CN107817165A - A kind of device for being used to determine steel stress corrosion behavior in corrosive environment - Google Patents

A kind of device for being used to determine steel stress corrosion behavior in corrosive environment Download PDF

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Publication number
CN107817165A
CN107817165A CN201711219247.2A CN201711219247A CN107817165A CN 107817165 A CN107817165 A CN 107817165A CN 201711219247 A CN201711219247 A CN 201711219247A CN 107817165 A CN107817165 A CN 107817165A
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CN
China
Prior art keywords
inner casing
base alloy
stress corrosion
medium
corrosive
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711219247.2A
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Chinese (zh)
Inventor
白江虎
李具仓
任娟红
陈立章
马艳丽
王军宏
孙爱楠
邵建勇
周培山
宋宗亮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiayuguan Tianyuan New Material LLC
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Jiayuguan Tianyuan New Material LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiayuguan Tianyuan New Material LLC filed Critical Jiayuguan Tianyuan New Material LLC
Priority to CN201711219247.2A priority Critical patent/CN107817165A/en
Publication of CN107817165A publication Critical patent/CN107817165A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N17/00Investigating resistance of materials to the weather, to corrosion, or to light
    • G01N17/006Investigating resistance of materials to the weather, to corrosion, or to light of metals
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0017Tensile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/003Generation of the force
    • G01N2203/005Electromagnetic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0067Fracture or rupture
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/022Environment of the test
    • G01N2203/0236Other environments
    • G01N2203/024Corrosive

Abstract

The present invention relates to oil gas field testing of materials field, discloses a kind of device for being used to determine steel stress corrosion behavior in corrosive environment, and described device includes inner casing, sample holding device, corrosive medium and is passed through system;The inner casing is seal casinghousing;The sample holding device includes being arranged on bottom nickel-base alloy sample rack, the top nickel-base alloy sample rack being arranged in the middle part of inner casing of inner shell bottom, fixed stainless steel magnetized medium, the inner casing are sequentially arranged above pressure sensor, electromagnet above the top nickel-base alloy sample rack;Filled with corrosive medium in the inner casing.Test of the present invention for sample under polynary environment provides effective device, and the device ensures the stability and accuracy of volatile media concentration in etchant solution in experimentation so that the experimental result accuracy tested out is high.

Description

A kind of device for being used to determine steel stress corrosion behavior in corrosive environment
Technical field
Present invention relates particularly to oil gas field testing of materials field, relates more specifically to a kind of for determining steel in corrosion ring The device of stress corrosion behavior in border.
Background technology
In oil gas field industry, the complexity of the Service Environment change of material, cause material in use, easily lose Brittle failure etc. is imitated, and stress corrosion cracking is one kind in numerous corrosion failure behaviors, because its Producing reason is that material is corroding In environment, under conditions of certain tension, unexpected generating material brittle failure, harmfulness pole in the case of the obvious omens of Chang Wu It is big to be evaluated, it is necessary to carry out related experiment test.
Slowly strained tensile is approved as stress corrosion test and assessment method, depth by numerous scholars, but because of test device The reason for, cause corrosive medium during test not seal so that its test device is only capable of testing some corrosion Jie using being limited Matter is the material of fixedness, and test effect is undesirable, such as tests chlorion stress corrosion behavioral study, rotten for volatile-type Medium is lost, stress corrosion test evaluation can not be carried out.
The content of the invention
It is volatilizable due to having in corrosive medium to solve the stress corrosion of material under corrosion system in the prior art evaluation Gas, causes the existing experimental provision used can not carry out evaluation problem, and the present invention provides a kind of for determining steel in corrosion ring The device of stress corrosion behavior in border.
The present invention adopts the following technical scheme that:A kind of dress for being used to determine steel stress corrosion behavior in corrosive environment Put, described device includes inner casing, sample holding device, corrosive medium and is passed through system;The inner casing is seal casinghousing;The sample Clamping device includes being arranged on the bottom nickel-base alloy sample rack of inner shell bottom, the top nickel-base alloy sample being arranged in the middle part of inner casing Frame, the fixed stainless steel magnetized medium in top nickel-base alloy sample rack top;The inner casing is sequentially arranged above pressure sensor, electricity Magnet;Filled with corrosive medium in the inner casing.
Aluminium foam sandwich is set between the top nickel-base alloy sample rack and stainless steel magnetized medium.
Described device includes Research on Automatic Measuring System of Temperature, and the system includes heating wire, galvanic couple room, thermocouple, and the heating wire is set Put in corrosive medium of the inner wall outside for heating tensile sample region;Inner casing is stretched into the galvanic couple room;The thermocouple Insert galvanic couple room.
Cooling tube is set on the outside of the inner casing, and the cooling tube is arranged between stainless steel magnetized medium and inner casing top.
The heating wire on the outside of cooling tube with being respectively provided with foamed aluminium.
Shell is set on the outside of the foamed aluminium.
The present invention carries out the tension of slow strained tensile using electromagnet magnetic force, makes steel stress corrosion in corrosive environment The test of behavior can realize completion, enable in particular to ensure the high volatile corrosive medium sealing during slow strained tensile Property, security during experimenter's experiment is fully ensured that, while ensure that volatile media is dense in etchant solution in experimentation The stability and accuracy of degree so that the experimental result accuracy tested out is high.
Brief description of the drawings
Fig. 1 is apparatus of the present invention structural representation.
Symbol description
1st, electromagnet;2nd, shell;3rd, cooling water pipe;4th, pressure sensor;5th, foamed aluminium 6, inner casing;7th, at the top of inner casing;8th, corrode Medium solution;9th, top nickel-base alloy sample rack;10th, aluminium foam sandwich;11st, stainless steel magnetized medium;12nd, top sample rack fixes spiral shell Bolt;13rd, hydrogen sulfide access tube;14th, hydrogen sulfide is passed through control valve;15th, thermocouple room;16th, thermocouple;17th, discharging of waste liquid passage; 18th, discharging of waste liquid control valve;19th, carbon dioxide access tube;20th, carbon dioxide is passed through control valve;21st, sodium carbonate liquor is passed through Hole;22nd, sodium carbonate liquor is passed through control valve;23rd, bottom nickel-base alloy sample rack;24th, bottom sample rack fixing bolt;25th, sample is solid Clamp;26th, heating wire;27th, tensile sample;28th, fixing bolt at the top of inner casing.
Embodiment
The invention will be further described with reference to the accompanying drawings and detailed description.
A kind of device for being used to determine steel stress corrosion behavior in corrosive environment, described device include inner casing 6, sample Clamping device, corrosive medium are passed through system;The inner casing is seal casinghousing;The sample holding device includes being arranged on inner casing 6 The bottom nickel-base alloy sample rack 23 of bottom, the top nickel-base alloy sample rack 9 for being arranged on the middle part of inner casing 6, the top nickel-base alloy sample The fixed stainless steel magnetized medium 11 in the top of frame 9, the inner casing 6 is sequentially arranged above pressure sensor 4, electromagnet 1;The inner casing It is interior filled with corrosive medium.
Because etchant gas is difficult to control in test process, usually there is leakage problem in the test of sample in tradition, Jeopardize staff's health, make sample can not complete to test in such circumstances.Based on this, the present invention innovatively use by Electromagnet 1, pressure sensor 4 and the three of stainless steel magnetized medium 11 are used cooperatively, to test energy of the sample under corrosive environment It is enough to realize.
Aluminium foam sandwich 10 is set between the top nickel-base alloy sample rack 9 and stainless steel magnetized medium 11.The top, Bottom nickel-base alloy sample rack 9,23 fixes sample bottom, it is further preferred that setting examination in upper and lower part nickel-base alloy sample rack 23 Sample geometrical clamp 25, sample is fixed on top nickel-base alloy sample rack 9 and bottom nickel-base alloy respectively with two sample fixation clamps 25 In sample rack 23, aluminium foam sandwich 10 is loaded in top nickel-base alloy sample rack 9, stainless steel magnetized medium 11 is put above, uses top Sample rack fixing bolt 12 connects top nickel-base alloy sample rack 9, aluminium foam sandwich 10 and stainless steel magnetized medium 11.Foam Aluminium interlayer 10 is located among stainless steel casing 2 and nickel-base alloy inner casing 6, plays insulation separated magnetic effect, and whole sealing system plays envelope Fill the effect of corrosive medium.
Described device includes Research on Automatic Measuring System of Temperature, and the system includes heating wire 26, galvanic couple room 15, thermocouple 16, the electricity Heated filament 26 is arranged on the corrosive medium that inner wall outside is used to heat tensile sample region;Inner casing is stretched into the galvanic couple room 15; The thermocouple 16 inserts galvanic couple room 15, by passing through temperature feedback control heating wire 26 so that test temperature is balanced.
Cooling tube 3 is set on the outside of the inner casing, the cooling tube 3 be arranged at the top of stainless steel magnetized medium 11 and inner casing 7 it Between, cooling water pipe 3 keeps inner casing upper temp in room temperature state.Inner casing upper temp is set in room temperature state to be to ensure top Electromagnet and stainless steel magnetic conduction between magnetic field and electromagnetic force be affected by temperature, temperature is too high to be caused under electromagnetic force Drop, can cause to stretch hypodynamic state.
The heating wire 26 is respectively provided with foamed aluminium 5 with the outside of cooling tube 3., can using foamed aluminium every magnetic and heat insulating ability Ensure experimenter's electromagnetic radiation, and can ensure that the holding of the temperature of sample local environment is stable.
The outside of foamed aluminium 5 sets shell 2.
The course of work:Open 7 at the top of inner casing, tensile sample 27 is fixed on bottom nickel-base alloy sample with sample fixation clamp 25 On frame, pour into the solution of sodium chloride-containing and be fixed on tensile sample 27 in nickel-base alloy inner casing 6, then with sample fixation clamp 25 In portion's nickel-base alloy sample rack 9, aluminium foam sandwich 10 is loaded in top nickel-base alloy sample rack 9, puts stainless steel magnetized medium above 11, top nickel-base alloy sample rack 9, aluminium foam sandwich 10 and stainless steel magnetized medium 11 are connected with top sample rack fixing bolt 12 Get up;The solution of sodium chloride-containing is poured into again, is covered 7 at the top of inner casing, is sealed with 7 fixing bolts at the top of inner casing close;7 at the top of inner casing On bleed off pressure force snesor 4, discharge magnet 1 on pressure sensor 4.
Open sodium carbonate liquor to be passed through control valve 22, be passed through nitrogen at sodium carbonate liquor access apertures 21, remove corrosion and be situated between Oxygen in matter;Closing control valve 22 opens hydrogen sulfide and is passed through control valve 14, is passed through in hydrogen sulfide on entrance 13 and is passed through hydrogen sulfide;Beat Open carbon dioxide and be passed through control valve 20, carbon dioxide is passed through in carbon dioxide access apertures 19.Keep the pressure and two of hydrogen sulfide Carbon oxide pressure, form ternary corrosion system.
Thermocouple 16 is inserted in thermocouple room 15, the heating of the galvanization of heating wire 26, passes through temperature feedback control heating wire 26 so that test temperature reaches requirement of experiment, while opens cooling water pipe 3 and keep upper temp in room temperature state.
Electromagnet 1 is powered, and magnetization stainless steel magnetized medium 11, attracts stainless steel magnetized medium 11, and then drive top nickel Based alloy sample rack 9 pulls tensile sample 27, it is stressed corrosion in corrosive medium by tension, is sensed by power The electric current of the feedback regulation electromagnet 1 of device 4 and then the suction for controlling electromagnet;And force value and record force value are set.
After tensile sample 27 is broken, closing hydrogen sulfide is passed through control valve 14 and carbon dioxide is passed through control valve 20, opens useless Liquid exhaust-control valve 18, drained into discharging of waste liquid hole 17 by waste liquid is corroded in sodium carbonate liquor or in sodium hydroxide solution;Wait to hold When corrosive medium in device is drained soon, opens sodium carbonate liquor and be passed through control valve 22, it is molten to the sodium carbonate that is passed through a small amount of in device Liquid, then by discharging of waste liquid hole 17 exclude waste liquid, after such 5-6 time, can opening apparatus, remove tensile sample 27, carry out fracture divide Analysis.
Because oil gas field corrosive environment is complex, multiclass corrosive medium is frequently accompanied by, is influenced each other, to the stress of material Corrosion evaluation proposes higher requirement, and H2S、CO2、Cl-Corrosion as mainly several corrosive environments, its composition Corrosive medium system H2S-CO2-Cl-The stress corrosion evaluation of material is volatilizable due to having in corrosive medium under ternary corrosion system H2S and CO2It gas, can not seal, cause the existing experimental provision used not evaluated, cause H2S-CO2-Cl-Ternary is rotten The difficulty that material selection under erosion system becomes, present invention is particularly suitable for H2S-CO2-Cl-Ternary corrosion system.
When corrosive medium is H2S-CO2-Cl-During ternary corrosion system, the corrosive medium is passed through system by corrosive medium Into inner casing 6.The corrosive medium is passed through system and is passed through including carbon dioxide access tube 20, discharging of waste liquid passage 17, hydrogen sulfide Pipe 13, sodium carbonate liquor access tube 21, the corrosive medium is passed through system, and to be arranged on top nickel-base alloy sample rack 9 Ni-based with bottom Between alloy sample rack 23;Carbon dioxide is set to be passed through control valve 20 on the carbon dioxide access tube 20;Hydrogen sulfide access tube 13 Upper setting hydrogen sulfide is passed through control valve 14;Sodium carbonate liquor is set to be passed through control valve 22 on sodium carbonate liquor access tube 21;Waste liquid Discharging of waste liquid control valve 18 is set on discharge-channel 17.
The present invention carries out the tension of slow strained tensile using electromagnet magnetic force, it is ensured that during slow strained tensile High volatile corrosive medium sealing, security during experimenter's experiment is fully ensured that, while ensured rotten in experimentation Lose the stability and accuracy of volatile media concentration in solution so that the experimental result tested out has accuracy;Utilize bubble Foam aluminium every magnetic and heat insulating ability, it is ensured that experimenter's electromagnetic radiation, and the holding of the temperature of sample local environment can be ensured It is stable;The present invention can carry out material and download H in different temperatures, various concentrations condition2S-CO2-Cl-The stress of ternary corrosion system Corrosion test and evaluation, different temperatures, the polynary sulfide hydrogen of various concentrations complicated condition can not be carried out by overcoming other equipment Stress corrosion is tested, wide adaptability.

Claims (6)

1. a kind of device for being used to determine steel stress corrosion behavior in corrosive environment, it is characterised in that described device includes Inner casing(6), sample holding device, corrosive medium be passed through system;The inner casing(6)For seal casinghousing;The sample holding device Including being arranged on inner casing(6)The bottom nickel-base alloy sample rack of bottom(23), be arranged on inner casing(6)The top nickel-base alloy sample at middle part Frame(9), the top nickel-base alloy sample rack(9)Stainless steel magnetized medium is fixed in top(11);The inner casing(6)It is sequentially arranged above Pressure sensor(4), electromagnet(1);The inner casing(6)It is interior filled with corrosive medium.
2. the device according to claim 1 for being used to determine steel stress corrosion behavior in corrosive environment, its feature exist In the top nickel-base alloy sample rack(9)With stainless steel magnetized medium(11)Between aluminium foam sandwich is set(10).
3. the device according to claim 1 for being used to determine steel stress corrosion behavior in corrosive environment, its feature exist In described device includes Research on Automatic Measuring System of Temperature, and the system includes heating wire(26), galvanic couple room(15), thermocouple(16), the electricity Heated filament(26)It is arranged on the corrosive medium that inner wall outside is used to heat tensile sample region;The galvanic couple room(15)In stretching into Shell;The thermocouple(16)Insert galvanic couple room(15).
4. the device according to claim 1 for being used to determine steel stress corrosion behavior in corrosive environment, its feature exist In setting cooling tube on the outside of the inner casing(3), the cooling tube(3)It is arranged on stainless steel magnetized medium(11)With inner casing top(7) Between.
5. the device according to claim 1 for being used to determine steel stress corrosion behavior in corrosive environment, its feature exist In the heating wire(26)With cooling tube(3)Outside is respectively provided with foamed aluminium(5).
6. the device according to claim 1 for being used to determine steel stress corrosion behavior in corrosive environment, its feature exist In the foamed aluminium(5)Outside sets shell(2).
CN201711219247.2A 2017-11-28 2017-11-28 A kind of device for being used to determine steel stress corrosion behavior in corrosive environment Pending CN107817165A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108760550A (en) * 2018-05-17 2018-11-06 郝文峰 The experimental provision that material internal deforms under a kind of measurement corrosive environment
CN110361260A (en) * 2018-04-11 2019-10-22 上海航空材料结构检测股份有限公司 Stress corrosion testing device and test method of the thick sample in Strong oxdiative solution
CN111795923A (en) * 2020-08-24 2020-10-20 兰州金川科力远电池有限公司 Method for rapidly testing corrosion resistance of hydrogen storage alloy powder
CN112198048A (en) * 2020-12-07 2021-01-08 南京仪汇仪器设备有限公司 Textile fiber strength detection equipment

Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2320545A1 (en) * 1975-08-06 1977-03-04 Sulzer Ag Environmental testing of materials - uses electromagnetic nonmechanical drive to control tester in isolated environmental chamber
FR2366558A1 (en) * 1976-09-30 1978-04-28 Saint Etienne Fondation Ind Mi Accelerated tests for corrosion - are performed in corrosive atmosphere with strain force and temp. applied to sample
EP0195735A1 (en) * 1985-02-21 1986-09-24 Institut De Recherches De La Siderurgie Francaise (Irsid) Machine for the tension testing of metallic specimens in an enclosure
JPH0892677A (en) * 1994-09-27 1996-04-09 Sumitomo Metal Ind Ltd Nickel-based alloy excellent in corrosion resistance in high temperature water
CN201348587Y (en) * 2009-01-20 2009-11-18 兰州大学 Magnetic suspension direct tensile test device
WO2009157808A2 (en) * 2008-06-23 2009-12-30 Tuzhikov Oleg Olegovich Method for determining the service life of structural materials under aggressive conditions and a device for carrying out said method
CN201555795U (en) * 2009-11-03 2010-08-18 中国船舶重工集团公司第七二五研究所 Device applied to high-temperature stress corrosion test of large-size sample
CN103592176A (en) * 2013-11-19 2014-02-19 南京工业大学 Electromagnetic loading device for concrete durability test
CN103926146A (en) * 2014-04-11 2014-07-16 西南石油大学 Constant-load stress corrosion testing device of small test sample and testing method thereof
CN105388101A (en) * 2015-12-02 2016-03-09 中国石油天然气集团公司 Combined-loading stress corrosion testing apparatus and method
CN106323784A (en) * 2016-08-05 2017-01-11 中国船舶重工集团公司第七二五研究所 Intermittent immersion corrosion test method and device based on slow tensile stress corrosion testing machine
CN106442136A (en) * 2016-10-18 2017-02-22 北京科技大学 Device for testing stress corrosion behavior of metal material under fluid high pressure
CN106501162A (en) * 2016-11-02 2017-03-15 西南石油大学 A kind of High Temperature High Pressure dynamic galvanic corrosion experimental technique and device
CN106769474A (en) * 2017-01-14 2017-05-31 常州大学 Loading biaxial tension stress sample Experiment in Erosive Electrochemistry device and method of testing

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2320545A1 (en) * 1975-08-06 1977-03-04 Sulzer Ag Environmental testing of materials - uses electromagnetic nonmechanical drive to control tester in isolated environmental chamber
FR2366558A1 (en) * 1976-09-30 1978-04-28 Saint Etienne Fondation Ind Mi Accelerated tests for corrosion - are performed in corrosive atmosphere with strain force and temp. applied to sample
EP0195735A1 (en) * 1985-02-21 1986-09-24 Institut De Recherches De La Siderurgie Francaise (Irsid) Machine for the tension testing of metallic specimens in an enclosure
JPH0892677A (en) * 1994-09-27 1996-04-09 Sumitomo Metal Ind Ltd Nickel-based alloy excellent in corrosion resistance in high temperature water
WO2009157808A2 (en) * 2008-06-23 2009-12-30 Tuzhikov Oleg Olegovich Method for determining the service life of structural materials under aggressive conditions and a device for carrying out said method
CN201348587Y (en) * 2009-01-20 2009-11-18 兰州大学 Magnetic suspension direct tensile test device
CN201555795U (en) * 2009-11-03 2010-08-18 中国船舶重工集团公司第七二五研究所 Device applied to high-temperature stress corrosion test of large-size sample
CN103592176A (en) * 2013-11-19 2014-02-19 南京工业大学 Electromagnetic loading device for concrete durability test
CN103926146A (en) * 2014-04-11 2014-07-16 西南石油大学 Constant-load stress corrosion testing device of small test sample and testing method thereof
CN105388101A (en) * 2015-12-02 2016-03-09 中国石油天然气集团公司 Combined-loading stress corrosion testing apparatus and method
CN106323784A (en) * 2016-08-05 2017-01-11 中国船舶重工集团公司第七二五研究所 Intermittent immersion corrosion test method and device based on slow tensile stress corrosion testing machine
CN106442136A (en) * 2016-10-18 2017-02-22 北京科技大学 Device for testing stress corrosion behavior of metal material under fluid high pressure
CN106501162A (en) * 2016-11-02 2017-03-15 西南石油大学 A kind of High Temperature High Pressure dynamic galvanic corrosion experimental technique and device
CN106769474A (en) * 2017-01-14 2017-05-31 常州大学 Loading biaxial tension stress sample Experiment in Erosive Electrochemistry device and method of testing

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110361260A (en) * 2018-04-11 2019-10-22 上海航空材料结构检测股份有限公司 Stress corrosion testing device and test method of the thick sample in Strong oxdiative solution
CN108760550A (en) * 2018-05-17 2018-11-06 郝文峰 The experimental provision that material internal deforms under a kind of measurement corrosive environment
CN111795923A (en) * 2020-08-24 2020-10-20 兰州金川科力远电池有限公司 Method for rapidly testing corrosion resistance of hydrogen storage alloy powder
CN112198048A (en) * 2020-12-07 2021-01-08 南京仪汇仪器设备有限公司 Textile fiber strength detection equipment

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