CN107788378A - One kind is used for puerperous donkey-hide gelatin beans cake and preparation method thereof - Google Patents
One kind is used for puerperous donkey-hide gelatin beans cake and preparation method thereof Download PDFInfo
- Publication number
- CN107788378A CN107788378A CN201710996761.0A CN201710996761A CN107788378A CN 107788378 A CN107788378 A CN 107788378A CN 201710996761 A CN201710996761 A CN 201710996761A CN 107788378 A CN107788378 A CN 107788378A
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- parts
- donkey
- hide gelatin
- coix seed
- puerperous
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Abstract
The invention belongs to food processing technology field, and in particular to one kind is used for puerperous donkey-hide gelatin beans cake and preparation method thereof, is made up of following raw material：Semen Coicis extract, motherwort, Poria cocos, cassia twig, ginger, jujube, donkey-hide gelatin, rde bean sand, brown sugar, agar, Shaoxing rice wine, water.The present invention invigorating qi and benefiting blood, beautifying face and moistering lotion donkey-hide gelatin beans cake in add the traditional Chinese medicine ingredients such as motherwort, Poria cocos, cassia twig and jujube, ginger and carry out compatibility, there is improvement sleep, set the mind at rest, improving appetite and other effects.The present invention is also especially added with coix seed oil, coixan, coixenolide as functional component, be advantageous to improve puerperal anemia symptom, the inflammatory reactions such as mastitis, hysteritis can be suppressed, it can speed up the recovery of puerpera's muscle power, supplemented the nutrients in time for puerpera, obtained donkey-hide gelatin beans cake is nutritious, cater to appetite, recovers have booster action to puerpera's puerperium, has wide market prospects.
Description
Technical field
The present invention relates to food processing technology field, and in particular to one kind is used for puerperous donkey-hide gelatin beans cake and its preparation side
Method.
Background technology
Puerperium, which refers to give birth to each organ of puerpera's whole body from placenta, recovers in addition to mammary gland to needed for normal unpregnancy state
In one period, it is generally specified as 6-8 weeks, China is among the people will to be commonly called as " being confined in childbirth " this period.The gestational period is one quite special
There occurs larger change, childbirth for different period, the status function of each organ of puerpera's whole body and the psychology of puerpera
After need a period of time recovered.Just because of puerperium be after women produces and its special period, easy generation are a lot
Health problem, if be not noted that, these problems, which can also continue, has influence on the health of puerpera in the future, therefore to puerperium
Health care should attach great importance to.
The common health problem of postpartum women mainly has the following aspects：
1st, generate heat：Some puerperas because stages of labor is longer, physical demands, fatigue and body temperature have slight elevated phenomenon,
After childbirth 3-4 days, due to the swelling of mammary gland, pain, it is also possible to body temperature rise is had, as breast height is congested, lymphatic vessel swelling,
Body temperature can raise suddenly.
2nd, mastitis：Body temperature continues high fever often more than 39 DEG C, and with mammiferous red and swollen heat pain.
3rd, galactostasis：Breast increase skin anxiety surface phlebectasia, engorgement of breasts, influences time of blood and lymph
Stream, regional glandular enlargement can be caused, breast forms to harden feels pain to puerpera.Severe patient, mammary gland pipe choking, milk exclude
It is not smooth, formed " become silted up breast ".
4th, urinary hesitancy and constipation：In the progress of labor, bladder, which is pressurized, causes myxedema, and congested and Muscle tensility reduces, with
And the reason such as perineal wound pain, uncomfortable bed urination, urinary hesitancy easily occurs.Due to postpartum stomach wall and Pelvic floor dried meat floss
Relax, activity is few, therefore constipation easily occurs.
5th, late puerperal hemorrhage：Part Placenta remnants, postpartum uterus local infection, endometrium adaptability increase it is long,
Cesarean postoperate monitor etc. is all the reason for causing late puerperal hemorrhage.
6th, puerperium lochiorrhagia：Lochia refers to that postpartum uterine decidua (particularly decidua at placenta attachment) comes off, blood,
The phenomenon that downright bad decidua tissue is discharged from vagina, puerperium are the main generation phases of lochia.Lochia has the smell of blood, but odorless,
Its color and content time to time change, typically continue 4~6 weeks, total amount is 250ml~500ml.Such as beyond the above-mentioned time also
There is more lochia to discharge, referred to as prolonged lochia.
Physical demands is big during due to childbirth, and each organ needs to recover in body, and the digestion power of puerpera weakens, and secretes again
Milk supplies neonatal growth, so dietetic nutrition is extremely important.Postpartum diet should being rich in nutrition, enough heat and moisture.Experience
Gestation and the exciting and anxiety of childbirth, puerpera's nerve extremely loosen, plus the worry to baby and puerperous discomfort
The unstable of puerpera's mood is caused, therefore helps puerpera's mitigation is uncomfortable to recover particularly significant to puerpera's puerperium.
The content of the invention
In order to solve the above problems, the invention provides one kind to be used for puerperous donkey-hide gelatin beans cake and preparation method thereof,
Invigorating qi and benefiting blood, beautifying face and moistering lotion donkey-hide gelatin beans cake in add the traditional Chinese medicine ingredients such as motherwort, Poria cocos, cassia twig and jujube, ginger and carry out
Compatibility, for the adverse reaction of postpartum women, there is improvement sleep, set the mind at rest, improving appetite and other effects.The present invention is also special
Coix seed oil, coixan, coixenolide are added as functional component, a kind of battalion is provided for postpartum women health problem
Support and enrich, cater to puerpera's appetite, recovering the cake food that has booster action to puerpera's puerperium.
The present invention can be achieved through the following technical solutions：
One kind is used for puerperous donkey-hide gelatin beans cake, is made up of the raw material of following weight parts：Semen Coicis extract 0.08~
0.10 part, 2.5~3.5 parts of motherwort, 7~11 parts of Poria cocos, 4~6 parts of cassia twig, 8~10 parts of ginger, 17~21 parts of jujube, donkey-hide gelatin
25~37 parts, 150~160 parts of rde bean sand, 63~79 parts of brown sugar, 115~125 parts of agar, 25~35 parts of Shaoxing rice wine, water 70~80
Part.Wherein, the Semen Coicis extract is made up of the raw material of following weight parts：2~3 parts of coix seed oil, coixan 2~
3 parts, 5~6 parts of coixenolide.
Preferably, it is a kind of to be used for puerperous donkey-hide gelatin beans cake, it is made up of the raw material of following weight parts：Semen Coicis extract
0.09 part, 3 parts of motherwort, 9 parts of Poria cocos, 5 parts of cassia twig, 9 parts of ginger, 19 parts of jujube, 31 parts of donkey-hide gelatin, rde bean husky 155 parts, brown sugar
71 parts, 120 parts of agar, 30 parts of Shaoxing rice wine, 75 parts of water.Wherein, the Semen Coicis extract is made up of the raw material of following weight parts：
2.5 parts of coix seed oil, 2.5 parts of coixan, 5.5 parts of coixenolide.
Preferably, the coix seed oil extracting method is：Dry coix seed be crushed into 20 mesh sieves, it is then overcritical
CO2Extraction, wherein, extraction kettle 1L, temperature 45 C, pressure 26MPa, the temperature 45 C of separating still 1, pressure 6.0MPa, separating still 2
35 DEG C of temperature, pressure 5.0MPa, CO2Flow is 30L/h, extracts 1.5h；Coix seed oil is obtained by extraction, then seals and is kept in dark place.
Preferably, the coixenolide extracting method is：Dry coix seed be crushed into 80 mesh sieves, be 1 by solid-liquid ratio:
10 add ethyl acetate, extract 16h at 4 DEG C, total immersion carries 2 times, merging filtrate after filtering, concentrates the filtrate to the 1/10 of original volume
Afterwards, with isometric petroleum ether extraction, petroleum ether is removed, dries, obtains coixenolide.
Preferably, the coixan extracting method is：(1) dry coix seed be crushed into 80 mesh sieves, by feed liquid
Than for 1:2 add petroleum ether in coix seed, and backflow extraction 60min, reclaims petroleum ether, obtain degreasing Job's tears under the conditions of 60 DEG C
Benevolence；(2) it is 1 by solid-liquid ratio by distilled water:15 are added in the degreasing coix seed of step (1), and pH is adjusted with 1mol/L HCl solution
To 5.2,100min is extracted in 100 DEG C of waters bath with thermostatic control, cools the temperature to room temperature, 2.5% mixed enzyme is added, using ultrasonic wave
Enzyme process assisted extraction, pH to 6.5 is adjusted with 0.1mol/L NaOH solution, digest 120min under the conditions of 45 DEG C successively, 100 DEG C
Under the conditions of ultrasonic extraction 25min after enzyme deactivation 10min, add 4 times of ethanol of volume 95%, stand 6h, filtration drying, obtain coix seed
Polysaccharide crude extract；(3) it is 1 by solid-liquid ratio by distilled water:2 add in the coixan crude extract obtained by dissolving step (2), then
Add 15% trichloroacetic acid isometric with distilled water, shake 10h, 3000r/min centrifugation 20min, after take supernatant, with dialysis
Bag flowing water dialysis 7d, 95% ethanol that equivalent is added in gained dialyzate carry out alcohol precipitation, taking precipitate, dried；(4) will distillation
Water is 1 by solid-liquid ratio:2 add in the sediment obtained by step (3), after SephadexG-75 column chromatographies, with 0~1mol/
LNaCl solution gradients elute, and sulfuric acid-phynol method identification saccharide portion, merge polysaccharide reacting positive part, are dialysed with distilled water
3d, gained dialyzate are concentrated under reduced pressure drying, and it is coixan to obtain white extract.Wherein, it is mixed in the step (2)
Synthase includes pectase and neutral proteinase, usage ratio 3:2.
The present invention also provides a kind of preparation method for puerperous donkey-hide gelatin beans cake, comprises the following steps：
(1) crush：It is 50~100 μm that the motherwort of aforementioned proportion, Poria cocos, cassia twig, ginger, jujube are crushed into particle diameter
Powder；
(2) donkey-hide gelatin is changed：Donkey-hide gelatin is added after Shaoxing rice wine is boiled, stirs to it and melts completely, obtain donkey-hide gelatin solution；
(3) agar is changed：25~35 DEG C of 10~20 parts of warm water is added into rde bean sand, sweetened bean paste liquid is made in mixing；With remaining
Amount bubble opens agar, and heating melts agar, obtains agar solution, mixes sweetened bean paste liquid and agar solution, obtains mixed solution；
(4) boil：Boiled after liquid obtained by step (2) and step (3) is all well mixed, add step (1) institute
Powder, brown sugar are obtained, small fire is boiled to glue water content about 14~16%, is obtained glue and is hung flag；
(5) batch mixing：The glue that Semen Coicis extract is added to step (4) is hung in flag, is stirred, and reverse mould cooling, is obtained
Donkey-hide gelatin beans cake.
Each main composition mechanism of action of the present invention is as follows：
Coix seed, it is that grass family is annual or the dry mature kernal of herbaceos perennial Job's tears.China is mostly
Qu Junyou is cultivated.Its is cool in nature, sweet, light, has the functions such as invigorating the spleen, tonifying lung, dampness removing, heat-clearing.Coix seed is rich in protein, a variety of
Amino acid, vitamin and mineral, therefore it is described as " king of world grass ".In coix seed containing various active into
Point, mainly including unsaturated fatty acids, lipid, lactams and carbohydrate etc..
Coix seed oil main component includes triglycerides, oleic acid, linoleic acid, palmitic acid, leukotrienes etc., wherein oleic acid and Asia
Oleic acid is main unrighted acid, has good antioxidation, also has the function that pain easing and hemostasis, be advantageous to improve
Puerperal anemia symptom, and there is anti-inflammatory efficacy, the inflammatory reactions such as puerperal mastitis, hysteritis can be significantly inhibited.
Coixan, which has, improves exercise tolerance, improves effect of the body to the load-bearing capacity of motion；During physical exertion
Energy is obtained mainly by glycolysis, and coixan the generation of delay fatigue, can increase by improving the storage level of hepatic glycogen
Sharp movement ability.Puerpera can accumulate substantial amounts of serum urea in postpartum, so as to cause postpartum pregnant woman easily tired out, the soreness of waist, and muscles and bones
Pain, coixan significantly reduce the content of serum urea, suppress the generation of serum urea, can speed up disappearing for puerpera's fatigue
The recovery of solution and muscle power.
Coixenolide can improve the postpartum weakness of the spleen and the stomach state, reduce the alimentary canals such as diarrhoea, constipation that puerperium often has
The generation of symptom, while digestive efficiency of puerpera's stomach to diet is improved, help to supplement nutrition needed for puerpera's postpartum in time.
The present invention possesses following beneficial effect：
It is provided by the invention a kind of for puerperous donkey-hide gelatin beans cake and preparation method thereof, in invigorating qi and benefiting blood, beautifying face and moistering lotion
Donkey-hide gelatin beans cake in add motherwort, Poria cocos, cassia twig compatibility, have promote postpartum qi and blood normal operation the effect of, can aid in solving
Certainly stagnation of QI and blood, the deficiency of vital energy can not be taken the photograph the problems such as blood, YinXuXueRe, reduce the morbidity of puerperium lochiorrhagia and late puerperal hemorrhage
Rate, a variety of adverse reactions caused by the use of the treatment methods such as clinical antibiotics and oxytocin can be avoided.In addition, also add
Jujube and ginger compatibility, the sleep of puerperal women can be improved, the mood in stable puerpera's postpartum, also there is the function of rendering palatable,
Appetite can be improved so that this product edibility dramatically increases.The present invention is also especially added with coix seed oil, coixan, the heart of a lotus seed
Seed of jog's tears ester is advantageous to improve puerperal anemia symptom as functional component, and has anti-inflammatory efficacy, and it is newborn to significantly inhibit puerperium
The inflammatory reactions such as adenositis, hysteritis, the resolution of puerpera's fatigue and the recovery of muscle power are can speed up, improve puerpera's stomach to diet
Digestive efficiency, help to supplement nutrition needed for puerpera's postpartum in time, obtained donkey-hide gelatin beans cake is nutritious, cater to puerpera's appetite,
Recover have booster action to puerpera's puerperium, there are wide market prospects.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
One kind is used for puerperous donkey-hide gelatin beans cake, is made up of the raw material of following weight parts：0.08 part of Semen Coicis extract,
2.5 parts of motherwort, 7 parts of Poria cocos, 4 parts of cassia twig, 8 parts of ginger, 17 parts of jujube, 25 parts of donkey-hide gelatin, rde bean are husky 150 parts, 63 parts of brown sugar,
115 parts of agar, 25 parts of Shaoxing rice wine, 70 parts of water.
Wherein, the Semen Coicis extract is made up of the raw material of following weight parts：2 parts of coix seed oil, coixan 2
Part, 5 parts of coixenolide.
The coix seed oil extracting method is：Dry coix seed be crushed into 20 mesh sieves, then supercritical CO2Extraction,
Wherein, extraction kettle 1L, temperature 45 C, pressure 26MPa, the temperature 45 C of separating still 1, pressure 6.0MPa, the temperature 35 of separating still 2
DEG C, pressure 5.0MPa, CO2Flow is 30L/h, extracts 1.5h；Coix seed oil is obtained by extraction, then seals and is kept in dark place.
The coixenolide extracting method is：Dry coix seed be crushed into 80 mesh sieves, be 1 by solid-liquid ratio:10 add
Ethyl acetate, 16h is extracted at 4 DEG C, total immersion carries 2 times, merging filtrate after filtering, after concentrating the filtrate to the 1/10 of original volume, uses
Isometric petroleum ether extraction, petroleum ether is removed, dry, obtain coixenolide.
The coixan extracting method is：(1) dry coix seed be crushed into 80 mesh sieves, is 1 by solid-liquid ratio:2
Petroleum ether is added in coix seed, backflow extraction 60min, reclaims petroleum ether, obtain degreasing coix seed under the conditions of 60 DEG C；(2) will
Distilled water is 1 by solid-liquid ratio:15 are added in the degreasing coix seed of step (1), and pH to 5.2 is adjusted with 1mol/L HCl solution,
Extract 100min in 100 DEG C of waters bath with thermostatic control, cool the temperature to room temperature, add 2.5% mixed enzyme, mixed enzyme include pectase and
Neutral proteinase, usage ratio 3:2, using ultrasonic wave enzyme process assisted extraction, with 0.1mol/L NaOH solution adjust pH to
6.5, digest 120min under the conditions of 45 DEG C successively, ultrasonic extraction 25min after enzyme deactivation 10min, adds 4 times under the conditions of 100 DEG C
The ethanol of volume 95%, 6h is stood, filtration drying, obtains coixan crude extract；(3) it is 1 by solid-liquid ratio by distilled water:2 add
In coixan crude extract obtained by dissolving step (2), 15% trichloroacetic acid isometric with distilled water, concussion are added
10h, 3000r/min centrifuge 20min, after take supernatant, dialysed 7d with bag filter flowing water, equivalent added in the gained dialyzate
95% ethanol carries out alcohol precipitation, taking precipitate, dries；(4) it is 1 by solid-liquid ratio by distilled water:2 add the precipitation obtained by step (3)
In thing, after SephadexG-75 column chromatographies, eluted with 0~1mol/LNaCl solution gradients, sulfuric acid-phynol method identification polysaccharide portion
Point, merge polysaccharide reacting positive part, dialysed 3d with distilled water, gained dialyzate is concentrated under reduced pressure drying, obtains white extract
As coixan.
A kind of above-mentioned preparation method for puerperous donkey-hide gelatin beans cake, comprises the following steps：
(1) crush：The motherwort of aforementioned proportion, Poria cocos, cassia twig, ginger, jujube are crushed to the powder that particle diameter is 50 μm；
(2) donkey-hide gelatin is changed：Donkey-hide gelatin is added after Shaoxing rice wine is boiled, stirs to it and melts completely, obtain donkey-hide gelatin solution；
(3) agar is changed：25 DEG C of 10 parts of warm water is added into rde bean sand, sweetened bean paste liquid is made in mixing；Bubbled open with excess water
Agar, heating melt agar, obtain agar solution, mix sweetened bean paste liquid and agar solution, obtain mixed solution；
(4) boil：Boiled after liquid obtained by step (2) and step (3) is all well mixed, add step (1) institute
Powder, brown sugar are obtained, small fire is boiled to glue water content about 14%, is obtained glue and is hung flag；
(5) batch mixing：The glue that Semen Coicis extract is added to step (4) is hung in flag, is stirred, and reverse mould cooling, is obtained
Donkey-hide gelatin beans cake.
Embodiment 2
One kind is used for puerperous donkey-hide gelatin beans cake, is made up of the raw material of following weight parts：0.09 part of Semen Coicis extract,
3 parts of motherwort, 9 parts of Poria cocos, 5 parts of cassia twig, 9 parts of ginger, 19 parts of jujube, 31 parts of donkey-hide gelatin, rde bean are husky 155 parts, 71 parts of brown sugar, fine jade
120 parts of fat, 30 parts of Shaoxing rice wine, 75 parts of water.
Wherein, the Semen Coicis extract is made up of the raw material of following weight parts：2.5 parts of coix seed oil, coix seed are more
Sugared 2.5 parts, 5.5 parts of coixenolide.
The coix seed oil extracting method is：Dry coix seed be crushed into 20 mesh sieves, then supercritical CO2Extraction,
Wherein, extraction kettle 1L, temperature 45 C, pressure 26MPa, the temperature 45 C of separating still 1, pressure 6.0MPa, the temperature 35 of separating still 2
DEG C, pressure 5.0MPa, CO2Flow is 30L/h, extracts 1.5h；Coix seed oil is obtained by extraction, then seals and is kept in dark place.
The coixenolide extracting method is：Dry coix seed be crushed into 80 mesh sieves, be 1 by solid-liquid ratio:10 add
Ethyl acetate, 16h is extracted at 4 DEG C, total immersion carries 2 times, merging filtrate after filtering, after concentrating the filtrate to the 1/10 of original volume, uses
Isometric petroleum ether extraction, petroleum ether is removed, dry, obtain coixenolide.
The coixan extracting method is：(1) dry coix seed be crushed into 80 mesh sieves, is 1 by solid-liquid ratio:2
Petroleum ether is added in coix seed, backflow extraction 60min, reclaims petroleum ether, obtain degreasing coix seed under the conditions of 60 DEG C；(2) will
Distilled water is 1 by solid-liquid ratio:15 are added in the degreasing coix seed of step (1), and pH to 5.2 is adjusted with 1mol/L HCl solution,
Extract 100min in 100 DEG C of waters bath with thermostatic control, cool the temperature to room temperature, add 2.5% mixed enzyme, mixed enzyme include pectase and
Neutral proteinase, usage ratio 3:2, using ultrasonic wave enzyme process assisted extraction, with 0.1mol/L NaOH solution adjust pH to
6.5, digest 120min under the conditions of 45 DEG C successively, ultrasonic extraction 25min after enzyme deactivation 10min, adds 4 times under the conditions of 100 DEG C
The ethanol of volume 95%, 6h is stood, filtration drying, obtains coixan crude extract；(3) it is 1 by solid-liquid ratio by distilled water:2 add
In coixan crude extract obtained by dissolving step (2), 15% trichloroacetic acid isometric with distilled water, concussion are added
10h, 3000r/min centrifuge 20min, after take supernatant, dialysed 7d with bag filter flowing water, equivalent added in the gained dialyzate
95% ethanol carries out alcohol precipitation, taking precipitate, dries；(4) it is 1 by solid-liquid ratio by distilled water:2 add the precipitation obtained by step (3)
In thing, after SephadexG-75 column chromatographies, eluted with 0~1mol/LNaCl solution gradients, sulfuric acid-phynol method identification polysaccharide portion
Point, merge polysaccharide reacting positive part, dialysed 3d with distilled water, gained dialyzate is concentrated under reduced pressure drying, obtains white extract
As coixan.
A kind of above-mentioned preparation method for puerperous donkey-hide gelatin beans cake, comprises the following steps：
(1) crush：The motherwort of aforementioned proportion, Poria cocos, cassia twig, ginger, jujube are crushed to the powder that particle diameter is 80 μm；
(2) donkey-hide gelatin is changed：Donkey-hide gelatin is added after Shaoxing rice wine is boiled, stirs to it and melts completely, obtain donkey-hide gelatin solution；
(3) agar is changed：30 DEG C of 15 parts of warm water is added into rde bean sand, sweetened bean paste liquid is made in mixing；Bubbled open with excess water
Agar, heating melt agar, obtain agar solution, mix sweetened bean paste liquid and agar solution, obtain mixed solution；
(4) boil：Boiled after liquid obtained by step (2) and step (3) is all well mixed, add step (1) institute
Powder, brown sugar are obtained, small fire is boiled to glue water content about 15%, is obtained glue and is hung flag；
(5) batch mixing：The glue that Semen Coicis extract is added to step (4) is hung in flag, is stirred, and reverse mould cooling, is obtained
Donkey-hide gelatin beans cake.
Embodiment 3
One kind is used for puerperous donkey-hide gelatin beans cake, is made up of the raw material of following weight parts：0.10 part of Semen Coicis extract,
3.5 parts of motherwort, 11 parts of Poria cocos, 6 parts of cassia twig, 10 parts of ginger, 21 parts of jujube, 37 parts of donkey-hide gelatin, rde bean husky 160 parts, brown sugar 79
Part, 125 parts of agar, 35 parts of Shaoxing rice wine, 80 parts of water.
Wherein, the Semen Coicis extract is made up of the raw material of following weight parts：3 parts of coix seed oil, coixan 3
Part, 6 parts of coixenolide.
The coix seed oil extracting method is：Dry coix seed be crushed into 20 mesh sieves, then supercritical CO2Extraction,
Wherein, extraction kettle 1L, temperature 45 C, pressure 26MPa, the temperature 45 C of separating still 1, pressure 6.0MPa, the temperature 35 of separating still 2
DEG C, pressure 5.0MPa, CO2Flow is 30L/h, extracts 1.5h；Coix seed oil is obtained by extraction, then seals and is kept in dark place.
The coixenolide extracting method is：Dry coix seed be crushed into 80 mesh sieves, be 1 by solid-liquid ratio:10 add
Ethyl acetate, 16h is extracted at 4 DEG C, total immersion carries 2 times, merging filtrate after filtering, after concentrating the filtrate to the 1/10 of original volume, uses
Isometric petroleum ether extraction, petroleum ether is removed, dry, obtain coixenolide.
The coixan extracting method is：(1) dry coix seed be crushed into 80 mesh sieves, is 1 by solid-liquid ratio:2
Petroleum ether is added in coix seed, backflow extraction 60min, reclaims petroleum ether, obtain degreasing coix seed under the conditions of 60 DEG C；(2) will
Distilled water is 1 by solid-liquid ratio:15 are added in the degreasing coix seed of step (1), and pH to 5.2 is adjusted with 1mol/L HCl solution,
Extract 100min in 100 DEG C of waters bath with thermostatic control, cool the temperature to room temperature, add 2.5% mixed enzyme, mixed enzyme include pectase and
Neutral proteinase, usage ratio 3:2, using ultrasonic wave enzyme process assisted extraction, with 0.1mol/L NaOH solution adjust pH to
6.5, digest 120min under the conditions of 45 DEG C successively, ultrasonic extraction 25min after enzyme deactivation 10min, adds 4 times under the conditions of 100 DEG C
The ethanol of volume 95%, 6h is stood, filtration drying, obtains coixan crude extract；(3) it is 1 by solid-liquid ratio by distilled water:2 add
In coixan crude extract obtained by dissolving step (2), 15% trichloroacetic acid isometric with distilled water, concussion are added
10h, 3000r/min centrifuge 20min, after take supernatant, dialysed 7d with bag filter flowing water, equivalent added in the gained dialyzate
95% ethanol carries out alcohol precipitation, taking precipitate, dries；(4) it is 1 by solid-liquid ratio by distilled water:2 add the precipitation obtained by step (3)
In thing, after SephadexG-75 column chromatographies, eluted with 0~1mol/LNaCl solution gradients, sulfuric acid-phynol method identification polysaccharide portion
Point, merge polysaccharide reacting positive part, dialysed 3d with distilled water, gained dialyzate is concentrated under reduced pressure drying, obtains white extract
As coixan.
A kind of above-mentioned preparation method for puerperous donkey-hide gelatin beans cake, comprises the following steps：
(1) crush：The motherwort of aforementioned proportion, Poria cocos, cassia twig, ginger, jujube are crushed to the powder that particle diameter is 100 μm
End；
(2) donkey-hide gelatin is changed：Donkey-hide gelatin is added after Shaoxing rice wine is boiled, stirs to it and melts completely, obtain donkey-hide gelatin solution；
(3) agar is changed：35 DEG C of 20 parts of warm water is added into rde bean sand, sweetened bean paste liquid is made in mixing；Bubbled open with excess water
Agar, heating melt agar, obtain agar solution, mix sweetened bean paste liquid and agar solution, obtain mixed solution；
(4) boil：Boiled after liquid obtained by step (2) and step (3) is all well mixed, add step (1) institute
Powder, brown sugar are obtained, small fire is boiled to glue water content about 16%, is obtained glue and is hung flag；
(5) batch mixing：The glue that Semen Coicis extract is added to step (4) is hung in flag, is stirred, and reverse mould cooling, is obtained
Donkey-hide gelatin beans cake.
Comparative example 1
Difference with embodiment 1 is, without addition Semen Coicis extract in composition of raw materials, is specially：Motherwort 2.5
Part, 150 parts of 7 parts of Poria cocos, 4 parts of cassia twig, 8 parts of ginger, 17 parts of jujube, 25 parts of donkey-hide gelatin, rde bean sand, 63 parts of brown sugar, agar 115
Part, 25 parts of Shaoxing rice wine, 70 parts of water.
Comparative example 2
Difference with embodiment 1 is, without addition motherwort, Poria cocos, cassia twig in composition of raw materials, is specially：Coix seed
0.08 part of extract, 8 parts of ginger, 17 parts of jujube, 25 parts of donkey-hide gelatin, rde bean are husky 150 parts, 63 parts of brown sugar, 115 parts of agar, Shaoxing rice wine
25 parts, 70 parts of water.
Efficacy validation
Experimental example 1
Select 50 puerperas at random to be tested, be divided into 5 groups, every group of 10 people, respectively to 5 kinds of different donkey-hide gelatin beans cakes of preparation
Eaten, daily the morning and evening one, clinical assay, experimental result such as table 1 below are carried out to experimenter after eating one week：
Table 1
| Embodiment | Liver glycogen reserves amount/g | Serum urea/mmol/L | Dietary fiber/g |
| Embodiment 1 | 187 | 5.9 | 2.3 |
| Embodiment 2 | 189 | 5.3 | 2.5 |
| Embodiment 3 | 183 | 5.6 | 2.4 |
| Comparative example 1 | 161 | 7.1 | 1.5 |
| Comparative example 2 | 169 | 6.3 | 1.7 |
By upper table, for comparative example 1-2, puerpera eats Ah prepared by embodiment 1-3 technical scheme
After glue beans cake, internal liver glycogen reserves amount and dietary fiber increase, and serum urea reduces substantially, illustrates that coix seed carries
Take thing the generation of delay fatigue, locomitivity can be strengthened by improving the storage level of hepatic glycogen；Significantly reduce containing for serum urea
Amount, suppresses the generation of serum urea, can speed up the resolution of puerpera's fatigue and the recovery of muscle power；Puerpera's stomach is improved simultaneously to drink
The digestive efficiency of food, help to supplement nutrition needed for puerpera's postpartum in time.
Experimental example 2
30 puerperas of selection are observed, and the suitable puerpera 30 of simultaneous selection physical condition is as a control group.It is real
Test group donkey-hide gelatin beans cake long-term consumption prepared using embodiment 1, daily 200g.Donkey-hide gelatin beans prepared by the not edible present invention of control group
Cake, full diet, experimental result such as table 2 below：
Table 2
As seen from the above table, the donkey-hide gelatin beans cake of index of the present invention is eaten after one week, the 92% ruddy gloss of the person's of participating in the experiment skin, is slept
Abundance, appetite rising, the mood of sleeping are relatively stable；After two weeks, the 95% ruddy gloss of the person's of participating in the experiment skin, sufficient sleeping, appetite rises,
Mood is relatively stable；After three weeks, the 97% ruddy gloss of the person's of participating in the experiment skin, sufficient sleeping, appetite rise, are emotionally stable.And use
The puerpera of full diet as a control group, vim and vigour deficiency, sleep insufficiency, anxious state of mind are big.
In summary, the donkey-hide gelatin beans cake that prepared by the present invention, there is calm effectiveness, sleeping for puerperal women can be improved
Sleep, the mood in stable puerpera's postpartum, also there is the function of rendering palatable, cater to the appetite of puerpera so that this product edibility significantly increases
Add.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect scope.
Claims (9)
1. one kind is used for puerperous donkey-hide gelatin beans cake, it is characterised in that is made up of the raw material of following weight parts：Coix seed extracts
0.08~0.10 part of thing, 2.5~3.5 parts of motherwort, 7~11 parts of Poria cocos, 4~6 parts of cassia twig, 8~10 parts of ginger, jujube 17~21
Part, 25~37 parts of donkey-hide gelatin, 150~160 parts of rde bean sand, 63~79 parts of brown sugar, 115~125 parts of agar, 25~35 parts of Shaoxing rice wine,
70~80 parts of water.
2. one kind according to claim 1 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that the Semen Coicis extract
It is made up of the raw material of following weight parts：2~3 parts of coix seed oil, 2~3 parts of coixan, 5~6 parts of coixenolide.
3. one kind according to claim 1 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that by the original of following weight parts
Material forms：0.09 part of Semen Coicis extract, 3 parts of motherwort, 9 parts of Poria cocos, 5 parts of cassia twig, 9 parts of ginger, 19 parts of jujube, donkey-hide gelatin 31
Part, 155 parts of rde bean sand, 71 parts of brown sugar, 120 parts of agar, 30 parts of Shaoxing rice wine, 75 parts of water.
4. one kind according to claim 2 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that the Semen Coicis extract
It is made up of the raw material of following weight parts：2.5 parts of coix seed oil, 2.5 parts of coixan, 5.5 parts of coixenolide.
5. one kind according to claim 2 or 4 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that the coix seed oil
Extracting method is：Dry coix seed be crushed into 20 mesh sieves, then supercritical CO2Extraction, wherein, extraction kettle 1L, temperature
45 DEG C, pressure 26MPa, the temperature 45 C of separating still 1, pressure 6.0MPa, 35 DEG C of 2 temperature of separating still, pressure 5.0MPa, CO2Flow
For 30L/h, 1.5h is extracted；Coix seed oil is obtained by extraction, then seals and is kept in dark place.
6. one kind according to claim 2 or 4 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that the coixenolide
Extracting method is：Dry coix seed be crushed into 80 mesh sieves, be 1 by solid-liquid ratio:10 add ethyl acetate, are extracted at 4 DEG C
16h, total immersion carry 2 times, merging filtrate after filtering, after concentrating the filtrate to the 1/10 of original volume, with isometric petroleum ether extraction,
Petroleum ether is removed, dries, obtains coixenolide.
7. one kind according to claim 2 or 4 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that the coix seed is more
Sugared extracting method is：
(1) dry coix seed be crushed into 80 mesh sieves, is 1 by solid-liquid ratio:2 add petroleum ether in coix seed, in 60 DEG C of bars
Backflow extraction 60min, reclaims petroleum ether, obtains degreasing coix seed under part；
(2) it is 1 by solid-liquid ratio by distilled water:15 add in the degreasing coix seed of step (1), are adjusted with 1mol/L HCl solution
PH to 5.2,100min is extracted in 100 DEG C of waters bath with thermostatic control, cools the temperature to room temperature, 2.5% mixed enzyme is added, using ultrasound
Ripple enzyme process assisted extraction, pH to 6.5 is adjusted with 0.1mol/L NaOH solution, digest 120min under the conditions of 45 DEG C successively, 100
Ultrasonic extraction 25min after enzyme deactivation 10min under the conditions of DEG C, 4 times of ethanol of volume 95% are added, stand 6h, filtration drying, obtain Job's tears
Benevolence polysaccharide crude extract；
(3) it is 1 by solid-liquid ratio by distilled water:2 add in the coixan crude extract obtained by dissolving steps (2), add with
15% isometric trichloroacetic acid of distilled water, shake 10h, 3000r/min centrifugation 20min, after take supernatant, with bag filter flowing water
Dialyse 7d, and 95% ethanol that equivalent is added in gained dialyzate carries out alcohol precipitation, taking precipitate, dries；
(4) it is 1 by solid-liquid ratio by distilled water:2 add in the sediment obtained by step (3), after SephadexG-75 column chromatographies,
Eluted with 0~1mol/LNaCl solution gradients, sulfuric acid-phynol method identification saccharide portion, merge polysaccharide reacting positive part, with steaming
Distilled water is dialysed 3d, and gained dialyzate is concentrated under reduced pressure drying, and it is coixan to obtain white extract.
8. one kind according to claim 7 is used for puerperous donkey-hide gelatin beans cake, it is characterised in that in the step (2)
Mixed enzyme includes pectase and neutral proteinase, usage ratio 3:2.
9. a kind of method for puerperous donkey-hide gelatin beans cake prepared as described in any one of claim 1~8, including following step
Suddenly：
(1) crush：The motherwort of aforementioned proportion, Poria cocos, cassia twig, ginger, jujube are crushed to the powder that particle diameter is 50~100 μm
End；
(2) donkey-hide gelatin is changed：Donkey-hide gelatin is added after Shaoxing rice wine is boiled, stirs to it and melts completely, obtain donkey-hide gelatin solution；
(3) agar is changed：25~35 DEG C of 10~20 parts of warm water is added into rde bean sand, sweetened bean paste liquid is made in mixing；Use excess water
Agar is bubbled open, heating melts agar, obtains agar solution, mixes sweetened bean paste liquid and agar solution, obtains mixed solution；
(4) boil：Boiled after liquid obtained by step (2) and step (3) is all well mixed, add powder obtained by step (1)
End, brown sugar, small fire are boiled to glue water content about 14~16%, are obtained glue and are hung flag；
(5) batch mixing：The glue that Semen Coicis extract is added to step (4) is hung in flag, is stirred, and reverse mould cooling, obtains donkey-hide gelatin
Beans cake.
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| CN110613043A (en) * | 2019-10-09 | 2019-12-27 | 聊城大学 | Donkey-hide gelatin gel tea cake prepared from donkey-hide gelatin jujube processing by-product donkey-hide gelatin jujube pulp |
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Application publication date: 20180313 |