CN107823263A - A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof - Google Patents

A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof Download PDF

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CN107823263A
CN107823263A CN201711295301.1A CN201711295301A CN107823263A CN 107823263 A CN107823263 A CN 107823263A CN 201711295301 A CN201711295301 A CN 201711295301A CN 107823263 A CN107823263 A CN 107823263A
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medicine composition
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谈发金
王志锋
柳卓
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KANGSHOU PHARMACY Co Ltd HUNAN
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/60Moraceae (Mulberry family), e.g. breadfruit or fig
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • A61K31/44Non condensed pyridines; Hydrogenated derivatives thereof
    • A61K31/4402Non condensed pyridines; Hydrogenated derivatives thereof only substituted in position 2, e.g. pheniramine, bisacodyl
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/39Complex extraction schemes, e.g. fractionation or repeated extraction steps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying

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  • Natural Medicines & Medicinal Plants (AREA)
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Abstract

The present invention relates to technical field of traditional Chinese medicine, more particularly to a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof, include the raw material and auxiliary material of following parts by weight:92 95 parts of Ficus microcarpa dried cream powder,0.2 0.4 parts of chlorphenamine maleate,25 parts of 3 parts of silica 1 and talcum powder,By the Ficus microcarpa through pre-treatment,Add water to cook secondary,For the first time plus 5 times of water is measured,Extract 1.5 2 hours,Second plus 5 times of amounts of water,Extract 0.5 1 hours,Collecting decoction,It is concentrated into the clear cream that relative density is 1.10~1.20 (80 DEG C),Let cool,Ethanol is added to alcohol content up to 60%,Stand more than 12 hours,Filtration,Filtrate recycling ethanol,It is concentrated into the thick paste that relative density is 1.30 (50 DEG C),Less than 80 DEG C dryings,It is ground into fine powder,Add chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder,Mix,Load capsule to produce,With antibechic,Eliminating the phlegm,Relieving asthma,Anti-inflammatory and other effects,It can be widely used for cough and asthma and chronic bronchitis;The preparation method is easy simultaneously, and formula is simple, therapeutic effect is good.

Description

A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof
Technical field
The present invention relates to technical field of traditional Chinese medicine, more particularly to a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and its preparation side Method.
Background technology
Motherland's medical science think it is more due to internal organs loss, deficiency of Yin Tianjin is few, it is strong in the fire of deficiency type cause throat discomfort, lose it is foster in moistening, long it, The bright bright Tianjin of the fire of deficiency type is draped over one's shoulders, and with depression of QI, catharsis is not smooth, and causes qi depression to blood stasis phlegm to coagulate.Qi and blood phlegm-turbidity and blood stasis hinders, and opens lucid yang failing to raise, Failure in sending down turbid yin is so that qi and blood week capable not smooth retardance air flues and passages through which vital energy circulates.Therefore throat appearance is dry and astringent vexed swollen, such as thing infraction, utters a sound or a word and cough up not , war proclamation setting forth the purpose of the expedition and enumerating the crimes of the enemy pain, dry are not intended to drink, and protracted course of disease, throat transmucosal is dark red, rear wall, delete Suo Zenghou, curtain pearl hyperplasia, local vascular expands Open and reticulate, dimly red tongue or raw lean point, separately then because of feeding desorder, overfeeding is pungent, thermophilic tobacco and wine, lung stomach intrinsic heat.Upper steaming throat, gas Blood stasis is stagnant, phlegm it is turbid condensation and be this disease, control suitable regulating QI and promoting blood circulation to remove blood stasis, enriching yin nutrient solution, smooth throat.
Chronic pharyngitis category traditional Chinese medicine larynx numbness category, the disease system due to long-time by pessimal stimulation and addiction tobacco and wine it is pungent it Product, consumption hinder lung kidney body fluid, cause YIN fluid being insufficient, flaring up of deficient fire, follow through upper steaming, and smoked bright throat forms.Its total interpretation of the cause, onset and process of an illness of chronic pharyngitis It is lung-kidney deficiency, and existing medicine is poor to the therapeutic effect of this above-mentioned symptom.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of formula proposed is simple, prepares Method is easy, and therapeutic effect is good, has antibechic, eliminating the phlegm, relievings asthma, preventing phlegm from forming and stopping coughing Chinese medicine composition of anti-inflammatory and preparation method thereof.
To achieve these goals, present invention employs following technical scheme:
A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition, include the raw material and auxiliary material of following parts by weight:Ficus microcarpa dried cream powder 92-95 parts, horse Come sour chlorphenamine 0.2-0.4 parts, -3 parts of silica 1 and talcum powder 2-5 parts.
Further, the Ficus microcarpa dried cream powder is made up of Ficus microcarpa.
Present invention also offers a kind of preparation method of preventing phlegm from forming and stopping coughing Chinese medicine composition, by the Ficus microcarpa through pre-treatment, Add water to cook secondary, for the first time plus 5 times of water amount, extract 1.5-2 hours, second plus 5 times of amounts of water, extract 0.5-1 hours, merge Decocting liquid, the clear cream that relative density is 1.10~1.20 (80 DEG C) is concentrated into, is let cool, added ethanol to alcohol content up to 60%, stand 12 More than hour, filtration, filtrate recycling ethanol, the thick paste that relative density is 1.30 (50 DEG C) is concentrated into, less than 80 DEG C dry, pulverize Into fine powder, chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder are added, is mixed, loads capsule and produces.
Further, by the Ficus microcarpa net medicinal material point input extractor, decoct 2 times, add 5 times of amount water for the first time, boil 1.5-2 hours are carried, extract solution is filtered with 200 mesh stainless steel mesh, and filtrate is all put into receiver, standby;Second plus 5 Amount water again, is boiled and carries 0.5-1 hour filtrates, and is filtered with 200 mesh stainless steel mesh, and filtrate is all squeezed into receiver, and with Extraction filtrate merges for the first time.
Further, the extract solution in above-mentioned receiver is sucked in haplo-effect concentrator by vacuum, opens steam valve and carry out Heating, thickening temperature control exist(70~80 DEG C), vacuum degree control exists(- 0.03~-0.08Mpa), continuously extract solution is concentrated It is complete to proportion be 1.10~1.20(80℃), Alcohol-settling tank is pumped into by material pipe.
Further, 200kg95% ethanol is first added, then the thick paste for concentrating gained is pumped into Alcohol-settling tank, after adding decoction The concentration of alcohol precipitation ethanol is measured, then it is 60% to add 95% ethanol to concentration, stands more than 12 hours, takes supernatant, it is stand-by.
Further, by the supernatant suction single-effect external circulation evaporator after above-mentioned alcohol precipitation, open steam valve and added Heat(Steam pressure:0.05~0.09 Mpa), for temperature control below 80 DEG C, normal pressure reclaims ethanol to decoction without being carried out after alcohol taste Concentration;Steam valve is opened to be heated(Steam pressure:0.05~0.09 Mpa), temperature control exists(70~80 DEG C), vacuum Control exists(- 0.03~-0.08Mpa) concentrated;Continuous concentration is 1.30 (50 DEG C of surveys) to relative density, is received in clean area Received between cream in the stainless steel cask that cream disinfects to cleaning.
Further, the thick paste after above-mentioned concentration is put into baking tray, puts in vacuum drier and done in 70~80 DEG C of vacuum It is dry, vacuum -0.03~-0.08Mpa, dry extract is dried 8~10 hours to obtain, the clean container for receiving dry cream inner lining plastic bag is contained Dress.
Further, Ficus microcarpa dry cream is crushed, crushes 80 mesh sieves of screen cloth, the material after crushing uses liner respectively The clean container of polybag contains.
Compared with prior art, the invention has the advantages that:A kind of preventing phlegm from forming and stopping coughing Chinese medicine group of the present invention The preparation method of compound, including the raw material such as Ficus microcarpa dried cream powder, chlorphenamine maleate, silica and talcum powder and auxiliary material, And mix Ficus microcarpa dried cream powder, chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, get product, there is town Cough, eliminating the phlegm, relieving asthma, anti-inflammatory and other effects, can be widely used for cough and asthma and chronic bronchitis;The preparation method is easy simultaneously, formula Simply, therapeutic effect is good.
Brief description of the drawings
Fig. 1 is the process chart of the present invention.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.
Embodiment one:A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition, include the raw material and auxiliary material of following parts by weight:Ficus microcarpa dry cream 5 parts of 92 parts of powder, 0.4 part of chlorphenamine maleate, 3 parts of silica and talcum powder.Wherein, the Ficus microcarpa dried cream powder is by leaflet Banyan is made.
Present invention also offers a kind of preparation method of preventing phlegm from forming and stopping coughing Chinese medicine composition, by the Ficus microcarpa through pre-treatment, Add water to cook secondary, for the first time plus 5 times of water amount, extract 1.5 hours, second plus 5 times of amounts of water, extract 0.5 hour, merge and decoct Liquid, be concentrated into the clear cream that relative density is 1.10 (80 DEG C), let cool, add ethanol to alcohol content up to 60%, stand 12 hours with On, filtration, filtrate recycling ethanol, be concentrated into relative density be 1.30 (50 DEG C) thick paste, less than 80 DEG C dry, pulverize into it is thin Powder, chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder are added, mixed, loaded capsule and produce.
Specifically, by the Ficus microcarpa net medicinal material point input extractor, decoct 2 times, add 5 times of amount water for the first time, boil and carry 1.5 hours, extract solution was filtered with 200 mesh stainless steel mesh, and filtrate is all put into receiver, standby;Second plus 5 times of amounts Water, boil and carry 0.5 hour filtrate, and with 200 mesh stainless steel mesh filter, filtrate is all squeezed into receiver, and with for the first time Filtrate is extracted to merge.
Specifically, the extract solution in above-mentioned receiver is sucked in haplo-effect concentrator by vacuum, open steam valve and added Heat, thickening temperature control exist(70℃), vacuum degree control exists(- 0.03~Mpa), continuously extract solution has been concentrated to proportion it is 1.10(80℃), Alcohol-settling tank is pumped into by material pipe.
Specifically, first adding 200kg95% ethanol, then the thick paste for concentrating gained is pumped into Alcohol-settling tank, surveyed after adding decoction The concentration of alcohol precipitation ethanol is measured, then it is 60% to add 95% ethanol to concentration, stands more than 12 hours, takes supernatant, it is stand-by.
Specifically, by the supernatant suction single-effect external circulation evaporator after above-mentioned alcohol precipitation, open steam valve and heated (Steam pressure:0.05Mpa), for temperature control below 80 DEG C, normal pressure reclaims ethanol to decoction without being concentrated after alcohol taste;Open Steam valve is heated(Steam pressure:0.05Mpa), temperature control exists(70℃), vacuum degree control exists(- 0.03Mpa) carry out Concentration;Continuous concentration is 1.30 (50 DEG C of surveys) to relative density, and the stainless steel that cream disinfects to cleaning is received between clean area receives cream In bucket.
Specifically, the thick paste after above-mentioned concentration is put into baking tray, put in vacuum drier in 70 DEG C of vacuum drying, vacuum Degree -0.03Mpa, dry extract is dried 8 hours to obtain, the clean container for receiving dry cream inner lining plastic bag contains.
Finally, Ficus microcarpa dry cream is crushed, crushes 80 mesh sieves of screen cloth, the material after crushing uses plastic lining respectively The clean container of bag contains, and adds chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, mixes, and loads capsule and is .
Embodiment two:A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition, include the raw material and auxiliary material of following parts by weight:Ficus microcarpa dry cream 2 parts of 95 parts of powder, 0.2 part of chlorphenamine maleate, silica 1 part and talcum powder.Wherein, the Ficus microcarpa dried cream powder is by leaflet Banyan is made.
Present invention also offers a kind of preparation method of preventing phlegm from forming and stopping coughing Chinese medicine composition, by the Ficus microcarpa through pre-treatment, Add water to cook secondary, for the first time plus 5 times of water amount, extract 1.8 hours, second plus 5 times of amounts of water, extract 0.8 hour, merge and decoct Liquid, be concentrated into the clear cream that relative density is 1.15 (80 DEG C), let cool, add ethanol to alcohol content up to 60%, stand 12 hours with On, filtration, filtrate recycling ethanol, be concentrated into relative density be 1.30 (50 DEG C) thick paste, less than 80 DEG C dry, pulverize into it is thin Powder, chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder are added, mixed, loaded capsule and produce.
Specifically, by the Ficus microcarpa net medicinal material point input extractor, decoct 2 times, add 5 times of amount water for the first time, boil and carry 1.8 hours, extract solution was filtered with 200 mesh stainless steel mesh, and filtrate is all put into receiver, standby;Second plus 5 times of amounts Water, boil and carry 0.8 hour filtrate, and with 200 mesh stainless steel mesh filter, filtrate is all squeezed into receiver, and with for the first time Filtrate is extracted to merge.
Specifically, the extract solution in above-mentioned receiver is sucked in haplo-effect concentrator by vacuum, open steam valve and added Heat, thickening temperature control exist(75℃), vacuum degree control exists(- 0.05Mpa), it is 1.15 continuously to have concentrated extract solution to proportion (80℃), Alcohol-settling tank is pumped into by material pipe.
Specifically, first adding 200kg95% ethanol, then the thick paste for concentrating gained is pumped into Alcohol-settling tank, surveyed after adding decoction The concentration of alcohol precipitation ethanol is measured, then it is 60% to add 95% ethanol to concentration, stands more than 12 hours, takes supernatant, stand-by
Specifically, by the supernatant suction single-effect external circulation evaporator after above-mentioned alcohol precipitation, open steam valve and heated(Steam Pressure:0.07Mpa), for temperature control below 80 DEG C, normal pressure reclaims ethanol to decoction without being concentrated after alcohol taste;Open steam Valve is heated(Steam pressure:0.07 Mpa), temperature control exists(75℃), vacuum degree control exists(- 0.05Mpa) carry out it is dense Contracting;Continuous concentration is 1.30 (50 DEG C of surveys) to relative density, and the stainless steel cask that cream disinfects to cleaning is received between clean area receives cream In.
Specifically, the thick paste after above-mentioned concentration is put into baking tray, put in vacuum drier in 75 DEG C of vacuum drying, vacuum Degree -0.05Mpa, dry extract is dried 9 hours to obtain, the clean container for receiving dry cream inner lining plastic bag contains.
Finally, Ficus microcarpa dry cream is crushed, crushes 80 mesh sieves of screen cloth, the material after crushing uses plastic lining respectively The clean container of bag contains, and adds chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, mixes, and loads capsule and is .
Embodiment three:A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition, include the raw material and auxiliary material of following parts by weight:Ficus microcarpa dry cream 3 parts of 94 parts of powder, 0.3 part of chlorphenamine maleate, 2 parts of silica and talcum powder.Wherein, the Ficus microcarpa dried cream powder is by leaflet Banyan is made.
Present invention also offers a kind of preparation method of preventing phlegm from forming and stopping coughing Chinese medicine composition, by the Ficus microcarpa through pre-treatment, Add water to cook secondary, for the first time plus 5 times of water amount, extract 2 hours, second plus 5 times of amounts of water, extract 1 hour, collecting decoction is dense The clear cream that relative density is 1.20 (80 DEG C) is reduced to, is let cool, ethanol is added to alcohol content up to 60%, stands more than 12 hours, filter Cross, filtrate recycling ethanol, be concentrated into the thick paste that relative density is 1.30 (50 DEG C), less than 80 DEG C dry, pulverize into fine powder, add Chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, mix, load capsule and produce.
Specifically, by the Ficus microcarpa net medicinal material point input extractor, decoct 2 times, add 5 times of amount water for the first time, boil and carry 2 Hour, extract solution is filtered with 200 mesh stainless steel mesh, filtrate is all put into receiver, standby;Second plus 5 times of amount water, Boil and carry 1 hour filtrate, and filtered with 200 mesh stainless steel mesh, filtrate is all squeezed into receiver, and filtered with first time extraction Liquid merges.
Specifically, the extract solution in above-mentioned receiver is sucked in haplo-effect concentrator by vacuum, open steam valve and added Heat, thickening temperature control exist(80℃), vacuum degree control exists(0.08Mpa), it is 1.20 continuously to have concentrated extract solution to proportion (80℃), Alcohol-settling tank is pumped into by material pipe.
Specifically, first adding 200kg95% ethanol, then the thick paste for concentrating gained is pumped into Alcohol-settling tank, surveyed after adding decoction The concentration of alcohol precipitation ethanol is measured, then it is 60% to add 95% ethanol to concentration, stands more than 12 hours, takes supernatant, it is stand-by.
Specifically, by the supernatant suction single-effect external circulation evaporator after above-mentioned alcohol precipitation, open steam valve and heated (Steam pressure:0.09 Mpa), for temperature control below 80 DEG C, normal pressure reclaims ethanol to decoction without being concentrated after alcohol taste;Beat Steam valve is driven to be heated(Steam pressure:0.09 Mpa), temperature control exists(80℃), vacuum degree control exists(- 0.08Mpa) enter Row concentration;Continuous concentration is 1.30 (50 DEG C survey) to relative density, received between clean area receives cream cream to cleaning disinfect it is stainless In steel drum.
Specifically, the thick paste after above-mentioned concentration is put into baking tray, put in vacuum drier in 80 DEG C of vacuum drying, vacuum Degree -0.08Mpa, dry extract is dried 10 hours to obtain, the clean container for receiving dry cream inner lining plastic bag contains.
Finally, Ficus microcarpa dry cream is crushed, crushes 80 mesh sieves of screen cloth, the material after crushing uses plastic lining respectively The clean container of bag contains, and adds chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, mixes, and loads capsule and is .
In summary, preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof, by Ficus microcarpa dried cream powder, chlorphenamine maleate Quick and appropriate amount of auxiliary materials silica and talcum powder mix, and get product, have antibechic, eliminating the phlegm, relieving asthma, anti-inflammatory and other effects can be wide It is general to be used for cough and asthma and chronic bronchitis;The preparation method is easy simultaneously, and formula is simple, therapeutic effect is good.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (9)

1. a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition, it is characterised in that raw material and auxiliary material including following parts by weight:Ficus microcarpa dry cream Powder 92-95 parts, chlorphenamine maleate 0.2-0.4 parts, -3 parts of silica 1 and talcum powder 2-5 parts.
A kind of 2. preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 1, it is characterised in that the Ficus microcarpa dried cream powder by Ficus microcarpa is made.
3. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 2, it is characterised in that will be described small Ye Rong adds water to cook secondary through pre-treatment, for the first time plus 5 times of amounts of water, extracts 1.5-2 hours, second plus 5 times of amounts of water, extraction 0.5-1 hours, collecting decoction, the clear cream that relative density is 1.10~1.20 (80 DEG C) is concentrated into, is let cool, add ethanol to containing alcohol Amount stands more than 12 hours up to 60%, filtration, filtrate recycling ethanol, is concentrated into the thick paste that relative density is 1.30 (50 DEG C), and 80 Fine powder is dry, pulverize into below DEG C, adds chlorphenamine maleate and appropriate amount of auxiliary materials silica and talcum powder, is mixed, is loaded Capsule produces.
4. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 3, it is characterised in that will be described small In leaf banyan net medicinal material point input extractor, decoct 2 times, add 5 times of amount water for the first time, boil and carry 1.5-2 hours, 200 mesh of extract solution Stainless steel mesh is filtered, and filtrate is all put into receiver, standby;Second plus 5 times of amount water, boil and carry 0.5-1 hour filtrates, And filtered with 200 mesh stainless steel mesh, filtrate is all squeezed into receiver, and merges with first time extraction filtrate.
5. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 4, it is characterised in that by above-mentioned storage Extract solution in flow container is sucked in haplo-effect concentrator by vacuum, is opened steam valve and is heated, and thickening temperature control exists(70~80 ℃), vacuum degree control exists(- 0.03~-0.08Mpa), it is 1.10~1.20 continuously to have concentrated extract solution to proportion(80℃), Alcohol-settling tank is pumped into by material pipe.
6. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 5, it is characterised in that first add 200kg95% ethanol, then the thick paste for concentrating gained is pumped into Alcohol-settling tank, the concentration of alcohol precipitation ethanol is measured after adding decoction, then mend Ethanol to the concentration for adding 95% is 60%, stands more than 12 hours, takes supernatant, stand-by.
7. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 6, it is characterised in that by above-mentioned alcohol In supernatant suction single-effect external circulation evaporator after heavy, open steam valve and heated(Steam pressure:0.05~0.09 Mpa), for temperature control below 80 DEG C, normal pressure reclaims ethanol to decoction without being concentrated after alcohol taste;Steam valve is opened to be heated (Steam pressure:0.05~0.09 Mpa), temperature control exists(70~80 DEG C), vacuum degree control exists(- 0.03~-0.08Mpa) Concentrated;Continuous concentration is 1.30 (50 DEG C of surveys) to relative density, and receiving cream to cleaning between clean area receives cream disinfects not In rust steel drum.
8. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 7, it is characterised in that will be above-mentioned dense Thick paste after contracting is put into baking tray, is put in vacuum drier and is dried in vacuo in 70~80 DEG C, vacuum -0.03~-0.08Mpa, Dry extract is dried 8~10 hours to obtain, the clean container for receiving dry cream inner lining plastic bag contains.
9. the preparation method of a kind of preventing phlegm from forming and stopping coughing Chinese medicine composition according to claim 8, it is characterised in that by Ficus microcarpa Dry cream is crushed, and crushes 80 mesh sieves of screen cloth, and the material after crushing is contained with the clean container of inner lining plastic bag respectively.
CN201711295301.1A 2017-12-08 2017-12-08 A kind of preventing phlegm from forming and stopping coughing Chinese medicine composition and preparation method thereof Pending CN107823263A (en)

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