CN107724116A - A kind of bristles coloring agent - Google Patents
A kind of bristles coloring agent Download PDFInfo
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- CN107724116A CN107724116A CN201710853913.1A CN201710853913A CN107724116A CN 107724116 A CN107724116 A CN 107724116A CN 201710853913 A CN201710853913 A CN 201710853913A CN 107724116 A CN107724116 A CN 107724116A
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Abstract
The invention discloses a kind of bristles coloring agent, its raw material includes：Natural dye, chrome yellow, talcum powder, rare earth, alum, alum, calcium carbonate, zinc sulfate, potassium chloride, sodium hydroxide, chitosan, sodium benzoate, penetrating agent JFC, polyvinyl alcohol, propane diols, catechin, APG, hydroxymethyl cellulose, propylene glycol methyl ether acetate, PTPP, polyacrylate, ethyl benzoate, epoxidized soybean oil, butyl titanate, deionized water.A kind of bristles coloring agent proposed by the present invention, pollution is small, and staining efficiency is high, upper color depth and uniformly, bristles have good light resistance and temperature tolerance after dyeing, not fugitive color, good color fastness, while bristles wearability and pliability are improved, effectively extend the service life of bristles product.
Description
Technical field
The present invention relates to coloring agent technical field, more particularly to a kind of bristles coloring agent.
Background technology
Bristles refer to pig neck and more than 5 centimetres of bristle of back growth, be commonly used for preparing daily bruss, paintbrush,
Machine brush etc..The color of bristles mainly has black, white, yellow and pattern.Natural yellow bristles yield is few, can not meet reality
Production needs, and coloring agent used in bristles is big in the presence of pollution at present, and staining efficiency is low, shallow and uneven, bristles after dyeing of painting
Light resistance and temperature tolerance are poor, fugitive color, and can not effectively improve bristles wearability and pliability, and influence bristles product uses the longevity
Life.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of bristles coloring agent, and pollution is small, dyeing effect
Rate is high, upper color depth and uniformly, and bristles have good light resistance and temperature tolerance after dyeing, not fugitive color, good color fastness, carry simultaneously
High bristles wearability and pliability, effectively extend the service life of bristles product.
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：Natural dye 12-18 parts, chrome yellow
1-1.5 parts, talcum powder 0.5-1 parts, rare earth 0.5-1 parts, alum 0.2-0.4 parts, alum 0.1-0.3 parts, calcium carbonate
0.1-0.2 parts, zinc sulfate 0.2-0.4 parts, potassium chloride 0.4-0.6 parts, sodium hydroxide 0.1-0.4 parts, chitosan 0.4-0.8 parts,
Sodium benzoate 0.6-0.8 parts, penetrating agent JFC 0.2-0.4 parts, polyvinyl alcohol 0.2-0.5 parts, propane diols 0.4-0.8 parts, catechu
Plain 0.02-0.1 parts, APG 0.6-1.2 parts, hydroxymethyl cellulose 0.2-0.4 parts, propylene glycol methyl ether acetate 0.2-0.5
Part, PTPP 0.1-0.3 parts, polyacrylate 0.2-0.4 parts, ethyl benzoate 0.2-0.4 parts, epoxidized soybean oil 0.6-
1.5 parts, butyl titanate 0.2-0.6 parts, deionized water 50-80 parts.
In embodiment, the parts by weight of natural dye can also be 13,14,15,16,17 parts, the parts by weight of chrome yellow
Can also be 1.1,1.2,1.25,1.3,1.4 parts, the parts by weight of talcum powder can also be 0.6,0.7,0.75,0.8,0.9 part,
The parts by weight of rare earth can also be 0.6,0.7,0.75,0.8,0.9 part, the parts by weight of alum can also be 0.24,0.28,
0.3rd, 0.32,0.35,0.38 part, the parts by weight of alum can also be 0.14,0.18,0.22,0.25,0.28 part, carbonic acid
The parts by weight of calcium can also be 0.12,0.14,0.15,0.16,0.18 part, the parts by weight of zinc sulfate can also be 0.24,0.28,
0.3rd, 0.32,0.35,0.38 part, the parts by weight of potassium chloride can also be 0.44,0.48,0.5,0.52,0.55,0.58 part, hydrogen
The parts by weight of sodium oxide molybdena can also be 0.15,0.2,0.25,0.3,0.35 part, the parts by weight of chitosan can also be 0.45,
0.5th, 0.55,0.6,0.65,0.7 part, the parts by weight of sodium benzoate can also be 0.64,0.68,0.72,0.75,0.78 part, ooze
Saturating agent JFC parts by weight can also be 0.24,0.28,0.3,0.32,0.35,0.38 part, and the parts by weight of polyvinyl alcohol can be with
For 0.25,0.3,0.35,0.4,0.45 part, the parts by weight of propane diols can also be 0.25,0.3,0.35,0.4,0.45 part, youngster
The parts by weight of theine can also be 0.14,0.18,0.22,0.25,0.28 part, the parts by weight of APG can also be 0.7,
0.8th, 0.85,0.9,1,1.1 part, the parts by weight of hydroxymethyl cellulose can also be 0.24,0.28,0.3,0.32,0.35,0.38
Part, the parts by weight of propylene glycol methyl ether acetate can also be 0.25,0.3,0.35,0.4,0.45 part, the weight of PTPP
Part can also be 0.14,0.18,0.2,0.22,0.25,0.28 part, the parts by weight of polyacrylate can also be 0.24,0.28,
0.3rd, 0.32,0.35,0.38 part, the parts by weight of ethyl benzoate can also be 0.24,0.28,0.3,0.32,0.35,0.38
Part, the parts by weight of epoxidized soybean oil can also be 0.7,0.8,1,1.2,1.3,1.4 part, and the parts by weight of butyl titanate can be with
For 0.25,0.3,0.35,0.4,0.5 part, the parts by weight of deionized water can also be 55,60,65,70,75 parts.
Preferably, its raw material includes by weight：Natural dye 14-17 parts, chrome yellow 1.1-1.4 parts, talcum powder 0.6-0.9
Part, rare earth 0.6-0.9 parts, alum 0.25-0.35 parts, alum 0.15-0.25 parts, calcium carbonate 0.12-0.18 parts, sulphur
Sour zinc 0.25-0.35 parts, potassium chloride 0.45-0.55 parts, sodium hydroxide 0.2-0.3 parts, chitosan 0.5-0.7 parts, sodium benzoate
0.65-0.75 parts, penetrating agent JFC 0.25-0.35 parts, polyvinyl alcohol 0.3-0.4 parts, propane diols 0.5-0.7 parts, catechin
0.04-0.08 parts, APG 0.7-1.1 parts, hydroxymethyl cellulose 0.25-0.35 parts, propylene glycol methyl ether acetate 0.3-0.4
Part, PTPP 0.15-0.25 parts, polyacrylate 0.25-0.35 parts, ethyl benzoate 0.25-0.35 parts, epoxy soybean
Oily 0.8-1.2 parts, butyl titanate 0.3-0.5 parts, deionized water 60-70 parts.
Preferably, natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 2-4 time, merging extract solution obtains
Material B；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
S3, material B, material D mixed with curcumin, obtain natural dye.
Preferably, in S1, the weight ratio between rheum officinale, mango core and solvent orange 2 A is 1-3:2-5:25-30.
Preferably, in S1, solvent orange 2 A is the ethanol water that volume fraction is 55-62%.
Preferably, in S1, Extracting temperature is 82-90 DEG C, extraction time 30-40min.
Preferably, in S2, the weight ratio between banana skin, corn flour, solvent C is 1-2:2-4:25-30.
Preferably, in S2, solvent C is the ethanol water that volume fraction is 72-80%.
Preferably, in S2, technological parameter is as follows in microwave processing process：Microwave power is 300-350W, and the microwave time is
7-13min。
Preferably, in S3, the weight ratio between material B, material D, curcumin is 6-10:3-5:1-1.5.
Inventive article is made using conventional fabrication process.
In a kind of bristles coloring agent proposed in the present invention, for natural dye by optimizing preparation technology, effectively extraction is big
Pigment in Huang, mango core, banana skin and corn flour, is mixed with curcumin, and obtained natural dye is green, biodegradable
Property it is good, there is the function such as good antibacterial, antiultraviolet, add in inventive article, Color is obvious, bright in luster, with
Chrome yellow, talcum powder, rare earth, alum, alum, calcium carbonate, zinc sulfate, potassium chloride, sodium hydroxide, chitosan, benzene first
Sour sodium, penetrating agent JFC, polyvinyl alcohol, propane diols, catechin, APG, hydroxymethyl cellulose, propylene glycol methyl ether acetate,
PTPP, polyacrylate, ethyl benzoate, epoxidized soybean oil, butyl titanate and deionized water coordinate, and have collaboration
Effect, there is the effect such as good wetting and dredging pore to bristles, be effectively improved bristles surface-active, osmotic effect is good, dye
Color depth, dye-uptake is high, and colouring is uniform, good color fastness, is effectively improved bristles wearability, light resistance, temperature tolerance, and effectively improve pig
The mechanical properties such as hair on the neck elasticity, pliability, synthesis improve bristles quality, effectively extend the service life of bristles product.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：12 parts of natural dye, chrome yellow 1.5
Part, 0.5 part of talcum powder, 1 part of rare earth, 0.2 part of alum, 0.3 part of alum, 0.1 part of calcium carbonate, 0.4 part of zinc sulfate, chlorine
Change 0.4 part of potassium, 0.4 part of sodium hydroxide, 0.4 part of chitosan, 0.8 part of sodium benzoate, 0.2 part of penetrating agent JFC, polyvinyl alcohol 0.5
Part, 0.4 part of propane diols, 0.1 part of catechin, 0.6 part of APG, 0.4 part of hydroxymethyl cellulose, propylene glycol methyl ether acetate
0.2 part, 0.3 part of PTPP, 0.2 part of polyacrylate, 0.4 part of ethyl benzoate, 0.6 part of epoxidized soybean oil, metatitanic acid four
0.6 part of butyl ester, 50 parts of deionized water.
Embodiment 2
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：18 parts of natural dye, 1 part of chrome yellow,
1 part of talcum powder, 0.5 part of rare earth, 0.4 part of alum, 0.1 part of alum, 0.2 part of calcium carbonate, 0.2 part of zinc sulfate, chlorination
0.6 part of potassium, 0.1 part of sodium hydroxide, 0.8 part of chitosan, 0.6 part of sodium benzoate, 0.4 part of penetrating agent JFC, polyvinyl alcohol 0.2
Part, 0.8 part of propane diols, 0.02 part of catechin, 1.2 parts of APG, 0.2 part of hydroxymethyl cellulose, propylene glycol methyl ether acetate
0.5 part, 0.1 part of PTPP, 0.4 part of polyacrylate, 0.2 part of ethyl benzoate, 1.5 parts of epoxidized soybean oil, metatitanic acid four
0.2 part of butyl ester, 80 parts of deionized water.
Wherein, natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 2 times, merge extract solution and obtain thing
Expect B；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
S3, material B, material D mixed with curcumin, obtain natural dye.
Embodiment 3
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：14.5 parts of natural dye, chrome yellow
1.25 parts, 0.8 part of talcum powder, 0.75 part of rare earth, 0.32 part of alum, 0.22 part of alum, 0.15 part of calcium carbonate, sulfuric acid
0.3 part of zinc, 0.52 part of potassium chloride, 0.25 part of sodium hydroxide, 0.62 part of chitosan, 0.7 part of sodium benzoate, penetrating agent JFC 0.3
Part, 0.35 part of polyvinyl alcohol, 0.6 part of propane diols, 0.06 part of catechin, 1 part of APG, 0.32 part of hydroxymethyl cellulose, third
0.35 part of glycol methyl ether acetate, 0.22 part of PTPP, 0.3 part of polyacrylate, 0.3 part of ethyl benzoate, epoxy are big
1 part of soya-bean oil, 0.4 part of butyl titanate, 70 parts of deionized water.
Wherein, natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 3 times, merge extract solution and obtain thing
Expect B；Wherein, the weight ratio between rheum officinale, mango core and solvent orange 2 A is 2:3:28；Solvent orange 2 A is the ethanol water that volume fraction is 60%
Solution；Extracting temperature is 85 DEG C, extraction time 35min；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
Wherein, the weight ratio between banana skin, corn flour, solvent C is 1.5:3:28；Solvent C is the ethanol water that volume fraction is 75%
Solution；Technological parameter is as follows in microwave processing process：Microwave power is 320W, and the microwave time is 10min；
S3, by material B, material D and curcumin using weight ratio as 8:4:1.2 mixing, obtain natural dye.
Embodiment 4
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：13.5 parts of natural dye, chrome yellow
1.25 parts, 0.6 part of talcum powder, 0.65 part of rare earth, 0.25 part of alum, 0.15 part of alum, 0.12 part of calcium carbonate, sulfuric acid
0.25 part of zinc, 0.45 part of potassium chloride, 0.2 part of sodium hydroxide, 0.55 part of chitosan, 0.65 part of sodium benzoate, penetrating agent JFC
0.25 part, 0.25 part of polyvinyl alcohol, 0.45 part of propane diols, 0.04 part of catechin, 0.75 part of APG, hydroxymethyl cellulose
0.25 part, 0.25 part of propylene glycol methyl ether acetate, 0.15 part of PTPP, 0.25 part of polyacrylate, ethyl benzoate
0.25 part, 0.75 part of epoxidized soybean oil, 0.3 part of butyl titanate, 60 parts of deionized water.
Wherein, natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 4 times, merge extract solution and obtain thing
Expect B；Wherein, the weight ratio between rheum officinale, mango core and solvent orange 2 A is 3:5:30；Solvent orange 2 A is the ethanol water that volume fraction is 62%
Solution；Extracting temperature is 90 DEG C, extraction time 30min；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
Wherein, the weight ratio between banana skin, corn flour, solvent C is 2:4:30；Solvent C is that the ethanol that volume fraction is 80% is water-soluble
Liquid；Technological parameter is as follows in microwave processing process：Microwave power is 350W, and the microwave time is 7min；
S3, by material B, material D and curcumin using weight ratio as 10:5:1.5 mixing, obtain natural dye.
Embodiment 5
A kind of bristles coloring agent proposed by the present invention, its raw material include by weight：16.5 parts of natural dye, chrome yellow
1.4 parts, 0.85 part of talcum powder, 0.8 part of rare earth, 0.35 part of alum, 0.25 part of alum, 0.18 part of calcium carbonate, sulfuric acid
0.35 part of zinc, 0.5 part of potassium chloride, 0.3 part of sodium hydroxide, 0.7 part of chitosan, 0.75 part of sodium benzoate, penetrating agent JFC 0.35
Part, 0.4 part of polyvinyl alcohol, 0.7 part of propane diols, 0.08 part of catechin, 1 part of APG, 0.35 part of hydroxymethyl cellulose, the third two
0.45 part of alcohol methyl ether acetate, 0.25 part of PTPP, 0.34 part of polyacrylate, 0.35 part of ethyl benzoate, epoxy are big
1.4 parts of soya-bean oil, 0.5 part of butyl titanate, 70 parts of deionized water.
Wherein, natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 2 times, merge extract solution and obtain thing
Expect B；Wherein, the weight ratio between rheum officinale, mango core and solvent orange 2 A is 1:2:25；Solvent orange 2 A is the ethanol water that volume fraction is 55%
Solution；Extracting temperature is 82 DEG C, extraction time 40min；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
Wherein, the weight ratio between banana skin, corn flour, solvent C is 1:2:25；Solvent C is that the ethanol that volume fraction is 72% is water-soluble
Liquid；Technological parameter is as follows in microwave processing process：Microwave power is 300W, and the microwave time is 13min；
S3, by material B, material D and curcumin using weight ratio as 6:3:1 mixing, obtains natural dye.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (10)
1. a kind of bristles coloring agent, it is characterised in that its raw material includes by weight：Natural dye 12-18 parts, chrome yellow 1-
1.5 parts, talcum powder 0.5-1 parts, rare earth 0.5-1 parts, alum 0.2-0.4 parts, alum 0.1-0.3 parts, calcium carbonate
0.1-0.2 parts, zinc sulfate 0.2-0.4 parts, potassium chloride 0.4-0.6 parts, sodium hydroxide 0.1-0.4 parts, chitosan 0.4-0.8 parts,
Sodium benzoate 0.6-0.8 parts, penetrating agent JFC 0.2-0.4 parts, polyvinyl alcohol 0.2-0.5 parts, propane diols 0.4-0.8 parts, catechu
Plain 0.02-0.1 parts, APG 0.6-1.2 parts, hydroxymethyl cellulose 0.2-0.4 parts, propylene glycol methyl ether acetate 0.2-0.5
Part, PTPP 0.1-0.3 parts, polyacrylate 0.2-0.4 parts, ethyl benzoate 0.2-0.4 parts, epoxidized soybean oil 0.6-
1.5 parts, butyl titanate 0.2-0.6 parts, deionized water 50-80 parts.
2. bristles coloring agent according to claim 1, it is characterised in that its raw material includes by weight：Natural dye 14-
17 parts, chrome yellow 1.1-1.4 parts, talcum powder 0.6-0.9 parts, rare earth 0.6-0.9 parts, alum 0.25-0.35 parts, alum
0.15-0.25 parts, calcium carbonate 0.12-0.18 parts, zinc sulfate 0.25-0.35 parts, potassium chloride 0.45-0.55 parts, sodium hydroxide
0.2-0.3 parts, chitosan 0.5-0.7 parts, sodium benzoate 0.65-0.75 parts, penetrating agent JFC 0.25-0.35 parts, polyvinyl alcohol
0.3-0.4 parts, propane diols 0.5-0.7 parts, catechin 0.04-0.08 parts, APG 0.7-1.1 parts, hydroxymethyl cellulose
0.25-0.35 parts, propylene glycol methyl ether acetate 0.3-0.4 parts, PTPP 0.15-0.25 parts, polyacrylate 0.25-
0.35 part, ethyl benzoate 0.25-0.35 parts, epoxidized soybean oil 0.8-1.2 parts, butyl titanate 0.3-0.5 parts, deionized water
60-70 parts.
3. bristles coloring agent according to claim 1 or claim 2, it is characterised in that natural dye is prepared by following technique：
S1, rheum officinale and mango core cleaned, dry, crush, then add solvent orange 2 A and extract 2-4 time, merging extract solution obtains material
B；
S2, mixed after banana skin is crushed with corn flour, add solvent C, microwave treatment, filter, concentration, obtain material D；
S3, material B, material D mixed with curcumin, obtain natural dye.
4. according to bristles coloring agent any one of claim 1-3, it is characterised in that in S1, rheum officinale, mango core with it is molten
Weight ratio between agent A is 1-3:2-5:25-30.
5. according to bristles coloring agent any one of claim 1-4, it is characterised in that in S1, solvent orange 2 A is volume fraction
For 55-62% ethanol water.
6. according to bristles coloring agent any one of claim 1-5, it is characterised in that in S1, Extracting temperature 82-90
DEG C, extraction time 30-40min.
7. according to bristles coloring agent any one of claim 1-6, it is characterised in that in S2, banana skin, corn flour,
Weight ratio between solvent C is 1-2:2-4:25-30.
8. according to bristles coloring agent any one of claim 1-7, it is characterised in that in S2, solvent C is volume fraction
For 72-80% ethanol water.
9. according to bristles coloring agent any one of claim 1-8, it is characterised in that in S2, in microwave processing process
Technological parameter is as follows：Microwave power is 300-350W, and the microwave time is 7-13min.
10. according to bristles coloring agent any one of claim 1-9, it is characterised in that in S3, material B, material D, ginger
Weight ratio between flavine is 6-10:3-5:1-1.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710853913.1A CN107724116A (en) | 2017-09-20 | 2017-09-20 | A kind of bristles coloring agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710853913.1A CN107724116A (en) | 2017-09-20 | 2017-09-20 | A kind of bristles coloring agent |
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| CN107724116A true CN107724116A (en) | 2018-02-23 |
Family
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| CN201710853913.1A Withdrawn CN107724116A (en) | 2017-09-20 | 2017-09-20 | A kind of bristles coloring agent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111021102A (en) * | 2019-12-30 | 2020-04-17 | 珠海华大浩宏化工有限公司 | Silicon-free re-dyeing auxiliary and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107177993A (en) * | 2017-07-03 | 2017-09-19 | 吴江市意胜纺织有限公司 | A kind of textile dyestuff added with chitosan and preparation method thereof |
-
2017
- 2017-09-20 CN CN201710853913.1A patent/CN107724116A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107177993A (en) * | 2017-07-03 | 2017-09-19 | 吴江市意胜纺织有限公司 | A kind of textile dyestuff added with chitosan and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 何瑾馨: "《染料化学 第2版》", 31 October 2016, 中国纺织出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111021102A (en) * | 2019-12-30 | 2020-04-17 | 珠海华大浩宏化工有限公司 | Silicon-free re-dyeing auxiliary and preparation method thereof |
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