CN107829320A - A kind of dye penetrant and preparation method thereof - Google Patents

A kind of dye penetrant and preparation method thereof Download PDF

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Publication number
CN107829320A
CN107829320A CN201710983539.7A CN201710983539A CN107829320A CN 107829320 A CN107829320 A CN 107829320A CN 201710983539 A CN201710983539 A CN 201710983539A CN 107829320 A CN107829320 A CN 107829320A
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CN
China
Prior art keywords
parts
dye penetrant
dimethicone
deionized water
ammonium chloride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710983539.7A
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Chinese (zh)
Inventor
储平
徐有琦
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Jiangsu New Lucky Polytron Technologies Inc
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Jiangsu New Lucky Polytron Technologies Inc
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Priority to CN201710983539.7A priority Critical patent/CN107829320A/en
Publication of CN107829320A publication Critical patent/CN107829320A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/623Aliphatic, aralophatic or cycloaliphatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/5214Polymers of unsaturated compounds containing no COOH groups or functional derivatives thereof
    • D06P1/5228Polyalkenyl alcohols, e.g. PVA
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5264Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds
    • D06P1/5292Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds containing Si-atoms
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642Compounds containing nitrogen
    • D06P1/645Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/653Nitrogen-free carboxylic acids or their salts
    • D06P1/6533Aliphatic, araliphatic or cycloaliphatic

Abstract

The invention discloses a kind of dye penetrant and preparation method thereof, the dye penetrant is made up of the raw material of following parts by weight:10 20 parts of SAS, 35 parts of turkey red oil, 10 15 parts of dioctyl sodium sulfosuccinate, 57 parts of polyvinyl alcohol, 57 parts of dimethyl diallyl ammonium chloride, 35 parts of sodium citrate, 37 parts of lauroylamidopropyl betaine, 35 parts of dimethicone, 30 40 parts of deionized water.The dye penetrant homogenized diet of the present invention is excellent, can substantially increase the absorptivity of dyestuff.The dye penetrant manufacturing process of the present invention is simple to operation, and low in raw material price is easily obtained, and nontoxic, and human body is not stimulated, and volatility is low, and penetration is strong, conflicts with other auxiliary agents while using not producing.

Description

A kind of dye penetrant and preparation method thereof
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of dye penetrant and preparation method thereof.
Background technology
Bleeding agent has been as its name suggests osmosis, and with fixed hydrophilic lipophilic group, in the surface energy of solution Align, and the material that can be remarkably decreased surface tension.
In dyeing and finishing process, in order that the material such as dyestuff is quickly penetrated into fabric and gone, it is necessary to add bleeding agent. It is poor with other auxiliary agent interworking effects but existing dye penetrant fastness to alkali is not high, capillary effect is poor, white powder point is had during high-temperature boiling Produce, so as to influence using effect.Some dye penetrants also contain APEO, not easily biological-degradable, are unfavorable for environmental protection.
The content of the invention
It is an object of the invention to provide a kind of dye penetrant and preparation method thereof, to solve to carry in above-mentioned background technology The problem of going out.
To achieve the above object, the present invention provides following technical scheme:
A kind of dye penetrant, according to important number, including following components:SAS 10-20 parts, turkey red oil 3- 5 parts, dioctyl sodium sulfosuccinate 10-15 parts, polyvinyl alcohol 5-7 parts, dimethyl diallyl ammonium chloride 5-7 parts, citric acid Sodium 3-5 parts, lauroylamidopropyl betaine 3-7 parts, dimethicone 3-5 parts, deionized water 30-40 parts.
Preferably, described dye penetrant, according to parts by weight, including following components:10 parts of SAS, too Ancient 3 parts of oil, 10 parts of dioctyl sodium sulfosuccinate, 5 parts of polyvinyl alcohol, 5 parts of dimethyl diallyl ammonium chloride, sodium citrate 3 Part, 3 parts of lauroylamidopropyl betaine, 3 parts of dimethicone, 30 parts of deionized water.
Preferably, described dye penetrant, according to parts by weight, including following components:15 parts of SAS, too Ancient 4 parts of oil, 13 parts of dioctyl sodium sulfosuccinate, 6 parts of polyvinyl alcohol, 6 parts of dimethyl diallyl ammonium chloride, sodium citrate 4 Part, 5 parts of lauroylamidopropyl betaine, 4 parts of dimethicone, 35 parts of deionized water.
Preferably, described dye penetrant, according to parts by weight, including following components:20 parts of SAS, too Ancient 5 parts of oil, 15 parts of dioctyl sodium sulfosuccinate, 7 parts of polyvinyl alcohol, 7 parts of dimethyl diallyl ammonium chloride, sodium citrate 5 Part, 7 parts of lauroylamidopropyl betaine, 5 parts of dimethicone, 40 parts of deionized water.
A kind of preparation method of dye penetrant, is comprised the following steps that:
Step 1, deionized water 30-40 parts are added in a kettle, and rise temperature is to 50-60 DEG C;
Step 2, add SAS 10-20 parts, turkey red oil 3-5 parts, dioctyl sodium sulfosuccinate 10-15 parts, Polyvinyl alcohol 5-7 parts, 500-1000 revs/min, stir 10-20 minutes;
Step 3,30-40 DEG C is cooled to, adds dimethyl diallyl ammonium chloride 5-7 parts, lauroylamidopropyl betaine 3-7 parts, 500-1000 revs/min, stir 20-30 minutes;
Step 4, it is cooled to 20-30 DEG C, adds sodium citrate 3-5 parts, dimethicone 3-5 parts, 500-1000 revs/min Clock, stir 20-30 minutes;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, dye penetrant manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic, Volatility is low, and human body is not stimulated.
2nd, dye penetrant homogenized diet of the invention is excellent, can substantially increase the absorptivity of dyestuff.
3rd, mutual compatibility, synergy between various raw materials used in dye penetrant of the invention, it is excellent to collectively constitute performance Different product.
4th, dye penetrant of the invention does not produce poisonous gas or solid matter in application process.
5th, dye penetrant penetration of the invention is strong, conflicts with other auxiliary agents while using not producing.
6th, technique is simplified, safe operation is simple, is easy to industrialized production.
7th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of dye penetrant, according to important number, including following components:SAS 10- 20 parts, turkey red oil 3-5 parts, dioctyl sodium sulfosuccinate 10-15 parts, polyvinyl alcohol 5-7 parts, dimethyl diallyl ammonium chloride 5-7 parts, sodium citrate 3-5 parts, lauroylamidopropyl betaine 3-7 parts, dimethicone 3-5 parts, deionized water 30-40 parts.
Present invention also offers a kind of preparation method of dye penetrant, comprise the following steps that:
Step 1, deionized water 30-40 parts are added in a kettle, and rise temperature is to 50-60 DEG C;
Step 2, add SAS 10-20 parts, turkey red oil 3-5 parts, dioctyl sodium sulfosuccinate 10-15 parts, Polyvinyl alcohol 5-7 parts, 500-1000 revs/min, stir 10-20 minutes;
Step 3,30-40 DEG C is cooled to, adds dimethyl diallyl ammonium chloride 5-7 parts, lauroylamidopropyl betaine 3-7 parts, 500-1000 revs/min, stir 20-30 minutes;
Step 4, it is cooled to 20-30 DEG C, adds sodium citrate 3-5 parts, dimethicone 3-5 parts, 500-1000 revs/min Clock, stir 20-30 minutes;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of dye penetrant, according to important number, including following components:SAS 10 Part, 3 parts of turkey red oil, 10 parts of dioctyl sodium sulfosuccinate, 5 parts of polyvinyl alcohol, 5 parts of dimethyl diallyl ammonium chloride, lemon Sour 3 parts of sodium, 3 parts of lauroylamidopropyl betaine, 3 parts of dimethicone, 30 parts of deionized water.
Present invention also offers a kind of preparation method of dye penetrant, comprise the following steps that:
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 50 DEG C;
Step 2,10 parts of SAS, 3 parts of turkey red oil, 10 parts of dioctyl sodium sulfosuccinate, polyvinyl alcohol 5 are added Part, 500 revs/min, stir 20 minutes;
Step 3,30 DEG C are cooled to, adds 5 parts of dimethyl diallyl ammonium chloride, 3 parts of lauroylamidopropyl betaine, 500 revs/min, stir 20 minutes;
Step 4,20 DEG C are cooled to, 3 parts of sodium citrate, 3 parts of dimethicone is added, 500 revs/min, stirs 20 minutes;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of dye penetrant, according to important number, including following components:SAS 15 Part, 4 parts of turkey red oil, 13 parts of dioctyl sodium sulfosuccinate, 6 parts of polyvinyl alcohol, 6 parts of dimethyl diallyl ammonium chloride, lemon Sour 4 parts of sodium, 5 parts of lauroylamidopropyl betaine, 4 parts of dimethicone, 35 parts of deionized water.
Present invention also offers a kind of preparation method of dye penetrant, comprise the following steps that:
Step 1,35 parts of deionized water is added in a kettle, and rise temperature is to 55 DEG C;
Step 2,15 parts of SAS, 4 parts of turkey red oil, 13 parts of dioctyl sodium sulfosuccinate, polyvinyl alcohol 6 are added Part, 900 revs/min, stir 15 minutes;
Step 3,35 DEG C are cooled to, adds 6 parts of dimethyl diallyl ammonium chloride, 5 parts of lauroylamidopropyl betaine, 900 revs/min, stir 25 minutes;
Step 4,25 DEG C are cooled to, 4 parts of sodium citrate, 4 parts of dimethicone is added, 900 revs/min, stirs 25 minutes;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of dye penetrant, according to important number, including following components:SAS 20 Part, 5 parts of turkey red oil, 15 parts of dioctyl sodium sulfosuccinate, 7 parts of polyvinyl alcohol, 7 parts of dimethyl diallyl ammonium chloride, lemon Sour 5 parts of sodium, 7 parts of lauroylamidopropyl betaine, 5 parts of dimethicone, 40 parts of deionized water.
Present invention also offers a kind of preparation method of dye penetrant, comprise the following steps that:
Step 1,40 parts of deionized water is added in a kettle, and rise temperature is to 60 DEG C;
Step 2,20 parts of SAS, 5 parts of turkey red oil, 15 parts of dioctyl sodium sulfosuccinate, polyvinyl alcohol 7 are added Part, 1000 revs/min, stir 10 minutes;
Step 3,40 DEG C are cooled to, adds 7 parts of dimethyl diallyl ammonium chloride, 7 parts of lauroylamidopropyl betaine, 1000 revs/min, stir 30 minutes;
Step 4,30 DEG C are cooled to, 5 parts of sodium citrate, 5 parts of dimethicone is added, 1000 revs/min, stirs 30 points Clock;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of dye penetrant, according to important number, including following components:SAS 20 Part, 4 parts of turkey red oil, 15 parts of dioctyl sodium sulfosuccinate, 7 parts of polyvinyl alcohol, 7 parts of dimethyl diallyl ammonium chloride, lemon Sour 3 parts of sodium, 5 parts of lauroylamidopropyl betaine, 4 parts of dimethicone, 30 parts of deionized water.
Present invention also offers a kind of preparation method of dye penetrant, comprise the following steps that:
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 60 DEG C;
Step 2,20 parts of SAS, 4 parts of turkey red oil, 15 parts of dioctyl sodium sulfosuccinate, polyvinyl alcohol 7 are added Part, 1000 revs/min, stir 10 minutes;
Step 3,30 DEG C are cooled to, adds 7 parts of dimethyl diallyl ammonium chloride, 5 parts of lauroylamidopropyl betaine, 900 revs/min, stir 20 minutes;
Step 4,20 DEG C are cooled to, 3 parts of sodium citrate, 4 parts of dimethicone is added, 1000 revs/min, stirs 20 points Clock;
Step 5, stirring is closed down, the liquid dye penetrant prepared;
Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
The bleeding agent of embodiment 1,2,3,4 is carried out to alkali resistance (naoh concentration 50g/L), sedimentation time survey Examination, test result are as follows:
Embodiment Alkali resistance Sedimentation time (s) Dye-uptake (%)
1 Compared with clarification, foam has a bit 13.5 95
2 Clarification, foam are few 10.2 97
3 Clarification, basic non-foam 7.5 99
4 Clarification, foam are few 8.7 98
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (5)

  1. A kind of 1. dye penetrant, it is characterised in that:The dye penetrant includes the raw material of following parts by weight:Secondary alkyl sulphur Sour sodium 10-20 parts, turkey red oil 3-5 parts, dioctyl sodium sulfosuccinate 10-15 parts, polyvinyl alcohol 5-7 parts, the allyl of dimethyl two Ammonium chloride 5-7 parts, sodium citrate 3-5 parts, lauroylamidopropyl betaine 3-7 parts, dimethicone 3-5 parts, deionized water 30-40 parts.
  2. A kind of 2. dye penetrant according to claim 1, it is characterised in that:According to parts by weight, including following components: 10 parts of SAS, 3 parts of turkey red oil, 10 parts of dioctyl sodium sulfosuccinate, 5 parts of polyvinyl alcohol, dimethyl diallyl 5 parts of ammonium chloride, 3 parts of sodium citrate, 3 parts of lauroylamidopropyl betaine, 3 parts of dimethicone, 30 parts of deionized water.
  3. A kind of 3. dye penetrant according to claim 1, it is characterised in that:According to parts by weight, including following components: 15 parts of SAS, 4 parts of turkey red oil, 13 parts of dioctyl sodium sulfosuccinate, 6 parts of polyvinyl alcohol, dimethyl diallyl 6 parts of ammonium chloride, 4 parts of sodium citrate, 5 parts of lauroylamidopropyl betaine, 4 parts of dimethicone, 35 parts of deionized water.
  4. A kind of 4. dye penetrant according to claim 1, it is characterised in that:According to parts by weight, including following components: 20 parts of SAS, 5 parts of turkey red oil, 15 parts of dioctyl sodium sulfosuccinate, 7 parts of polyvinyl alcohol, dimethyl diallyl 7 parts of ammonium chloride, 5 parts of sodium citrate, 7 parts of lauroylamidopropyl betaine, 5 parts of dimethicone, 40 parts of deionized water.
  5. A kind of a kind of 5. preparation method of any described dye penetrant in 1-4 using the claims, it is characterised in that: Comprise the following steps that:
    Step 1, deionized water 30-40 parts are added in a kettle, and rise temperature is to 50-60 DEG C;
    Step 2, SAS 10-20 parts, turkey red oil 3-5 parts, dioctyl sodium sulfosuccinate 10-15 parts, poly- second are added Enol 5-7 parts, 500-1000 revs/min, stir 10-20 minutes;
    Step 3,30-40 DEG C is cooled to, adds dimethyl diallyl ammonium chloride 5-7 parts, lauroylamidopropyl betaine 3-7 Part, 500-1000 revs/min, stir 20-30 minutes;
    Step 4,20-30 DEG C is cooled to, sodium citrate 3-5 parts, dimethicone 3-5 parts is added, 500-1000 revs/min, stirs Mix 20-30 minutes;
    Step 5, stirring is closed down, the liquid dye penetrant prepared;
    Step 6, stand and be cooled in stirred tank liquid dye penetrant and be less than 20 DEG C, blowing encapsulation, finished product.
CN201710983539.7A 2017-10-20 2017-10-20 A kind of dye penetrant and preparation method thereof Pending CN107829320A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201710983539.7A CN107829320A (en) 2017-10-20 2017-10-20 A kind of dye penetrant and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107829320A true CN107829320A (en) 2018-03-23

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111809413A (en) * 2020-07-27 2020-10-23 湖州市千金金耀制丝有限公司 Chromatic aberration-free short-process reactive dye dyeing method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103725041A (en) * 2013-12-31 2014-04-16 浙江亿得化工有限公司 Acid dye and gravure ink as well as preparation method and application of gravure ink
CN105002755A (en) * 2015-07-01 2015-10-28 广东灵捷制造化工有限公司 Rapid alkali-resistant penetrating agent, and preparation method thereof
CN106087483A (en) * 2016-07-27 2016-11-09 刘慧宝 A kind of novel environment friendly low bubble dye penetrant
CN106245376A (en) * 2016-07-27 2016-12-21 刘慧宝 A kind of alkaline-resisting dye penetrant of novel environment friendly

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103725041A (en) * 2013-12-31 2014-04-16 浙江亿得化工有限公司 Acid dye and gravure ink as well as preparation method and application of gravure ink
CN105002755A (en) * 2015-07-01 2015-10-28 广东灵捷制造化工有限公司 Rapid alkali-resistant penetrating agent, and preparation method thereof
CN106087483A (en) * 2016-07-27 2016-11-09 刘慧宝 A kind of novel environment friendly low bubble dye penetrant
CN106245376A (en) * 2016-07-27 2016-12-21 刘慧宝 A kind of alkaline-resisting dye penetrant of novel environment friendly

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111809413A (en) * 2020-07-27 2020-10-23 湖州市千金金耀制丝有限公司 Chromatic aberration-free short-process reactive dye dyeing method

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Application publication date: 20180323