CN107802028A - A kind of multifunction tobacco humectant and preparation method thereof - Google Patents
A kind of multifunction tobacco humectant and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
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- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/42—Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
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Abstract
The invention discloses a kind of multifunction tobacco humectant and preparation method thereof, belong to technical field of tobacco processing.Diatom, spirulina, Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are stirred by the present invention, obtain mixed liquor；Add ethanol solution into mixed liquor, chitosan liquid, animal charred bone meal, plants essential oil and dopamine solution be stirred, and obtains mixed slurry；Hydrogen peroxide is added dropwise into above-mentioned gained mixed slurry, produces multifunction tobacco humectant.Multifunction tobacco humectant provided by the invention has excellent water retention property, during the burning and sucking of cigarette, reduces harmful substance and injury, and tobacco comfortable taste are produced to human body.
Description
Technical field
The invention discloses a kind of multifunction tobacco humectant and preparation method thereof, belong to technical field of tobacco processing.
Background technology
Tobacco leaf is loose porous material, and from thermodynamically saying, it is higher that it absorbs the potentiality of moisture.Just because of tobacco leaf material
The porosity characteristic of material, scattered and disappeared also comparatively fast, so as to cause in higher temperature and compared with low humidity, free moisture, capillary water grade
Cigarette is relatively easy to drying.In cigarette products production process, addition humectant is able to maintain that moisture in cut tobacco, improves its physics guarantor
Lubricant nature energy.At present, conventional humectant is the polyols such as propane diols, glycerine, diethylene glycol (DEG), sorbierite.However, glycerine and
Though the humid keeping performance of propane diols is good, not ideal for the improvement of cigarette sensory quality.In recent years, have developed a variety of
New humectant substitutes traditional humectant, while cigarette interior quality is improved, can also reduce to health
Harm, this meets the trend that humectant develops in tobacco business.
Dynamic water adsorption analysis technology（DVS）It is the Main Means for studying material moisture absorption or the wet behavior of solution, general principle
It is in setting relative humidity（RH）Measured matter quality is studied in environment, temperature programming or thermostatic process to change with time rule
Rule.At present, the multiple fields such as pharmacy, food, biomaterial are widely used to.The Integration ofTechnology high accuracy balance, temperature control
The superior functionalitys such as scope is wide, the wet ability of control is strong, automatization level is high, are advantageous to establish the constant environmental monitoring tobacco sample of humiture
The trickle change of moisture in product.This method is simple and easy to do, and reliable and stable, helps to analyze different type humectant and cigarette is former
Expect the difference in terms of the physics humid keeping performance.The physics humectation of cigarette is relevant with its equilibrium moisture content, microstructure etc., all
It is to judge a whether qualified important indicator of cigarette finished product.At present, on tobacco product physics humectation detection method also
Report is had no, we also need further to study tobacco humectant, using dynamic water adsorption analysis technology（DVS）To cigarette
The physics humid keeping performance of silk is analyzed and researched, and compares variety classes humectant in pipe tobacco equilibrium moisture content, surface micro-structure, mistake
The otherness of the physics humectation effect such as water rate and the wet behavior of isothermal absorption-solution, it is intended to for the exploitation of related tobacco humectant from now on
Research with humectation technology provides theoretical reference.
The content of the invention
The present invention solves the technical problem of：For traditional tobacco humectant water retention property it is bad the problem of, there is provided
A kind of multifunction tobacco humectant and preparation method thereof.
In order to solve the above-mentioned technical problem, the technical solution adopted in the present invention is：
A kind of multifunction tobacco humectant, is made up of the raw material of following parts by weight：20~30 portions of diatoms, 20~30 parts of spirals
Algae, 10~20 parts of Fruit peel extracts, 10~20 parts of ivy extract solutions, 10~20 parts of Flos Lonicerae extractive solutions, 8~10 parts of dioxygens
Water, 10~20 parts of ethanol solutions, 50~60 parts of water, 10~20 parts of chitosan liquid, 10~20 parts of animal charred bone meals, 10~20 parts
Plants essential oil, 8~10 parts of dopamine solutions；
The preparation process of the multifunction tobacco humectant is：
（1）Each raw material is weighed by raw material composition；
（2）Diatom, spirulina, Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are stirred, must be mixed
Liquid；
（3）Ethanol solution, chitosan liquid, animal charred bone meal, plants essential oil and dopamine solution stirring are added into mixed liquor
Mixing, obtains mixed slurry；
（4）Hydrogen peroxide is added dropwise into above-mentioned gained mixed slurry, produces multifunction tobacco humectant.
The diatom is any one in chrysophyceae or bulk kelp.
The spirulina is blunt top spirulina, any one in spirulina maxim and India's spirulina.
The preparation process of the Fruit peel extract is：Pericarp is dried, crushes, obtains dry pericarp powder；Gained is dried
Pericarp powder and water in mass ratio 1：50~1：100 heating stirrings mix, and filtering, obtain Fruit peel extract；The pericarp is apple
Skin, any one in peach skin or pear skin.
The preparation process of the ivy extract solution is：Ivy is dried, crushes, obtains dry ivy powder；By institute
Ivy powder and water in mass ratio 1 must be dried：50~1：100 heating stirrings mix, and filtering, obtain ivy extract solution.
The preparation process of the Flos Lonicerae extractive solution is：Honeysuckle is dried, crushes, obtains dry Honeysuckle Flower；By institute
Honeysuckle Flower and water in mass ratio 1 must be dried：50~1：100 heating stirrings mix, and filtering, obtain Flos Lonicerae extractive solution.
The preparation process of the chitosan liquid is：By chitosan and water in mass ratio 1：50~1：After 100 mixing swellings, add
Thermal agitation is dissolved, and produces chitosan liquid.
The animal charred bone meal preparation process is：By Animal Bone ball mill grinding, sieving, nitrogen charging insulation charing, produce dynamic
Thing charred bone meal；The Animal Bone is pig bone, any one in ox bone or chicken bone.
The plants essential oil is refined jasmine oil, any one in camellia essential oil or rose ethereal oil.
The beneficial effects of the invention are as follows：
（1）The present invention is by adding diatom, spirulina and dopamine solution, first, because containing a large amount of active groups in dopamine,
In mixed process, it is adsorbed in tobacco leaf surface hole so that tobacco leaf surface hole is rich in active group, secondly, because diatom has
Amphitrichous, spirulina is in thread, then is acted on through hydrogen peroxide oxidation, and diatom and spirulina are killed, therefore part diatom and spirulina
Corpse can be embedded in tobacco leaf surface hole, and the tubular structure of diatom and spirulina will stay in tobacco leaf surface, by tobacco leaf table
Face forms a large amount of similar tubulose string structures so that and the moisture in tobacco leaf slowly oozes out, and reaches good water retention,
Meanwhile frustule is cladded with siliceous containing a large amount of active groups, by the oxidation of hydrogen peroxide, active group is further lifted
Activity so that the hydrophilic radical increase in system, further enhance the water retention property of system, and the tubulose of diatom and spirulina
Structure can absorb caused harmful substance during the burning and sucking of cigarette；
（2）The present invention is by adding Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and plants essential oil, pericarp extraction
Liquid, spring rattan extract solution, Flos Lonicerae extractive solution all have good humid keeping performance, on the one hand, Fruit peel extract, spring rattan extract solution,
Active ingredient has higher self-ignition point in Flos Lonicerae extractive solution, will not directly be evaporated during the burning and sucking of cigarette, most of
Can completely burned, harmful substance will not be produced, also it is avoided that harm of smoking material enters human body, on the other hand, plants essential oil from
Burning-point is relatively low, and most plants essential oil absorbs the heat of the overwhelming majority during the burning and sucking of cigarette, and is burning and sucking cigarette
Distillation zone takes the lead in evaporating, and avoids because Fruit peel extract, spring rattan extract solution, Flos Lonicerae extractive solution are burning and sucking the distillation zone rate of cigarette
First evaporate and do not generate harmful substance by completely burned, meanwhile, plants essential oil evaporation, cigarette perfume can be enriched, improve relaxing for tobacco
Appropriateness；
（3）The present invention is by adding animal charred bone meal, and animal charred bone meal has certain water retention property, by adding DOPA
Amine aqueous solution, contain a large amount of active groups in dopamine, be adsorbed in animal charred bone meal, during the burning and sucking of cigarette, pass through
Dopamine absorption property is good, the generation material during result of combustion of tobacco can be fixed in charred bone meal, avoid harmful substance
Into human body, the injury to caused by human body is reduced.
Embodiment
Pericarp is placed in baking oven and dries 1~2h, obtains dry pericarp, then is placed in pericarp is dried in ball mill, in rotating speed
Under the conditions of 600~700r/min, 40~50min is crushed, obtains dry pericarp powder；Gained is dried into pericarp powder and presses matter with water
Measure ratio 1：50~1：100 add in No. 1 beakers, and No. 1 beaker then is placed in into digital display tests the speed in constant temperature blender with magnetic force, in temperature
For 50~60 DEG C, under the conditions of rotating speed is 400~500r/min, after heating stirring mixes 40~50min, filtering, pericarp extraction is obtained
Liquid；Ivy is placed in baking oven and dries 1~2h, obtains dry ivy, then is placed in ivy is dried in ball mill, in rotating speed
Under the conditions of 600~700r/min, 40~50min is crushed, obtains dry ivy powder；Gained is dried into ivy powder and water
In mass ratio 1：50~1：100 add in No. 2 beakers, and No. 2 beakers then are placed in into digital display tests the speed in constant temperature blender with magnetic force, in
Temperature is 50~60 DEG C, under the conditions of rotating speed is 400~500r/min, after heating stirring mixes 40~50min, and filtering, get Chang Chun
Rattan extract solution；Honeysuckle is placed in baking oven and dries 1~2h, obtains dry honeysuckle, then is placed in honeysuckle is dried in ball mill,
Under the conditions of rotating speed is 600~700r/min, 40~50min is crushed, obtains dry Honeysuckle Flower；Gained is dried into honeysuckle powder
End and water in mass ratio 1：50~1：100 add in No. 3 beakers, and No. 3 beakers then are placed in into digital display tests the speed temperature constant magnetic stirring
In device, it is 50~60 DEG C in temperature, under the conditions of rotating speed is 400~500r/min, after heating stirring mixes 40~50min, filters,
Obtain Flos Lonicerae extractive solution；By chitosan and water in mass ratio 1：50~1：100 add in No. 4 beakers, are stirred with glass bar
After 20~30min, stand 3~4h of swelling, then No. 4 beakers moved into digital displays and tested the speed constant temperature blender with magnetic force, in temperature be 95~
100 DEG C, under the conditions of rotating speed is 400~500r/min, heating stirring dissolves 40~50min, produces chitosan liquid；By Animal Bone ball
In grinding machine, under the conditions of rotating speed is 400~500r/min, after ball mill grinding, the sieve of 50~60 mesh is crossed, obtains Animal Bone powder, will
Animal Bone powder is placed in retort, and argon gas is filled with into stove with 50~60mL/min, under the conditions of temperature is 450~600 DEG C,
Under nitrogen protective condition, insulation 1~2h of charing, animal charred bone meal is produced；Count in parts by weight, take 20~30 parts of silicon successively
Algae, 20~30 parts of spirulinas, 10~20 parts of Fruit peel extracts, 10~20 parts of ivy extract solutions, 10~20 parts of honeysuckle extractions
Liquid, 8~10 parts of mass fractions are 20~30% hydrogen peroxide, and 10~20 parts of mass fractions are 40~50% ethanol solutions, 50~60 parts
Water, 10~20 parts of chitosan liquid, 10~20 parts of animal charred bone meals, 10~20 parts of plants essential oils, 8~10 parts of mass concentrations are
2g/L dopamine solution, first diatom, spirulina, Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are added
In three-necked flask, under the conditions of rotating speed is 400~500r/min, 50~60min is stirred, obtains mixed liquor；Burnt again to three mouthfuls
It is 40~50% ethanol solutions that mass fraction is added in bottle, and chitosan liquid, animal charred bone meal, plants essential oil and mass concentration are
2g/L dopamine solutions are stirred, and obtain mixed slurry；Then with constant pressure funnel with 2.5~3.3mL/min speed to
It is 20~30% hydrogen peroxide that mass fraction is added dropwise in three-necked flask, produces multifunction tobacco humectant.The diatom is chrysophyceae or huge
Any one in algae.The spirulina is blunt top spirulina, any one in spirulina maxim and India's spirulina.It is described
Pericarp is apple skin, any one in peach skin or pear skin.The Animal Bone is pig bone, any one in ox bone or chicken bone.
The plants essential oil is refined jasmine oil, any one in camellia essential oil or rose ethereal oil.
Example 1
Pericarp is placed in baking oven and dries 2h, obtains dry pericarp, then is placed in pericarp is dried in ball mill, in rotating speed be 700r/
Under the conditions of min, 50min is crushed, obtains dry pericarp powder；Gained is dried into pericarp powder and water in mass ratio 1：100 add No. 1
In beaker, No. 1 beaker is then placed in digital display and tested the speed in constant temperature blender with magnetic force, in temperature be 60 DEG C, rotating speed 500r/min
Under the conditions of, after heating stirring mixing 50min, filtering, obtain Fruit peel extract；Ivy is placed in baking oven and dries 2h, obtains drying
Ivy, then be placed in ivy is dried in ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Chang Chun
Rattan powder；Gained is dried into ivy powder and water in mass ratio 1：100 are added in No. 2 beakers, and No. 2 beakers then are placed in into number
In the aobvious constant temperature blender with magnetic force that tests the speed, in temperature be 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min,
Filtering, obtains ivy extract solution；Honeysuckle is placed in baking oven and dries 2h, obtains dry honeysuckle, then be placed in honeysuckle is dried
In ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Honeysuckle Flower；Gained is dried into honeysuckle powder
End and water in mass ratio 1：100 add in No. 3 beakers, and No. 3 beakers then are placed in into digital display tests the speed in constant temperature blender with magnetic force, in
Temperature is 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min, filtering, obtains Flos Lonicerae extractive solution；By shell
Glycan and water in mass ratio 1：100 add in No. 4 beakers, after being stirred 30min with glass bar, stand swelling 4h, then by No. 4
Beaker moves into digital display and tested the speed constant temperature blender with magnetic force, is 100 DEG C in temperature, under the conditions of rotating speed is 500r/min, heating stirring is molten
50min is solved, produces chitosan liquid；By in Animal Bone ball mill, under the conditions of rotating speed is 500r/min, after ball mill grinding, 60 are crossed
Purpose is sieved, and obtains Animal Bone powder, Animal Bone powder is placed in retort, argon gas is filled with into stove with 60mL/min, in temperature
Under the conditions of 600 DEG C, under nitrogen protective condition, insulation charing 2h, animal charred bone meal is produced；Count in parts by weight, successively
Take 30 portions of diatoms, 30 parts of spirulinas, 20 parts of Fruit peel extracts, 20 parts of ivy extract solutions, 20 parts of Flos Lonicerae extractive solutions, 10 parts of matter
Amount fraction is 30% hydrogen peroxide, and 20 parts of mass fractions are 50% ethanol solution, 60 parts of water, 20 parts of chitosan liquid, 20 parts of animals charings
Bone meal, 20 parts of plants essential oils, 10 parts of mass concentrations are 2g/L dopamine solution, first by diatom, spirulina, and Fruit peel extract,
Ivy extract solution, Flos Lonicerae extractive solution and water are added in three-necked flask, under the conditions of rotating speed is 500r/min, are stirred
60min, obtain mixed liquor；It is 50% ethanol solution that mass fraction is added into three-necked flask again, chitosan liquid, animal charred bone meal,
Plants essential oil and mass concentration are that 2g/L dopamine solutions are stirred, and obtain mixed slurry；Then with constant pressure funnel with
It is 30% hydrogen peroxide that mass fraction is added dropwise into three-necked flask for 3.3mL/min speed, produces multifunction tobacco humectant.It is described
Diatom is chrysophyceae.The spirulina is blunt top spirulina.The pericarp is apple skin.The Animal Bone is pig bone.The plant
Essential oil is refined jasmine oil.
Example 2
Pericarp is placed in baking oven and dries 2h, obtains dry pericarp, then is placed in pericarp is dried in ball mill, in rotating speed be 700r/
Under the conditions of min, 50min is crushed, obtains dry pericarp powder；Gained is dried into pericarp powder and water in mass ratio 1：100 add No. 1
In beaker, No. 1 beaker is then placed in digital display and tested the speed in constant temperature blender with magnetic force, in temperature be 60 DEG C, rotating speed 500r/min
Under the conditions of, after heating stirring mixing 50min, filtering, obtain Fruit peel extract；Ivy is placed in baking oven and dries 2h, obtains drying
Ivy, then be placed in ivy is dried in ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Chang Chun
Rattan powder；Gained is dried into ivy powder and water in mass ratio 1：100 are added in No. 2 beakers, and No. 2 beakers then are placed in into number
In the aobvious constant temperature blender with magnetic force that tests the speed, in temperature be 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min,
Filtering, obtains ivy extract solution；Honeysuckle is placed in baking oven and dries 2h, obtains dry honeysuckle, then be placed in honeysuckle is dried
In ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Honeysuckle Flower；Gained is dried into honeysuckle powder
End and water in mass ratio 1：100 add in No. 3 beakers, and No. 3 beakers then are placed in into digital display tests the speed in constant temperature blender with magnetic force, in
Temperature is 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min, filtering, obtains Flos Lonicerae extractive solution；By shell
Glycan and water in mass ratio 1：100 add in No. 4 beakers, after being stirred 30min with glass bar, stand swelling 4h, then by No. 4
Beaker moves into digital display and tested the speed constant temperature blender with magnetic force, is 100 DEG C in temperature, under the conditions of rotating speed is 500r/min, heating stirring is molten
50min is solved, produces chitosan liquid；By in Animal Bone ball mill, under the conditions of rotating speed is 500r/min, after ball mill grinding, 60 are crossed
Purpose is sieved, and obtains Animal Bone powder, Animal Bone powder is placed in retort, argon gas is filled with into stove with 60mL/min, in temperature
Under the conditions of 600 DEG C, under nitrogen protective condition, insulation charing 2h, animal charred bone meal is produced；Count in parts by weight, successively
Taking 20 parts of Fruit peel extracts, 20 parts of ivy extract solutions, 20 parts of Flos Lonicerae extractive solutions, 10 parts of mass fractions are 30% hydrogen peroxide, 20
Part mass fraction is 50% ethanol solution, 60 parts of water, 20 parts of chitosan liquid, 20 parts of animal charred bone meals, 20 parts of plants essential oils, 10
The dopamine solution that part mass concentration is 2g/L, first Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are added
In three-necked flask, under the conditions of rotating speed is 500r/min, 60min is stirred, obtains mixed liquor；Matter is added into three-necked flask again
Amount fraction is 50% ethanol solution, and chitosan liquid, animal charred bone meal, plants essential oil and mass concentration are 2g/L dopamine solutions
It is stirred, obtains mixed slurry；Quality point is then added dropwise into three-necked flask with 3.3mL/min speed with constant pressure funnel
Number is 30% hydrogen peroxide, produces multifunction tobacco humectant.The pericarp is apple skin.The Animal Bone is pig bone.The plant
Essential oil is refined jasmine oil.
Example 3
By chitosan and water in mass ratio 1：100 add in No. 4 beakers, after being stirred 30min with glass bar, stand swelling
4h, then No. 4 beakers are moved into digital displays and tested the speed constant temperature blender with magnetic force, in temperature be 100 DEG C, under the conditions of rotating speed is 500r/min,
Heating stirring dissolves 50min, produces chitosan liquid；By in Animal Bone ball mill, under the conditions of rotating speed is 500r/min, ball milling powder
After broken, the sieve of 60 mesh is crossed, Animal Bone powder is obtained, Animal Bone powder is placed in retort, argon is filled with into stove with 60mL/min
Gas, under the conditions of temperature is 600 DEG C, under nitrogen protective condition, insulation charing 2h, produce animal charred bone meal；By weight
Number meter, takes 30 portions of diatoms, 30 parts of spirulinas, 10 parts of mass fractions are 30% hydrogen peroxide, and 20 parts of mass fractions are 50% ethanol successively
Solution, 60 parts of water, 20 parts of chitosan liquid, 20 parts of animal charred bone meals, the dopamine solution that 10 parts of mass concentrations are 2g/L, first will
Diatom, spirulina and water are added in three-necked flask, under the conditions of rotating speed is 500r/min, is stirred 60min, is obtained mixed liquor；
It is 50% ethanol solution that mass fraction is added into three-necked flask again, and chitosan liquid, animal charred bone meal and mass concentration are 2g/L
Dopamine solution is stirred, and obtains mixed slurry；Then use constant pressure funnel with 3.3mL/min speed into three-necked flask
Dropwise addition mass fraction is 30% hydrogen peroxide, produces multifunction tobacco humectant.The diatom is chrysophyceae.The spirulina is blunt top
Spirulina.The pericarp is apple skin.The Animal Bone is pig bone.
Example 4
Pericarp is placed in baking oven and dries 2h, obtains dry pericarp, then is placed in pericarp is dried in ball mill, in rotating speed be 700r/
Under the conditions of min, 50min is crushed, obtains dry pericarp powder；Gained is dried into pericarp powder and water in mass ratio 1：100 add No. 1
In beaker, No. 1 beaker is then placed in digital display and tested the speed in constant temperature blender with magnetic force, in temperature be 60 DEG C, rotating speed 500r/min
Under the conditions of, after heating stirring mixing 50min, filtering, obtain Fruit peel extract；Ivy is placed in baking oven and dries 2h, obtains drying
Ivy, then be placed in ivy is dried in ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Chang Chun
Rattan powder；Gained is dried into ivy powder and water in mass ratio 1：100 are added in No. 2 beakers, and No. 2 beakers then are placed in into number
In the aobvious constant temperature blender with magnetic force that tests the speed, in temperature be 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min,
Filtering, obtains ivy extract solution；Honeysuckle is placed in baking oven and dries 2h, obtains dry honeysuckle, then be placed in honeysuckle is dried
In ball mill, under the conditions of rotating speed is 700r/min, 50min is crushed, obtains dry Honeysuckle Flower；Gained is dried into honeysuckle powder
End and water in mass ratio 1：100 add in No. 3 beakers, and No. 3 beakers then are placed in into digital display tests the speed in constant temperature blender with magnetic force, in
Temperature is 60 DEG C, under the conditions of rotating speed is 500r/min, after heating stirring mixing 50min, filtering, obtains Flos Lonicerae extractive solution；By shell
Glycan and water in mass ratio 1：100 add in No. 4 beakers, after being stirred 30min with glass bar, stand swelling 4h, then by No. 4
Beaker moves into digital display and tested the speed constant temperature blender with magnetic force, is 100 DEG C in temperature, under the conditions of rotating speed is 500r/min, heating stirring is molten
50min is solved, produces chitosan liquid；Count in parts by weight, take 30 portions of diatoms successively, 30 parts of spirulinas, 20 parts of Fruit peel extracts, 20
Part ivy extract solution, 20 parts of Flos Lonicerae extractive solutions, 10 parts of mass fractions are 30% hydrogen peroxide, and 20 parts of mass fractions are 50% ethanol
Solution, 60 parts of water, 20 parts of chitosan liquid, 20 parts of plants essential oils, the dopamine solution that 10 parts of mass concentrations are 2g/L, first by silicon
Algae, spirulina, Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are added in three-necked flask, are in rotating speed
Under the conditions of 500r/min, 60min is stirred, obtains mixed liquor；It is that 50% ethanol is molten to add mass fraction into three-necked flask again
Liquid, chitosan liquid, plants essential oil and mass concentration are that 2g/L dopamine solutions are stirred, and obtain mixed slurry；Then use constant pressure
Mass fraction is added dropwise as 30% hydrogen peroxide into three-necked flask using 3.3mL/min speed in dropping funel, produces multifunction tobacco guarantor
Moisten agent.The diatom is chrysophyceae.The spirulina is blunt top spirulina.The pericarp is apple skin.The plants essential oil is jasmine
Jasmine essential oil.
Comparative example：The tobacco humectant of Guangzhou trade Co., Ltd.
The gained of example 1 to 4 tobacco humectant and comparative example product are subjected to performance detection, specific detection method is as follows：
Sample is placed on and spontaneously dries 24h at room temperature, humectant is fully absorbed by pipe tobacco, sample is finally put into temperature
To balance 48h in 20 DEG C, the climatic chamber of RH=60%, in case experiment is used.Equilibrium moisture content determines, using classical way YC/
T31.Testing result is as shown in table 1：
Table 1：
| Detection method | Example 1 | Example 2 | Example 3 | Example 4 | Comparative example |
| Equilibrium moisture content/% | 15.23 | 14.42 | 14.15 | 14.45 | 13.41 |
From the testing result of table 1, present invention gained multifunction tobacco humectant has excellent water retention property, in the combustion of cigarette
During suction, reduce harmful substance and injury, and tobacco comfortable taste are produced to human body.
Claims (9)
- A kind of 1. multifunction tobacco humectant, it is characterised in that：It is made up of the raw material of following parts by weight：20~30 parts of silicon Algae, 20~30 parts of spirulinas, 10~20 parts of Fruit peel extracts, 10~20 parts of ivy extract solutions, 10~20 parts of honeysuckle extractions Liquid, 8~10 parts of hydrogen peroxide, 10~20 parts of ethanol solutions, 50~60 parts of water, 10~20 parts of chitosan liquid, 10~20 portions of boneblaces Change bone meal, 10~20 parts of plants essential oils, 8~10 parts of dopamine solutions；The preparation process of the multifunction tobacco humectant is：（1）Each raw material is weighed by raw material composition；（2）Diatom, spirulina, Fruit peel extract, ivy extract solution, Flos Lonicerae extractive solution and water are stirred, must be mixed Liquid；（3）Ethanol solution, chitosan liquid, animal charred bone meal, plants essential oil and dopamine solution stirring are added into mixed liquor Mixing, obtains mixed slurry；（4）Hydrogen peroxide is added dropwise into above-mentioned gained mixed slurry, produces multifunction tobacco humectant.
- A kind of 2. multifunction tobacco humectant according to claim 1, it is characterised in that：The diatom is in chrysophyceae or bulk kelp Any one.
- A kind of 3. multifunction tobacco humectant according to claim 1, it is characterised in that：The spirulina is blunt top spiral Algae, any one in spirulina maxim and India's spirulina.
- A kind of 4. multifunction tobacco humectant according to claim 1, it is characterised in that：The preparation of the Fruit peel extract Cheng Wei：Pericarp is dried, crushes, obtains dry pericarp powder；Gained is dried into pericarp powder and water in mass ratio 1：50~1：100 Heating stirring mixes, and filtering, obtains Fruit peel extract；The pericarp is apple skin, any one in peach skin or pear skin.
- A kind of 5. multifunction tobacco humectant according to claim 1, it is characterised in that：The preparation of the ivy extract solution Process is：Ivy is dried, crushes, obtains dry ivy powder；Gained is dried into ivy powder and water in mass ratio 1： 50~1：100 heating stirrings mix, and filtering, obtain ivy extract solution.
- A kind of 6. multifunction tobacco humectant according to claim 1, it is characterised in that：The preparation of the Flos Lonicerae extractive solution Process is：Honeysuckle is dried, crushes, obtains dry Honeysuckle Flower；Gained is dried into Honeysuckle Flower and water in mass ratio 1： 50~1：100 heating stirrings mix, and filtering, obtain Flos Lonicerae extractive solution.
- A kind of 7. multifunction tobacco humectant according to claim 1, it is characterised in that：The preparation process of the chitosan liquid For：By chitosan and water in mass ratio 1：50~1：After 100 mixing swellings, heating stirring dissolving, chitosan liquid is produced.
- A kind of 8. multifunction tobacco humectant according to claim 1, it is characterised in that：It is prepared by the animal charred bone meal Cheng Wei：By Animal Bone ball mill grinding, sieving, nitrogen charging insulation charing, animal charred bone meal is produced；The Animal Bone is pig bone, ox Any one in bone or chicken bone.
- A kind of 9. multifunction tobacco humectant according to claim 1, it is characterised in that：The plants essential oil is jasmine essence Any one in oil, camellia essential oil or rose ethereal oil.
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