CN107698890A - A kind of processing technology of floor film - Google Patents
A kind of processing technology of floor film Download PDFInfo
- Publication number
- CN107698890A CN107698890A CN201710970508.8A CN201710970508A CN107698890A CN 107698890 A CN107698890 A CN 107698890A CN 201710970508 A CN201710970508 A CN 201710970508A CN 107698890 A CN107698890 A CN 107698890A
- Authority
- CN
- China
- Prior art keywords
- roll
- linear velocity
- floor film
- processing technology
- film
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
- C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
- C08J2327/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C08J2327/06—Homopolymers or copolymers of vinyl chloride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2451/00—Characterised by the use of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
- C08J2451/04—Characterised by the use of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers grafted on to rubbers
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Casting Or Compression Moulding Of Plastics Or The Like (AREA)
Abstract
The invention discloses a kind of processing technology of floor film, it is related to floor film manufacture field.The processing technology of the floor film of the present invention, comprises the following steps：(1) dispensing mixes：Weigh PVC resin powder, impact resilience MBS resins, ACR processing aids, diisooctyl phthalate, in-lubricant, the external lubricant of 3~10 parts by weight, phosphate ester flame retardants, high-speed stirred, then cold stirring and obtain mixed material；(2) extrude, plastify, calendering formation；(3) cooling, Ageing Treatment；(4) draw, wind, packaging.The floor film composition proportion of the present invention is reasonable, and technological design is reasonable, enhances the toughness, wearability, fire-retardant temperature tolerance of floor film, and light transmittance is higher, is adapted to large-scale industrial production.
Description
Technical field：
The present invention relates to floor film processing technique field, and in particular to a kind of processing technology of floor film.
Background technology：
Floor film is extremely important in decorations industry, because it has superpower shockproof, anticollision, antifriction, corrosion-resistant
Characteristic, omnibearing protection can be carried out to finishing ground, floor, be effectively prevented sharp objects in fitment process and fall pair
Ground is caused to damage, and sole can also be avoided to be worn to caused by ground friction.During using traditional floor film manufacturing procedure, easily
There is viscous wheel phenomenon；Easily occurring albefaction in product drawing process seriously influences apparent transparency, while easily occurs being difficult to roll up
Phenomena such as taking.Therefore, it is necessary to develop it is a kind of can ensure floor film toughness, wearability, fire-retardant temperature tolerance, mechanical strength plus
Work technique.
The content of the invention：
The technical problems to be solved by the invention are to provide a kind of processing technology of floor film, raw material and technological design conjunction
Reason, toughness, wearability, fire-retardant temperature tolerance and the mechanical strength of floor film are enhanced, be adapted to large-scale industrial production.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：Weigh PVC resin powder, the impact resilience MBS trees of 10~25 parts by weight of 120~160 parts by weight
Fat, the ACR processing aids of 8~15 parts by weight, the diisooctyl phthalate of 6~12 parts by weight, the interior profit of 3~10 parts by weight
Lubrication prescription, the external lubricant of 3~10 parts by weight, the phosphate ester flame retardants of 1~5 parts by weight, are transported paramount by automatic charging machine
In fast mixer, 350~480r/min rotating speeds stir 20~30min, then 10~20min of cold stirring obtains mixed material；
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 160~180
DEG C extruding pelletization, two roller mills plasticizing is re-fed into, film is rolled into through five roll calendars；
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 10~15 DEG C；Cooling was after 25~40 DEG C of Ageing Treatments 8~12 hours；
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Further, the in-lubricant is one in Solsperse 2000, stearic amide, butyl stearate, calcium stearate
Kind or a variety of combinations.
Further, the external lubricant is one or more groups in paraffin, Tissuemat E, OPE
Close.
Further, the phosphate ester flame retardants be tricresyl phosphate, triphenyl phosphate, phosphoric acid tri-isopropyl benzene ester,
One or more combinations in trioctyl phosphate, cresyl diphenyl phosphate.
Further, the screw rod radical of step (2) planetary extruder is 12~16, the residence time of extruded material
For 25~35s.
Further, during the roll calendar of step (2) five calendering, it is 200 DEG C to control No.1 roll temperature, and linear velocity is
10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, linear velocity 20m/min；
No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
The beneficial effects of the invention are as follows：1st, floor film of the invention, using Corvic as main component, passes through addition
A variety of auxiliary agents, additive, composition proportion is reasonable, and technological design is reasonable, avoids the viscous wheel phenomenon of appearance, does not occur in calender line
Obvious albinism, it is easy to winding shaping, enhances toughness, wearability, fire-retardant temperature tolerance and the mechanical performance of floor film, thoroughly
Light rate is higher, is adapted to large-scale industrial production.
2nd, in floor film raw material of the invention, using conventional membrane material Corvic as matrix, shock resistance is added
The modifying agent impact resilience MBS resins of toughening type and ACR processing aids, the efficient isodecyl ester of plasticizer phthalic acid two are fire-retardant
The phosphate ester flame retardants of plasticising, inside and outside lubricant agent, the floor film of excellent performance can be processed；Wherein, impact resilience MBS resins
It is close with PVC solubility parameter with typical core shell structure, play a part of interface bonding agent, product can be obviously improved
Impact strength, cold resistance, processing fluidity；ACR processing aids melt in process after can with adhesion PVC particles,
Increase is interior to rub, raising cutting torsion, heat in generation, makes the uniformity of temperature profile in material, gelation degree is homogeneous, so as to promote
PVC materials it is homogenous plasticized；External lubricant can improve the hot metal surface friction of polymer and process equipment；In-lubricant
Can play a part of reduce polymer molecule between cohesive force, improve mobility.
3rd, select planetary extruder in floor film processing technology of the invention, during extrusion, its heat exchange area is big, disperses to mix
Conjunction ability is strong, and residence time of material is short, will not decompose denaturation；Five roll calendars are selected in calendering, can be each by accurately controlling
The temperature and linear velocity of roller, ensure that film quality is uniform and stable；Chill roll controls to adjust water temperature using die heater, and no condensation is existing
As, and heat transfer is accelerated, cool efficiency high.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：The ACR processing for weighing 135kg PVC resin powder, 15kg impact resilience MBS resins, 10kg helps
Agent, 9kg diisooctyl phthalate, 5kg in-lubricant stearic amide, 6kg external lubricant Tissuemat E, 2kg
Phosphate ester flame retardants phosphoric acid tri-isopropyl benzene ester, is transported into homogenizer, 400r/min rotating speeds stir by automatic charging machine
25min is mixed, then cold stirring 16min obtains mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 166 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 12 DEG C；Cooling was after 32 DEG C of Ageing Treatments 10 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Embodiment 2
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：The ACR processing for weighing 145kg PVC resin powder, 22kg impact resilience MBS resins, 13kg helps
Agent, 7kg diisooctyl phthalate, 5kg in-lubricant calcium stearate, 7kg external lubricant OPE,
2kg phosphate ester flame retardants cresyl diphenyl phosphates, are transported into homogenizer, 380r/min by automatic charging machine
Rotating speed stirs 30min, then cold stirring 20min obtains mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 180 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 15 DEG C；Cooling was after 40 DEG C of Ageing Treatments 8 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Embodiment 3
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：The ACR processing for weighing 150kg PVC resin powder, 17kg impact resilience MBS resins, 11kg helps
Agent, 10kg diisooctyl phthalate, 5kg in-lubricant butyl stearate, 5kg external lubricant, 3kg phosphoric acid esters
Fire retardant tricresyl phosphate, is transported into homogenizer by automatic charging machine, 420r/min rotating speeds stirring 25min, then
Cold stirring 18min obtains mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 172 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 10 DEG C；Cooling was after 30 DEG C of Ageing Treatments 9 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Embodiment 4
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：The ACR processing for weighing 155kg PVC resin powder, 22kg impact resilience MBS resins, 13kg helps
Agent, 12kg diisooctyl phthalate, 9kg in-lubricant Solsperse 2000,6kg external lubricant paraffin, 4kg phosphoric acid
Esters fire retardant trioctyl phosphate, is transported into homogenizer by automatic charging machine, 450r/min rotating speeds stirring 23min,
Cold stirring 15min obtains mixed material again.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 180 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 10 DEG C；Cooling was after 36 DEG C of Ageing Treatments 11 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Embodiment 5
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：The ACR processing for weighing 160kg PVC resin powder, 25kg impact resilience MBS resins, 15kg helps
Agent, 10kg diisooctyl phthalate, 9kg in-lubricant butyl stearate, 8kg external lubricant Tissuemat E, 2kg
Phosphate ester flame retardants phosphoric acid tri-isopropyl benzene ester, transported by automatic charging machine into homogenizer, 480r/min rotating speeds
20min is stirred, then cold stirring 20min obtains mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 160~180
DEG C extruding pelletization, two roller mills plasticizing is re-fed into, film is rolled into through five roll calendars；Wherein, the screw rod of planetary extruder
Radical is 12~16, and the residence time of extruded material is 25~35s.When five roll calendars roll, the No.1 roll temperature is controlled to be
200 DEG C, linear velocity 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, line
Speed is 20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, and linear velocity is
30m/min。
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 15 DEG C；Cooling was after 40 DEG C of Ageing Treatments 12 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
Comparative example 1
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：Weigh 135kg PVC resin powder, 10kg ACR processing aids, 9kg phthalic acid two
Isodecyl ester, 5kg in-lubricant stearic amide, 6kg external lubricant Tissuemat E, 2kg phosphate ester flame retardants tricresyl phosphates
Isopropyl phenyl ester, is transported into homogenizer by automatic charging machine, 400r/min rotating speeds stirring 25min, then cold stirring 16min
Obtain mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 166 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 12 DEG C；Cooling was after 32 DEG C of Ageing Treatments 10 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
The comparative example 1 is compared with Example 1, no to add impact resilience MBS resins in the feed.
Comparative example 2
A kind of processing technology of floor film, comprises the following steps：
(1) dispensing mixes：Weigh 135kg PVC resin powder, 15kg impact resilience MBS resins, 9kg phthalic acid
Two isodecyl esters, 5kg in-lubricant stearic amide, 6kg external lubricant Tissuemat E, 2kg phosphate ester flame retardants phosphoric acid
Tri-isopropyl benzene ester, is transported into homogenizer by automatic charging machine, 400r/min rotating speeds stirring 25min, then cold stirring
16min obtains mixed material.
(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, in 166 DEG C of extrusions
It is granulated, is re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；Wherein, the screw rod radical of planetary extruder is
12~16, the residence time of extruded material is 25~35s.When five roll calendars roll, it is 200 DEG C to control No.1 roll temperature,
Linear velocity is 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min；No. three roll temperatures are 190 DEG C, and linear velocity is
20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roll temperatures are 180 DEG C, linear velocity 30m/min.
(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, will enter water temperature using die heater
Degree adjustment control is at 12 DEG C；Cooling was after 32 DEG C of Ageing Treatments 10 hours.
(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min line drawing
Speed is passed through thin film winder, and the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；Pack
To the floor film.
The comparative example 2 is compared with Example 1, no to add ACR processing aids in the feed.
The floor film performance test results of embodiment and comparative example are as shown in table 1.
The embodiment of table 1. and comparative example floor film performance test results
As can be seen from the above table, the floor film that the present invention processes has excellent mechanical property, such as tensile strength, fracture
Elongation, light transmittance, wear-resisting rate, fire resistance are preferable.Impact resilience MBS resins and ACR processing aids are to the floor film product
Multinomial performance influences notable.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (6)
- A kind of 1. processing technology of floor film, it is characterised in that：Comprise the following steps：(1) dispensing mixes：Weigh the PVC resin powders of 120~160 parts by weight, the impact resilience MBS resins of 10~25 parts by weight, 8~ The ACR processing aids of 15 parts by weight, the diisooctyl phthalate of 6~12 parts by weight, the in-lubricant of 3~10 parts by weight, 3 The phosphate ester flame retardants of the external lubricant of~10 parts by weight, 1~5 parts by weight, transported by automatic charging machine to high-speed stirred In machine, 350~480r/min rotating speeds stir 20~30min, then 10~20min of cold stirring obtains mixed material；(2) extrude, plastify, calendering formation：The mixed material of step (1) is passed through in planetary extruder, squeezed in 160~180 DEG C Go out to be granulated, be re-fed into two roller mills plasticizing, film is rolled into through five roll calendars；(3) cooling, Ageing Treatment：The film rolled is passed through chill roll cooling down, adjusted inflow temperature using die heater Whole control is at 10~15 DEG C；Cooling was after 25~40 DEG C of Ageing Treatments 8~12 hours；(4) draw, wind, packaging：Film after Ageing Treatment is taken in the presence of roller with 25~30m/min linear velocity drawing Thin film winder is passed through, the preheating temperature of thin film winder is 40~50 DEG C, and linear velocity is 35~45m/min；It is packaged to be institute State floor film.
- 2. the processing technology of floor film according to claim 1, it is characterised in that：The in-lubricant be Solsperse 2000, One or more combinations in stearic amide, butyl stearate, calcium stearate.
- 3. the processing technology of floor film according to claim 1, it is characterised in that：The external lubricant is paraffin, poly- second One or more combinations in alkene wax, OPE.
- 4. the processing technology of floor film according to claim 1, it is characterised in that：The phosphate ester flame retardants are phosphoric acid Front three phenyl ester, triphenyl phosphate, phosphoric acid tri-isopropyl benzene ester, trioctyl phosphate, one kind in cresyl diphenyl phosphate or more The combination of kind.
- 5. the processing technology of floor film according to claim 1, it is characterised in that：Step (2) planetary extruder Screw rod radical is 12~16, and the residence time of extruded material is 25~35s.
- 6. the processing technology of floor film according to claim 1, it is characterised in that：The roll calendar pressure of step (2) five Delay, it is 200 DEG C to control No.1 roll temperature, linear velocity 10m/min；No. two roll temperatures are 195 DEG C, linear velocity 15m/min； No. three roll temperatures are 190 DEG C, linear velocity 20m/min；No. four roll temperatures are 185 DEG C, linear velocity 25m/min；No. five roller temperatures Spend for 180 DEG C, linear velocity 30m/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710970508.8A CN107698890A (en) | 2017-10-18 | 2017-10-18 | A kind of processing technology of floor film |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710970508.8A CN107698890A (en) | 2017-10-18 | 2017-10-18 | A kind of processing technology of floor film |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107698890A true CN107698890A (en) | 2018-02-16 |
Family
ID=61182592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710970508.8A Pending CN107698890A (en) | 2017-10-18 | 2017-10-18 | A kind of processing technology of floor film |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107698890A (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108485105A (en) * | 2018-03-16 | 2018-09-04 | 浙江港龙新材料股份有限公司 | A kind of factory formula and preparation method thereof of PVC floor print film |
| CN108794936A (en) * | 2018-07-09 | 2018-11-13 | 衢州龙威新材料股份有限公司 | The blanket type floor film that foams and preparation method thereof |
| CN109337233A (en) * | 2018-09-03 | 2019-02-15 | 李永平 | A kind of zero shrinkage floor film |
| CN109354804A (en) * | 2018-10-24 | 2019-02-19 | 江苏名阳高分子新材料有限公司 | A kind of PVC floor film of superpower wear-resistant and preparation method thereof |
| CN109370086A (en) * | 2018-09-03 | 2019-02-22 | 李永平 | One kind zero shrinks the super film processing method of ultra-wide |
| CN109651733A (en) * | 2018-12-28 | 2019-04-19 | 安徽嘉阳新材料科技有限公司 | Fire-retardant, shock resistance printing basement membrane preparation method |
| CN109705493A (en) * | 2018-12-28 | 2019-05-03 | 安徽嘉阳新材料科技有限公司 | High intensity printing basement membrane and preparation method thereof |
| CN109735022A (en) * | 2018-12-28 | 2019-05-10 | 安徽嘉阳新材料科技有限公司 | The preparation method of high-weatherability printing basement membrane |
| CN111171471A (en) * | 2019-12-31 | 2020-05-19 | 安徽天安新材料有限公司 | PVC decorative film and production process of PVC film |
| CN111923459A (en) * | 2020-07-01 | 2020-11-13 | 湖北环福塑料制品有限公司 | Process for calendering sheet into film |
| CN111925605A (en) * | 2020-07-23 | 2020-11-13 | 安徽嘉阳新材料科技有限公司 | PVC hard floor film and processing technology thereof |
| CN112341730A (en) * | 2020-11-24 | 2021-02-09 | 镇江恒昌彩艺科技有限公司 | Degradable floor composite wear-resistant layer and PVC floor film one-step forming process |
| CN112341729A (en) * | 2020-11-24 | 2021-02-09 | 镇江恒昌彩艺科技有限公司 | One-step forming process of antibacterial wear-resistant layer composite PVC floor film |
| CN114196132A (en) * | 2021-12-22 | 2022-03-18 | 海宁市华立实业有限公司 | Manufacturing process of flame-retardant floor film |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044804A (en) * | 2012-12-11 | 2013-04-17 | 浙江博泰塑胶有限公司 | Flame-retardant transparent floor film and production technology thereof |
| CN103540062A (en) * | 2013-10-17 | 2014-01-29 | 江苏晨洁家化制造有限公司 | PVC (Polyvinyl Chloride) diaphragm and manufacturing method thereof |
| CN103602009A (en) * | 2013-11-26 | 2014-02-26 | 山东瑞丰高分子材料股份有限公司 | High-transparency no-flow line hard PVC (polyvinyl chloride) calendered sheet and preparation method thereof |
| CN103756197A (en) * | 2014-01-26 | 2014-04-30 | 东莞市悠悠美居家居制造有限公司 | High-definition transparent PVC (polyvinyl chloride) film and preparation method thereof |
| CN103951912A (en) * | 2014-04-28 | 2014-07-30 | 广东冠盛塑胶有限公司 | Low-phenol environment-friendly floor tile and manufacturing method thereof |
| CN105647064A (en) * | 2016-03-09 | 2016-06-08 | 广州宏信塑胶工业有限公司 | Weatherable PVC (polyvinyl chloride) plastic wallpaper and preparation method thereof |
| CN105924828A (en) * | 2016-05-14 | 2016-09-07 | 江阴宏凯塑胶有限公司 | Uvioresistant, wear-resistant and scratch-resistant credit card surface layer and preparation method thereof |
| CN106751195A (en) * | 2016-12-14 | 2017-05-31 | 安徽圣源橡塑科技有限公司 | A kind of PVC ecological floors |
-
2017
- 2017-10-18 CN CN201710970508.8A patent/CN107698890A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044804A (en) * | 2012-12-11 | 2013-04-17 | 浙江博泰塑胶有限公司 | Flame-retardant transparent floor film and production technology thereof |
| CN103540062A (en) * | 2013-10-17 | 2014-01-29 | 江苏晨洁家化制造有限公司 | PVC (Polyvinyl Chloride) diaphragm and manufacturing method thereof |
| CN103602009A (en) * | 2013-11-26 | 2014-02-26 | 山东瑞丰高分子材料股份有限公司 | High-transparency no-flow line hard PVC (polyvinyl chloride) calendered sheet and preparation method thereof |
| CN103756197A (en) * | 2014-01-26 | 2014-04-30 | 东莞市悠悠美居家居制造有限公司 | High-definition transparent PVC (polyvinyl chloride) film and preparation method thereof |
| CN103951912A (en) * | 2014-04-28 | 2014-07-30 | 广东冠盛塑胶有限公司 | Low-phenol environment-friendly floor tile and manufacturing method thereof |
| CN105647064A (en) * | 2016-03-09 | 2016-06-08 | 广州宏信塑胶工业有限公司 | Weatherable PVC (polyvinyl chloride) plastic wallpaper and preparation method thereof |
| CN105924828A (en) * | 2016-05-14 | 2016-09-07 | 江阴宏凯塑胶有限公司 | Uvioresistant, wear-resistant and scratch-resistant credit card surface layer and preparation method thereof |
| CN106751195A (en) * | 2016-12-14 | 2017-05-31 | 安徽圣源橡塑科技有限公司 | A kind of PVC ecological floors |
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108485105A (en) * | 2018-03-16 | 2018-09-04 | 浙江港龙新材料股份有限公司 | A kind of factory formula and preparation method thereof of PVC floor print film |
| CN108794936A (en) * | 2018-07-09 | 2018-11-13 | 衢州龙威新材料股份有限公司 | The blanket type floor film that foams and preparation method thereof |
| CN109337233A (en) * | 2018-09-03 | 2019-02-15 | 李永平 | A kind of zero shrinkage floor film |
| CN109370086A (en) * | 2018-09-03 | 2019-02-22 | 李永平 | One kind zero shrinks the super film processing method of ultra-wide |
| CN109354804A (en) * | 2018-10-24 | 2019-02-19 | 江苏名阳高分子新材料有限公司 | A kind of PVC floor film of superpower wear-resistant and preparation method thereof |
| CN109735022B (en) * | 2018-12-28 | 2021-03-26 | 安徽嘉阳新材料科技有限公司 | Preparation method of high-weather-resistance printing base film |
| CN109651733A (en) * | 2018-12-28 | 2019-04-19 | 安徽嘉阳新材料科技有限公司 | Fire-retardant, shock resistance printing basement membrane preparation method |
| CN109735022A (en) * | 2018-12-28 | 2019-05-10 | 安徽嘉阳新材料科技有限公司 | The preparation method of high-weatherability printing basement membrane |
| CN109705493A (en) * | 2018-12-28 | 2019-05-03 | 安徽嘉阳新材料科技有限公司 | High intensity printing basement membrane and preparation method thereof |
| CN109705493B (en) * | 2018-12-28 | 2021-02-09 | 安徽嘉阳新材料科技有限公司 | High-strength printing base film and preparation method thereof |
| CN109651733B (en) * | 2018-12-28 | 2020-12-01 | 安徽嘉阳新材料科技有限公司 | Preparation method of flame-retardant and impact-resistant printing base film |
| CN111171471A (en) * | 2019-12-31 | 2020-05-19 | 安徽天安新材料有限公司 | PVC decorative film and production process of PVC film |
| CN111171471B (en) * | 2019-12-31 | 2021-12-21 | 安徽天安新材料有限公司 | PVC decorative film and production process of PVC film |
| CN111923459A (en) * | 2020-07-01 | 2020-11-13 | 湖北环福塑料制品有限公司 | Process for calendering sheet into film |
| CN111925605A (en) * | 2020-07-23 | 2020-11-13 | 安徽嘉阳新材料科技有限公司 | PVC hard floor film and processing technology thereof |
| CN111925605B (en) * | 2020-07-23 | 2022-05-27 | 安徽嘉阳新材料科技有限公司 | PVC hard floor film and processing technology thereof |
| CN112341730A (en) * | 2020-11-24 | 2021-02-09 | 镇江恒昌彩艺科技有限公司 | Degradable floor composite wear-resistant layer and PVC floor film one-step forming process |
| CN112341729A (en) * | 2020-11-24 | 2021-02-09 | 镇江恒昌彩艺科技有限公司 | One-step forming process of antibacterial wear-resistant layer composite PVC floor film |
| CN114196132A (en) * | 2021-12-22 | 2022-03-18 | 海宁市华立实业有限公司 | Manufacturing process of flame-retardant floor film |
| CN114196132B (en) * | 2021-12-22 | 2023-09-26 | 海宁市华立实业有限公司 | Manufacturing process of flame-retardant floor film |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107698890A (en) | A kind of processing technology of floor film | |
| CN104017310B (en) | A kind of biaxially orienting polyvinyl chloride pipe and preparation method thereof | |
| CN102276948B (en) | Preparation method of biaxially stretched polyvinyl fluoride film | |
| CN103059537B (en) | High-rigidity high-fluidity PC/ABS (polycarbonate/acrylonitrile-butadiene-styrene) alloy and preparation method thereof | |
| CN104356527A (en) | PVC base material with low shrinkage and preparation method and preparation equipment thereof | |
| CN105348746B (en) | A kind of plastic filler parent granule and preparation method thereof | |
| CN107216517B (en) | Preparation method of ultrahigh molecular weight polyethylene 3D printing supplies | |
| CN102911454A (en) | PVC (polyvinyl chloride)/ABS (acrylonitrile butadiene styrene copolymer)/CPE (chlorinated polyethylene) pipe with high impact resistance and method for preparing same | |
| CN101934592A (en) | Preparation technology of PET/PETG shrink film | |
| CN104231417A (en) | Polyolefin barium sulfate transparent masterbatch and preparation method thereof | |
| CN105818384A (en) | 3D printing method of fiber-grade flame retardant product based on reactive extrusion | |
| CN104371227A (en) | Fluorine-containing plastic processing assistant and preparation method thereof | |
| CN102911456A (en) | PVC (polyvinyl chloride)/ASA (acrylonitrile styrene acrylate) pipe with high impact resistance and method for preparing same | |
| CN107459735A (en) | Environment-protective polychloroethylene material composition and its preparation method and application | |
| CN104140586B (en) | Halogen-free flame-retardant POE material and preparation method thereof | |
| CN114045043A (en) | High-impact wood-plastic helmet composite material and preparation method thereof | |
| CN110423480A (en) | A kind of preparation method of high density Wood plastic composite | |
| CN109955452A (en) | A kind of isotactic polypropylene extrusion foaming device and technique | |
| CN106700343A (en) | Modified PVC wallboard and production method thereof | |
| CN106009427A (en) | Special material for white polyvinylidene fluoride cast film | |
| CN111978623A (en) | Preparation method of winding film and winding film prepared by preparation method | |
| CN113912962B (en) | PVC plastic cloth and preparation method thereof | |
| CN106751119B (en) | A kind of mixed ingredients and preparation method thereof that can promote PVC-M pipe quality and processability | |
| CN105566678A (en) | Talcum powder nucleation masterbatch and producing process thereof | |
| CN113910719B (en) | PVC drain pipe with low retraction rate and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180216 |