CN107821422A - A kind of Pesticidal combination containing destruxins and Acetamiprid and its application - Google Patents
A kind of Pesticidal combination containing destruxins and Acetamiprid and its application Download PDFInfo
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- CN107821422A CN107821422A CN201711095562.9A CN201711095562A CN107821422A CN 107821422 A CN107821422 A CN 107821422A CN 201711095562 A CN201711095562 A CN 201711095562A CN 107821422 A CN107821422 A CN 107821422A
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- Prior art keywords
- acetamiprid
- destruxins
- pesticidal combination
- combination containing
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
Abstract
The present invention relates to a kind of Pesticidal combination containing destruxins and Acetamiprid and its application, the existing chemical pesticide side effect of purpose solution is big, it is serious to remain, pollutes environment, influence agricultural product quality and safety and easily causes the technical problem that insect develops immunity to drugs, and the technical solution adopted by the present invention is：A kind of Pesticidal combination containing destruxins and Acetamiprid, the active component of the Pesticidal combination are made up of destruxins and Acetamiprid, and the weight ratio of the destruxins and Acetamiprid is (9~1)：(1~9).The application of the Pesticidal combination, the Pesticidal combination are applied to preventing and treating fruit tree and vegetable-crop pest-insect.The Pesticidal combination of the present invention can improve the quick-acting and lasting effect of medicament, expand insecticidal spectrum, there is obvious synergistic function in insects such as the aphid on preventing and treating multiple kinds of crops, aleyrodids, significantly reduce Pesticide use amount, improve prevention effect, reduce production cost.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of Pesticidal combination containing destruxins and Acetamiprid and
It is applied.
Background technology
At present, control of agricultural pest still depends on chemical pesticide, and thus caused " 3R " is (resistance to the action of a drug, rampant, residual again
Stay toxicity) significant problem such as side effect, environmental pollution, agricultural product quality and safety receives much concern, and in the recent period, the Ministry of Science and Technology starts medicine
Fertile " double to subtract " project, therefore it is trend of the times to develop green, safe efficient, environment-protection pesticide.
Aphid, aphid, aphid are commonly called as, belong to Semiptera (Hemiptera), including adelgid Superfamily (Adelgoidea) and aphid
Superfamily (Aphidoidea), it is a kind of important crop pests, is worldwide widely distributed.Aphid host is more
Sample, the generation cycle is short, generating capacity is big, causes mould by direct feeding plant juice, the propagation viroses of plant and secretion honeydew
Growing influences the normal growth and development of crops, and its Rampant damage can cause huge economic loss to crops, have a strong impact on
Production estimation, and difficulty of prevention and cure is big, cost is high.Apple yellow aphid (Aphis citricola von der Goot) also known as embroider line
Chrysanthemum aphid, it is a kind for aphid, the areas such as Hebei, the Inner Mongol, Shanxi, Shandong, Henan is distributed mainly in China, be China's apple
Fruit producing region is common and a kind of one of the more serious foliar pest of hazard ratio.It is clustered in host's tender tip with larvae aphid, adult aphid, tender leaf is carried on the back
Face and the thorn suction of young fruit surface are caused harm, and chlorisis spot is often presented in aggrieved blade, after rearwardly cupping transverse curl or crispatura, when serious, leaf
Piece is in blood red early fallout.When population density is big, often there are ant and its symbiosis, have a strong impact on the photosynthesis and branch of blade
Normal growth, cause tree vigo(u)r weak, influence the yield of apple.At present, the use of chemical insecticide is still control apple yellow aphid
Main method.But the development of such pest resistance to insecticide is gradually exacerbated to high intensity using chemical pesticide, adds pests control
Cost and difficulty, also aggravate Pesticide Residue, and the residual exceeding standard rate of agriculture remains high, and causes food and problems of ecological security.Cause
This, green, safe efficient, the less toxic anti-novel agrochemical to eliminate aphis of exploitation is into the task of top priority.
Destruxins (destruxins) is also known as destruxin or destroys element, is Metarhizium anisopliae (Metarhizium
Anisopliae a kind of cyclic depsipeptides secondary metabolites caused by), is made up of, main function 5 amino acid and 1 carboxylic acid
In the immunity of haemolymph of insect, Insect immunity defence capability is set to decline or lose.Its to Lepidoptera, Homoptera, Orthoptera,
The various pests of Diptera, coleoptera etc. 20 have tag, stomach toxicity, according to food and avoidance effect.Destruxins and some entomogenous fungis
Or commodity Mixture Use of Insecticides has synergistic effect, such as with beauveria bassiana, Paecilomyces javanicus, green muscardine fungus are mixed to improve to cigarette
The preventive effect of aleyrodid, prodenia litura, grub etc.；It is mixed with Bt, AVM, imidacloprid etc. also to significantly improve to dragon spruce leaf roll
The preventive effect of moth, diamondback moth and Bemisia tabaci.Due to destruxins diverse biological activities, mechanism of action is unique, and shows efficient, low
The features such as malicious, degradable, noresidue, stable prevention effect, there is good green novel pesticide Development volue.
The general entitled Acetamiprid of Acetamiprid English, also known as acetamiprid, are a kind of new chlorination nicotinic insecticides,
Have the characteristics that efficient, less toxic, environmentally safe.Acetamiprid has stomach toxicity, tags and absorbability, and mechanism of action is unique, main to make
For the nAChR of insect nerve system synapses, the stimulation of interference insect nervous system is conducted, and causes god
Block through system pass, cause accumulation of the neurotransmitter acetylcholine in synapses, it is final dead so as to cause insect paralysis
Die.Acetamiprid insecticidal spectrum is wide, activity is high, to Lepidoptera (diamondback moth, heart-eating worm etc.), Semiptera (aphid, aleyrodid, leafhopper etc.) evil
Worm is efficient, to people and animals' low toxicity, suitable for the insect on the crops such as preventing and treating fruit tree, vegetables.
Have not yet to see destruxins and the report of Acetamiprid compounding.
The content of the invention
Present invention aim to address existing chemical pesticide side effect is big, residual is serious, pollution environment, influence agricultural product
Quality safety and easily cause the technical problem that insect develops immunity to drugs, there is provided a kind of killing containing destruxins and Acetamiprid
Worm composition and its application, the Pesticidal combination have notable synergistic function, can significantly reduce Pesticide use amount with
And agricultural chemicals improves prevention effect excessively using agricultural chemicals " 3R " problem brought.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of Pesticidal combination containing destruxins and Acetamiprid, the active component of the Pesticidal combination is by green muscardine fungus
Element and Acetamiprid composition, the weight ratio of the destruxins and Acetamiprid is (9~1)：(1~9).
Further, the weight ratio of the destruxins and Acetamiprid is 8:2.
Further, the weight ratio of the destruxins and Acetamiprid is 5:5.
Further, the weight ratio of the destruxins and Acetamiprid is 4:6.
Further, the destruxins is the mixed of any one or its arbitrary proportion in destruxins A, B, C, D, E
Compound.
Further, the Pesticidal combination also includes assistant agent, the gross weight of the active component destruxins and Acetamiprid
It is 1~30% to measure percentage, and the percentage by weight of the assistant agent is 70~99%.
Further, the total weight percent of the active component destruxins and Acetamiprid is 10~30%.
Further, the formulation of the Pesticidal combination is that missible oil, microemulsion, suspending agent, wettable powder and moisture dissipate
Granula.
The application of above-mentioned Pesticidal combination, the Pesticidal combination are applied to preventing and treating fruit tree and vegetable-crop pest-insect.
Further, the Pesticidal combination is applied to anti-eliminate aphis and aleyrodid.
The beneficial effects of the invention are as follows：
The present invention is compounded the mutually different pesticide activity component destruxins of two kinds of mechanisms of action and Acetamiprid, and
Pass through substantial amounts of Toxicity Determination and field control effectiveness test, it is determined that the optimum compound proportion example of the two, the two is according to preferable
Obvious Synergistic is shown to various crop pests such as aphid, aleyrodid etc. within the specific limits after ratio compounding to make
With, and the different formulations of pesticide can be prepared according to being actually needed, easy to use, prevention effect stabilization；
The Pesticidal combination of the present invention can improve the quick-acting and lasting effect of medicament, expand insecticidal spectrum, a variety of preventing and treating
There is obvious synergistic function during the insects such as aphid, aleyrodid on crops, not only significantly reduce Pesticide use amount, carry
High prevention effect, production cost is reduced, and be also greatly reduced agricultural chemicals excessively using the various risks brought, meet state
Family's agricultural chemicals " zero growth rate " and green, safe efficient, the less toxic requirement of novel pesticide, are suitable for large-scale promotion and application.
Embodiment
The present invention is described in further details with reference to embodiment.
Embodiment 1
20% destruxins acetamiprid EC
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is missible oil, described
The percentage by weight of each component is in composition：
Destruxins A16%, Acetamiprid 4%, dimethylformamide 10%, agriculture breast No. 500 8%, castor oil 1%, epoxy
Change soya-bean oil 11%, Butacide 0.5%, surplus is supplied with dimethylbenzene.
The preparation method of the missible oil is：Destruxins A and Acetamiprid are dissolved in dimethylformamide, then remaining is each
Component adds, and is uniformly mixed i.e. available 20% destruxins acetamiprid EC.
Embodiment 2
10% destruxins acetamiprid suspending agent
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is suspending agent, institute
The percentage by weight for stating each component in composition is：
Destruxins B1%, Acetamiprid 9%, neopelex 9%, APES 8%, EO/PO
Block polyether 12%, epoxidized soybean oil 0.5%, castor oil 0.5%, xanthans 1%, Butacide 0.5%, ethylene glycol 5%, benzene first
Sour sodium 4%, surplus is supplied with deionized water.
The preparation method of the suspending agent is：By above-mentioned wetting agent neopelex, dispersant alkyl phenol polyoxy
Vinethene, defoamer epoxidized soybean oil, stabilizer sodium benzoate, synergist Butacide, antifreeze ethylene glycol etc. add blender
In, it is well mixed through high speed shear, adds destruxins B, Acetamiprid and deionized water, be milled in ball mill in composition
The particle diameter of 90% material adds thickener xanthans and further stirred, you can obtain 10% green muscardine fungus below 5 microns
Plain acetamiprid suspending agent.
Embodiment 3
10% destruxins acetamiprid micro emulsion agent
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is microemulsion, institute
The percentage by weight for stating each component in composition is：
Destruxins C5%, Acetamiprid 5%, cyclohexanone 8%, micro emulsion emulsifying agent JX-0401#20%, surplus deionization
Water is supplied.
The preparation method of the microemulsion is：Above-mentioned micro emulsion emulsifying agent JX-0401# and deionized water are well mixed, added
Enter the cyclohexanone solution of destruxins C and Acetamiprid, stir, you can obtain 10% destruxins acetamiprid micro emulsion agent.
Embodiment 4
15% destruxins acetamiprid wettable powder
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is wettable powder
Agent, the percentage by weight of each component is in the composition：
Destruxins D6%, Acetamiprid 9%, neopelex 10%, sodium lignin sulfonate 15%, surplus are high
Ridge soil is supplied.The preparation method of the wettable powder is：
Destruxins D, Acetamiprid, wetting agent neopelex, dispersant sodium lignin sulfonate and carrier is high
Ridge soil mixes in proportion, after ultra-fine pulverizer disintegrating, you can obtains 15% destruxins acetamiprid wettable powder.
Embodiment 5
27.5% destruxins acetamiprid water dispersible granules
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is water-dispersible grain
Agent, the percentage by weight of each component is in the composition：
Destruxins E22.5%, Acetamiprid 5%, pull open powder 4%, naphthalene sulfonic acid-formaldehyde condensation product 6%, ammonium sulfate 5%, breast
Agent 0201B#5%, Arabic gum 4%, surplus white carbon supply.
The preparation method of the water dispersible granules is：Destruxins E and Acetamiprid are proportionally added into carrier white carbon
In, then add emulsifying agent 0201B#, wetting agent pull open powder, dispersant naphthalene sulfonic acid-formaldehyde condensation product, disintegrant ammonium sulfate, bonding
Agent Arabic gum is well mixed, and appropriate deionized water is added after air-flow crushing, after mediating, be granulated, dry, sieve
Obtain 27.5% destruxins acetamiprid water dispersible granules.
Embodiment 6
30% destruxins acetamiprid water dispersible granules
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is water-dispersible grain
Agent, the percentage by weight of each component is in the composition：
Destruxins A, B, C, D, E mixture 27%, Acetamiprid 3%, pull open powder 4%, naphthalene sulfonic acid-formaldehyde condensation product
6%, ammonium sulfate 5%, emulsifying agent 0201B#5%, Arabic gum 4%, surplus white carbon supply.
The preparation method of the water dispersible granules is the same as embodiment 5.
Embodiment 7
1% destruxins acetamiprid water dispersible granules
A kind of Pesticidal combination containing destruxins and Acetamiprid in the present embodiment, said composition is water-dispersible grain
Agent, the percentage by weight of each component is in the composition：
Destruxins 0.4%, Acetamiprid 0.6%, pull open powder 4%, naphthalene sulfonic acid-formaldehyde condensation product 6%, ammonium sulfate 5%, breast
Agent 0201B#5%, Arabic gum 4%, surplus white carbon supply.
The preparation method of the water dispersible granules is the same as embodiment 5.
Acetamiprid in above-described embodiment is pure substance or mixture containing Acetamiprid.
Present invention can apply to prevent and treat Semiptera and lepidoptera pest, aphid, powder on the crops such as fruit tree, vegetables, tobacco
The insects such as lice, leafhopper, coccid, diamondback moth, leaf roll snout moth's larva, heart-eating worm.
Toxicity Determination of the destruxins with Acetamiprid to apple yellow aphid
Toxicity Determination uses the infusion process that FAO (Food and Agriculture Organization of the United Nation) (FAO, 1980) is recommended, by destruxins and pyridine worm
Amidine is respectively according to weight than 10:0、9:1、8:2、7:3、6:4、5:5、4:6、3:7、2:8、9:1、0:10 ratio is compounded,
And the decoction of different concentration gradients is made into deionized water, it is complete with Apple Leaves of the tweezers gripping with apple yellow aphid
Immerse in ready decoction, taken out after soaking 10s (with manual time-keeping), sop up unnecessary decoction rapidly with filter paper, then with thin
Writing brush weeds out larvae aphid and has wing adult aphid, while the aptery adult aphid by Individual Size unanimously, the apple leaf of picking to fresh and healthy
On the blade back of piece, the blade is placed in preprepared and is covered with the diameter 15cm culture dish of moisturizing filter paper, with rubber band
Seal culture dish.30 are often handled, is repeated 3 times, using deionized water as blank control；The death toll of apple yellow aphid is investigated after 48h,
Calculate the death rate, corrected mortality, LC50Value, coefficient correlation, virulence regression equation, being total to for intermixture is calculated with reference to the abundant methods of Sun Yun
Malicious coefficient CTC values.Result of the test is as shown in table 1.
The Toxicity Determination of the destruxins of table 1 and Acetamiprid to apple yellow aphid
As can be seen from Table 1, the weight proportion of destruxins and Acetamiprid is in (9~1)：It is yellow to apple in the range of (1~9)
The preventing and treating of aphid has certain synergistic function, wherein, when the two compound proportion is 8:2；5:5 and 4:When 6, co-toxicity coefficient is equal
More than 213, synergistic function is more obvious.
Field control effectiveness test of the destruxins with Acetamiprid to apple yellow aphid
In order to further verify the practical application effect of the present invention, Insecticidal combinations of the present invention have been carried out in Yuncheng
Thing prevents and treats the field control effectiveness test of apple yellow aphid, using 1% destruxins suspending agent and 3% acetamiprid EC as comparison medicament, adopts
Blade face even spraying is carried out with Singapore PJ-16 types knapsack sprayer, investigates insect population before medicine, 7d, 14d after medicine
Investigation apple yellow aphid number living, calculates preventive effect.
According to each day survival insect population number after insect population before medicine and medicine, each treatment region and control are calculated respectively by following equation
The Revision insect recluced rate and prevention effect in area.
Field control effectiveness test of the different agents of table 2 processing to apple yellow aphid
Have after destruxins it can be seen from the result of table 2 and Acetamiprid compounding to the preventive effect of apple yellow aphid preferably quick-acting
Property and lasting effect, compared with single dose, the preventive effect of 14 days can also maintain more than 80% after medicine.Wherein, after the medicine of embodiment 3 14 days it is right
For the preventive effect of apple yellow aphid up to 90.65%, prevention effect is optimal.Do not find the Pesticidal combination preparation of the present invention to apple during experiment
The beneficial organism such as fruit growing way and natural enemy has any harmful effect, at the same time, during experiment finds the Pesticidal combination of the present invention
Preparation also has certain preventive and therapeutic effect to European red mite, illustrates the Pesticidal combination of the present invention and has preferable security, is worth
The popularization and application in production.
The present invention Pesticidal combination in addition to the active ingredient (s, also containing in Pesticide formulation commonly use surfactant,
Wetting agent, dispersant, emulsifying agent, stabilizer, filler or carrier etc., and be prepared into be adapted to what is agriculturally used according to the actual requirements
Any one formulation, including but not limited to missible oil, microemulsion, aqueous emulsion, suspending agent, wettable powder and water dispersible granules etc..
It can be selected to be processed into the type of dosage form to correspond to actual needs according to the difference of controlling object, use environment etc. in specifically used.
Claims (10)
- A kind of 1. Pesticidal combination containing destruxins and Acetamiprid, it is characterised in that：The Pesticidal combination activity into Divide and be made up of destruxins and Acetamiprid, the weight ratio of the destruxins and Acetamiprid is (9~1)：(1~9).
- A kind of 2. Pesticidal combination containing destruxins and Acetamiprid according to claim 1, it is characterised in that：It is described The weight of destruxins and Acetamiprid ratio is 8:2.
- A kind of 3. Pesticidal combination containing destruxins and Acetamiprid according to claim 1, it is characterised in that：It is described The weight of destruxins and Acetamiprid ratio is 5:5.
- A kind of 4. Pesticidal combination containing destruxins and Acetamiprid according to claim 1, it is characterised in that：It is described The weight of destruxins and Acetamiprid ratio is 4:6.
- A kind of 5. Pesticidal combination containing destruxins and Acetamiprid according to claim 1, it is characterised in that：It is described Destruxins is the mixture of any one or its arbitrary proportion in destruxins A, B, C, D, E.
- 6. a kind of Pesticidal combination containing destruxins and Acetamiprid according to Claims 1 to 5 any one, it is special Sign is：The Pesticidal combination also includes assistant agent, and the total weight percent of the active component destruxins and Acetamiprid is 1 ~30%, the percentage by weight of the assistant agent is 70~99%.
- A kind of 7. Pesticidal combination containing destruxins and Acetamiprid according to claim 6, it is characterised in that：It is described The total weight percent of active component destruxins and Acetamiprid is 10~30%.
- A kind of 8. Pesticidal combination containing destruxins and Acetamiprid according to claim 1, it is characterised in that：It is described The formulation of Pesticidal combination is missible oil, microemulsion, suspending agent, wettable powder and water dispersible granules.
- 9. the application of Pesticidal combination described in claim 1-8 any one, it is characterised in that：The Pesticidal combination is applied to Prevent and treat fruit tree and vegetable-crop pest-insect.
- 10. application according to claim 9, it is characterised in that：The Pesticidal combination is applied to prevent eliminating aphis and aleyrodid.
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Cited By (1)
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Application publication date: 20180323 |