CN107723133A - A kind of glass material minute surface cleaning combination and its preparation technology - Google Patents

A kind of glass material minute surface cleaning combination and its preparation technology Download PDF

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Publication number
CN107723133A
CN107723133A CN201711183708.5A CN201711183708A CN107723133A CN 107723133 A CN107723133 A CN 107723133A CN 201711183708 A CN201711183708 A CN 201711183708A CN 107723133 A CN107723133 A CN 107723133A
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CN
China
Prior art keywords
parts
cleaning combination
minute surface
calgon
poly
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201711183708.5A
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Chinese (zh)
Inventor
施享
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Maanshan Songhe Information Technology Co Ltd
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Maanshan Songhe Information Technology Co Ltd
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Priority to CN201711183708.5A priority Critical patent/CN107723133A/en
Publication of CN107723133A publication Critical patent/CN107723133A/en
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0078—Compositions for cleaning contact lenses, spectacles or lenses
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/06—Phosphates, including polyphosphates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2096—Heterocyclic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of glass material minute surface cleaning combination and its preparation technology; cleaning combination component includes 10 30 parts of dodecyl sodium sulfate, 5 15 parts of tetrahydrofuran, 4 12 parts of disodium EDTA, 8 20 parts of chelating agent, 10 20 parts of LAA, 8 18 parts of calgon, 10 25 parts of poly- sodium propionate, 14 parts of alkalinity regulator in parts by weight; preparation technology of the present invention is simple; obtained cleaning combination cleaning performance is good, and nontoxic, environmentally friendly, protection minute surface is not easy to damage.

Description

A kind of glass material minute surface cleaning combination and its preparation technology
Technical field
The present invention relates to cleaning combination preparing technical field, specially a kind of glass material minute surface cleaning combination and its Preparation technology.
Background technology
As bespectacled people is more and more, there is frost in winter, and there is fog summer, causes production to give birth to bespectacled people Very big pain living, or even bring potential safety hazard.The cleaning agent of minute surface dirt at present, is divided into alkaline cleaner and synthesis of detergent Agent.But all there is some shortcomings, such as alkaline cleaner can remove the dirt of glass surface for they, but can send out surface layer of glass It is raw damaged, cause " latent wound " and make glass embrittlement；Also have definitely corrosiveness in synthetic detergent because it except containing Also contain other auxiliary agents outside surfactant, also have corrosiveness to glasses minute surface, while can also contain glass surface Calcium ion is removed with other metalloform-selectives and makes glass surface roughening.
The content of the invention
It is above-mentioned to solve it is an object of the invention to provide a kind of glass material minute surface cleaning combination and its preparation technology The problem of being proposed in background technology.
To achieve the above object, the present invention provides following technical scheme：A kind of glass material minute surface cleaning combination, cleaning Composition component includes dodecyl sodium sulfate 10-30 parts, tetrahydrofuran 5-15 parts, disodium ethylene diamine tetraacetate in parts by weight Salt 4-12 parts, chelating agent 8-20 parts, LAA 10-20 parts, calgon 8-18 parts, poly- sodium propionate 10- 25 parts, alkalinity regulator 1-4 parts.
Preferably, the preferable composition proportion of cleaning combination component includes 20 parts of dodecyl sodium sulfate, tetrahydrofuran 10 Part, 8 parts of disodium EDTA, 14 parts of chelating agent, 15 parts of LAA, 13 parts of calgon, gather 18 parts of sodium propionate, 3 parts of alkalinity regulator.
Preferably, its preparation technology comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation technology of the present invention is simple, obtained cleaning combination Cleaning performance is good, and nontoxic, environmentally friendly, protection minute surface is not easy to damage；Wherein, calgon, the poly- sodium propionate added in the present invention, Cleaning efficiency can be improved, in addition, the preparation technology that the present invention uses is simple to operate, cost is low, using heating water bath, Neng Goufang Only active ingredient is lost in, and is obtained through overtesting, the effective clearance rate of cleaning combination produced by the present invention reaches 98.5%, and does not damage Hinder specular surface.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects Enclose.
The present invention provides following technical scheme：A kind of glass material minute surface cleaning combination, cleaning combination component is by weight Measuring number includes dodecyl sodium sulfate 10-30 parts, tetrahydrofuran 5-15 parts, disodium EDTA 4-12 parts, chelating Agent 8-20 parts, LAA 10-20 parts, calgon 8-18 parts, poly- sodium propionate 10-25 parts, basicity regulation Agent 1-4 parts.
Embodiment one：
Cleaning combination component includes 10 parts of dodecyl sodium sulfate, 5 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid two in parts by weight 4 parts of sodium salt, 8 parts of chelating agent, 10 parts of LAA, 8 parts of calgon, 10 parts of poly- sodium propionate, basicity regulation 1 part of agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Embodiment two：
Cleaning combination component includes 30 parts of dodecyl sodium sulfate, 15 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid in parts by weight 12 parts of disodium salt, 20 parts of chelating agent, 20 parts of LAA, 18 parts of calgon, 25 parts of poly- sodium propionate, basicity 4 parts of conditioning agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Embodiment three：
Cleaning combination component includes 15 parts of dodecyl sodium sulfate, 7 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid two in parts by weight 6 parts of sodium salt, 9 parts of chelating agent, 12 parts of LAA, 10 parts of calgon, 13 parts of poly- sodium propionate, basicity regulation 2 parts of agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Example IV：
Cleaning combination component includes 25 parts of dodecyl sodium sulfate, 13 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid in parts by weight 10 parts of disodium salt, 18 parts of chelating agent, 16 parts of LAA, 15 parts of calgon, 22 parts of poly- sodium propionate, basicity 3 parts of conditioning agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Embodiment five：
Cleaning combination component includes 14 parts of dodecyl sodium sulfate, 12 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid in parts by weight 6 parts of disodium salt, 10 parts of chelating agent, 14 parts of LAA, 12 parts of calgon, 14 parts of poly- sodium propionate, basicity 2 parts of conditioning agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Embodiment six：
Cleaning combination component includes 20 parts of dodecyl sodium sulfate, 10 parts of tetrahydrofuran, ethylenediamine tetra-acetic acid in parts by weight 8 parts of disodium salt, 14 parts of chelating agent, 15 parts of LAA, 13 parts of calgon, 18 parts of poly- sodium propionate, basicity 3 parts of conditioning agent.
The preparation technology of the present embodiment comprises the following steps：
A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
Preparation technology of the present invention is simple, and obtained cleaning combination cleaning performance is good, and nontoxic, environmentally friendly, protection minute surface is not easy Damage；Wherein, calgon, the poly- sodium propionate added in the present invention, it is possible to increase cleaning efficiency, in addition, the present invention uses Preparation technology it is simple to operate, cost is low, using heating water bath, active ingredient can be prevented to be lost in, be obtained through overtesting, this hair The bright obtained effective clearance rate of cleaning combination reaches 98.5%, and does not damage specular surface.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (3)

  1. A kind of 1. glass material minute surface cleaning combination, it is characterised in that：Cleaning combination component includes 12 in parts by weight Sodium alkyl sulfonate 10-30 parts, tetrahydrofuran 5-15 parts, disodium EDTA 4-12 parts, chelating agent 8-20 parts, lauroyl Both sexes guanidine-acetic acid sodium 10-20 parts, calgon 8-18 parts, poly- sodium propionate 10-25 parts, alkalinity regulator 1-4 parts.
  2. A kind of 2. glass material minute surface cleaning combination according to claim 1, it is characterised in that：Cleaning combination component Preferable composition proportion includes 20 parts of dodecyl sodium sulfate, 10 parts of tetrahydrofuran, 8 parts of disodium EDTA, chelating 14 parts of agent, 15 parts of LAA, 13 parts of calgon, 18 parts of poly- sodium propionate, 3 parts of alkalinity regulator.
  3. 3. realize a kind of preparation technology of glass material minute surface cleaning combination described in claim 1, it is characterised in that：It is made Standby technique comprises the following steps：
    A, disodium EDTA, chelating agent, LAA, calgon, poly- sodium propionate are mixed Stirring at low speed in agitator tank is added afterwards, and stir speed (S.S.) is 200 revs/min, time 25min, obtains mixed liquor A；
    B, added after mixing dodecyl sodium sulfate, tetrahydrofuran in agitator tank and carry out high-speed stirred, added in whipping process Mixed liquor A and alkalinity regulator, stir speed (S.S.) are 2000 revs/min, time 15min, obtain mixed liquid B；
    C, mixed liquid B is put into heating water bath in water-bath, heating-up temperature is 55 DEG C, time 13min, is slowly cooled to afterwards Room temperature, that is, obtain cleaning combination.
CN201711183708.5A 2017-11-23 2017-11-23 A kind of glass material minute surface cleaning combination and its preparation technology Withdrawn CN107723133A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711183708.5A CN107723133A (en) 2017-11-23 2017-11-23 A kind of glass material minute surface cleaning combination and its preparation technology

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Application Number Priority Date Filing Date Title
CN201711183708.5A CN107723133A (en) 2017-11-23 2017-11-23 A kind of glass material minute surface cleaning combination and its preparation technology

Publications (1)

Publication Number Publication Date
CN107723133A true CN107723133A (en) 2018-02-23

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104726213A (en) * 2013-12-23 2015-06-24 邓忠玺 Environmentally friendly glass mirror surface cleaning agent
CN104726222A (en) * 2013-12-23 2015-06-24 邓忠玺 Environmentally friendly glass curtain wall cleaning agent
CN105062706A (en) * 2015-08-14 2015-11-18 上海奈拓化工科技有限公司 High-precision ultrasonic cleaning agent for glass mould used in resin optical lens mold closing
CN105154250A (en) * 2015-09-11 2015-12-16 上海婉静纺织科技有限公司 Composition for decontaminating and glazing automobile shell
CN106590985A (en) * 2016-12-08 2017-04-26 青岛友诚高新技术有限公司 Disinfecting and sterilizing dishwashing liquid

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104726213A (en) * 2013-12-23 2015-06-24 邓忠玺 Environmentally friendly glass mirror surface cleaning agent
CN104726222A (en) * 2013-12-23 2015-06-24 邓忠玺 Environmentally friendly glass curtain wall cleaning agent
CN105062706A (en) * 2015-08-14 2015-11-18 上海奈拓化工科技有限公司 High-precision ultrasonic cleaning agent for glass mould used in resin optical lens mold closing
CN105154250A (en) * 2015-09-11 2015-12-16 上海婉静纺织科技有限公司 Composition for decontaminating and glazing automobile shell
CN106590985A (en) * 2016-12-08 2017-04-26 青岛友诚高新技术有限公司 Disinfecting and sterilizing dishwashing liquid

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Application publication date: 20180223

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