micro external application, right A variety of common skin uncomfortable diseases produce significant maintenance effect.Its mechanism is that bear gall has the work for emulsifying and degrading human sebaceous With again the sebum fragment of degraded can be absorbed by human body skin to be recycled, and it absorbs and rebuilding course causes skin accessory organ's Stress reaction, promote subcutaneous blood microcirculation, strengthen the metabolism of sebum, strengthen the self-loopa nutrition of human body skin sebum, So as to adjust the physiological function of skin.

The content of the invention

In view of the deficienciess of the prior art, it is an object of the present invention to provide property topical compositions the effect of a kind of juice containing bear gall Thing, to solve the problems mentioned in the above background technology.

To achieve these goals, the present invention is to realize by the following technical solutions：A kind of the effect of juice containing bear gall Property topical composition, is made up of following raw material：It is rose, sanchi flower, biological carbohydrate gum -1, rose rhodobryum herb, glycerine, Jojoba wax, red Red-spotted stonecrop, testis et penis canitis, mulberry fruit, octadecyl alcolol, Morinda officinalis, lanolin, bear gall juice, niacinamide, Scleroglucan.

Further, epoxychloropropane hydrolysis, the glycerine for the sodium chloride-containing that generation glycerol content is 5-20% are carried out in solution The aqueous solution, concentrated, desalination, distillation, obtain the glycerine in raw material.

Further, take high 15-18 centimetres, root is sturdy, and cone, root neck has most fibrous roots, and rhizome is short, thick shape, circle The dry root and rhizome of the rhodiola root of cylindricality, excavated after autumn scape is withered, remove tertia, cleaned, dry, carried with water extraction method Take, obtain the rhodiola root in raw material.

Further, add alchlor with the wool washing sewage of wool, obtain lanolated mud slurry, suck moisture, obtain rotten Mud, mud 600kg is taken, add benzene 480kg, stirring while adding, 56 DEG C of insulation 1h of heating, stopping is stirred, and precipitates 1h, benzene liquid after clarification Lanolin 6%-40% is dissolved, is moved into destilling tower, heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, obtains sheep to containing lanolin Hair fat crude product, takes lanolin crude product 2100kg to put into reaction pot, is heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added In lanolin crude product, 45min is stirred, precipitates half an hour, benzene lipid layer adds light ethanol, adds water, 60 DEG C of heating and thermal insulation, it is small to stir half When, half an hour is precipitated, acid treatment benzene fat is obtained, takes acid treatment benzene fat to add ethanol 180kg, be gradually added 300g/L sodium hydroxide solutions About 70kg, pH9 is adjusted, adds water 180kg, be incubated 60 DEG C, be continuously agitated from being added ethanol, be further continued for stirring to adding water to finish 10min, stand, precipitate 1h, benzene lipid layer adds light ethanol, stirs, and precipitates 1h, must neutralize benzene fat, takes and neutralizes benzene fat, adds 3.8% peroxide Change hydrogen 24kg, stirring, be incubated 60 DEG C, precipitate 35min, keep pH8-9, add light ethanol, precipitate 2h, obtain commercial benzene fat, to refined Benzene fat is distilled, and 110 DEG C of liquid temperature is evaporated in vacuo untill not distilling, and is cooled to 60 DEG C, is added ethanol, is stirred, and precipitates 1h, separation Go out lower floor's lanolin, add ethanol, heating stirring 10min discards ethanol, and decompression is steamed ethanol to the greatest extent, the filtering of spun silk cloth, obtained in raw material Lanolin.

Further, nicotinic acid, boric acid and ammoniacal liquor are put into reaction pot, ammonia is passed through under stirring, rising temperature for dissolving, is then distilled Reclaim ammonia, to 120 °C after move into dewatering pan and continue to concentrate, when temperature is up to being initially added into liquefied ammonia after 145 DEG C, and 185~190 Continue logical ammonia at DEG C and react 20~30h, be then cooled to 130 DEG C, add distilled water diluting, add activated carbon, and under 70-80 °C Logical ammonia decolouring 2h, is filtered, filtrate cold analysis 24h in water, fractional crystallization while hot after reaction, and is washed with ethanol, dry raw material In niacinamide.

Beneficial effects of the present invention：The present invention one kind juice containing bear gall the effect of property topical composition, by cosmetics Add appropriate bear gall juice in matrix, promote subcutaneous blood circulation, improve the metabolic capabilities of skin cell sebum, can be with Effective soft and moist, conditioning, protection skin, make skin naturally pure white, and tender, wrinkle is reduced and high resilience, is played and is prolonged The effect of slow skin senescence.

Embodiment

To be easy to understand the technical means, the inventive features, the objects and the advantages of the present invention, with reference to Embodiment, the present invention is expanded on further.

The present invention provides a kind of technical scheme：A kind of the effect of juice containing bear gall property topical composition, be made up of following raw material： Rose, sanchi flower, biological carbohydrate gum -1, rose rhodobryum herb, glycerine, Jojoba wax, rhodiola root, testis et penis canitis, mulberry fruit, octadecyl alcolol, Morinda offcinalis How My god, lanolin, bear gall juice, niacinamide, Scleroglucan.

Epoxychloropropane hydrolysis, the glycerine water solution for the sodium chloride-containing that generation glycerol content is 5-20%, warp are carried out in solution Concentration, desalination, distillation, obtain the glycerine in raw material.

Take high 15-18 centimetres, root is sturdy, and cone, root neck has most fibrous roots, and rhizome is short, thick shape, cylindrical red scape It dry root and rhizome, excavated after autumn scape is withered, remove tertia, cleaned, dry, extracted with water extraction method, obtained former Rhodiola root in material.

Add alchlor with the wool washing sewage of wool, obtain lanolated mud slurry, suck moisture, obtain mud, take mud 600kg, add benzene 480kg, stirring while adding, 56 DEG C of insulation 1h of heating, stopping is stirred, and precipitates 1h, benzene liquid dissolving wool after clarification Fat 6%-40%, move into destilling tower, heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, it is thick to obtain lanolin to containing lanolin Product, take lanolin crude product 2100kg to put into reaction pot, be heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added into lanolin In crude product, 45min is stirred, precipitates half an hour, benzene lipid layer adds light ethanol, adds water, 60 DEG C of heating and thermal insulation, stirs half an hour, precipitation Half an hour, acid treatment benzene fat is obtained, takes acid treatment benzene fat to add ethanol 180kg, be gradually added 300g/L sodium hydroxide solutions about 70kg, PH9 is adjusted, adds water 180kg, is incubated 60 DEG C, is continuously agitated from being added ethanol, is further continued for stirring 10min, stands to adding water to finish, 1h is precipitated, benzene lipid layer adds light ethanol, stirs, and precipitates 1h, must neutralize benzene fat, takes and neutralizes benzene fat, adds 3.8% hydrogen peroxide 24kg, stir Mix, be incubated 60 DEG C, precipitate 35min, keep pH8-9, add light ethanol, precipitate 2h, obtain commercial benzene fat, commercial benzene fat is steamed Evaporate, 110 DEG C of liquid temperature is evaporated in vacuo untill not distilling, and is cooled to 60 DEG C, is added ethanol, is stirred, and is precipitated 1h, is isolated lower floor's wool Fat, add ethanol, heating stirring 10min discards ethanol, and decompression steams ethanol to the greatest extent, the filtering of spun silk cloth, obtains the lanolin in raw material.

Nicotinic acid, boric acid and ammoniacal liquor are put into reaction pot, ammonia is passed through under stirring, rising temperature for dissolving, is then distilled to recover ammonia, extremely Moved into after 120 °C in dewatering pan and continue to concentrate, when temperature is up to being initially added into liquefied ammonia after 145 DEG C, and continued at 185~190 DEG C Logical ammonia reacts 20~30h, is then cooled to 130 DEG C, adds distilled water diluting, adds activated carbon, and leads to ammonia under 70-80 °C and decolourize 2h, filter, filtrate cold analysis 24h in water, fractional crystallization, and washed with ethanol, the nicotinoyl in dry raw material while hot after reaction Amine.

As one embodiment of the present of invention：The present invention one kind juice containing bear gall the effect of property topical composition, by Appropriate bear gall juice is added in cosmetic base, promotes subcutaneous blood circulation, improves the metabolic energy of skin cell sebum Power, can it is effectively soft and moist, conditioning, protection skin, make skin naturally pure white, it is tender, wrinkle reduce and high resilience, Play a part of delay skin aging.

The general principle and principal character and advantages of the present invention of the present invention has been shown and described above, for this area skill For art personnel, it is clear that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing substantially from the present invention spirit or In the case of essential characteristic, the present invention can be realized in other specific forms.Which point therefore, no matter from the point of view of, all should incite somebody to action Embodiment regards exemplary as, and be it is nonrestrictive, the scope of the present invention by appended claims rather than on state Bright restriction, it is intended that all changes fallen in the implication and scope of the equivalency of claim are included in the present invention It is interior.

Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims (5)

1. A kind of 1. the effect of juice containing bear gall property topical composition, it is characterised in that：It is made up of following raw material：Rose, sanchi flower, Biological carbohydrate gum -1, rose rhodobryum herb, glycerine, Jojoba wax, rhodiola root, testis et penis canitis, mulberry fruit, octadecyl alcolol, Morinda officinalis, lanolin, bear gall Juice, niacinamide, Scleroglucan.
2. 2. the effect of one kind juice containing bear gall according to claim 1 property topical composition, it is characterised in that：Carried out in solution Epoxychloropropane hydrolyzes, and the glycerine water solution for the sodium chloride-containing that generation glycerol content is 5-20%, concentrated, desalination, distillation, obtains Glycerine in raw material.
3. 3. the effect of one kind juice containing bear gall according to claim 1 property topical composition, it is characterised in that：Take high 15-18 Centimetre, root is sturdy, and cone, root neck has most fibrous roots, and rhizome is short, thick shape, the dry root and rhizome of cylindrical rhodiola root, Excavated after autumn scape is withered, remove tertia, cleaned, dry, extracted with water extraction method, obtain the rhodiola root in raw material.
4. 4. the effect of one kind juice containing bear gall according to claim 1 property topical composition, it is characterised in that：With washing for wool Hair sewage adds alchlor, obtains lanolated mud slurry, sucks moisture, obtain mud, take mud 600kg, add benzene 480kg, side Edged stirs, and heats 56 DEG C of insulation 1h, stops stirring, precipitate 1h, benzene liquid dissolves lanolin 6%-40% after clarification, moves into destilling tower Interior, heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, obtains lanolin crude product, take lanolin crude product 2100kg to containing lanolin Reaction pot is put into, is heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added in lanolin crude product, stirs 45min, precipitation Half an hour, benzene lipid layer add light ethanol, add water, 60 DEG C of heating and thermal insulation, stir half an hour, precipitate half an hour, obtain acid treatment benzene fat, take Acid treatment benzene fat adds ethanol 180kg, is gradually added 300g/L sodium hydroxide solutions about 70kg, adjusts pH9, adds water 180kg, insulation 60 DEG C, it is continuously agitated from being added ethanol to adding water to finish, is further continued for stirring 10min, stands, precipitate 1h, benzene lipid layer adds light ethanol, Stirring, 1h is precipitated, benzene fat must be neutralized, taken and neutralize benzene fat, add 3.8% hydrogen peroxide 24kg, stirred, be incubated 60 DEG C, precipitate 35min, PH8-9 is kept, adds light ethanol, 2h is precipitated, obtains commercial benzene fat, commercial benzene fat is distilled, 110 DEG C of liquid temperature is evaporated in vacuo to steaming Untill not going out, 60 DEG C are cooled to, adds ethanol, is stirred, 1h is precipitated, isolates lower floor's lanolin, add ethanol, heating stirring 10min, Ethanol is discarded, decompression steams ethanol to the greatest extent, the filtering of spun silk cloth, obtains the lanolin in raw material.
5. 5. the effect of one kind juice containing bear gall according to claim 1 property topical composition, it is characterised in that：By nicotinic acid, boron Acid and ammoniacal liquor input reaction pot, ammonia is passed through under stirring, rising temperature for dissolving, is then distilled to recover ammonia, to 120 °C after move into dewatering pan Inside continue to concentrate, when temperature is up to being initially added into liquefied ammonia after 145 DEG C, and continues logical ammonia at 185~190 DEG C and react 20~30h, so After be cooled to 130 DEG C, add distilled water diluting, add activated carbon, and lead to ammonia decolouring 2h under 70-80 °C, filtered while hot after reaction, Filtrate cold analysis 24h in water, fractional crystallization, and washed with ethanol, the niacinamide in dry raw material.