CN107446666A - A kind of wire rope fat and its preparation technology - Google Patents

A kind of wire rope fat and its preparation technology Download PDF

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Publication number
CN107446666A
CN107446666A CN201710696180.5A CN201710696180A CN107446666A CN 107446666 A CN107446666 A CN 107446666A CN 201710696180 A CN201710696180 A CN 201710696180A CN 107446666 A CN107446666 A CN 107446666A
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Prior art keywords
parts
wire rope
rope fat
agent
fat
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Granted
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CN201710696180.5A
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Chinese (zh)
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CN107446666B (en
Inventor
任晓辰
吴韦岐
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New Mstar Technology Ltd New Zealand Xi'an
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New Mstar Technology Ltd New Zealand Xi'an
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06Organic compounds derived from inorganic acids or metal salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02Pour-point; Viscosity index
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08Resistance to extreme temperature
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10Semi-solids; greasy

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention belongs to protective agent technical field, more particularly to a kind of wire rope fat and its preparation technology.The wire rope fat is counted including following component, 0.3 part~1.2 parts of 56 parts~63 parts, No. 2 35 parts~42 parts of rust-proofing waxes of RA5 hot asphalts regenerative agent, 1 part~2.5 parts of 80# microwaxes and antirust agent in parts by weight;The preparation technology of the wire rope fat, conditional parameter is low, equipment is simple, by the control of technological parameter in preparation method, makes that the wire rope fat shelf-life is longer, adhesive force is stronger, viscosity is bigger, dropping point is higher, oil content is also higher and cryogenic property is more preferable.

Description

A kind of wire rope fat and its preparation technology
Technical field
The invention belongs to protective agent technical field, more particularly to a kind of wire rope fat and its preparation technology.
Background technology
Wire rope fat is by organic thickening agent group and high viscosity oil petroleum refined by naphthenic, and added with anti-oxidant, anticorrosion, anti- The refined wirerope barrier cream formed of the multiple additives such as corrosion, anti-extreme pressure.Wire rope surface grease can be divided into hydrocarbon-based type by its composition The different types such as wire rope surface grease, pitch shaped steel wire rope face grease, soap base type barrier cream.Hydrocarbon-based type wire rope surface grease, one As using waste and old paraffin, ceresine prepare, dropping point is relatively low, and for use temperature range at -30 DEG C~60 DEG C or so, dosage is larger.
Wire rope surface grease is coated on stock and a kind of barrier cream for being twisted rear steel wire rope surface, on the one hand it is to subtract that it, which is acted on, The few steel wire rope friction in stock between steel wire and friction of steel wire rope and rope sheave groove in use, to reduce the mill of steel wire rope Damage;On the other hand it is to protect steel wire rope not corroded during transport, storage and use.This requires wire rope surface grease to produce Product have following performance:Excellent adhesion, permeance property, good antirust, Corrosion Protection and good extruding are wear-resistant Performance.
And wire rope fat drips point of the prior art is relatively low, easily slide at high temperature, and kinematic viscosity is small, corrosivity By force, low temperature properties are poor, and its preparation technology complexity manufacturing cost is also of a relatively high.
The content of the invention
The invention provides a kind of wire rope fat and its preparation technology, solves wire rope of the prior art The technical problem that fat kinematic viscosity is small, oil content is low and low temperature properties are poor, the technical problem further solved are that manufacturing process is complicated The high technical problem of cost.
Concrete technical scheme is that the wire rope fat is counted including following component in parts by weight, and RA5 hot asphalts are again 0.3 part~1.2 parts of 56 parts~63 parts, No. 2 35 parts~42 parts of rust-proofing waxes of raw agent, 1 part~2.5 parts of 80# microwaxes and antirust agent.This RA5 hot asphalts regenerative agent described in invention is the RA5 hot asphalt regenerative agents of sinopec Jingmen petro-chemical corporation production.No. 2 Rust-proofing wax is No. 2 rust-proofing waxes of sinopec Nanyang Oil Field company production, and wherein moisture is less than 0.5%, and melt drop temperature is 75 DEG C, motion Viscosity is 28mm2/s。
The further wire rope fat is counted including 61 parts, No. 2 antirusts of RA5 hot asphalts regenerative agent in parts by weight 0.7 part of 37 parts of wax, 1.3 parts of 80# microwaxes and antirust agent.
The further wire rope fat is counted including 56 parts, No. 2 antirusts of RA5 hot asphalts regenerative agent in parts by weight 0.3 part of 42 parts of wax, 1.7 parts of 80# microwaxes and antirust agent.
Further above-mentioned antirust agent is T701.
Present invention also offers a kind of preparation technology of wire rope fat, following steps are specifically included, (1) weighs RA5 Hot asphalt regenerative agent, 110 DEG C~130 DEG C then are warming up to stirring, then maintain the temperature at 110 DEG C~130 DEG C and enter for 2 hours Row dehydration;(2) stop stirring and sequentially add No. 2 rust-proofing waxes and 80# microwaxes weighed;(3) 120 DEG C are maintained the temperature at ~140 DEG C, stir 2 hours;(4) cooled down, temperature carries out middle control analysis when being less than 100 DEG C, according to country to barrier cream Production requirement, middle control analysis experiment is carried out, color requires that brown to dark brown, dropping point is not less than 65 DEG C, and kinematic viscosity is not less than 20mm2/ s, 65 DEG C, 1h does not slide, the qualified rear addition antirust agent such as -30 DEG C of wire rope fat of cryogenic property do not solidify;(5) drop Temperature is packed, finished product while stirring to 80 DEG C~90 DEG C.
Temperature is 122 DEG C after being heated up in further above-mentioned steps (1).
The further step (3) maintains the temperature at 125 DEG C, stirs 2 hours.
Beneficial effect, by the component of RA5 hot asphalts regenerative agent, No. 2 rust-proofing waxes, 80# microwaxes and antirust agent with containing The design of amount makes the wire rope fat in the present invention reach dropping point more than 65 DEG C, carries out 60 DEG C of landing experiments and does not slide, moves Viscosity is more than national standard 20mm2/ s, salt mist experiment result are more than 7;By the control of technological parameter in preparation method, make steel wire Restricting, the barrier cream shelf-life is longer, adhesive force is stronger, viscosity is bigger, dropping point is higher, oil content is also higher and cryogenic property is more preferable.
Brief description of the drawings
In order to illustrate more clearly of technical scheme, embodiment will be described below needed for accompanying drawing make it is simple Introduce, it should be apparent that, drawings in the following description are only some embodiments of the present invention, to those of ordinary skill in the art For, on the premise of not paying creative work, other accompanying drawings can also be obtained according to these accompanying drawings, these accompanying drawings institute is straight The technical scheme for connecing to obtain should also belong to protection scope of the present invention.
Fig. 1 is the process chart of the present invention.
Fig. 2 is the examination and test of products report related data of the present invention.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, below to the specific reality of the present invention The mode of applying elaborates.Many details are elaborated in the following description in order to fully understand the present invention.But this Invention can be implemented with being much different from other manner described here, and those skilled in the art can be without prejudice to the present invention Similar improvement is done in the case of intension, therefore the present invention is not limited by following public embodiment.
For embodiment 1 so that 1000kg wire rope fat is pressed as an example, wherein product weight component is as follows, and RA5 hot asphalts are again Raw agent 560kg, No. 2 rust-proofing wax 410kg, 80# microwax 10kg and boron amide class antirust agent 20kg.Heretofore described R A5 heat Mix the RA5 hot asphalt regenerative agents that bitumen regenerant is the production of sinopec Jingmen petro-chemical corporation;No. 2 rust-proofing waxes are sinopec Nanyang No. 2 rust-proofing waxes of Oilfield Company production, wherein moisture are less than 0.5%, and melt drop temperature is 75 DEG C, kinematic viscosity 28mm2/s;The two It can be obtained by outsourcing.By the component of RA5 hot asphalts regenerative agent, No. 2 rust-proofing waxes, 80# microwaxes and antirust agent with containing The design of amount makes the wire rope fat in the present invention reach dropping point more than 65 DEG C, carries out 60 DEG C of landing experiments and does not slide, moves Viscosity is more than national standard 22mm2/ s, has reached 32.5mm2/s;It is 17 that salt mist experiment result, which is more than 7,;The shelf-life of product is more It is long, adhesive force is stronger, viscosity is bigger, dropping point is higher, oil content also it is higher as in the present embodiment oil content reached 56% and Cryogenic property is more preferable.
For optimum embodiment so that 1000kg wire rope fat is pressed as an example, wherein product weight component is as follows, RA5 hot asphalts Regenerative agent 610kg, No. 2 rust-proofing wax 370kg, 80# microwax 13kg and T701 antirust agent 7kg.Heretofore described RA5 heat is mixed Bitumen regenerant is the RA5 hot asphalt regenerative agents of sinopec Jingmen petro-chemical corporation production.No. 2 rust-proofing waxes are sinopec Nanyang oil No. 2 rust-proofing waxes of Tian companies production, wherein moisture are less than 0.5%, and melt drop temperature is 75 DEG C, kinematic viscosity 36mm2/s.Pass through RA5 hot asphalts regenerative agent, No. 2 rust-proofing waxes, 80# microwaxes and the component of T701 antirust agent and the design of content make in the present invention Wire rope fat reach dropping point more than 81 DEG C, carry out 60 DEG C and slide experiment not to slide, kinematic viscosity 35mm2/ s, salt fog Experimental result is 17.The dropping point of the product is up to 81 DEG C, and salt haze value has also been up to 19, and oil content is also up to 61%, Parameters are optimal.
For embodiment 3 so that 1000kg wire rope fat is pressed as an example, wherein product weight component is as follows, and RA5 hot asphalts are again Raw agent 560kg, No. 2 rust-proofing wax 420kg, 80# microwax 17kg and T701 antirust agent 3kg.Heretofore described RA5 heat mixes drip Blue or green regenerative agent is the RA5 hot asphalt regenerative agents of sinopec Jingmen petro-chemical corporation production.No. 2 rust-proofing waxes are sinopec Nanyang Oil Field No. 2 rust-proofing waxes of company's production, wherein moisture are less than 0.5%, and melt drop temperature is 75 DEG C, kinematic viscosity 28mm2/s.Pass through RA5 Hot asphalt regenerative agent, No. 2 rust-proofing waxes, 80# microwaxes and the component of T701 antirust agent and the design of content make in the present invention Wire rope fat reaches dropping point more than 65 DEG C, carries out 60 DEG C of landing experiments and does not slide, kinematic viscosity is more than national standard 20mm2/ s, has reached 32.5mm2/ s, salt mist experiment result are more than 7, have reached 17;Shelf-life of product is longer, adhesive force more By force, viscosity is bigger, dropping point is higher, oil content is also higher and cryogenic property is more preferable.
Embodiment 4 is as shown in figure 1, prepare the technique of above-mentioned wire rope fat, specially:First by RA5 hot asphalts Regenerative agent is squeezed into T2 kettles and measured, and obtains 610kgRA5 hot asphalt regenerative agents, the RA5 hot asphalts that then will be measured Regenerative agent is squeezed into T1 kettles, is then started to stir and is heated, and treats that temperature is raised to 110 DEG C~130 DEG C, then RA5 heat is mixed Bitumen regenerant maintains the temperature at 110 DEG C~130 DEG C and carries out dehydration in 2 hours;Next stop stirring sequentially adding in advance No. 2 rust-proofing wax 370kg and 80# microwax 13kg weighed;Then heating is carried out again maintains the temperature at 120 DEG C~140 DEG C, and And stir 2 hours;Next cooled down, middle control analysis is carried out when temperature is less than 100 DEG C, according to country to barrier cream Production requirement, analysis experiment is carried out, color requires that brown to dark brown, dropping point is not less than 65 DEG C, and kinematic viscosity is not less than 20mm2/ s, 65 DEG C, 1h does not slide, and -30 DEG C of wire rope fat of cryogenic property do not solidify, and parameters add after the assay was approved Enter T701 antirust agent 7kg, continue stirring and allow product to be cooled down, treat that temperature is down to 80 DEG C~90 DEG C, then carry out while stirring Packaging, last finished product.The preparation technology is simple, the wire rope fat shelf-life is longer, adhesive force is stronger, viscosity is bigger, Dropping point is higher, oil content is also higher and cryogenic property is more preferable.
Embodiment 5 is as shown in figure 1, prepare the technique of above-mentioned wire rope fat, specially:First by RA5 hot asphalts Regenerative agent is squeezed into T2 kettles and measured, and obtains 610kgRA5 hot asphalt regenerative agents, the RA5 hot asphalts that then will be measured Regenerative agent is squeezed into T1 kettles, is then started to stir and is heated, and treats that temperature is raised to 122 DEG C, then RA5 hot asphalts are regenerated Agent maintains the temperature at 122 DEG C and carries out dehydration in 2 hours;Next stop stirring and sequentially add No. 2 antirusts weighed in advance Wax 370kg and 80# microwax 13kg;Then heating is carried out again and maintains the temperature at 125 DEG C, and is stirred 2 hours;Next enter Row cooling, carries out middle control analysis when temperature is less than 100 DEG C, according to production requirement of the country to barrier cream, carries out analysis experiment, Color requires that brown to dark brown, dropping point is not less than 65 DEG C, and kinematic viscosity is not less than 20mm2/ s, 65 DEG C, 1h does not slide, low temperature - 30 DEG C of wire rope fat of performance do not solidify, and parameters add T701 antirust agent 7kg after the assay was approved, continue stirring and allow Product is cooled down, and is treated that temperature is down to 85 DEG C, is then packed while stirring, last finished product.The preparation technology is simple, The wire rope fat shelf-life is longer, adhesive force is stronger, viscosity is bigger, dropping point is higher, oil content is also higher and cryogenic property more It is good.Wire rope fat wire rope fat shelf-life for being prepared under the conditions of this technological parameter is longer, adhesive force is stronger, oil-containing Amount is also of a relatively high.
Fig. 2 is the wire rope fat test experiments result of the present invention tested by Wuxi petrochina, as a result may be used To find out, the wire rope fat color in the present invention is the uniform ointment of dark brown, and drop temperature is 75 DEG C, and kinematic viscosity is 32.25mm2/ s, erosion test are also qualified;Landing experiment, low temperature properties experiment also all meet national requirements in addition, and damp and hot Experimental result is 35, salt mist experiment result is 17 to be significantly better than that national design standard.

Claims (7)

  1. A kind of 1. wire rope fat, it is characterised in that:The wire rope fat is counted including following component in parts by weight, 56 parts~63 parts, No. 2 35 parts~42 parts of rust-proofing waxes of RA5 hot asphalts regenerative agent, 1 part~2.5 parts of 80# microwaxes and antirust agent 0.3 part~1.2 parts.
  2. 2. wire rope fat according to claim 1, it is characterised in that:The wire rope fat is counted in parts by weight Including 0.7 part of 61 parts, No. 2 37 parts of rust-proofing waxes of RA5 hot asphalts regenerative agent, 1.3 parts of 80# microwaxes and antirust agent.
  3. 3. wire rope fat according to claim 1, it is characterised in that:The wire rope fat is counted in parts by weight Including 0.3 part of 56 parts, No. 2 42 parts of rust-proofing waxes of RA5 hot asphalts regenerative agent, 1.7 parts of 80# microwaxes and antirust agent.
  4. 4. according to any described wire rope fat in claims 1 to 3, it is characterised in that:The antirust agent is prevented for T701 Rust agent.
  5. A kind of 5. technique for preparing wire rope fat, it is characterised in that:Comprise the following steps, (1) weighs RA5 hot asphalts again Raw agent, is then warming up to 110 DEG C~130 DEG C with stirring, maintains the temperature at 110 DEG C~130 DEG C and carries out dehydration in 2 hours; (2) stop stirring and sequentially add No. 2 rust-proofing waxes and 80# microwaxes weighed;(3) 120 DEG C~140 DEG C are maintained the temperature at, is stirred Mix 2 hours;(4) cooled down, temperature carries out middle control analysis when being less than 100 DEG C, antirust agent is added after qualified;(5) 80 are cooled to DEG C~90 DEG C, it is packaged while stirring, finished product.
  6. 6. the technique according to claim 5 for preparing wire rope fat, it is characterised in that:Heated up in the step (1) Temperature is 122 DEG C afterwards.
  7. 7. the technique according to claim 7 for preparing wire rope fat, it is characterised in that:Step (3) maintains the temperature at 125 DEG C, stir 2 hours.
CN201710696180.5A 2017-08-15 2017-08-15 Steel wire rope protective grease and preparation process thereof Active CN107446666B (en)

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CN107446666B CN107446666B (en) 2020-11-27

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110734803A (en) * 2019-10-17 2020-01-31 西安玛珂特新材料科技股份有限公司 high-end steel wire rope grease

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104250575A (en) * 2013-06-25 2014-12-31 中国石油天然气股份有限公司 Wire-rope grease composition with excellent performances and preparation method thereof
CN105713706A (en) * 2016-01-21 2016-06-29 泰尔精蜡(上海)有限公司 Asphalt type wire rope surface grease

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104250575A (en) * 2013-06-25 2014-12-31 中国石油天然气股份有限公司 Wire-rope grease composition with excellent performances and preparation method thereof
CN105713706A (en) * 2016-01-21 2016-06-29 泰尔精蜡(上海)有限公司 Asphalt type wire rope surface grease

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110734803A (en) * 2019-10-17 2020-01-31 西安玛珂特新材料科技股份有限公司 high-end steel wire rope grease

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