CN107821731A - A kind of Semen sojae atricolor enzymatic protein spray coating liquor and preparation method thereof - Google Patents
A kind of Semen sojae atricolor enzymatic protein spray coating liquor and preparation method thereof Download PDFInfo
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- CN107821731A CN107821731A CN201711087323.9A CN201711087323A CN107821731A CN 107821731 A CN107821731 A CN 107821731A CN 201711087323 A CN201711087323 A CN 201711087323A CN 107821731 A CN107821731 A CN 107821731A
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- Prior art keywords
- spray coating
- coating liquor
- semen sojae
- sojae atricolor
- enzymatic protein
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
- A23J1/148—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds by treatment involving enzymes or microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
- A23J1/142—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds by extracting with organic solvents
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Peptides Or Proteins (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention belongs to soybean protein production technical field, and in particular to a kind of Semen sojae atricolor enzymatic protein spray coating liquor, and its preparation method is further disclosed, the Semen sojae atricolor enzymatic protein spray coating liquor is favorably improved the rate of dispersion of Semen sojae atricolor enzymatic protein.Semen sojae atricolor enzymatic protein spray coating liquor of the present invention, using phosphatide and sucrose fatty ester as main component, solvent is done instead of soybean oil with the process water Jing Guo osmosis filtration simultaneously, for the oil phase spray coating liquor of solvent is done with soybean oil in the prior art, the dispersive property and dissolution velocity of gained Semen sojae atricolor enzymatic protein are substantially improved gained aqueous phase spray coating liquor.
Description
Technical field
The invention belongs to soybean protein production technical field, and in particular to a kind of Semen sojae atricolor enzymatic protein spray coating liquor, go forward side by side one
The open its preparation method of step, the Semen sojae atricolor enzymatic protein spray coating liquor are favorably improved the rate of dispersion of Semen sojae atricolor enzymatic protein.
Background technology
Semen sojae atricolor enzymatic protein be using soybean as raw material, with biotechnology carry out conversion processing and through high temperature drying and
Into, a high-quality protein of adaptation young animal digestive physiology characteristic.In Semen sojae atricolor enzymatic protein protein content 90% with
On, amino acid classes have nearly 20 kinds, and contain a variety of essential amino acids.Semen sojae atricolor enzymatic protein is nutritious, meets children
Age animal and flesh-eater, aquatic livestock are to the particular/special requirement of protein quality.
In Semen sojae atricolor enzymatic protein, due to eliminating most raffinose and stachyose, the anti-of glycinin is eliminated
Originality, and other ANFs such as SNSP and phytic acid are also handled, so, the anti-nutrition in Semen sojae atricolor enzymatic protein
The factor is relatively low；And because the original spherical structure of soybean protein has been destroyed, peptide chain is in extended position, internal enzyme effect position
Point fully exposure so that its digestibility is improved；In addition, Semen sojae atricolor enzymatic protein has unique fragrance, it is favorably improved
Palatability so that animal prefers to search for food, and the extremely digestible characteristic of Semen sojae atricolor enzymatic protein, also causes its feed intake original text and holds
Long.
In the prior art, the typical production process of Semen sojae atricolor enzymatic protein is alkali extraction-acid precipitation, i.e., soaks dregs of beans with weak lye
40 minutes or so so that protein dissolution is separated after removing insoluble fiber with seperator, left containing albumen in weak lye
Solution, then flocculant (be usually food grade hydrochloric acid) is added into protein solution, albumen precipitation is out reclaimed, then right
The albumen of recovery carries out ferment treatment, and Semen sojae atricolor enzymatic protein is obtained after obtaining protein enzymatic hydrolyzate drying and processing.But by above-mentioned first
The Semen sojae atricolor enzymatic protein powder that step processing obtains only has the general performance of Semen sojae atricolor enzymatic protein, for many application fields,
Its performance can not meet process requirements, it is necessary to by being sprayed to dried enzymolysis protein powder, to be suitable for
The Semen sojae atricolor enzymatic protein of different manufacture field performance requirements.
The content of the invention
Therefore, the technical problems to be solved by the invention are to provide a kind of Semen sojae atricolor enzymatic protein spray coating liquor, with further
Improve the solubility property of Semen sojae atricolor enzymatic protein.
In order to solve the above technical problems, a kind of Semen sojae atricolor enzymatic protein spray coating liquor of the present invention, the spray coating liquor include
The component of following parts by weight：The parts by weight of phosphatidase 5-10, sucrose fatty ester 1-4 parts by weight, water 20-30 parts by weight.
Preferably, the spray coating liquor includes the component of following parts by weight：The parts by weight of phosphatidase 6-9, sucrose fatty ester 2-3 weights
Measure part, water 22-28 parts by weight.
More excellent, the spray coating liquor includes the component of following parts by weight：The parts by weight of phosphatide 7.8, the weight of sucrose fatty ester 2.4
Measure part, the parts by weight of water 25.8.
The water is the process water by osmosis filtration.
The invention also discloses a kind of method for preparing described Semen sojae atricolor enzymatic protein spray coating liquor, including by a selected amount of water
The step of heating, and sequentially adding a selected amount of phosphatide and sucrose fatty ester, mix, produce.
The heating-up temperature for controlling water is 60-70 DEG C.
While being additionally included in the addition phosphatide and sucrose fatty ester, the step of shear treatment is carried out with high speed shear pump
Suddenly.
Also include carrying out gained spray coating liquor into the step of insulation preserves in 70 DEG C.
The invention also discloses purposes of the described Semen sojae atricolor enzymatic protein spray coating liquor in Semen sojae atricolor enzymatic protein production process,
In terms of the Semen sojae atricolor enzymatic protein butt, the quantity for spray of the spray coating liquor is 1-3 ‰.
The spray coating liquor is sprayed by measuring pump by two Fluid sprayers.
The spray coating liquor is persistently incubated and stirred in spraying process, to prevent the spray coating liquor layering and precipitating.
Semen sojae atricolor enzymatic protein spray coating liquor of the present invention, using phosphatide and sucrose fatty ester as main component, while with
Process water by osmosis filtration makees solvent instead of soybean oil, and gained aqueous phase spray coating liquor is compared in the prior art with soybean oil
For doing the oil phase spray coating liquor of solvent, the dispersive property and dissolution velocity of gained Semen sojae atricolor enzymatic protein are substantially improved.
Semen sojae atricolor enzymatic protein spray coating liquor of the present invention, done with the process water Jing Guo osmosis filtration instead of soybean oil molten
Agent, after testing, total plate count ＜ 500cfu/g, E.coli LT .LT.LT 3.0cfu/g, the yeast and mold ＜ 50cfu/g of process water
It is interior, the rate of dispersion of protein powder is improved while microbial growth is avoided.
Brief description of the drawings
In order that present disclosure is more likely to be clearly understood, specific embodiment and combination below according to the present invention
Accompanying drawing, the present invention is further detailed explanation, wherein,
Fig. 1 is the schematic diagram that the present invention is sprayed using two Fluid sprayers.
Embodiment
Embodiment 1
Semen sojae atricolor enzymatic protein spray coating liquor described in the present embodiment, including following component：Phosphatidase 5 kg, sucrose fatty ester
4kg, process water 20kg.
The method that the present embodiment prepares described Semen sojae atricolor enzymatic protein spray coating liquor, including：A selected amount of water is heated to 60-
70 DEG C, and a selected amount of phosphatide and sucrose fatty ester are sequentially added, while shear treatment is carried out extremely with high speed shear pump
Solution uniform dissolution, the spray coating liquor is produced, and gained spray coating liquor is placed in 70 DEG C of insulation water-bath interlayers and carries out insulation preservation.
Embodiment 2
Semen sojae atricolor enzymatic protein spray coating liquor described in the present embodiment, including following component：Phosphatidase 1 0kg, sucrose fatty ester
1kg, process water 30kg.
The preparation method of Semen sojae atricolor enzymatic protein spray coating liquor is the same as embodiment 1 described in the present embodiment.
Embodiment 3
Semen sojae atricolor enzymatic protein spray coating liquor described in the present embodiment, including following component：Phosphatidase 6 kg, sucrose fatty ester
3kg, process water 22kg.
The preparation method of Semen sojae atricolor enzymatic protein spray coating liquor is the same as embodiment 1 described in the present embodiment.
Embodiment 4
Semen sojae atricolor enzymatic protein spray coating liquor described in the present embodiment, including following component：Phosphatide 9kg, sucrose fatty ester
2kg, process water 28kg.
The preparation method of Semen sojae atricolor enzymatic protein spray coating liquor is the same as embodiment 1 described in the present embodiment.
Embodiment 5
Semen sojae atricolor enzymatic protein spray coating liquor described in the present embodiment, including following component：Phosphatide 7.8kg, sucrose fatty ester
2.4kg, process water 25.8kg.
The preparation method of Semen sojae atricolor enzymatic protein spray coating liquor is the same as embodiment 1 described in the present embodiment.
Comparative example 1
Semen sojae atricolor enzymatic protein spray coating liquor described in this comparative example, including following component：Phosphatidase 5 .4kg, sucrose fatty ester
1.8kg, soybean oil 4.8kg.
Application examples
The spraying process of spray coating liquor of the present invention is that two Fluid sprayer commonly used in the prior art is sprayed, that is, presses
Sprayed according to the application method of two Fluid sprayers.The process that two Fluid sprayers as giving Fig. 1 are sprayed is shown
It is intended to, liquid (spray coating liquor) is transported to nozzle by flow channel for liquids under pressure, and compressed air is arrived by gas flow
Up to nozzle, both mix at nozzle produces atomization mass (circular spray pattern), and in " B " distance, atomization mass can keep ratio
More regular sectorial area, such as " A ", after beyond distance " D ", atomization mass becomes turbulent flow to angular dimension, and shape changes, attached
A, B, D parameter can change according to second fluid nozzle model difference in figure, as long as spray coating liquor is atomized uniformly and selects any type
Number nozzle.
Spraying schematic diagram as shown in Figure 1, respectively with spray coating liquor made from embodiment 1-5 and comparative example 1, led to by measuring pump
Cross the two Fluid sprayers Semen sojae atricolor enzymatic protein commercially available to prior art and carry out spray treatment, respectively obtain corresponding protein sample.
In terms of the Semen sojae atricolor enzymatic protein butt, the quantity for spray for controlling the spray coating liquor is 1-3 ‰, and is needed in spraying process pair
The spray coating liquor carries out continuing insulation, and is formulated stirrer gear in tank and persistently stirs, and prevents spray coating liquor layering and precipitating.
Experimental example dispersiveness detection
50-55 DEG C of 100 ± 0.1g of distilled water is added in 250ml beaker, 5.0 ± 0.1g eggs are weighed with electronic balance
White sample (spray coating liquor is made by embodiment 1-5 and comparative example respectively to obtain through spraying) is poured into beaker, with glass bar close to burning
Wall of cup stirs and starts timing clockwise, the time required to mixing speed control is write down in about 3 circles/s, during to no dry powder, is
Rate of dispersion.
After testing, handling the rate of dispersion of Semen sojae atricolor enzymatic protein sample obtained through spray coating liquor described in embodiment 1-5 is
10-15s, and the rate of dispersion for the Semen sojae atricolor enzymatic protein sample that the processing of spray coating liquor described in example obtains is 25-29s by contrast.Can
See, the dissolving of albumen greatly improved compared to oiliness spray coating liquor common in the art in aqueous phase spray coating liquor of the present invention
Speed.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (10)
1. a kind of Semen sojae atricolor enzymatic protein spray coating liquor, it is characterised in that the spray coating liquor includes the component of following parts by weight：Phosphatidase 5-
10 parts by weight, sucrose fatty ester 1-4 parts by weight, water 20-30 parts by weight.
2. Semen sojae atricolor enzymatic protein spray coating liquor according to claim 1, it is characterised in that the spray coating liquor includes following weight
The component of part：The parts by weight of phosphatide 7.8, the parts by weight of sucrose fatty ester 2.4, the parts by weight of water 25.8.
3. Semen sojae atricolor enzymatic protein spray coating liquor according to claim 1 or 2, it is characterised in that the water is by counter-infiltration
The process water of filtering.
A kind of 4. method for preparing the Semen sojae atricolor enzymatic protein spray coating liquor described in claim any one of 1-3, it is characterised in that including
The step of a selected amount of water is heated, and sequentially adds a selected amount of phosphatide and sucrose fatty ester, mix, produce.
5. the method according to claim 4 for preparing the Semen sojae atricolor enzymatic protein spray coating liquor, it is characterised in that control water
Heating-up temperature is 60-70 DEG C.
6. the method for preparing the Semen sojae atricolor enzymatic protein spray coating liquor according to claim 5 or 6, it is characterised in that also wrap
Include while the phosphatide and sucrose fatty ester is added, the step of shear treatment is carried out with high speed shear pump.
7. the method for preparing the Semen sojae atricolor enzymatic protein spray coating liquor according to claim any one of 4-6, it is characterised in that
Also include carrying out gained spray coating liquor into the step of insulation preserves in 70 DEG C.
8. use of the Semen sojae atricolor enzymatic protein spray coating liquor described in claim any one of 1-3 in Semen sojae atricolor enzymatic protein production process
On the way, it is characterised in that in terms of the Semen sojae atricolor enzymatic protein butt, the quantity for spray of the spray coating liquor is 1-3 ‰.
9. purposes according to claim 8, it is characterised in that the spray coating liquor is carried out by measuring pump by two Fluid sprayers
Spraying.
10. purposes according to claim 8 or claim 9, it is characterised in that the spray coating liquor in spraying process persistently insulation and
Stirring, to prevent the spray coating liquor layering and precipitating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711087323.9A CN107821731B (en) | 2017-11-07 | 2017-11-07 | Soybean enzymolysis protein spraying liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711087323.9A CN107821731B (en) | 2017-11-07 | 2017-11-07 | Soybean enzymolysis protein spraying liquid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107821731A true CN107821731A (en) | 2018-03-23 |
| CN107821731B CN107821731B (en) | 2021-03-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711087323.9A Active CN107821731B (en) | 2017-11-07 | 2017-11-07 | Soybean enzymolysis protein spraying liquid and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106798072A (en) * | 2016-12-30 | 2017-06-06 | 山东禹王生态食业有限公司 | A kind of protein preparation method for improving soybean protein isolate dispersiveness |
| CN107047923A (en) * | 2017-05-19 | 2017-08-18 | 山东禹王生态食业有限公司 | A kind of preparation method of soybean protein isolate |
| CN107312813A (en) * | 2017-07-28 | 2017-11-03 | 山东禹王生态食业有限公司 | A kind of preparation method of microorganism specialized soybean protein isolate |
-
2017
- 2017-11-07 CN CN201711087323.9A patent/CN107821731B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106798072A (en) * | 2016-12-30 | 2017-06-06 | 山东禹王生态食业有限公司 | A kind of protein preparation method for improving soybean protein isolate dispersiveness |
| CN107047923A (en) * | 2017-05-19 | 2017-08-18 | 山东禹王生态食业有限公司 | A kind of preparation method of soybean protein isolate |
| CN107312813A (en) * | 2017-07-28 | 2017-11-03 | 山东禹王生态食业有限公司 | A kind of preparation method of microorganism specialized soybean protein isolate |
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| Publication number | Publication date |
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| CN107821731B (en) | 2021-03-26 |
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