CN107760438A - A kind of processing method of sesame oil - Google Patents

A kind of processing method of sesame oil Download PDF

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Publication number
CN107760438A
CN107760438A CN201711236130.5A CN201711236130A CN107760438A CN 107760438 A CN107760438 A CN 107760438A CN 201711236130 A CN201711236130 A CN 201711236130A CN 107760438 A CN107760438 A CN 107760438A
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Prior art keywords
sesame
sesame oil
oil
processing method
pressing
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CN201711236130.5A
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Chinese (zh)
Inventor
宋代江
方厚凯
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Bengbu Jianghuai Grain And Oil Co Ltd
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Bengbu Jianghuai Grain And Oil Co Ltd
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Priority to CN201711236130.5A priority Critical patent/CN107760438A/en
Publication of CN107760438A publication Critical patent/CN107760438A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Fats And Perfumes (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention discloses a kind of processing method of sesame oil, including:Sesame is added in sodium hydrate aqueous solution and soaked, washs, peel, drying, microwave treatment must pre-process sesame;Pretreatment sesame is added into single pressing in hydraulic oil press and obtains single pressing sesame oil and squeezing sesame-send cake;Squeezing sesame-send cake is added into twice pressing in hydraulic oil press and obtains twice pressing sesame oil;Single pressing sesame oil and twice pressing sesame oil are mixed into obtain crude oil;Crushed after radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf are air-dried, carbon dioxide supercritical extraction obtains plant extracts after microwave treatment;Plant extracts, resveratrol, organic acid are added in crude oil, decolourizes, stand, filtering the sesame oil that must decolourize;Diatomite is added after decolouring sesame oil is cooled down, is stood, filtering.The processing method of sesame oil proposed by the present invention, process is simple, and beneficial to industrialization, oil yield is high, remains the protein in sesame-send cake, and obtained sesame oil is of light color, and transparency is high, quality better.

Description

A kind of processing method of sesame oil
Technical field
The present invention relates to sesame oil technical field, more particularly to a kind of processing method of sesame oil.
Background technology
Sesame is not only containing the grease and protein enriched, also good health care and medical value.In recent years, Chinese sesame And the consumption figure of sesame converted products increases year by year.Sesame oil has special fragrance, just likes always for people since ancient times Table oil.At present, the production technology of sesame oil has water substitution and milling process.Milling process due to automatic control level it is high, Can be to turn into major way developed in recent years the advantages that continuous production, but the sesame oil that traditional milling process is produced Color and luster is bad, poor transparency, and nutrition and active material loss are big, while sesame protein gross distortion and destruction, cause sesame Numb cake, slag can only cause the waste of sesame protein resource as cheap feed applications.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of processing method of sesame oil, the letter of its process Single, beneficial to industrialization, and oil yield is high, while remains the protein in sesame-send cake, and obtained sesame oil is of light color, transparency Height, quality better.
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 40-45 DEG C of sodium hydrate aqueous solution and soaks 40-50min, washed to neutrality, after decortication Dry, then carry out microwave treatment 10-15min and obtain pre-processing sesame, wherein, the power of microwave treatment is 600-700W;
S2, single pressing 30-50min will be carried out in pretreatment sesame addition hydraulic oil press, release obtains single pressing Sesame oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 55-65 DEG C, and the pressure of single pressing is 50-60MPa;Will pressure Squeeze progress twice pressing 10-35min in sesame-send cake addition hydraulic oil press and obtain twice pressing sesame oil, wherein, twice pressing Temperature be 45-55 DEG C, the pressure of twice pressing is 65-70MPa;Single pressing sesame oil and twice pressing sesame oil are mixed Obtain crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then progress microwave treatment 10-30min, micro- The power of ripple processing is 100-250W, then obtains plant extracts through carbon dioxide supercritical extraction;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;
S5, decolouring sesame oil is cooled to 0-7 DEG C, adds diatomite and stir, stand, filter after obtain sesame oil.
Preferably, in S1, the solid-to-liquid ratio of sesame and sodium hydrate aqueous solution is 1:2-3.5g/mL.
Preferably, it is 3-6wt% to be dried in S1, after decortication to water content.
Preferably, in S2, added after pretreatment sesame is wrapped up with cotton in hydraulic oil press.
Preferably, in S2, loose rear add in hydraulic oil press of sesame-send cake will be squeezed and carry out twice pressing.
Preferably, in S3, radix glycyrrhizae, Momordica grosvenori, the bark of eucommia, the weight ratio of garlic cauline leaf are 2-5:1-4:2-10:2-9.
Preferably, in S3, during carbon dioxide supercritical extraction, pressure 20-25MPa, temperature 53-57 DEG C, extraction time 1.2-2h.
Preferably, in S4, per in 1kg crude oils, plant extracts 100-150mg, resveratrol 200-250mg are added, Organic acid 30-100mg.
Preferably, in S4, the organic acid is one or two kinds of mixture in phytic acid, citric acid.
Preferably, in S5, the speed of stirring is 15-20r/min.
Preferably, in S5, the time of standing is 10-15h.
The processing method of sesame oil of the present invention, sesame is added in sodium hydrate aqueous solution and soaked, and peeled Processing, sesame oil mouthfeel bitterness is avoided, improve the quality of gained sesame oil;Microwave treatment is carried out, improves follow-up squeezing Oil yield, while the peroxide value of sesame oil can be improved, improve the inoxidizability of sesame oil, extend the storage of sesame oil Phase;Cold pressing is carried out using oil press, remains the nutriment of sesame oil to greatest extent, while improve the color of sesame oil Pool, acid value and peroxide value, so as to get the shallow limpid, fragrant taste of sesame oil colours, oxidation resistance is good;With radix glycyrrhizae, Momordica grosvenori, The bark of eucommia, garlic cauline leaf are the plant extracts that raw material obtains, and on the one hand provide a variety of nutriments for human body, assign sesame oil Certain healthcare function, while coordinate with resveratrol and organic acid, the oxidation resistance of sesame oil can be significantly improved, it is therefore prevented that Because stability reduces caused by decortication is handled the defects of, the stability of sesame oil is improved, makes color and luster, the acid of gained sesame oil Valency, peroxide value meet the standard of country.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 45 DEG C of sodium hydrate aqueous solution and soaks 40min, washed to neutrality, dried after decortication, so Microwave treatment 15min is carried out afterwards to obtain pre-processing sesame, wherein, the power of microwave treatment is 600W;
S2, single pressing 30min will be carried out in pretreatment sesame addition hydraulic oil press, release obtains single pressing sesame Oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 65 DEG C, and the pressure of single pressing is 50MPa;Squeezing sesame-send cake is added Enter to carry out twice pressing 35min in hydraulic oil press to obtain twice pressing sesame oil, wherein, the temperature of twice pressing is 45 DEG C, The pressure of twice pressing is 70MPa;Single pressing sesame oil and twice pressing sesame oil are mixed to get crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then carry out microwave treatment 10min, microwave The power of processing is 250W, then obtains plant extracts through carbon dioxide supercritical extraction;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;
S5, decolouring sesame oil is cooled to 0 DEG C, adds diatomite and stir, stand, filter after obtain sesame oil.
Embodiment 2
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 40 DEG C of sodium hydrate aqueous solution and soaks 50min, washed to neutrality, dried after decortication, so Microwave treatment 10min is carried out afterwards to obtain pre-processing sesame, wherein, the power of microwave treatment is 700W;
S2, single pressing 50min will be carried out in pretreatment sesame addition hydraulic oil press, release obtains single pressing sesame Oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 55 DEG C, and the pressure of single pressing is 60MPa;Squeezing sesame-send cake is added Enter to carry out twice pressing 10min in hydraulic oil press to obtain twice pressing sesame oil, wherein, the temperature of twice pressing is 55 DEG C, The pressure of twice pressing is 65MPa;Single pressing sesame oil and twice pressing sesame oil are mixed to get crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then carry out microwave treatment 30min, microwave The power of processing is 100W, then obtains plant extracts through carbon dioxide supercritical extraction;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;
S5, decolouring sesame oil is cooled to 7 DEG C, adds diatomite and stir, stand, filter after obtain sesame oil.
Embodiment 3
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 43 DEG C of sodium hydrate aqueous solution and soaks 44min, washed to neutrality, dried extremely after decortication Water content is 6wt%, then carries out microwave treatment 12min and obtains pre-processing sesame, wherein, sesame and sodium hydrate aqueous solution Solid-to-liquid ratio is 1:2g/mL, the power of microwave treatment is 630W;
S2, will pretreatment sesame wrapped up with cotton after add hydraulic oil press in carry out single pressing 33min, release obtains Single pressing sesame oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 63 DEG C, and the pressure of single pressing is 54MPa;Will Progress twice pressing 30min in hydraulic oil press is added after squeezing sesame-send cake is loose and obtains twice pressing sesame oil, wherein, it is secondary The temperature of squeezing is 48 DEG C, and the pressure of twice pressing is 68MPa;Single pressing sesame oil and twice pressing sesame oil are mixed To crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then carry out microwave treatment 16min, microwave The power of processing is 220W, then obtains plant extracts through carbon dioxide supercritical extraction;Wherein, radix glycyrrhizae, Momordica grosvenori, Du Secondary, garlic cauline leaf weight ratio is 2:4:2:9;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;Wherein, per in 1kg crude oils, the plant extracts of addition is 100mg, resveratrol 250mg, organic acid 30mg;Institute It is phytic acid to state organic acid;
S5, decolouring sesame oil is cooled to 2 DEG C, adds diatomite and stir, the speed of stirring is 15r/min, is stood 15h, sesame oil is obtained after filtering.
Embodiment 4
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 42 DEG C of sodium hydrate aqueous solution and soaks 48min, washed to neutrality, dried extremely after decortication Water content is 3wt%, then carries out microwave treatment 14min and obtains pre-processing sesame, wherein, sesame and sodium hydrate aqueous solution Solid-to-liquid ratio is 1:3.5g/mL, the power of microwave treatment is 680W;
S2, will pretreatment sesame wrapped up with cotton after add hydraulic oil press in carry out single pressing 42min, release obtains Single pressing sesame oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 57 DEG C, and the pressure of single pressing is 58MPa;Will Progress twice pressing 15min in hydraulic oil press is added after squeezing sesame-send cake is loose and obtains twice pressing sesame oil, wherein, it is secondary The temperature of squeezing is 53 DEG C, and the pressure of twice pressing is 66MPa;Single pressing sesame oil and twice pressing sesame oil are mixed To crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then carry out microwave treatment 26min, microwave The power of processing is 150W, then obtains plant extracts through carbon dioxide supercritical extraction;Wherein, radix glycyrrhizae, Momordica grosvenori, Du Secondary, garlic cauline leaf weight ratio is 5:1:10:2;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;Wherein, per in 1kg crude oils, the plant extracts of addition is 150mg, resveratrol 200mg, organic acid 100mg; The organic acid is citric acid;
S5, decolouring sesame oil is cooled to 6 DEG C, adds diatomite and stir, the speed of stirring is 20r/min, is stood 10h, sesame oil is obtained after filtering.
Embodiment 5
A kind of processing method of sesame oil proposed by the present invention, comprises the following steps:
S1, sesame is added in 43 DEG C of sodium hydrate aqueous solution and soaks 45min, washed to neutrality, dried extremely after decortication Water content is 4wt%, then carries out microwave treatment 13min and obtains pre-processing sesame, wherein, sesame and sodium hydrate aqueous solution Solid-to-liquid ratio is 1:2.8g/mL, the power of microwave treatment is 650W;
S2, will pretreatment sesame wrapped up with cotton after add hydraulic oil press in carry out single pressing 40min, release obtains Single pressing sesame oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 60 DEG C, and the pressure of single pressing is 55MPa;Will Progress twice pressing 30min in hydraulic oil press is added after squeezing sesame-send cake is loose and obtains twice pressing sesame oil, wherein, it is secondary The temperature of squeezing is 48 DEG C, and the pressure of twice pressing is 67MPa;Single pressing sesame oil and twice pressing sesame oil are mixed To crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then carry out microwave treatment 30min, microwave The power of processing is 200W, then obtains plant extracts through carbon dioxide supercritical extraction;Wherein, radix glycyrrhizae, Momordica grosvenori, Du Secondary, garlic cauline leaf weight ratio is 3:3:5:4;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame Sesame oil;Wherein, per in 1kg crude oils, the plant extracts of addition is 110mg, resveratrol 220mg, organic acid 70mg;Institute It is 3 that organic acid, which is stated, as phytic acid, the mixture of citric acid, and the weight ratio of phytic acid, citric acid:2;
S5, decolouring sesame oil is cooled to 5 DEG C, adds diatomite and stir, the speed of stirring is 17r/min, is stood 14h, sesame oil is obtained after filtering.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (10)

1. a kind of processing method of sesame oil, it is characterised in that comprise the following steps:
S1, sesame is added in 40-45 DEG C of sodium hydrate aqueous solution and soaks 40-50min, washed to neutrality, dried after decortication, Then microwave treatment 10-15min is carried out to obtain pre-processing sesame, wherein, the power of microwave treatment is 600-700W;
S2, single pressing 30-50min will be carried out in pretreatment sesame addition hydraulic oil press, release obtains single pressing sesame Oil and squeezing sesame-send cake, wherein, the temperature of single pressing is 55-65 DEG C, and the pressure of single pressing is 50-60MPa;Sesame will be squeezed Numb cake adds progress twice pressing 10-35min in hydraulic oil press and obtains twice pressing sesame oil, wherein, the temperature of twice pressing Spend for 45-55 DEG C, the pressure of twice pressing is 65-70MPa;Single pressing sesame oil and twice pressing sesame oil are mixed to get Crude oil;
S3, crushed after air-drying radix glycyrrhizae, Momordica grosvenori, the bark of eucommia and garlic cauline leaf, then progress microwave treatment 10-30min, at microwave The power of reason is 100-250W, then obtains plant extracts through carbon dioxide supercritical extraction;
S4, by plant extracts, resveratrol and organic acid add crude oil in, stood after decolouring, be filtrated to get decolouring sesame oil;
S5, decolouring sesame oil is cooled to 0-7 DEG C, adds diatomite and stir, stand, filter after obtain sesame oil.
2. the processing method of sesame oil according to claim 1, it is characterised in that in S1, sesame is water-soluble with sodium hydroxide The solid-to-liquid ratio of liquid is 1:2-3.5g/mL.
3. the processing method of sesame oil according to claim 1 or claim 2, it is characterised in that in S1, dried after decortication to aqueous Measure as 3-6wt%.
4. according to the processing method of sesame oil any one of claim 1-3, it is characterised in that in S2, will pre-process Sesame is added in hydraulic oil press after being wrapped up with cotton.
5. according to the processing method of sesame oil any one of claim 1-4, it is characterised in that in S2, sesame will be squeezed Added after numb cake is loose in hydraulic oil press and carry out twice pressing.
6. according to the processing method of sesame oil any one of claim 1-5, it is characterised in that in S3, radix glycyrrhizae, arhat Fruit, the bark of eucommia, the weight ratio of garlic cauline leaf are 2-5:1-4:2-10:2-9.
7. according to the processing method of sesame oil any one of claim 1-6, it is characterised in that in S4, per 1kg crude oils In, add plant extracts 100-150mg, resveratrol 200-250mg, organic acid 30-100mg.
8. according to the processing method of sesame oil any one of claim 1-7, it is characterised in that described organic in S4 Acid is phytic acid, one or two kinds of mixture in citric acid.
9. according to the processing method of sesame oil any one of claim 1-8, it is characterised in that in S5, the speed of stirring Rate is 15-20r/min.
10. according to the processing method of sesame oil any one of claim 1-9, it is characterised in that in S5, standing when Between be 10-15h.
CN201711236130.5A 2017-11-30 2017-11-30 A kind of processing method of sesame oil Withdrawn CN107760438A (en)

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CN108998198A (en) * 2018-06-29 2018-12-14 襄阳三珍生态农业有限公司 A kind of processing technology of coldly-squeezed sesame oil
CN109161434A (en) * 2018-08-15 2019-01-08 合肥市金乡味工贸有限责任公司 A kind of preparation method of high oxidation stability coldly-squeezed sesame oil

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CN107125335A (en) * 2017-05-25 2017-09-05 含山县正隆油脂有限公司 A kind of formula of sesame oil

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108998198A (en) * 2018-06-29 2018-12-14 襄阳三珍生态农业有限公司 A kind of processing technology of coldly-squeezed sesame oil
CN109161434A (en) * 2018-08-15 2019-01-08 合肥市金乡味工贸有限责任公司 A kind of preparation method of high oxidation stability coldly-squeezed sesame oil

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Application publication date: 20180306