CN107805942A - 一种季醚铵酯柔软剂及其制备方法 - Google Patents

一种季醚铵酯柔软剂及其制备方法 Download PDF

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CN107805942A
CN107805942A CN201711119575.5A CN201711119575A CN107805942A CN 107805942 A CN107805942 A CN 107805942A CN 201711119575 A CN201711119575 A CN 201711119575A CN 107805942 A CN107805942 A CN 107805942A
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ether ammonium
ammonium ester
softening agent
season
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方国健
潘伟丽
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Huzhou Nanxun Jinjibao Textile Co Ltd
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Huzhou Nanxun Jinjibao Textile Co Ltd
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

本发明公开了一种季醚铵酯柔软剂，按质量份计，包含氨基硅油25～35份、季醚铵酯45～50份、羟苯甲酸甲酯2～6份、对羟苯甲酸丁酯1～3份、香料1～5份和去离子水150～200份。本发明可以适用于纯棉面料，能有效提高纯棉面料的柔软度，且不会对面料造成损伤。

Description

一种季醚铵酯柔软剂及其制备方法
技术领域
本发明涉及一种季醚铵酯柔软剂，属于纺织处理技术领域。
背景技术
织物经过前处理和一系列染整加式后，由于去除了天然油脂蜡质，往往会降低其原有的平滑感，使手感变得粗糙。另外，有些织物需经过高温处理，如树脂整理，合纤的热定型、腈纶的汽蒸膨化以及涂料印花等，也会使织物手感变得粗硬。大部分合纤织物以及纯毛、棉绒织物经洗涤或肥皂洗后，都有变硬、手感粗糙，穿着不舒服等问题，为了克服这个缺点，就需要使用柔软剂来加以改善。随着合纤织物发发展，人们对织物的柔软整理要求日益迫切，柔软剂的重要性也就显得尤为重要。
发明内容
本发明的目的在于，提供一种季醚铵酯柔软剂。它可以适用于纯棉面料，能有效提高纯棉面料的柔软度，且不会对面料造成损伤。
本发明的技术方案：一种季醚铵酯柔软剂，其特点是,按质量份计，包含氨基硅油25～35份、季醚铵酯45～50份、羟苯甲酸甲酯2～6份、对羟苯甲酸丁酯1～3份、香料1～5份和去离子水150～200份。
前述的季醚铵酯柔软剂中，作为优选，按质量份计，包含氨基硅油28～32份、季醚铵酯47～48份、羟苯甲酸甲酯3～4份、对羟苯甲酸丁酯2～3份、香料3～4份和去离子水170～180份。
前述的季醚铵酯柔软剂的制备方法是：将去离子水加热到60℃,缓慢加入醚铵酯、羟苯甲酸甲酯和对羟苯甲酸丁酯，使用搅拌器，在300rpm速度下混合10～15分钟,以每分钟1℃的速度冷却到25℃，加入氨基硅油和香料,使用搅拌器，在250rpm速度下混合25～30分钟。
与现有技术相比，本发明利用季醚铵酯柔软剂对纯棉面料进行处理，能有效在纯棉面料上附着亲水基团，从而能够有效降低纯棉面料表面摩擦力，提高纯棉面料的柔软性能。而且本发明的柔软剂的自然降解能力强，更加绿色环保。
具体实施方式
下面结合实施例对本发明作进一步的说明，但并不作为对本发明限制的依据。
实施例。一种季醚铵酯柔软剂，按质量份计，包含氨基硅油25～35份、季醚铵酯45～50份、羟苯甲酸甲酯2～6份、对羟苯甲酸丁酯1～3份、香料1～5份和去离子水150～200份。作为优选，所述季醚铵酯柔软剂，按质量份计，包含氨基硅油28～32份、季醚铵酯47～48份、羟苯甲酸甲酯3～4份、对羟苯甲酸丁酯2～3份、香料3～4份和去离子水170～180份。所述季醚铵酯柔软剂的制备方法是：将去离子水加热到60℃,缓慢加入醚铵酯、羟苯甲酸甲酯和对羟苯甲酸丁酯，使用搅拌器，在300rpm速度下混合10～15分钟,以每分钟1℃的速度冷却到25℃，加入氨基硅油和香料,使用搅拌器，在250rpm速度下混合25～30分钟，该方法制备的季醚铵酯柔软剂分散度高，黏度可低至30cps，配制增柔液时分散更快。
本发明的季醚铵酯柔软剂的使用实例，将季醚铵酯柔软剂以3％～5％质量百分比混合在水中，形成增柔液，将纯棉面料在40℃～60℃下，采用浴比30:1的方式，浸泡在增柔液中30分钟，离心脱水后，在100℃～120℃下干燥。

Claims (3)

1.一种季醚铵酯柔软剂，其特征在于：按质量份计，包含氨基硅油25～35份、季醚铵酯45～50份、羟苯甲酸甲酯2～6份、对羟苯甲酸丁酯1～3份、香料1～5份和去离子水150～200份。
2.根据权利要求1所述的季醚铵酯柔软剂，其特征在于：按质量份计，包含氨基硅油28～32份、季醚铵酯47～48份、羟苯甲酸甲酯3～4份、对羟苯甲酸丁酯2～3份、香料3～4份和去离子水170～180份。
3.根据权利要求1或2所述的季醚铵酯柔软剂的制备方法，其特征在于：将去离子水加热到60℃,缓慢加入醚铵酯、羟苯甲酸甲酯和对羟苯甲酸丁酯，使用搅拌器，在300rpm速度下混合10～15分钟,以每分钟1℃的速度冷却到25℃，加入氨基硅油和香料,使用搅拌器，在250rpm速度下混合25～30分钟。
CN201711119575.5A 2017-11-14 2017-11-14 一种季醚铵酯柔软剂及其制备方法 Withdrawn CN107805942A (zh)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736580A (zh) * 2009-12-21 2010-06-16 北京绿泽宇和科技有限公司 一种织物保养柔顺剂
CN104153199A (zh) * 2014-05-27 2014-11-19 北京洛娃日化有限公司 一种织物抗皱精华液
CN106521943A (zh) * 2016-11-29 2017-03-22 湖南日用化学科学研究所有限公司 一种洗衣房专用液体织物柔软剂及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736580A (zh) * 2009-12-21 2010-06-16 北京绿泽宇和科技有限公司 一种织物保养柔顺剂
CN104153199A (zh) * 2014-05-27 2014-11-19 北京洛娃日化有限公司 一种织物抗皱精华液
CN106521943A (zh) * 2016-11-29 2017-03-22 湖南日用化学科学研究所有限公司 一种洗衣房专用液体织物柔软剂及其制备方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
倪捷: ""织物用柔软剂的现状和发展新课题"", 《上海染料》 *
魏代军 等: ""3-椰油烷氧基丙胺合成工艺的研究"", 《中国洗涤用品工业》 *

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