CN107711875A - A kind of ovum worm special-purpose insecticide and preparation method thereof - Google Patents

A kind of ovum worm special-purpose insecticide and preparation method thereof Download PDF

Info

Publication number
CN107711875A
CN107711875A CN201711173922.2A CN201711173922A CN107711875A CN 107711875 A CN107711875 A CN 107711875A CN 201711173922 A CN201711173922 A CN 201711173922A CN 107711875 A CN107711875 A CN 107711875A
Authority
CN
China
Prior art keywords
parts
preparation
mixture
added
ethanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201711173922.2A
Other languages
Chinese (zh)
Inventor
施享
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Maanshan Songhe Information Technology Co Ltd
Original Assignee
Maanshan Songhe Information Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Maanshan Songhe Information Technology Co Ltd filed Critical Maanshan Songhe Information Technology Co Ltd
Priority to CN201711173922.2A priority Critical patent/CN107711875A/en
Publication of CN107711875A publication Critical patent/CN107711875A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/707—1,2,3- or 1,2,4-triazines; Hydrogenated 1,2,3- or 1,2,4-triazines
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals

Abstract

The present invention relates to a kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：10 20 parts of Profenofos, 47 parts of Acetamiprid, 56 parts of pymetrozine, 23 parts of gamma cyhalothrin, 10 15 parts of malathion, 48 parts of Tea Polyphenols, 34 parts of phoxim, 47 parts of orthene, 10 15 parts of nimbin, 35 parts of sorbic acid, 30 45 parts of ethanol, 50 60 parts of deionized water.Material of the present invention is easy to get, and antioxidant effect is good, and chemical stability is strong, has good insecticidal effect, and small toxicity is not volatile, latent time length, harmless.

Description

A kind of ovum worm special-purpose insecticide and preparation method thereof
Technical field
The present invention relates to field of pesticides, and in particular to a kind of ovum worm special-purpose insecticide and preparation method thereof.
Background technology
Pest problem in life is more, and insecticide variety is also a lot, but for ovum worm, incubation period length, by It is smaller in own vol, it is not easy to find at the beginning, but the later stage is exactly the outburst of large area, for general broad spectrum pesticide is come Say, it is difficult to accomplish to be inherently eliminated, and toxicity is larger mostly, the scope of application is smaller.
The content of the invention
A kind of ovum worm special-purpose insecticide and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is by weight Amount number is made up of following ratio：Profenofos 10-20 parts, Acetamiprid 4-7 parts, pymetrozine 5-6 parts, gamma cyhalothrin 2-3 Part, malathion 10-15 parts, Tea Polyphenols 4-8 parts, phoxim 3-4 parts, orthene 4-7 parts, nimbin 10-15 parts, sorb Sour 3-5 parts, ethanol 30-45 parts, deionized water 50-60 parts.
Further improvement of the present invention is：Its preparation method is as follows：
A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 1800-2000HZ, temperature is set to 30-35 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 10-15min；
B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 520-560r/min, obtains mixture B；
C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) 430- 450r/min, handled after stirring using centrifuge, frequency is set to 7800-8200HZ, filters out seminal fluid, obtains product.
Beneficial effects of the present invention：Material of the present invention is easy to get, and antioxidant effect is good, and chemical stability is strong, has good Insecticidal effect, small toxicity is not volatile, latent time length, harmless, applied widely.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Third bromine 14 parts of phosphorus, 5 parts of Acetamiprid, 5 parts of pymetrozine, 2 parts of gamma cyhalothrin, 12 parts of malathion, 6 parts of Tea Polyphenols, phoxim 4 Part, 5 parts of orthene, 12 parts of nimbin, 3 parts of sorbic acid, 35 parts of ethanol, 55 parts of deionized water.
Its preparation method is as follows：
A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 1900HZ, temperature is set to 32 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 11min；
B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 540r/min, obtains mixture B；
C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) is 435r/min, handled after stirring using centrifuge, frequency is set to 7900HZ, filters out seminal fluid, obtains product.
Embodiment 2
A kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Third bromine 20 parts of phosphorus, 4 parts of Acetamiprid, 6 parts of pymetrozine, 2 parts of gamma cyhalothrin, 15 parts of malathion, 4 parts of Tea Polyphenols, phoxim 4 Part, 4 parts of orthene, 15 parts of nimbin, 3 parts of sorbic acid, 45 parts of ethanol, 50 parts of deionized water.
Its preparation method is as follows：
A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 2000HZ, temperature is set to 30 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 15min；
B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 520r/min, obtains mixture B；
C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) is 450r/min, handled after stirring using centrifuge, frequency is set to 7800HZ, filters out seminal fluid, obtains product.
Embodiment 3
A kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Third bromine 10 parts of phosphorus, 7 parts of Acetamiprid, 5 parts of pymetrozine, 3 parts of gamma cyhalothrin, 10 parts of malathion, 8 parts of Tea Polyphenols, phoxim 3 Part, 7 parts of orthene, 10 parts of nimbin, 5 parts of sorbic acid, 30 parts of ethanol, 60 parts of deionized water.
Its preparation method is as follows：
A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 1800HZ, temperature is set to 35 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 10min；
B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 560r/min, obtains mixture B；
C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) is 430r/min, handled after stirring using centrifuge, frequency is set to 8200HZ, filters out seminal fluid, obtains product.
Embodiment 4
A kind of ovum worm special-purpose insecticide and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Third bromine 18 parts of phosphorus, 6 parts of Acetamiprid, 6 parts of pymetrozine, 2 parts of gamma cyhalothrin, 14 parts of malathion, 7 parts of Tea Polyphenols, phoxim 4 Part, 6 parts of orthene, 13 parts of nimbin, 4 parts of sorbic acid, 40 parts of ethanol, 58 parts of deionized water.
Its preparation method is as follows：
A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 1900HZ, temperature is set to 35 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 15min；
B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 530r/min, obtains mixture B；
C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) is 440r/min, handled after stirring using centrifuge, frequency is set to 8000HZ, filters out seminal fluid, obtains product.
In above example, embodiment 4 is most preferred embodiment, and good disinsection effect, incubation period length is relatively low to human toxicity, Almost fanout free region.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in Within protection scope of the present invention.

Claims (2)

  1. A kind of 1. ovum worm special-purpose insecticide and preparation method thereof, it is characterised in that：Raw material constituent is in parts by weight by following Ratio forms：Profenofos 10-20 parts, Acetamiprid 4-7 parts, pymetrozine 5-6 parts, gamma cyhalothrin 2-3 parts, malathion 10-15 parts, Tea Polyphenols 4-8 parts, phoxim 3-4 parts, orthene 4-7 parts, nimbin 10-15 parts, sorbic acid 3-5 parts, second Alcohol 30-45 parts, deionized water 50-60 parts.
  2. A kind of 2. ovum worm special-purpose insecticide according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method It is as follows：
    A, under normal temperature and pressure, Profenofos and Acetamiprid is added in ethanol in proper amount and are diluted, using ultrasonication, frequency is set For 1800-2000HZ, temperature is set to 30-35 DEG C, is being slowly added to pymetrozine, mixture A is obtained after 10-15min；
    B, by ethanol and deionized water according to 1:2 ratio allotment, by gamma cyhalothrin, malathion, phoxim and second Acyl acephatemet is added thereto stirring, stir speed (S.S.) 520-560r/min, obtains mixture B；
    C, mixture A is added in mixture B and stirred, sequentially add Tea Polyphenols, nimbin and sorbic acid, stir speed (S.S.) 430- 450r/min, handled after stirring using centrifuge, frequency is set to 7800-8200HZ, filters out seminal fluid, obtains product.
CN201711173922.2A 2017-11-22 2017-11-22 A kind of ovum worm special-purpose insecticide and preparation method thereof Withdrawn CN107711875A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711173922.2A CN107711875A (en) 2017-11-22 2017-11-22 A kind of ovum worm special-purpose insecticide and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711173922.2A CN107711875A (en) 2017-11-22 2017-11-22 A kind of ovum worm special-purpose insecticide and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107711875A true CN107711875A (en) 2018-02-23

Family

ID=61218024

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711173922.2A Withdrawn CN107711875A (en) 2017-11-22 2017-11-22 A kind of ovum worm special-purpose insecticide and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107711875A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107307019A (en) * 2017-08-15 2017-11-03 马鞍山中粮生物化学有限公司 A kind of vegetables special-purpose insecticide and preparation method thereof
CN107361083A (en) * 2017-08-18 2017-11-21 马鞍山中粮生物化学有限公司 A kind of efficient pesticides and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107307019A (en) * 2017-08-15 2017-11-03 马鞍山中粮生物化学有限公司 A kind of vegetables special-purpose insecticide and preparation method thereof
CN107361083A (en) * 2017-08-18 2017-11-21 马鞍山中粮生物化学有限公司 A kind of efficient pesticides and preparation method thereof

Similar Documents

Publication Publication Date Title
CN100397994C (en) Insect and mite killer with vegetable oil as base
CN103385251B (en) A kind of Pesticidal combination of pyriproxyfen-containing
CN103931648B (en) The peanut seed coat agent of a kind of aspergillus flavus-resistance mould
CN103027064B (en) Seed treatment preparation containing clothianidin
CN103238590B (en) Solvent composition for preparing neonicotinoid pesticide liquid preparation
CN104542618A (en) Synergetic acaricidal composition containing cyenopyrafen and etoxazole
CN103875680A (en) Seed coating for preventing aflatoxin contamination of peanuts
CN107711875A (en) A kind of ovum worm special-purpose insecticide and preparation method thereof
CN110800735B (en) Microemulsion with emamectin benzoate as effective component and preparation method thereof
CN102217638B (en) Pesticide composition for preventing and treating plant virus diseases
CN103865680A (en) Soft detergent powder
CN103598202A (en) Insecticidal composition containing emamectin benzoate and efficient cyhalothrin
CN103947655A (en) Insecticidal composition containing ivermectin and spirodiclofen
CN103070181A (en) Novel rice seed treatment agent
CN102754654A (en) Insecticide and fungicide combined agent for treating rice seeds
CN102701841B (en) Biological antimicrobial chelerythrine aqueous emulsion and preparation method thereof
CN106212468B (en) A kind of bactericidal composition of the fluorine bacterium azoles of alkene containing benzo and chitosan
CN104642369A (en) Prochloraz and isoprothiolane compound missible oil and preparation method thereof
CN104351257A (en) Ultra-low volume suspending agent containing nosema locustae and metarhizium anisopliae and used for grasshopper control as well as preparation method of suspending agent
CN102812967A (en) Nematode killing composition micro-capsule suspending agent, and production method and application thereof
CN107517959A (en) A kind of dispersible oil-suspending agent containing mesosulfuron and clodinafop-propargyl and preparation method thereof
CN103688964B (en) A kind of water dispersible granules and application containing Bassa
CN103636614B (en) Paddy field synergistic weeding composition containing oxadiargyl and mesotrione
WO2016070632A1 (en) Insect-killing mite-killing agent composition with synergistic effect
CN103975915B (en) A kind of assistant composition for emamectin benzoate microemulsion and application method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20180223

WW01 Invention patent application withdrawn after publication