CN107778081A - A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage - Google Patents
A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage Download PDFInfo
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- CN107778081A CN107778081A CN201710983897.8A CN201710983897A CN107778081A CN 107778081 A CN107778081 A CN 107778081A CN 201710983897 A CN201710983897 A CN 201710983897A CN 107778081 A CN107778081 A CN 107778081A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Plant Pathology (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Fertilizers (AREA)
Abstract
It is an object of the invention to provide a kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, Chinese herbal medicine is mainly extracted into Chinese herbal medicine in supercritical fluid extraction instrument Chinese medicine preparation and Chinese medicine dreg is prepared；Then fermentation fertilizer is prepared in Chinese medicine dreg mixing plant ash, stalk, fermentation of apple pulp；Liquid fertilizer is prepared in Chinese medicine preparation and manganese sulfate, boric acid, zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt, ammonium molybdate, is finally mixed with liquid fertilizer and fermentation fertilizer to obtain granular medicine fertilizer；Carbon dioxide supercritical extraction Chinese herbal medicine is used in the present invention, extraction efficiency is high, grows necessary nutrient, and the pest and disease damage for the herbal control tomato for passing through ecological, environmental protective containing tomato in the medicine fertilizer, has preferable biological degradability, more environmentally friendly.
Description
Technical field
The invention belongs to the technical field of the preparation of organic tomato medication fertilizer, and in particular to one kind is organic available for preventing and treating
The preparation method of the medicine fertilizer of tomato pest and disease damage.
Background technology
Organic tomato refers to the tomato planted according to the mode of production of organic agriculture, in the whole life of tomato
The production technical standard of organic food must be followed strictly during production, i.e., completely without using agricultural chemicals, chemical fertilizer, life in production process
The chemical substances such as long conditioning agent, without using gene engineering technique, while independent Organic Food Attestation mechanism must also be passed through
The quality control and examination of overall process, so as to ensure the pollution-free of it, eutrophy and high quality the characteristics of.
Medicine fertilizer is to be formulated agricultural chemicals and fertilizer according to a certain percentage to mix, and by certain technology by fertilizer and
Agricultural chemicals is stable at the novel ecological compound fertilizer formed in specific compound system, typically with the carrier of fertilizer used as pesticides.Pin
To organic tomato, existing medicine fertilizer can not meet to require, not only the absorptivity of tomato is not high, and cause high amount of drug residual
Stay, so that the salinization of soil aggravates while largely inorganic fertilizer and medicine is used, not only break up environment, also result in follow-up western red
The yield degradation of persimmon.
The content of the invention
It is main it is an object of the invention to provide a kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage
If Chinese herbal medicine is extracted into Chinese herbal medicine in supercritical fluid extraction instrument is prepared Chinese medicine preparation and Chinese medicine dreg；Then by
Fermentation fertilizer is prepared in medicine dregs of a decoction mixing plant ash, stalk, fermentation of apple pulp；By Chinese medicine preparation and manganese sulfate, boric acid,
Liquid fertilizer is prepared in zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt, ammonium molybdate, finally mixes liquid fertilizer and fermentation fertilizer
Granular medicine fertilizer is prepared in conjunction；Carbon dioxide supercritical extraction Chinese herbal medicine is used in the present invention, extraction efficiency is high, the medicine
In fertilizer necessary nutrient, and the pest and disease damage for the herbal control tomato for passing through ecological, environmental protective, tool are grown containing tomato
There is preferable biological degradability, it is more environmentally friendly.
The present invention is achieved through the following technical solutions：A kind of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage
Preparation method, mainly include the following steps that：
Step A：By wolfsbane, panax japonicus, dried peppermint leaf, garlic, capsicum leaf, elm bark high temperature sterilization, ground after drying and medicine is made
Powder, medicinal powder is placed in supercritical fluid extraction instrument, carries out co_2 supercritical fluid extraction, isolated Chinese medicinal liquor
And Chinese medicine dreg；
Step B：Caused Chinese medicine dreg mixing plant ash, stalk, pomace in step A are fermented, obtained after fermentation
Fermentation fertilizer；
Step C：By caused Chinese medicinal liquor manganese sulfate in step A, boric acid, zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt,
Liquid fertilizer is prepared in ammonium molybdate；By caused fermentation fertilizer in liquid fertilizer blend step B, drying granulation obtains medicine fertilizer.
In order to preferably realize the present invention, further, the step A traditional Chinese medicine powders are in extraction process, the extraction pressure
Power 25-40Mpa, 40-45 DEG C of extraction temperature, separator pressure 7-12Mpa, 45-60 DEG C of separator temperature, extraction time 3-6h.
In order to preferably realize the present invention, further, the step A traditional Chinese medicine powders are in extraction process, the extraction kettle
Pressure 35Mpa, 38 DEG C of extraction kettle temperature, separator pressure 7Mpa, 50 DEG C of separator temperature, extraction time 4h.
In order to preferably realize the present invention, further, the step A traditional Chinese medicine powders are in supercritical fluid extraction instrument with nothing
The mixed liquor of water-ethanol and carbon dioxide is as spe medium；The mass percent of the absolute ethyl alcohol is 5wt%-10wt%.
In order to preferably realize the present invention, further, the fermentation temperature in the step B is 35-45 DEG C.
In order to preferably realize the present invention, further, the temperature in the medicine fertilizer drying granulation process is 50-65 DEG C.
Contain K, N, P, Zn, Mn, B, Mg and Mo element in the medicine fertilizer.The K elements can promote plant stalk
It is healthy and strong；Promote the activation of enzyme in plant；Promote the utilization of plant pair luminous energy；Be advantageous to the normal respiration of plant, improve energy
Amount metabolism；Strengthen the synthesis and transhipment of material in plant；And it is anti-to strengthen the freeze proof of plant, cold-resistant and insect pest etc.
Property.N is the main component for forming protein, the development important role of growth and fruit to plant stem-leaf, while N
It is the part for synthesizing chlorophyll.P can promote being normally carried out for the various metabolism of plant, and be played in ATP reaction
Key effect, promote growth and development of plants good, while improve the cold-resistant and drought resistance of plant.Zn is main in plant
As the metal activation agent of enzyme, the aquation of carbon dioxide is catalyzed, promotes the fixation of carbon dioxide in photosynthesis.The Mn
Element is the activator of many enzymes in plant cell；The B element is the distinctive indispensable element of higher plant, can be with free shape
The sugar combination of state, makes sugar easily cross over plasma membrane, promotes the transport of sugar, and B has important shadow to the reproductive process of plant
Ring.Mg can activate various transphosphorylases and phosphokinase, can also activate plant in plant photosynthesis and respiratory
One of DNA and RNA building-up process, while be also the synthetic ingredient of chlorophyll.Mo participates in nitrogen metabolism in plant, promoted
The absorption and transhipment of phosphorus, while the transport to carbohydrate also plays an important role.
Beneficial effects of the present invention：
（1）The step A traditional Chinese medicine powders are in extraction process, the extracting pressure 25-40Mpa, 40-45 DEG C of extraction temperature, separation
Device pressure 7-12Mpa, 45-60 DEG C of separator temperature, extraction time 3-6h；The present invention uses carbon dioxide supercritical extraction Chinese medicine
Active ingredient, farthest ensure that not being destroyed for traditional Chinese medicine ingredients, while improve extraction ratio, fully extract Chinese medicine
Composition；
（2）The step A traditional Chinese medicine powders are used as extraction in supercritical fluid extraction instrument using the mixed liquor of absolute ethyl alcohol and carbon dioxide
Take medium；The mass percent of the absolute ethyl alcohol is 5wt%-10wt%；The present invention is extracted using polynary supercritical extraction method
Active ingredient in Chinese medicine, extraction efficiency are higher；
（3）The medicine fertilizer includes plant ash, stalk, pomace, and the present invention carries out secondary use, the vegetation using agricultural residue
Ash, stalk, pomace can provide abundant K, P element for the growth of tomato；
（4）Temperature in the medicine fertilizer drying granulation process is 50-65 DEG C, and the speed for accelerating drying maintains composition
Activity；
（5）The Chinese medicine preparation is extracted, in described by supercritical fluid extraction instrument in the case of CO 2 supercritical
The extraction efficiency of medicine is high, and isolated traditional Chinese medicine liquid and the dregs of a decoction, the dregs of a decoction mixing plant ash, stalk, pomace are fermented
Fermentation fertilizer is prepared；Chinese medicine is made full use of, realizes the full utilization of the energy.
Embodiment
Embodiment 1：
A kind of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, calculates according to mass parts and mainly consists of the following composition：Grass
Wood ash：5 parts；Stalk：25 parts；Pomace：3 parts；Manganese sulfate：2 parts；Boric acid：1.5 part；Zinc sulfate：4 parts；Calcium superphosphate：12 parts；
NaFeEDTA sodium salt：10 parts；Ammonium molybdate：1 part；Chinese medicine preparation：15 parts；
The Chinese medicine preparation is calculated in parts by weight mainly to be consisted of the following composition：Wolfsbane：4 parts；Panax japonicus：4 parts；Peppermint
Leaf：3 parts；Garlic：3 parts；Capsicum leaf：2 parts；10 parts of elm bark；Matrimony vine：3 parts.
A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, is mainly included the following steps that：
Step A：By wolfsbane, panax japonicus, dried peppermint leaf, garlic, capsicum leaf, elm bark high temperature sterilization 15min, system is ground after drying
Into medicinal powder, medicinal powder is placed in supercritical fluid extraction instrument, in extracting pressure 35Mpa, 40 DEG C of extraction temperature, separator pressure
Under conditions of 10Mpa, 50 DEG C of separator temperature, co_2 supercritical fluid extraction 4.5h, isolated Chinese medicinal liquor are carried out
And Chinese medicine dreg；
Step B：Caused Chinese medicine dreg mixing plant ash, stalk, pomace in step A are fermented at 35 DEG C, fermented
Fermentation fertilizer is obtained afterwards；
Step C：By caused Chinese medicinal liquor manganese sulfate in step A, boric acid, zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt,
Liquid fertilizer is prepared in ammonium molybdate；By caused fermentation fertilizer in liquid fertilizer blend step B, drying granulation obtains medicine fertilizer.
The step A traditional Chinese medicine powders are used as extraction in supercritical fluid extraction instrument using the mixed liquor of absolute ethyl alcohol and carbon dioxide
Take medium；The mass percent of the absolute ethyl alcohol is 8wt%.
The medicine being prepared fertilizer is used in the cultivation of organic tomato, count the gray mold of tomato, brown spot,
Leaf mold, droop, grub, the incidence of disease of mole cricket worm；5300 kilograms of the tomato per mu yield using medicine fertilizer is found after statistics,
And the incidence of disease is 3.5%；And the per mu yield for contrasting organic tomato of common inorganic fertilizer cultivation is 4800 kilograms or so, morbidity
Rate is 20% or so；It can be seen that the medicine fertilizer provides abundant growth elements for tomato and effectively reduced
The incidence of disease of the pest and disease damage of tomato.
The present invention is to realize preventing disease and pest by using Chinese medicine preparation, while waste be changed into values on side, by plant ash, stalk, apple
Slag is mixed with to obtain medicine fertilizer；Carbon dioxide supercritical extraction Chinese herbal medicine is used in the present invention, extraction efficiency is high, in the medicine fertilizer
Grow necessary nutrient, and the pest and disease damage for the herbal control tomato for passing through ecological, environmental protective containing tomato, have compared with
Good biological degradability, it is more environmentally friendly.
Embodiment 2：
A kind of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, calculates according to mass parts and mainly consists of the following composition：Grass
Wood ash：7 parts；Stalk：25 parts；Pomace：3 parts；Manganese sulfate：2 parts；Boric acid：1.5 part；Zinc sulfate：4 parts；Calcium superphosphate：12 parts；
NaFeEDTA sodium salt：12 parts；Ammonium molybdate：1 part；Chinese medicine preparation：18 parts；
The Chinese medicine preparation is calculated in parts by weight mainly to be consisted of the following composition：Wolfsbane：5 parts；Panax japonicus：4 parts；Peppermint
Leaf：4 parts；Garlic：3 parts；Capsicum leaf：3 parts；12 parts of elm bark；Matrimony vine：5 parts.
A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, is mainly included the following steps that：
Step A：By wolfsbane, panax japonicus, dried peppermint leaf, garlic, capsicum leaf, elm bark high temperature sterilization 15min, system is ground after drying
Into medicinal powder, medicinal powder is placed in supercritical fluid extraction instrument, in extracting pressure 35Mpa, 38 DEG C of extraction temperature, separator pressure
Under conditions of 7Mpa, 50 DEG C of separator temperature, co_2 supercritical fluid extraction 4h is carried out, isolated Chinese medicinal liquor is with
The medicine dregs of a decoction；
Step B：Caused Chinese medicine dreg mixing plant ash, stalk, pomace in step A are fermented at 40 DEG C, fermented
Fermentation fertilizer is obtained afterwards；
Step C：By caused Chinese medicinal liquor manganese sulfate in step A, boric acid, zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt,
Liquid fertilizer is prepared in ammonium molybdate；By caused fermentation fertilizer in liquid fertilizer blend step B, drying granulation obtains medicine fertilizer.
The step A traditional Chinese medicine powders are used as extraction in supercritical fluid extraction instrument using the mixed liquor of absolute ethyl alcohol and carbon dioxide
Take medium；The mass percent of the absolute ethyl alcohol is 6wt%.
The medicine being prepared fertilizer is used in the cultivation of organic tomato, count the gray mold of tomato, brown spot,
Leaf mold, droop, grub, the incidence of disease of mole cricket worm；5500 kilograms of the tomato per mu yield using medicine fertilizer is found after statistics,
And the incidence of disease is 3.3%；And the per mu yield for contrasting organic tomato of common inorganic fertilizer cultivation is 4800 kilograms or so, morbidity
Rate is 20% or so；It can be seen that the medicine fertilizer provides abundant growth elements for tomato and effectively reduced
The incidence of disease of the pest and disease damage of tomato.
The present invention is to realize preventing disease and pest by using Chinese medicine preparation, while waste be changed into values on side, by plant ash, stalk, apple
Slag is mixed with to obtain medicine fertilizer；Carbon dioxide supercritical extraction Chinese herbal medicine is used in the present invention, extraction efficiency is high, in the medicine fertilizer
Grow necessary nutrient, and the pest and disease damage for the herbal control tomato for passing through ecological, environmental protective containing tomato, have compared with
Good biological degradability, it is more environmentally friendly.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, it is every according to
Any simply modification, the equivalent variations made according to the technical spirit of the present invention to above example, each fall within the protection of the present invention
Within the scope of.
Claims (6)
1. a kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage, it is characterised in that mainly including following
Step：
Step A：By wolfsbane, panax japonicus, dried peppermint leaf, garlic, capsicum leaf, elm bark high temperature sterilization, ground after drying and medicine is made
Powder, medicinal powder is placed in supercritical fluid extraction instrument, carries out co_2 supercritical fluid extraction, isolated Chinese medicinal liquor
And Chinese medicine dreg；
Step B：Caused Chinese medicine dreg mixing plant ash, stalk, pomace in step A are fermented, obtained after fermentation
Fermentation fertilizer；
Step C：By caused Chinese medicinal liquor manganese sulfate in step A, boric acid, zinc sulfate, calcium superphosphate, NaFeEDTA sodium salt,
Liquid fertilizer is prepared in ammonium molybdate；By caused fermentation fertilizer in liquid fertilizer blend step B, drying granulation obtains medicine fertilizer.
2. a kind of preparation method of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage according to claim 1, it is special
Sign is that the step A traditional Chinese medicine powders are in extraction process, the extracting pressure 25-40Mpa, 35-45 DEG C of extraction temperature, separation
Device pressure 7-12Mpa, 45-60 DEG C of separator temperature, extraction time 3-6h.
3. a kind of preparation method of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage according to claim 2, it is special
Sign is that the step A traditional Chinese medicine powders are in extraction process, the extraction kettle pressure 35Mpa, 38 DEG C of extraction kettle temperature, separator
Pressure 7Mpa, 50 DEG C of separator temperature, extraction time 4h.
4. a kind of preparation method of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage according to claim 2, it is special
Sign is that the step A traditional Chinese medicine powders are used as extraction in supercritical fluid extraction instrument using the mixed liquor of absolute ethyl alcohol and carbon dioxide
Take medium；The mass percent of the absolute ethyl alcohol is 5wt%-10wt%.
5. a kind of preparation method of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage according to claim 1, it is special
Sign is that the fermentation temperature in the step B is 35-45 DEG C.
A kind of 6. preparation side of medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage according to claim any one of 1-5
Method, it is characterised in that the temperature in the medicine fertilizer drying granulation process is 50-65 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710983897.8A CN107778081A (en) | 2017-10-20 | 2017-10-20 | A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710983897.8A CN107778081A (en) | 2017-10-20 | 2017-10-20 | A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage |
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| Publication Number | Publication Date |
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| CN107778081A true CN107778081A (en) | 2018-03-09 |
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| CN201710983897.8A Withdrawn CN107778081A (en) | 2017-10-20 | 2017-10-20 | A kind of preparation method for the medicine fertilizer that can be used for preventing and treating organic tomato pest and disease damage |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108739208A (en) * | 2018-06-28 | 2018-11-06 | 全椒县马塘湖农作物种植专业合作社 | A kind of implantation methods improving cotton disease resistance insect pest ability |
-
2017
- 2017-10-20 CN CN201710983897.8A patent/CN107778081A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108739208A (en) * | 2018-06-28 | 2018-11-06 | 全椒县马塘湖农作物种植专业合作社 | A kind of implantation methods improving cotton disease resistance insect pest ability |
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Application publication date: 20180309 |