CN107691509A - A kind of air freshener and preparation method thereof - Google Patents
A kind of air freshener and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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Abstract
The invention belongs to technical field of air purification, more particularly to a kind of air freshener and preparation method thereof, including following raw material to be prepared：Fresh mangosteen, red bean, pot marigold, aloe, centella, glycerine, Lavender, EDETATE DISODIUM, silica gel, sulfuric acid, solubilizer, emulsifying agent, shown by testing experiment of disinfection effect, air freshener prepared by the present invention is up to 87.78% in sterilization a moment to microorganism killing rate, 72.14% is up to the inhibiting rate of microorganism after 4h is sprayed, eye irritation experiment shows, air freshener prepared by the present invention does not injure for rabbit eyes, is a kind of safe and reliable, preferable air freshener of effect.
Description
Technical field
The invention belongs to technical field of air purification, more particularly to a kind of air freshener and preparation method thereof.
Background technology
With expanding economy, ecological environment is gradually deteriorated, air quality degradation, so as to promote purification of air skill
The development of art.In recent years, the defects of many air fresheners are come out one after another, but this air freshener is most obvious, it is that it contains
The injury that some compositions may be brought to human body.
Current market sales of air freshener species is a lot, but is essentially all to be made up of compositions such as ether, essence,
These materials in atmosphere after chemical breakdown caused by some compositions of gas inherently air pollutants, this is aggravation in fact
The pollution level of air, it is long-term use of people is known from experience produce pessimal stimulation.This air freshener does not decompose harmful gas
Body, reaching the purpose of fresh air, its effect is to cover peculiar smell by distributing fragrance, rather than with causing peculiar smell in air
Gas react, simply by obscure people smell come " desalination " peculiar smell.In addition, the aromatic pair contained in air freshener
The nervous system of people can also produce harm, stimulate the respiratory mucosa etc. of child.
The content of the invention
The present invention in order to solve the above technical problems, provide a kind of air freshener and preparation method thereof, particular by
Following technical scheme is realized.
A kind of air freshener, include the raw material of following mass parts：Fresh mangosteen 20-50 parts, red bean 20-40 parts, golden small cup
Flower 10-30 parts, aloe 10-30 parts, centella 5-20 parts, glycerine 5-20 parts, Lavender 1-10 parts, EDETATE DISODIUM 1-10
Part, silica gel 1-10 parts, sulfuric acid 1-10 parts, solubilizer 1-10 parts, emulsifying agent 1-10 parts.
Further, described air freshener, the raw material of following mass parts is included：Fresh mangosteen 40-50 parts, red bean 30-
40 parts, pot marigold 25-30 parts, aloe 20-25 parts, centella 12-17 parts, glycerine 10-12 parts, Lavender 5-8 parts, EDTA
Disodium salt 3-6 parts, silica gel 2-5 parts, sulfuric acid 2-4 parts, solubilizer 1-3 parts, emulsifying agent 1-3 parts.
Further, described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester by
Mass ratio 1:0.25-0.3 is mixed.
Further, described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, poly alkyl alcohol
Oxygen ethene ether ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Further, described air freshener, including following preparation process：
1) mangosteen adds liquid nitrogen flash freezer grinding to be mixed with red bean powder, adds the ethanol of 2-3 times of mixed-powder quality, and utilization is micro-
Ripple extracts, and filtering, obtains filtrate 1, adds the ethyl acetate extraction of 1/2 times of mass of filtrate 1, takes upper liquid to carry out reduction vaporization recovery
Solvent, solid content 1 is obtained, freeze, obtain powder 1；
2) pot marigold crushes, and adds the deionized water mixing of 2-3 times of powder quality, and conversion system pressure extraction pot marigold has
Beneficial composition, filtering, filtrate 2 is obtained, add sulfuric acid mixing, 110-120r/min, 70-75 DEG C of stirring reaction 2-3h, filtering, obtain solid
1, solid 1 is dried, and obtains powder 2,；
3) aloe and centella are crushed, adds glycerine mixing, 5-6 DEG C of standing 2-3h, obtain mixture 1, add 2-3 times and mix
The deionized water of the mass of compound 1,3-4h is extracted under 50-53KHz supersonic frequencies, filter, obtain filtrate 3, silica gel is added in filtrate 3,
20-25 DEG C of standing 2-3h, is filtered, and obtains filtrate 4, and adding EDETATE DISODIUM in filtrate 4 mixes, and obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55-60 DEG C, 3000-3100r/min stirs
Dissolving is mixed, obtains solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10-12 times of mixed liquor quality, dress
Enter spray bottle, 660-670KPa is pressurized in spray bottle, both.
Further, described Microwave Extraction, it is to extract 7-8min in 450MHz, suspends 20-25min, 480MHz extractions 30-
35min, suspend 10-15min, 550MHz extractions 20-25min.
Further, described conversion system pressure, the mapping mode of pressure are lasting for 70MPa lasting 20min, 50MPa
10min, 100MPa continue 150min.
The beneficial effects of the present invention are：By carrying out variable frequency microwave extraction to mangosteen and red bean, pot marigold enters the present invention
Row transformation is extracted so that its benefit materials is able to larger utilization, and testing experiment of disinfection effect shows, air prepared by the present invention
Freshener is up to 87.78% in sterilization a moment to microorganism killing rate, and the inhibiting rate of microorganism is up to after 4h is sprayed
72.14%.Eye irritation experiment shows that air freshener prepared by the present invention does not injure for rabbit eyes.
In summary, the air freshener that prepared by the present invention is preferable to the inhibition of microorganism, and the duration is more long,
It is a kind of safe and reliable, preferable air freshener of effect.
Embodiment
The embodiment of the present invention is described in further detail below, but the invention is not limited in these realities
Mode is applied, any improvement or replacement on the present embodiment essence spirit, it is claimed to still fall within the claims in the present invention
Scope.
Embodiment 1
A kind of air freshener, including following raw material：Fresh mangosteen 40kg, red bean 30kg, pot marigold 25kg, aloe
20kg, centella 12kg, glycerine 10kg, Lavender 5kg, EDETATE DISODIUM 3kg, silica gel 2kg, sulfuric acid 2kg, solubilizer
1kg, emulsifying agent 1kg.
Described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester in mass ratio
1:0.25-0.3 is mixed.
Described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, AEO
Ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Described air freshener, including following preparation process：
1) mangosteen adds liquid nitrogen flash freezer grinding to be mixed with red bean powder, adds the ethanol of 2 times of mixed-powder quality, utilizes microwave
Extraction, filtering, filtrate 1 is obtained, add the ethyl acetate extraction of 1/2 times of mass of filtrate 1, take upper liquid to carry out reduction vaporization recovery molten
Agent, solid content 1 is obtained, freeze, obtain powder 1；
2) pot marigold crushes, and adds the deionized water mixing of 2 times of powder qualities, and conversion system pressure extraction pot marigold is beneficial
Composition, filtering, filtrate 2 is obtained, add sulfuric acid mixing, 110r/min, 70 DEG C of stirring reaction 2h, filtering, obtain solid 1, solid 1 is dry
It is dry, obtain powder 2；
3) aloe and centella are crushed, adds glycerine mixing, 5 DEG C of standing 2h, obtain mixture 1, add 2 times of mixtures 1
The deionized water of quality, 3h is extracted under 50KHz supersonic frequencies, filter, obtain filtrate 3, add silica gel in filtrate 3,20 DEG C of standing 2h,
Filter, obtain filtrate 4, adding EDETATE DISODIUM in filtrate 4 mixes, and obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55 DEG C, 3000r/min stirring and dissolvings,
Obtain solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10 times of mixed liquor quality, load spray
Bottle, 660KPa is pressurized in spray bottle, both.
Described Microwave Extraction, it is to extract 7min in 450MHz, suspends 20min, 480MHz extraction 30min, pause
10min, 550MHz extract 20min.
Described conversion system pressure, the mapping mode of pressure for 70MPa continue 20min, 50MPa continue 10min,
100MPa continues 150min.
Embodiment 2
A kind of air freshener, including following raw material：Fresh mangosteen 40kg, red bean 30kg, pot marigold 25kg, aloe
20kg, centella 12kg, glycerine 10kg, Lavender 5kg, EDETATE DISODIUM 3kg, silica gel 2kg, sulfuric acid 2kg, solubilizer
1kg, emulsifying agent 1kg.
Described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester in mass ratio
1:0.25-0.3 is mixed.
Described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, AEO
Ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Described air freshener, including following preparation process：
1) mangosteen, red bean mixing, crushing, the ethanol of 2 times of mixed-powder quality is added, using Microwave Extraction, filtering, must be filtered
Liquid 1, the ethyl acetate extraction of 1/2 times of mass of filtrate 1 is added, takes upper liquid to carry out reduction vaporization recycling design, obtains solid content 1,
It is lyophilized, obtain powder 1；
2) pot marigold crushes, and adds the deionized water mixing of 2 times of powder qualities, and conversion system pressure extraction pot marigold is beneficial
Composition, filtering, filtrate 2 is obtained, add sulfuric acid mixing, 110r/min, 70 DEG C of stirring reaction 2h, filtering, obtain solid 1, solid 1 is dry
It is dry, obtain powder 2；
3) aloe and centella are crushed, adds glycerine mixing, 5 DEG C of standing 2h, obtain mixture 1, add 2 times of mixtures 1
The deionized water of quality, 3h is extracted under 50KHz supersonic frequencies, filter, obtain filtrate 3, add silica gel in filtrate 3,20 DEG C of standing 2h,
Filter, obtain filtrate 4, adding EDETATE DISODIUM in filtrate 4 mixes, and obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55 DEG C, 3000r/min stirring and dissolvings,
Obtain solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10 times of mixed liquor quality, load spray
Bottle, 660KPa is pressurized in spray bottle, both.
Described Microwave Extraction, it is to extract 50min in 550MHz.
Described conversion system pressure, the mapping mode of pressure for 70MPa continue 20min, 50MPa continue 10min,
100MPa continues 150min.
Embodiment 3
A kind of air freshener, including following raw material：Fresh mangosteen 40kg, red bean 30kg, pot marigold 25kg, aloe
20kg, centella 12kg, glycerine 10kg, Lavender 5kg, EDETATE DISODIUM 3kg, silica gel 2kg, sulfuric acid 2kg, solubilizer
1kg, emulsifying agent 1kg.
Described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester in mass ratio
1:0.25-0.3 is mixed.
Described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, AEO
Ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Described air freshener, including following preparation process：
1) mangosteen adds liquid nitrogen flash freezer grinding to be mixed with red bean powder, adds the ethanol of 2 times of mixed-powder quality, utilizes microwave
Extraction, filtering, filtrate 1 is obtained, add the ethyl acetate extraction of 1/2 times of mass of filtrate 1, take upper liquid to carry out reduction vaporization recovery molten
Agent, solid content 1 is obtained, freeze, obtain powder 1；
2) pot marigold crushes, and the deionized water for adding 2 times of powder qualities decocts 2-3h, filtering, obtains filtrate 2, adds sulfuric acid
Mixing, 110r/min, 70 DEG C of stirring reaction 2h, filtering, solid 1 is obtained, solid 1 is dried, and obtains powder 2；
3) aloe and centella are crushed, adds glycerine mixing, 5 DEG C of standing 2h, obtain mixture 1, add 2 times of mixtures 1
The deionized water of quality, 3h is extracted under 50KHz supersonic frequencies, filter, obtain filtrate 3, add silica gel in filtrate 3,20 DEG C of standing 2h,
Filter, obtain filtrate 4, adding EDETATE DISODIUM in filtrate 4 mixes, and obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55 DEG C, 3000r/min stirring and dissolvings,
Obtain solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10 times of mixed liquor quality, load spray
Bottle, 660KPa is pressurized in spray bottle, both.
Described Microwave Extraction, it is to extract 7min in 450MHz, suspends 20min, 480MHz extraction 30min, pause
10min, 550MHz extract 20min.
Embodiment 4
A kind of air freshener, including following raw material：Fresh mangosteen 40kg, red bean 30kg, pot marigold 25kg, aloe
20kg, centella 12kg, glycerine 10kg, Lavender 5kg, EDETATE DISODIUM 3kg, silica gel 2kg, sulfuric acid 2kg, solubilizer
1kg, emulsifying agent 1kg.
Described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester in mass ratio
1:0.25-0.3 is mixed.
Described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, AEO
Ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Described air freshener, including following preparation process：
1) mangosteen adds liquid nitrogen flash freezer grinding to be mixed with red bean powder, adds the ethanol of 2 times of mixed-powder quality, utilizes microwave
Extraction, filtering, filtrate 1 is obtained, add the ethyl acetate extraction of 1/2 times of mass of filtrate 1, take upper liquid to carry out reduction vaporization recovery molten
Agent, solid content 1 is obtained, freeze, obtain powder 1；
2) pot marigold crushes, and adds the deionized water mixing of 2 times of powder qualities, and conversion system pressure extraction pot marigold is beneficial
Composition, filtering, filtrate 2 being obtained, add sulfuric acid mixing, 70 DEG C of stirring reaction 2h, filtering, obtain solid 1, solid 1 is dried, and obtains powder 2,
Wherein rotating speed is 110r/min；
3) aloe and centella are crushed, add glycerine mixing, obtain mixture 1, add 2 times of mass of mixture 1 go from
Sub- water, 3h being extracted under 50KHz supersonic frequencies, filtering, obtain filtrate 3, silica gel is added in filtrate 3,20 DEG C of standing 2h, filters, must filter
Liquid 4, EDETATE DISODIUM is added in filtrate 4 and is mixed, obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55 DEG C, 3000r/min stirring and dissolvings,
Obtain solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10 times of mixed liquor quality, load spray
Bottle, 660KPa is pressurized in spray bottle, both.
Described Microwave Extraction, it is to extract 7min in 450MHz, suspends 20min, 480MHz extraction 30min, pause
10min, 550MHz extract 20min.
Described conversion system pressure, the mapping mode of pressure for 70MPa continue 20min, 50MPa continue 10min,
100MPa continues 150min.
Embodiment 5
A kind of air freshener, including following raw material：Fresh mangosteen 40kg, red bean 30kg, pot marigold 25kg, aloe
20kg, centella 12kg, glycerine 10kg, Lavender 5kg, EDETATE DISODIUM 3kg, silica gel 2kg, sulfuric acid 2kg, solubilizer
1kg, emulsifying agent 1kg.
Described solubilizer, be by PEG-60 rilanit specials, polyoxyethylene sorbitan fatty acid ester in mass ratio
1:0.25-0.3 is mixed.
Described emulsifying agent, it is by triethanolamine, laruyl alcohol mono sulfosuccinates, AEO
Ammonium sulfate in mass ratio 0.4:2:0.5 mixes.
Described air freshener, including following preparation process：
1) mangosteen, red bean mixing, crushing, add the ethanol of 2 times of mixed-powder quality, Microwave Extraction, filtering, obtain filtrate 1,
The ethyl acetate extraction of 1/2 times of mass of filtrate 1 is added, takes upper liquid to carry out reduction vaporization recycling design, obtains solid content 1, freeze,
Obtain powder 1；
2) pot marigold crushes, and the deionized water for adding 2 times of powder qualities decocts 2-3h, filtering, obtains filtrate 2, adds sulfuric acid
Mixing, 70 DEG C of stirring reaction 2h, filtering, solid 1 is obtained, solid 1 is dried, and obtains powder 2, and wherein rotating speed is 110r/min；
3) aloe and centella are crushed, add glycerine mixing, obtain mixture 1, add 2 times of mass of mixture 1 go from
Sub- water, 3h being extracted under 50KHz supersonic frequencies, filtering, obtain filtrate 3, silica gel is added in filtrate 3,20 DEG C of standing 2h, filters, must filter
Liquid 4, EDETATE DISODIUM is added in filtrate 4 and is mixed, obtains extract solution 1；
4) powder 1, powder 2, Lavender, solubilizer, emulsifying agent are mixed, 55 DEG C, 3000r/min stirring and dissolvings,
Obtain solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10 times of mixed liquor quality, load spray
Bottle, 660KPa is pressurized in spray bottle, both.
Described Microwave Extraction, it is to extract 50min in 550MHz.
Experimental example
1st, air freshener effect is tested and assessed
The air freshener prepared according to the method for embodiment 1 is experimental group 1, according to application number CN201710214838.4
《One dust-collection sterilization air freshener prepares hair method》As a control group, prepared by 2 prescription methods of test disappears the air freshener of preparation
Toxic effect fruit, eye irritation.
The measure of Disinfection Effect：The previous day is tested, is 55m by 3 areas2Room door and window it is closed, kept during experiment
Laboratory temperature is 18-22 DEG C, relative humidity 45%-88%.About 75g air fresheners are used during experiment to upper, middle and lower and surrounding
Spraying, the measure for the effect that carried out disinfection using natural sedimentation.Natural sedimentation, if 5 sampled points, i.e., corner is diagonal indoors
Line intersection point is 1 sampled point, and the midpoints of the intersection point and four corner lines is other 4 sampled points, height of sampling 1.2-1.5m,
Sampled point should be away from more than wall 1m, and avoids at the air circulations such as air-conditioning, door and window.Sample 1 time, sterilized indoors before sterilization
Do not sampled after finishing at once 1,2,3 and 4h periods.Diameter 90mm nutrient agar panels are placed in sampled point during sampling
Place, open ware lid, exposure 5min.Sampling wild Oryza species put culture 48h in (35-37 DEG C) incubator, record each group different time
Interior media surface bacteria colony count.In kind it is compared using distilling water spray as negative control group.
Eye irritation：It is female 6, male 6, weight range 3.0-3.5kg from healthy regular grade new zealand rabbit 12,
3 groups are divided into, 24h checks that rabbit eyes are without exception before experiment, and tested material 0.1ml is drawn during experiment, instills one branch hole conjunctiva
It is intracapsular, 4s is passively closed, eyes are not rinsed after administration, opposite side makees normal control with physiological saline, 1,24,48 and after eye drip
The irido-corneal damage of 72h observation rabbit conjunctivas and recovery situation, while distilled water is carried out as negative control experiment.
Testing experiment of disinfection effect shows, air freshener prepared by the present invention is 1 after sterilization a moment and sterilization, 2,3,4h
Be substantially better than control group and negative control group to the killing rate of microorganism, and the air freshener of embodiment 1 its to microorganism
Inhibition is lasting compared with control group, and 72.14% is also up to the inhibiting rate of microorganism after 4h is shone in spray, while according to embodiment 5
The air freshener of preparation carries out disinfection measure of merit, finds air freshener bactericidal effect prepared by embodiment 5 compared with embodiment 1
Difference, also below control group, there was only 73.28% to the killing rate of microorganism in sterilization a moment, after spraying 4h, the killing to microorganism
Rate only has 38.4%.However, the difference of embodiment 1 and embodiment 5 is：
1st, to the not no use liquid nitrogen grinding of mangosteen, it is extracted under a kind of microwave frequency after being mixed with red bean；
2nd, the beneficiating ingredient extraction of pot marigold is extracted using decocting without change pressure；
3rd, aloe and centella crush, and add glycerine mixing, do not stand at low temperature.
In summary, so as to cause sterilization beneficiating ingredient lacking compared with embodiment 1 of embodiment 5, sterilizing rate is also compared with embodiment 1
It is low.
The air freshener Disinfection Effect of table 1
The eye irritation experimental result of table 2
Claims (7)
1. a kind of air freshener, it is characterised in that include the raw material of following mass parts：Fresh mangosteen 20-50 parts, red bean 20-
40 parts, pot marigold 10-30 parts, aloe 10-30 parts, centella 5-20 parts, glycerine 5-20 parts, Lavender 1-10 parts, EDTA
Disodium salt 1-10 parts, silica gel 1-10 parts, sulfuric acid 1-10 parts, solubilizer 1-10 parts, emulsifying agent 1-10 parts.
2. air freshener as claimed in claim 1, it is characterised in that include the raw material of following mass parts：Fresh mangosteen 40-
50 parts, red bean 30-40 parts, pot marigold 25-30 parts, aloe 20-25 parts, centella 12-17 parts, glycerine 10-12 parts, lavender essence
Oily 5-8 parts, EDETATE DISODIUM 3-6 parts, silica gel 2-5 parts, sulfuric acid 2-4 parts, solubilizer 1-3 parts, emulsifying agent 1-3 parts.
3. air freshener as claimed in claim 1 or 2, it is characterised in that described solubilizer, be that PEG-60 is hydrogenated into castor
Sesame oil, polyoxyethylene sorbitan fatty acid ester in mass ratio 1:0.25-0.3 is mixed.
4. air freshener as claimed in claim 1 or 2, it is characterised in that described emulsifying agent, be by triethanolamine, the moon
Cinnamic alcohol mono sulfosuccinates, AESA in mass ratio 0.4:2:0.5 mixes.
5. air freshener as claimed in claim 1, it is characterised in that including following preparation process：
1) mangosteen adds liquid nitrogen flash freezer grinding to be mixed with red bean powder, adds the ethanol of 2-3 times of mixed-powder quality, is carried using microwave
Take, filter, obtain filtrate 1, add the ethyl acetate extraction of 1/2 times of mass of filtrate 1, take upper liquid to carry out reduction vaporization recovery molten
Agent, solid content 1 is obtained, freeze, obtain powder 1；
2) pot marigold crushes, and adds the deionized water mixing of 2-3 times of powder quality, conversion system pressure extraction pot marigold beneficial into
Point, filtering, filtrate 2 is obtained, add sulfuric acid mixing, 110-120r/min, 70-75 DEG C of stirring reaction 2-3h, filtering, obtain solid 1, Gu
Body 1 is dried, and obtains powder 2；
3) aloe and centella are crushed, adds glycerine mixing, 5-6 DEG C of standing 2-3h, obtain mixture 1, add 2-3 times of mixture
The deionized water of 1 mass, 3-4h is extracted under 50-53KHz supersonic frequencies, filter, obtain filtrate 3, silica gel, 20-25 are added in filtrate 3
DEG C 2-3h is stood, filter, obtain filtrate 4, EDETATE DISODIUM is added in filtrate 4 and is mixed, obtains extract solution 1；
4) by powder 1, powder 2, Lavender, solubilizer, emulsifying agent mix, 55-60 DEG C, 3000-3100r/min stirring it is molten
Solution, obtains solution 1；
5) solution 1 and extract solution 1 mix, and obtain mixed liquor, add the deionized water mixing of 10-12 times of mixed liquor quality, load spray
Bottle, 660-670KPa is pressurized in spray bottle, both.
6. air freshener as claimed in claim 5, it is characterised in that described Microwave Extraction, be to extract 7- in 450MHz
8min, suspend 20-25min, 480MHz extraction 30-35min, suspend 10-15min, 550MHz extractions 20-25min.
7. air freshener as claimed in claim 5, it is characterised in that described conversion system pressure, the conversion side of pressure
Formula is that 70MPa continues the lasting 150min of 20min, 50MPa lasting 10min, 100MPa.
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| CN201710875732.9A CN107691509A (en) | 2017-09-25 | 2017-09-25 | A kind of air freshener and preparation method thereof |
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| CN201710875732.9A CN107691509A (en) | 2017-09-25 | 2017-09-25 | A kind of air freshener and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103394111A (en) * | 2013-06-29 | 2013-11-20 | 安徽榄菊日用制品有限公司 | Aerosol type air purifying agent and preparation method thereof |
| CN104922713A (en) * | 2014-03-17 | 2015-09-23 | 达金兰 | Aerosol type air refreshing agent |
| CN104940969A (en) * | 2015-06-20 | 2015-09-30 | 青岛恩高运动控制技术有限公司 | Faint scent type air purification spray |
| CN106267283A (en) * | 2016-08-25 | 2017-01-04 | 南丹县环境卫生管理站 | A kind of air freshener |
| CN106922756A (en) * | 2017-01-18 | 2017-07-07 | 陆开云 | A kind of delicate fragrance type air freshener |
| CN107027838A (en) * | 2017-04-01 | 2017-08-11 | 吴滨 | A kind of dust-collection sterilization air freshener preparation method |
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2017
- 2017-09-25 CN CN201710875732.9A patent/CN107691509A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103394111A (en) * | 2013-06-29 | 2013-11-20 | 安徽榄菊日用制品有限公司 | Aerosol type air purifying agent and preparation method thereof |
| CN104922713A (en) * | 2014-03-17 | 2015-09-23 | 达金兰 | Aerosol type air refreshing agent |
| CN104940969A (en) * | 2015-06-20 | 2015-09-30 | 青岛恩高运动控制技术有限公司 | Faint scent type air purification spray |
| CN106267283A (en) * | 2016-08-25 | 2017-01-04 | 南丹县环境卫生管理站 | A kind of air freshener |
| CN106922756A (en) * | 2017-01-18 | 2017-07-07 | 陆开云 | A kind of delicate fragrance type air freshener |
| CN107027838A (en) * | 2017-04-01 | 2017-08-11 | 吴滨 | A kind of dust-collection sterilization air freshener preparation method |
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