CN107674743A - A kind of composite solid lubricant material and its preparation technology - Google Patents

A kind of composite solid lubricant material and its preparation technology Download PDF

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Publication number
CN107674743A
CN107674743A CN201710970996.2A CN201710970996A CN107674743A CN 107674743 A CN107674743 A CN 107674743A CN 201710970996 A CN201710970996 A CN 201710970996A CN 107674743 A CN107674743 A CN 107674743A
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China
Prior art keywords
parts
oil
solid lubricant
fluorographite
preparation technology
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Pending
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CN201710970996.2A
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Chinese (zh)
Inventor
徐宏伟
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Individual
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Individual
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Priority to CN201710970996.2A priority Critical patent/CN107674743A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C10M2201/042—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C10M2215/082—Amides containing hydroxyl groups; Alkoxylated derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of composite solid lubricant material and its preparation technology, lubriation material component includes 20 40 parts of liquid paraffin, 10 20 parts of fluorographite, 5 15 parts of palmitoleic acid, 4 12 parts of lignin carbonate, 10 20 parts of dimethicone, 4 10 parts of isopropanol, 10 20 parts of SIMMONDSIA CHINENSIS SEED OIL, 49 parts of graphene, 39 parts of coconut oil alkanolamide, three red 4 12 parts of oil in parts by weight, preparation technology of the present invention is simple, obtained lubriation material greasy property is good, improve the service life of plant equipment, production cost is reduced, is economized on resources.

Description

A kind of composite solid lubricant material and its preparation technology
Technical field
The present invention relates to lubriation material preparing technical field, specially a kind of composite solid lubricant material and its preparation work Skill.
Background technology
Fretting wear is that plant equipment, space flight and aviation etc. have generally existing between the object of relative motion or relative motion trend Natural phenomena, according to the preliminary statistics, China every year caused by abrasion loss account for the 1% of gross national product, therefore, how Solve anti-attrition lubrication, the service life of prolonged mechanical part, reduce production cost, be current and significant period of time in future urgently Need to solve the problems, such as.
The content of the invention
It is an object of the invention to provide a kind of composite solid lubricant material and its preparation technology, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：A kind of composite solid lubricant material, lubriation material group Divide includes liquid paraffin 20-40 parts, fluorographite 10-20 parts, palmitoleic acid 5-15 parts, lignin carbonate 4- in parts by weight 12 parts, dimethicone 10-20 parts, isopropanol 4-10 parts, SIMMONDSIA CHINENSIS SEED OIL 10-20 parts, graphene 4-9 parts, coconut oil alkanol acyl Amine 3-9 parts, three red oily 4-12 parts.
Preferably, the preferable composition proportion of lubriation material component includes 30 parts of liquid paraffin, 15 parts of fluorographite, palm oil 10 parts of acid, 8 parts of lignin carbonate, 15 parts of dimethicone, 7 parts of isopropanol, 15 parts of SIMMONDSIA CHINENSIS SEED OIL, 7 parts of graphene, coconut oil 6 parts of alkanolamide, three red 8 parts of oil.
Preferably, its preparation technology comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation technology of the present invention is simple, obtained lubriation material profit Slip can be good, improves the service life of plant equipment, reduces production cost, economizes on resources；Wherein, the lotus lotus added in the present invention Bar oil, three red oil can increase lubricant effect；The fluorographite of addition can increase the abrasion resistance of lubriation material；The two of addition Methyl-silicone oil, it can prevent lubriation material from occurring oxidative phenomena.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects Enclose.
The present invention provides following technical scheme：A kind of composite solid lubricant material, lubriation material component are wrapped in parts by weight Include liquid paraffin 20-40 parts, fluorographite 10-20 parts, palmitoleic acid 5-15 parts, lignin carbonate 4-12 parts, dimethyl-silicon Oily 10-20 parts, isopropanol 4-10 parts, SIMMONDSIA CHINENSIS SEED OIL 10-20 parts, graphene 4-9 parts, coconut oil alkanolamide 3-9 parts, three red oil 4-12 parts.
Embodiment one：
Lubriation material component includes 20 parts of liquid paraffin, 10 parts of fluorographite, 5 parts of palmitoleic acid, lignin carbon in parts by weight 4 parts of hydrochlorate, 10 parts of dimethicone, 4 parts of isopropanol, 10 parts of SIMMONDSIA CHINENSIS SEED OIL, 4 parts of graphene, 3 parts of coconut oil alkanolamide, three Red 4 parts of oil.
The preparation technology of the present embodiment comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Embodiment two：
Lubriation material component includes 40 parts of liquid paraffin, 20 parts of fluorographite, 15 parts of palmitoleic acid, lignin carbon in parts by weight 12 parts of hydrochlorate, 20 parts of dimethicone, 10 parts of isopropanol, 20 parts of SIMMONDSIA CHINENSIS SEED OIL, 9 parts of graphene, 9 parts of coconut oil alkanolamide, Three red 12 parts of oil.
The preparation technology of the present embodiment comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Embodiment three：
Lubriation material component includes 25 parts of liquid paraffin, 12 parts of fluorographite, 7 parts of palmitoleic acid, lignin carbon in parts by weight 6 parts of hydrochlorate, 12 parts of dimethicone, 5 parts of isopropanol, 12 parts of SIMMONDSIA CHINENSIS SEED OIL, 5 parts of graphene, 4 parts of coconut oil alkanolamide, three Red 6 parts of oil.
The preparation technology of the present embodiment comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Example IV：
Lubriation material component includes 35 parts of liquid paraffin, 18 parts of fluorographite, 13 parts of palmitoleic acid, lignin carbon in parts by weight 11 parts of hydrochlorate, 18 parts of dimethicone, 9 parts of isopropanol, 18 parts of SIMMONDSIA CHINENSIS SEED OIL, 8 parts of graphene, 8 parts of coconut oil alkanolamide, three Red 10 parts of oil.
The preparation technology of the present embodiment comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Embodiment five：
Lubriation material component includes 30 parts of liquid paraffin, 15 parts of fluorographite, 10 parts of palmitoleic acid, lignin carbon in parts by weight 8 parts of hydrochlorate, 15 parts of dimethicone, 7 parts of isopropanol, 15 parts of SIMMONDSIA CHINENSIS SEED OIL, 7 parts of graphene, 6 parts of coconut oil alkanolamide, three Red 8 parts of oil.
The preparation technology of the present embodiment comprises the following steps：
A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
Preparation technology of the present invention is simple, and obtained lubriation material greasy property is good, improves the service life of plant equipment, drop Low production cost, economize on resources；Wherein, SIMMONDSIA CHINENSIS SEED OIL, the three red oil added in the present invention can increase lubricant effect；Addition Fluorographite can increase the abrasion resistance of lubriation material；The dimethicone of addition, it can prevent lubriation material from aoxidizing Phenomenon.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (3)

  1. A kind of 1. composite solid lubricant material, it is characterised in that：Lubriation material component includes liquid paraffin 20-40 in parts by weight Part, fluorographite 10-20 parts, palmitoleic acid 5-15 parts, lignin carbonate 4-12 parts, dimethicone 10-20 parts, isopropanol 4-10 parts, SIMMONDSIA CHINENSIS SEED OIL 10-20 parts, graphene 4-9 parts, coconut oil alkanolamide 3-9 parts, three red oily 4-12 parts.
  2. A kind of 2. composite solid lubricant material according to claim 1, it is characterised in that：Lubriation material component preferably into Distribution ratio includes 30 parts of liquid paraffin, 15 parts of fluorographite, 10 parts of palmitoleic acid, 8 parts of lignin carbonate, dimethicone 15 Part, 7 parts of isopropanol, 15 parts of SIMMONDSIA CHINENSIS SEED OIL, 7 parts of graphene, 6 parts of coconut oil alkanolamide, three red 8 parts of oil.
  3. 3. realize a kind of preparation technology of composite solid lubricant material described in claim 1, it is characterised in that：Its preparation technology Comprise the following steps：
    A, by palmitoleic acid, lignin carbonate, dimethicone, isopropanol, SIMMONDSIA CHINENSIS SEED OIL, graphene, coconut oil alkanol acyl Add in kneading machine and be kneaded after amine, three red oil mixing, melting temperature is 60 DEG C, time 10min, obtains mixture A；
    B, liquid paraffin, fluorographite are added in mixture A, 20min is stirred after mixing at normal temperatures, obtains mixture B；
    C, mixture B is stood into 7h at normal temperatures, that is, obtains solid lubricant.
CN201710970996.2A 2017-10-18 2017-10-18 A kind of composite solid lubricant material and its preparation technology Pending CN107674743A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4915856A (en) * 1987-07-10 1990-04-10 Durafilm Corporation Solid lubricant composition
CN101007981A (en) * 2006-01-25 2007-08-01 李政兆 Diesel car lubricant composition
CN102295977A (en) * 2011-07-13 2011-12-28 李胜 Novel lubricant for sewing machine and preparation method thereof
CN104178330A (en) * 2014-07-31 2014-12-03 青岛华承天机械制造有限公司 Low-cost composite solid lubricating material
CN104232268A (en) * 2014-08-31 2014-12-24 青岛锦绣水源商贸有限公司 Composite solid lubricating material with favorable antifriction and lubricating effects

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4915856A (en) * 1987-07-10 1990-04-10 Durafilm Corporation Solid lubricant composition
CN101007981A (en) * 2006-01-25 2007-08-01 李政兆 Diesel car lubricant composition
CN102295977A (en) * 2011-07-13 2011-12-28 李胜 Novel lubricant for sewing machine and preparation method thereof
CN104178330A (en) * 2014-07-31 2014-12-03 青岛华承天机械制造有限公司 Low-cost composite solid lubricating material
CN104232268A (en) * 2014-08-31 2014-12-24 青岛锦绣水源商贸有限公司 Composite solid lubricating material with favorable antifriction and lubricating effects

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