CN107828534A - A kind of efficient resist printing detergent for garment wash and preparation method thereof - Google Patents

A kind of efficient resist printing detergent for garment wash and preparation method thereof Download PDF

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Publication number
CN107828534A
CN107828534A CN201711125849.1A CN201711125849A CN107828534A CN 107828534 A CN107828534 A CN 107828534A CN 201711125849 A CN201711125849 A CN 201711125849A CN 107828534 A CN107828534 A CN 107828534A
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CN
China
Prior art keywords
resist printing
garment wash
stirred
efficient
minutes
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711125849.1A
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Chinese (zh)
Inventor
章数龙
姚宾燕
陈妃状
李钢
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GUANGZHOU APRO INDUSTRIAL Co Ltd
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GUANGZHOU APRO INDUSTRIAL Co Ltd
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Priority to CN201711125849.1A priority Critical patent/CN107828534A/en
Publication of CN107828534A publication Critical patent/CN107828534A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/83—Mixtures of non-ionic with anionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0021—Dye-stain or dye-transfer inhibiting compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2079—Monocarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/30—Amines; Substituted amines ; Quaternized amines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776—Heterocyclic compounds, e.g. lactam
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/008—Polymeric surface-active agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols

Abstract

The invention discloses a kind of efficient resist printing detergent for garment wash and preparation method thereof,It is made up of by mass percentage following components,Polyvinylpyrrolidone 5~15%,Horse propylene copolymer 10~40%,AEO 10~20%,SAS 5~15%,Linear alkyl benzene sulfonic acid 5~8%,Preservative 0.05~0.1%,Deionized water 1.9%~64.95%,The present invention uses polyvinylpyrrolidone,Horse propylene copolymer,AEO (paregal O) etc. is used as raw material,Each composition plays self-acting,And synergy is played between each other,With good resist printing effect,Prevent different fibrous materials during garment wash,Mutual staining before different colours clothing,Phenomena such as colour contamination,Improve the quality and value of product,The raw material of the present invention belongs to environment-friendly products,It is nontoxic,It is non-stimulated,Environmental protection,It is pollution-free.

Description

A kind of efficient resist printing detergent for garment wash and preparation method thereof
Technical field
The present invention relates to technical field of textile auxiliary agent, and in particular to a kind of efficient resist printing detergent for garment wash and Its preparation method.
Background technology
Clothing slopwork washing process, a kind of more special technique in habilimentation.Due to wash water effect increasingly It is welcomed by the people, so being widely used in various ready-made clothes, especially there are some new washing methods, even more in daily life Brilliance is added in work.Various textile garment fabrics, cotton, silk, hair, chemical fibre and its blending material；Tatting, knitting etc. Various colors are alternate；Jeans it is prevailing；Imitate old clothes prevalence ... etc. these promote the height of garment wash industry Speed development, simultaneously because complicated multiple material, more colors, the matched combined of bright color clothes, past during garment wash Toward meeting because material is different, color is different and the phenomenon of mutual staining occurs, deleterious effect is brought to the whole structure of ready-made clothes.
The content of the invention
It is an object of the invention to overcome above mentioned problem and provide a kind of efficient resist printing detergent for garment wash and Its preparation method, prevent ready-made clothes occur during industrial wash water mutual staining, colour contamination phenomena such as, improve ready-made clothes quality, valency Value.
To achieve the above object, the present invention adopts the technical scheme that a kind of efficient resist printing washing for garment wash Agent, it is made up of by mass percentage following components：Polyvinylpyrrolidone 5~15%, horse-propylene copolymer 10~40%, fat Alcohol APEO 10~20%, SAS 5~15%, linear alkyl benzene sulfonic acid 5~8%, preservative 0.05~ 0.1%th, surplus is deionized water.
Preferably, the horse-propylene copolymer is to use the polymerizate of maleic acid and acrylic anhydride in the presence of a catalyst.
Preferably, the AEO is C12-C18, ethylene oxide number n=20-35.
Preferably, the linear alkyl benzene acid that the linear alkyl benzene sulfonic acid is C6-C16 is one or more of.
Preferably, the preservative is the one or more in C6-C16 zephirans, sodium benzoate.
Preferably, described deionized water uses hyperfiltration, is gone using ion exchange resin, filter membrane etc. in water removal Obtained by ion thing, impurity.
A kind of preparation method of efficient resist printing detergent for garment wash, specific preparation process are：
Step 1：Horse-the propylene copolymer, SAS, linear alkyl benzene sulfonic acid, deionized water are blended in one Rise, stir 20~30 minutes；
Step 2：The polyvinylpyrrolidone is slowly added into the mixture for entering above-mentioned steps 1, added while stirring, entirely Portion is stirred for 20~30 minutes after adding；
Step 3：Add the AEO slowly to add into the mixture for entering above-mentioned steps 2, while stirring Add, be stirred for after all adding 10 minutes；
Step 4：The preservative is added, is stirred 10 minutes；
Step 5：The mixture being stirred is stood 24 hours, dispensed.
Beneficial effects of the present invention：
1st, present invention invention prepares a kind of efficient resist printing detergent for garment wash, prevents during garment wash not Phenomena such as mutual staining before same fibrous material, different colours clothing, colour contamination, improve the quality and value of product.
2nd, the raw material that the present invention uses is environment-friendly products, meets International Environmental Protection weaving association (Oeko-Tex Associationa the testing standards of textile Oeko-Tex Standard 100 and the world, the related textile of the country) worked out Environmental protection standard, belong to environment-friendly products, it is nontoxic, non-stimulated, environmentally friendly, pollution-free,.
3rd, the present invention is made using polyvinylpyrrolidone, horse-propylene copolymer, AEO (paregal O) etc. For raw material, each composition plays self-acting, and plays synergy between each other, has good resist printing effect.
Embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention It is described further.
Embodiment 1
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone 5%, horse-propylene copolymer 40%, peregal O-25 10%, SAS 7%, C12 linear alkyl benzene Acid 8%, sodium benzoate 0.1%, deionized water 29.9%.
The preparation method of the efficient resist printing detergent, specific preparation process are：
Step 1：Calculated by above-mentioned mass percent, weigh each component；
Step 2：Horse-propylene copolymer in component, SAS, linear alkyl benzene sulfonic acid, deionized water are mixed Together, stir 20 minutes；
Step 3：By in component polyvinylpyrrolidone slowly plus toward enter it is above-mentioned lack rapid 2 mixture in, while stirring Add, be stirred for after all adding 20 minutes.
Step 4：Add component in AEO slowly plus toward enter it is above-mentioned lack rapid 3 mixture in, while stirring Mix side to add, be stirred for after all adding 10 minutes.
Step 5：The preservative added in component, stir 10 minutes.
The polyvinylpyrrolidone of the present invention is a kind of non-ionic macromolecule compound, and horse-propylene copolymer is to use Malaysia Acid and the polymerizate of acrylic anhydride in the presence of a catalyst, SAS SAS60 are the washability having had, good Permeability.Deionized water uses hyperfiltration, ion thing, the impurity gone using ion exchange resin, filter membrane etc. in water removal Gained.
Embodiment 2
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone K30 10%, horse-propylene copolymer 30%, paregal O -30 13%, SAS 12%, C12 linear alkylbenzene (LAB)s Sulfonic acid 8%, sodium benzoate 0.1%, deionized water 36.9%.
The preparation method of the efficient resist printing detergent of the garment wash, specific preparation process are：
Step 1：Calculated by above-mentioned mass percent, weigh each component；
Step 2：Horse-propylene copolymer in component, SAS, linear alkyl benzene sulfonic acid, deionized water are mixed Together, stir 20 minutes；
Step 3：By in component polyvinylpyrrolidone slowly plus toward enter it is above-mentioned lack rapid 2 mixture in, while stirring Add, be stirred for after all adding 20 minutes.
Step 4：Add component in AEO slowly plus toward enter it is above-mentioned lack rapid 3 mixture in, while stirring Mix side to add, be stirred for after all adding 10 minutes.
Step 5：The preservative added in component, stir 10 minutes.
Step 6：The mixture being stirred is stood 24 hours, dispensed.
Embodiment 3
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone 8%, horse-propylene copolymer 20%, peregal O-25 12%, SAS 13%, C12 linear alkyl benzene Sulfonic acid 5%, C12 zephirans 0.1%, deionized water 41.9%.
This is used for the preparation method of the efficient resist printing detergent of garment wash, and specific preparation process is：
Step 1：Calculated by above-mentioned mass percent, weigh each component；
Step 2：Horse-propylene copolymer in component, SAS, linear alkyl benzene sulfonic acid, deionized water are mixed Together, stir 20 minutes；
Step 3：By in component polyvinylpyrrolidone slowly plus toward enter it is above-mentioned lack rapid 2 mixture in, while stirring Add, be stirred for after all adding 20 minutes.
Step 4：Add component in AEO slowly plus toward enter it is above-mentioned lack rapid 3 mixture in, while stirring Mix side to add, be stirred for after all adding 10 minutes.
Step 5：The preservative added in component, stir 10 minutes.
Step 6：The mixture being stirred is stood 24 hours, dispensed.
Embodiment 4
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone 12%, horse-propylene copolymer 25%, paregal O -20 15%, SAS 15%, C6 linear alkyl benzene Sulfonic acid 6%, C6 zephirans 0.06%, balance deionized water.Its preparation method is same as the previously described embodiments.
Embodiment 5
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone 14%, horse-propylene copolymer 15%, peregal O-25 16%, SAS 6%, C16 linear alkyl benzene Sulfonic acid 7%, C10 zephirans 0.06%, balance deionized water.Its preparation method and above-described embodiment phase Together.
Embodiment 6
A kind of efficient resist printing detergent for garment wash, it is made up of by mass percentage following components：Polyethylene pyrrole Pyrrolidone 15%, horse-propylene copolymer 5%, peregal O-25 20%, SAS 5%, C15 linear alkyl benzene Acid 8%, C16 zephirans 0.1%, balance deionized water.Its preparation method is same as the previously described embodiments.
Anti- dyeing effect experiment
Experimental method：1) A, B, C500mL beaker are taken, it is each to add 250mL running water；
2) toward addition 5g regular powders in A, stirred with glass bar, simulate laundry processes.；
3) toward addition 5g regular powders in B, any resist printing detergent 15mL of the present embodiment 1~6 is added, is stirred, mould Intend laundry processes.；
4) toward addition 5g regular powders in C, a piece of commercially available spring cube color masterbatch piece is added, is stirred with glass bar, mould Intend laundry processes.
5) there is color cloth toward being put into one piece of white pure cotton cloth and 2 pieces in A beakers, be also placed in, stir in same B, C so that Cloth enters in the aqueous solution completely, while timing；
6) aqueous solution is outwelled after about 3 to 5 minutes, takes out painting cloth, then toward addition 250mL running water in A, B, C beaker, stir Afterwards, white cotton A, B, C are removed, wrings out water.
7) A, B, C cloth are evened up, with the naked eye contrasts color.
Experimental result is as shown in table 1：
It can be seen that, efficient resist printing detergent of the invention that there is good resist printing effect, during can preventing garment wash Phenomena such as mutual staining before different fibrous materials, different colours clothing, colour contamination.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention God any modification, equivalent substitution and improvements done etc., should be included within the scope of protection of the invention with principle.

Claims (7)

1. a kind of efficient resist printing detergent for garment wash, it is characterised in that be made up of by mass percentage following components： Polyvinylpyrrolidone 5~15%, horse-propylene copolymer 10~40%, AEO 10~20%, secondary alkyl sulfonic acid Sodium 5~15%, linear alkyl benzene sulfonic acid 5~8%, preservative 0.05~0.1%, surplus are deionized water.
2. the efficient resist printing detergent according to claim 1 for garment wash, it is characterised in that the horse-the third is common Polymers is to use the polymerizate of maleic acid and acrylic anhydride in the presence of a catalyst.
3. the efficient resist printing detergent according to claim 1 for garment wash, it is characterised in that the poly alkyl alcohol Oxygen vinethene is C12-C18, ethylene oxide number n=20-35.
4. the efficient resist printing detergent according to claim 1 for garment wash, it is characterised in that the straight chained alkyl The linear alkyl benzene acid that benzene sulfonic acid is C6-C16 is one or more of.
5. the efficient resist printing detergent according to claim 1 for garment wash, it is characterised in that the preservative is One or more in C6-C16 zephirans, sodium benzoate.
6. the efficient resist printing detergent according to claim 1 for garment wash, it is characterised in that described deionization Water uses hyperfiltration, ion thing, the impurity gained gone using ion exchange resin, filter membrane etc. in water removal.
7. a kind of preparation method of efficient resist printing detergent for garment wash as described in any one of claim 1 to 6, its It is characterised by, specific preparation process is：
Step 1：Horse-the propylene copolymer, SAS, linear alkyl benzene sulfonic acid, deionized water are mixed, stirred Mix 20~30 minutes；
Step 2：The polyvinylpyrrolidone is slowly added into the mixture for entering above-mentioned steps 1, plus, all added while stirring It is stirred for after complete 20~30 minutes；
Step 3：Add the AEO slowly to add into the mixture for entering above-mentioned steps 2, add while stirring, entirely Portion is stirred for 10 minutes after adding；
Step 4：The preservative is added, is stirred 10 minutes；
Step 5：The mixture being stirred is stood 24 hours, dispensed.
CN201711125849.1A 2017-11-14 2017-11-14 A kind of efficient resist printing detergent for garment wash and preparation method thereof Pending CN107828534A (en)

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Application Number Priority Date Filing Date Title
CN201711125849.1A CN107828534A (en) 2017-11-14 2017-11-14 A kind of efficient resist printing detergent for garment wash and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110725144A (en) * 2019-10-14 2020-01-24 曹林 Preparation method of dye-resistant powder for ready-made clothes washing process
CN110964604A (en) * 2019-11-29 2020-04-07 南京市检捷生物信息科技有限公司 Anti-color-cross washing agent for clothes

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101130717A (en) * 2006-08-21 2008-02-27 上海德桑精细化工有限公司 Agent for cleaning dacron and blending dyeing material
CN101531956A (en) * 2009-04-27 2009-09-16 四川省纺织科学研究院 Environmental-friendly type foamless anti-staining detergent, preparing method and application thereof
CN102911805A (en) * 2012-10-25 2013-02-06 南京大地冷冻食品有限公司 Method for preparing novel efficient soaping agent for activated dyes
CN103923753A (en) * 2014-04-02 2014-07-16 湖州思祺服饰染整有限公司 Detergent and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101130717A (en) * 2006-08-21 2008-02-27 上海德桑精细化工有限公司 Agent for cleaning dacron and blending dyeing material
CN101531956A (en) * 2009-04-27 2009-09-16 四川省纺织科学研究院 Environmental-friendly type foamless anti-staining detergent, preparing method and application thereof
CN102911805A (en) * 2012-10-25 2013-02-06 南京大地冷冻食品有限公司 Method for preparing novel efficient soaping agent for activated dyes
CN103923753A (en) * 2014-04-02 2014-07-16 湖州思祺服饰染整有限公司 Detergent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110725144A (en) * 2019-10-14 2020-01-24 曹林 Preparation method of dye-resistant powder for ready-made clothes washing process
CN110964604A (en) * 2019-11-29 2020-04-07 南京市检捷生物信息科技有限公司 Anti-color-cross washing agent for clothes

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Application publication date: 20180323