CN107653101A - A kind of granulated sugar orange peel cleaning powder and preparation method thereof - Google Patents
A kind of granulated sugar orange peel cleaning powder and preparation method thereof Download PDFInfo
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- CN107653101A CN107653101A CN201710882644.1A CN201710882644A CN107653101A CN 107653101 A CN107653101 A CN 107653101A CN 201710882644 A CN201710882644 A CN 201710882644A CN 107653101 A CN107653101 A CN 107653101A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Agricultural Chemicals And Associated Chemicals (AREA)
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Abstract
The invention belongs to articles for washing field, and in particular to a kind of granulated sugar orange peel cleaning powder and preparation method thereof, the granulated sugar orange peel cleaning powder are mainly made by the raw material of following parts by weight：11 20 parts of granulated sugar orange peels, 12 14 parts of asarums, 6 10 parts of tsaokos, 79 portions of beggar-ticks, 10 16 parts of Guava Leafs, 6 10 parts of Wild Carrot Fruits, 27 parts of Gentiana rigescens, 48 parts of buttercups, 10 13 parts of capsules of weeping forsythia.Buttercup is added as foaming agent in granulated sugar orange peel cleaning powder, make cleaning powder that there is low foaming effect, and buttercup also acts as the effect of bactericide, add asarum, Guava Leaf, tsaoko, beggar-ticks, Gentiana rigescens have given full play to each composition cleaning, antibacterial effect after pulverizing process, make granulated sugar orange peel cleaning powder active matter content is high, detergent power is good, bactericidal effect is good, it is non-toxic, nonirritant, without being not easy to grow spoilage organisms after anaphylaxis, low bubble, water-saving, cleaning.
Description
【Technical field】
The invention belongs to articles for washing field, and in particular to a kind of granulated sugar orange peel cleaning powder and preparation method thereof.
【Background technology】
Main component is d-limonen, citral, limonoids in the volatile oil that orange peel is rich in, and is also contained
Nobiletin, orange peel glucoside, inositol, PABA etc..
Limonoids is a kind of triterpene compound being present in Rutaceae and Meliaceae plant, in Citrus
Rich content, it is one of main component for causing citrus fruits bitter taste.Limonoids mainly has cancer resistance, antibacterial
Property and antiviral property, there is emulsification, scattered, wetting, decontamination, and do not influenceed by water hardness, particularly in Escherichia coli, Song
The Grain-negative enteral pathogenic bacteria such as shigella dysenteriae, proteus, typhoid bacillus, paratyphosum Bacterium, Pseudomonas aeruginosa, comma bacillus are equal
There is inhibitory action.People, which also have, to be used directly as washing product by orange peel is soaked, though it is used directly as washing product
So there are certain washing functions, but it is still present that detergency is not strong, anti-inflammation power is not strong, active matter content is not high lacks
Point.
And cleaning product at this stage is mainly chemical synthesis, although its detergency is strong, there is chemical reagent in it, no
Security, long-term use of stimulation to skin, cause pachylosis dry and cracked, cleaning is incomplete, and residual causes to endanger body, simultaneously
Because being not easily decomposed, the pollution to ambient soil and water body is quite serious, and easily grows spoilage organisms again after cleaning.
【The content of the invention】
In view of problem above, the invention provides a kind of granulated sugar orange peel cleaning powder and preparation method thereof, the granulated sugar orange peel are clear
Clean powder, its active matter content is high, detergent power is good, bactericidal effect is good, it is non-toxic, nonirritant, without anaphylaxis, low bubble, water-saving,
It is not easy to grow spoilage organisms after cleaning, the ideal such as cleaning food Work tool, tableware and veterinary antibiotics in people's daily life can be used as
Safety and environmental protection washing product.The technical problems to be solved by the invention are realized using following technical scheme：
A kind of granulated sugar orange peel cleaning powder, is mainly made by the raw material of following parts by weight：11-20 part granulated sugar orange peel, 12-14 parts
Asarum, 6-10 parts tsaoko, 7-9 parts beggar-ticks, 10-16 parts Guava Leaf, 6-10 parts Wild Carrot Fruit, 2-7 parts Gentiana rigescens, 4-8 part hairs
Gelsemium, 10-13 part capsules of weeping forsythia.
Preferably, the granulated sugar orange peel cleaning powder is mainly made by the raw material of following parts by weight：11 parts of granulated sugar orange peels, 12 parts
Asarum, 6 parts of tsaokos, 7 portions of beggar-ticks, 10 parts of Guava Leafs, 6 parts of Wild Carrot Fruits, 2 parts of Gentiana rigescens, 4 parts of buttercups, 10 parts of capsules of weeping forsythia.
Preferably, the granulated sugar orange peel cleaning powder is mainly made by the raw material of following parts by weight：16 parts of granulated sugar orange peels, 13 parts
Asarum, 8 parts of tsaokos, 8 portions of beggar-ticks, 12 parts of Guava Leafs, 8 parts of Wild Carrot Fruits, 5 parts of Gentiana rigescens, 6 parts of buttercups, 12 parts of capsules of weeping forsythia.
Preferably, the granulated sugar orange peel cleaning powder is mainly made by the raw material of following parts by weight：20 parts of granulated sugar orange peels, 14 parts
Asarum, 10 parts of tsaokos, 9 portions of beggar-ticks, 16 parts of Guava Leafs, 10 parts of Wild Carrot Fruits, 7 parts of Gentiana rigescens, 8 parts of buttercups, 13 parts of capsules of weeping forsythia.
A kind of granulated sugar orange peel cleaning powder, its preparation method comprise the following steps：
1) extract
First the peeling of granulated sugar tangerine is cleaned up, skin is cut to every section 2-3 centimetres, puts water filling in container, water temperature 35-40 into
DEG C, the part by weight of granulated sugar orange peel and water is 1:1.4, water will cover pericarp, add sodium carbonate by the 3% of water injection rate, stirring is equal
It is even, sealing storage 1-3 days, 500 milliliters of ethanol, lid is covered, allow granulated sugar orange peel to soak 2 days, add acetic acid, adjust solution
PH to 7-8, finally produces extract with filter screen filtration；
2) crush
Asarum, tsaoko, beggar-ticks, Guava Leaf, Wild Carrot Fruit, Gentiana rigescens, buttercup, the capsule of weeping forsythia are mixed, produce mixture, will
Mixture is sprayed with atomization ethanol, is placed into container and is heated, and treats ethanol volatilization turning off stove, then entered with atomization ethanol
Row sprinkling, is heated, thing to be mixed is darkened, and mixture is put into disintegrating machine is crushed, and is broken into 2-5mm particle
Shape, produce medicinal powder；
3) powder processed
Decoction obtained by step 1) is mixed with step 2) gained medicinal powder, with 15% sodium hydroxide by decoction PH after stirring
Value is adjusted to 10-12, and immersion is press-filtered out liquid after 7~9 hours, pH value is adjusted to 3-4 with concentrated hydrochloric acid, in 60-70 DEG C of temperature
0.5 hour, cooling and standings, collected by suction precipitation, was washed to neutrality, is dried, sterilized with far infrared, i.e., after precipitating completely
Obtain granulated sugar orange peel cleaning powder.
Further, step 3) medicinal powder and decoction ratio are 1:3.
By adopting the above-described technical solution, the invention has the advantages that：
Buttercup is added in granulated sugar orange peel cleaning powder as foaming agent, makes cleaning powder that there is low foaming effect, Er Qiemao
Gelsemium also acts as the effect of bactericide, adds asarum, Guava Leaf, tsaoko, beggar-ticks, Gentiana rigescens and is fully sent out after pulverizing process
The cleaning of each composition, antibacterial effect have been waved, has made that granulated sugar orange peel cleaning powder active matter content is high, detergent power is good, bactericidal effect
It is good, non-toxic, nonirritant, without being not easy to grow spoilage organisms after anaphylaxis, low bubble, water-saving, cleaning.People's daily life can be used as
The preferable safety and environmental protection washing product such as middle cleaning food Work tool, tableware and veterinary antibiotics.
Asarum, alias：Asarum sieboldii, basin grass asarum, Aristolochiaceae, asarum perennial herb；Root-like stock it is upright or it is horizontal walk,
Diameter 2-3 millimeters, 1-2 centimetres of internode length, there is a plurality of fibrous root.Antibacterial, antivirus action kakuol preserved material, volatile oil etc. are blue to leather
Positive bacteria, hay bacillus and typhoid bacillus have certain In-vitro Inhibitory Effect, and decoction also has suppression to tubercle bacillus and typhoid bacillus
Make and use.Herba Asari volatile oil has inhibitory action, antibacterial to a variety of fungies such as Aspergillus flavus, black-koji mould, Candida albicans etc.
Active ingredient be safrole.α-asarone plays the role of to suppress Respiratory Syncytial Virus(RSV) propagation；
Guava Leaf, Chinese medicine name.For the leaf of myrtle guava, there is antibacterial, anti-cancer；
Tsaoko is one of large kind of Chinese herbal medicines, and tsaoko makees flavoring；Complete stool can extract aromatic oil.Fruit
It is used as medicine, there is drying damp and strengthening spleen, the function of eliminating phlegm preventing malaria.Cure mainly the diseases such as abdominal fullness and distention, gastric disorder causing nausea vomiting, dyspepsia malaria.In a lot of into
Medicine be unable to do without its formula, and to cholera, pestilence, malignant malaria has therapeutic action；
Beggar-ticks, annual herb, stem is upright, blunt four prismatic.The lower portion of the stem leaf is smaller, and rarely foliolate pinniform is answered
Leaf, both sides leaflet ellipse or ovate-elliptic.Flower head diameter 8-9 millimeters.Cure mainly：Acute icteric hepatitis, gastroenteritis,
Pain in rheumatoid joints, malaria, there is inhibitory action to staphylococcus aureus, Escherichia coli, typhoid bacillus and salmonella.
Gentiana rigescens, to rhizobia, Escherichia coli, hay bacillus, Agrobacterium tumefaciens etc. have effect.Gentiana rigescens grass water
Preserved material in vitro has different degrees of inhibitory action to dermatophytes such as trichophyton gypseum star nocardias.Test tube method is demonstrate,proved
Bright Gentiana rigescens decoction has in various degree to Pseudomonas aeruginosa, proteus, typhoid bacillus, shigella dysenteriae, staphylococcus aureus etc.
Inhibitory action；
Buttercup：It is Ranunculaceae, Ranunculus herbaceos perennial.This kind of herb contains protoanemonin, for foaming agent and kills
Microbial inoculum, smash external application to pieces, can preventing malaria, subside a swelling and control sore tinea.
【Embodiment】
The following examples can help those skilled in the art that the present invention is more fully understood, but cannot be with any
Mode limits the present invention.
Embodiment 1
A kind of granulated sugar orange peel cleaning powder, is mainly made by the raw material of following parts by weight：11 parts of granulated sugar orange peels, 12 parts of asarums, 6
Part tsaoko, 7 portions of beggar-ticks, 10 parts of Guava Leafs, 6 parts of Wild Carrot Fruits, 2 parts of Gentiana rigescens, 4 parts of buttercups, 10 parts of capsules of weeping forsythia；
Specific preparation method comprises the following steps：
1) extract
First the peeling of granulated sugar tangerine is cleaned up, skin is cut to 2 centimetres every section, puts water filling in container, 35 DEG C of water temperature, granulated sugar into
The part by weight of orange peel and water is 1:1.4, water will cover pericarp, add sodium carbonate by the 3% of water injection rate, stir, seal
Storage 1 day, 500 milliliters of ethanol, covers lid, allows granulated sugar orange peel to soak 2 days, adds acetic acid, adjusts solution PH most 7,
Finally extract is produced with filter screen filtration；
2) crush
Asarum, tsaoko, beggar-ticks, Guava Leaf, Wild Carrot Fruit, Gentiana rigescens, buttercup, the capsule of weeping forsythia are mixed, produce mixture, will
Mixture is sprayed with atomization ethanol, is placed into container and is heated, and treats ethanol volatilization turning off stove, then entered with atomization ethanol
Row sprinkling, is heated, thing to be mixed is darkened, and mixture is put into disintegrating machine is crushed, and is broken into 2mm particle
Shape, produce medicinal powder；
3) powder processed
Decoction obtained by step 1) is mixed with step 2) gained medicinal powder, with 15% sodium hydroxide by decoction PH after stirring
Value is adjusted to 10, and immersion is press-filtered out liquid after 7 hours, and pH value is adjusted to 3 with concentrated hydrochloric acid, in 60 DEG C of temperature 0.5 hour, cooling
Stand, collected by suction precipitation, is washed to neutrality, is dried, sterilized with far infrared, it is clear to produce granulated sugar orange peel after precipitating completely
Clean powder.
Embodiment 2
A kind of granulated sugar orange peel cleaning powder and preparation method thereof, is mainly made by the raw material of following parts by weight：16 portions of granulated sugar tangerines
Skin, 13 parts of asarums, 8 parts of tsaokos, 8 portions of beggar-ticks, 12 parts of Guava Leafs, 8 parts of Wild Carrot Fruits, 5 parts of Gentiana rigescens, 6 parts of buttercups, 12 parts of companies
Stick up；
Specific preparation method comprises the following steps：
1) extract
First the peeling of granulated sugar tangerine is cleaned up, skin is cut to 2 centimetres every section, puts water filling in container, 37 DEG C of water temperature, granulated sugar into
The part by weight of orange peel and water is 1:1.4, water will cover pericarp, add sodium carbonate by the 3% of water injection rate, stir, seal
Storage 2 days, 500 milliliters of ethanol, covers lid, allows granulated sugar orange peel to soak 2 days, adds acetic acid, regulation solution PH is most
7.5, finally produce extract with filter screen filtration；
2) crush
Asarum, tsaoko, beggar-ticks, Guava Leaf, Wild Carrot Fruit, Gentiana rigescens, buttercup, the capsule of weeping forsythia are mixed, produce mixture, will
Mixture is sprayed with atomization ethanol, is placed into container and is heated, and treats ethanol volatilization turning off stove, then entered with atomization ethanol
Row sprinkling, is heated, thing to be mixed is darkened, and mixture is put into disintegrating machine is crushed, and is broken into 4mm particle
Shape, produce medicinal powder；
3) powder processed
Decoction obtained by step 1) is mixed with step 2) gained medicinal powder, with 15% sodium hydroxide by decoction PH after stirring
Value is adjusted to 11, and immersion is press-filtered out liquid after 8 hours, and pH value is adjusted to 3-4 with concentrated hydrochloric acid, cold in 65 DEG C of temperature 0.5 hour
But stand, collected by suction precipitation, is washed to neutrality, is dried, sterilized with far infrared, produce granulated sugar orange peel after precipitating completely
Cleaning powder.
Embodiment 3
A kind of granulated sugar orange peel cleaning powder and preparation method thereof, is mainly made by the raw material of following parts by weight：20 portions of granulated sugar tangerines
Skin, 14 parts of asarums, 10 parts of tsaokos, 9 portions of beggar-ticks, 16 parts of Guava Leafs, 10 parts of Wild Carrot Fruits, 7 parts of Gentiana rigescens, 8 parts of buttercups, 13 parts
The capsule of weeping forsythia；
Specific preparation method comprises the following steps：
1) extract
First the peeling of granulated sugar tangerine is cleaned up, skin is cut to 3 centimetres every section, puts water filling in container, 40 DEG C of water temperature, granulated sugar into
The part by weight of orange peel and water is 1:1.4, water will cover pericarp, add sodium carbonate by the 3% of water injection rate, stir, seal
Storage 3 days, 500 milliliters of ethanol, covers lid, allows granulated sugar orange peel to soak 2 days, adds acetic acid, adjusts solution PH most 8,
Finally extract is produced with filter screen filtration；
2) crush
Asarum, tsaoko, beggar-ticks, Guava Leaf, Wild Carrot Fruit, Gentiana rigescens, buttercup, the capsule of weeping forsythia are mixed, produce mixture, will
Mixture is sprayed with atomization ethanol, is placed into container and is heated, and treats ethanol volatilization turning off stove, then entered with atomization ethanol
Row sprinkling, is heated, thing to be mixed is darkened, and mixture is put into disintegrating machine is crushed, and is broken into 2-5mm particle
Shape, produce medicinal powder；
3) powder processed
Decoction obtained by step 1) is mixed with step 2) gained medicinal powder, with 15% sodium hydroxide by decoction PH after stirring
Value is adjusted to 12, and immersion is press-filtered out liquid after 9 hours, and pH value is adjusted to 4 with concentrated hydrochloric acid, in 70 DEG C of temperature 0.5 hour, cooling
Stand, collected by suction precipitation, is washed to neutrality, is dried, sterilized with far infrared, it is clear to produce granulated sugar orange peel after precipitating completely
Clean powder.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.
Claims (6)
1. a kind of granulated sugar orange peel cleaning powder, it is characterised in that the granulated sugar orange peel cleaning powder is mainly by the raw material of following parts by weight
It is made：11-20 part granulated sugar orange peel, 12-14 parts asarum, 6-10 parts tsaoko, 7-9 parts beggar-ticks, 10-16 parts Guava Leaf, 6-10
Part Wild Carrot Fruit, 2-7 parts Gentiana rigescens, 4-8 parts buttercup, 10-13 part capsules of weeping forsythia.
2. granulated sugar orange peel cleaning powder as claimed in claim 1, it is characterised in that the granulated sugar orange peel cleaning powder is mainly by following
The raw material of parts by weight is made：11 parts of granulated sugar orange peels, 12 parts of asarums, 6 parts of tsaokos, 7 portions of beggar-ticks, 10 parts of Guava Leafs, 6 parts of southern cranes
Lice, 2 parts of Gentiana rigescens, 4 parts of buttercups, 10 parts of capsules of weeping forsythia.
3. granulated sugar orange peel cleaning powder as claimed in claim 1, it is characterised in that the granulated sugar orange peel cleaning powder is mainly by following
The raw material of parts by weight is made：16 parts of granulated sugar orange peels, 13 parts of asarums, 8 parts of tsaokos, 8 portions of beggar-ticks, 12 parts of Guava Leafs, 8 parts of southern cranes
Lice, 5 parts of Gentiana rigescens, 6 parts of buttercups, 12 parts of capsules of weeping forsythia.
4. granulated sugar orange peel cleaning powder as claimed in claim 1, it is characterised in that the granulated sugar orange peel cleaning powder is mainly by following
The raw material of parts by weight is made：20 parts of granulated sugar orange peels, 14 parts of asarums, 10 parts of tsaokos, 9 portions of beggar-ticks, 16 parts of Guava Leafs, 10 parts of south
Lappula echinata, 7 parts of Gentiana rigescens, 8 parts of buttercups, 13 parts of capsules of weeping forsythia.
5. the preparation method of granulated sugar orange peel cleaning powder as claimed in claim 1, it is characterised in that the granulated sugar orange peel cleaning powder
Preparation method comprise the following steps：
1) extract
First the peeling of granulated sugar tangerine is cleaned up, skin is cut to every section 2-3 centimetres, puts water filling in container, 35-40 DEG C of water temperature, sand into
The part by weight of sugared orange peel and water is 1:1.4, water will cover pericarp, add sodium carbonate by the 3% of water injection rate, stir, close
Seal up for safekeeping and put 1-3 days, 500 milliliters of ethanol, cover lid, allow granulated sugar orange peel to soak 2 days, add acetic acid, regulation solution PH to
7-8, finally produce extract with filter screen filtration；
2) crush
Asarum, tsaoko, beggar-ticks, Guava Leaf, Wild Carrot Fruit, Gentiana rigescens, buttercup, the capsule of weeping forsythia are mixed, mixture is produced, will mix
Thing is sprayed with atomization ethanol, is placed into container and is heated, and treats ethanol volatilization turning off stove, then sprayed with atomization ethanol
Spilling, heated, thing to be mixed is darkened, and mixture is put into disintegrating machine is crushed, and is broken into 2-5mm graininess,
Produce medicinal powder；
3) powder processed
Decoction obtained by step 1) is mixed with medicinal powder obtained by step 2), adjusted liquid PH value with 15% sodium hydroxide after stirring
Save and be press-filtered out liquid after 7~9 hours for 10-12, immersion, pH value is adjusted to 3-4 with concentrated hydrochloric acid, it is small in 60-70 DEG C of temperature 0.5
When, cooling and standings, collected by suction precipitation, is washed to neutrality, is dried, sterilized with far infrared, produce sand after precipitating completely
Sugared orange peel cleaning powder.
6. the preparation method of granulated sugar orange peel cleaning powder as claimed in claim 5, it is characterised in that step 3) medicinal powder and decoction ratio
Example is 1:3.
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| CN201710882644.1A CN107653101A (en) | 2017-09-26 | 2017-09-26 | A kind of granulated sugar orange peel cleaning powder and preparation method thereof |
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| CN201710882644.1A CN107653101A (en) | 2017-09-26 | 2017-09-26 | A kind of granulated sugar orange peel cleaning powder and preparation method thereof |
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Family
ID=61131271
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Application publication date: 20180202 |