CN107638380B - Preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for long time - Google Patents

Preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for long time Download PDF

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CN107638380B
CN107638380B CN201711065313.5A CN201711065313A CN107638380B CN 107638380 B CN107638380 B CN 107638380B CN 201711065313 A CN201711065313 A CN 201711065313A CN 107638380 B CN107638380 B CN 107638380B
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mosquito
brevibacillus laterosporus
repelling
water
essential oil
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CN107638380A (en
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吕丽娅
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Chongqing Jianerkang Pharmaceutical Technology Co ltd
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Abstract

The invention discloses a children mosquito-repellent floral water capable of repelling mosquitoes for a long time, which comprises the following components: water, mixed essential oil, plant essence, a bacillus brevis inoculum and the balance. According to the invention, the brevibacillus laterosporus microbial inoculum with a good insecticidal effect is added on the basis of the original floral water, and the brevibacillus laterosporus is matched with chrysanthemum and mint in the traditional Chinese medicine essential oil, so that the long-acting mosquito repelling effect can be achieved, the mosquito repelling time can reach 12-16 hours, and the overnight requirement can be met.

Description

Preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for long time
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time.
Background
The traditional mosquito-repellent toilet water is a perfume product prepared by adding a proper amount of mosquito repellent on the basis of common toilet water, and is used for repelling mosquitoes, removing miliaria, relieving itching, enabling skin to be fresh and comfortable and the like, wherein two common repellents are diethyltoluamide and mosquito repellent ester respectively. The deet or the deet is a sanitary pesticide component, and belongs to a slightly toxic product.
Chinese invention patent CN1548028A discloses a mosquito-repellent floral water, which comprises the following main components: plant essential oil, perfume essence, ethanol and water, rosemary, eucalyptus oil, pine needle oil, peppermint oil, borneol oil, chamomile, clove oil, thyme oil, geranium oil, rose oil, citronella oil and liquorice oil; but the mosquito repelling time of the product is only 5 to 7 hours.
In order to reduce toxicity, improve the safety level of products and achieve the effect of repelling mosquitoes for a longer time, the invention provides the children mosquito-repelling floral water for repelling the mosquitoes for a long time, which takes traditional Chinese medicines and microorganisms as main raw materials.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time.
The technical scheme of the invention is as follows:
a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time comprises the following steps:
A. mixing essential oils of flos Chrysanthemi, folium Eucalypti Globueli, herba Menthae, Borneolum Syntheticum, flos Caryophylli, flos Rosae Rugosae, and Glycyrrhrizae radix, and stirring to obtain mixed essential oil;
B. mixing ethanol and water, adding mixed essential oil and plant essence, stirring, and sterilizing;
C. adding the Brevibacillus laterosporus agent into the solution, homogenizing and filtering to obtain the product.
Brevibacillus laterosporus has functions of killing insects (Singer, 1996; 1997), killing threads (Favret, 1985), resisting bacteria (T. Foideldes, 2000), resisting tumors (Takeuchi, 1984), dissolving phosphorus (Duchumei, 2005), degrading organic pollutants (Crawford, 1976), producing lysine (Kamiyama T, 1994), and various enzyme substances (Tadashi, 1990).
The research on Brevibacillus laterosporus has been in history for nearly one hundred years, and the research in foreign countries has been very active, especially in Russia, America, UK, Japan, Belgium and other countries. Early studies focused primarily on the insecticidal activity of Brevibacillus laterosporus, which has toxic effects on larvae of mosquitoes, beetles (but not lepidopteran insects) and invertebrates such as nematodes and molluscs (Sinnova, 1996). Their insecticidal activity is mainly due to the toxic effect of the proteins contained in their spore-like inclusions or crystals on a wide variety of insects. The micromolecular bacterial toxin generated by the brevibacillus laterosporus can inhibit the hatching of nematode eggs or the development of larvae, and can prevent and control parasitic nematodes of animals and plants (Singer, 1996), and the brevibacillus laterosporus is prepared into powder in the United states to prevent and control the nematode diseases of animals. China has also paid more and more attention to the field, and the nematicidal result of Brevibacillus laterosporus of university of Yunnan has also been applied (Zhang Ke Dun, Tianbaoyu and Zhou Wei, 2004). The entire genome sequencing of three Brevibacillus laterosporus strains has been completed by the printing. Novo microbial Agents, produced by Novietz, Denmark, also contain Brevibacillus laterosporus. In recent years, studies on the bacteriostatic activity of brevibacillus laterosporus have been receiving more and more attention, and it is reported in the united states, japan, etc. that brevibacillus laterosporus can produce various antibacterial substances, including nonpeptide spermines, polyketides, peptide antibiotics, chitinases, etc. The antibacterial substances generated by the brevibacillus laterosporus are mainly used for preventing and treating gram-positive bacteria and candida which have clinically generated drug resistance, but the reports of the inhibition effect on household mosquitoes are few.
Chrysanthemum flower, name of traditional Chinese medicine. The plant taxonomy is perennial root herbaceous plant of Compositae and Chrysanthemum. The cultivation types of the multi-headed chrysanthemum, the single-bodied chrysanthemum, the big chrysanthemum, the cliff chrysanthemum, the artistic chrysanthemum, the plains chrysanthemum and the like are divided according to the cultivation form; the cultivation types are divided into garden holding, retreating holding, anti-holding, messy holding, open heart holding, feimei holding and the like according to the appearance shape of the petals. The chrysanthemum of different types is named with various kinds of names. The chrysanthemum is three of ten famous flowers in China, one of four monarch flowers (plum flower, orchid, bamboo and chrysanthemum) in the flower, and is also one of four cut flowers in the world (chrysanthemum, Chinese rose, carnation and gladiolus), and the yield is at the top. As the chrysanthemum has the grade of clearing cold and proud snow, the famous sentence of "picking chrysanthemum under east hedge, you see south mountain" is only in the way of ceramic. Chinese people have customs of chrysanthemum flower and chrysanthemum wine. Tang. Meng Haoyuan 'Lai' Lai Shi Maotai (ancient times of the department of Others): "when the day of heavy yang comes, chrysanthemum comes. The meaning of luckiness and longevity is given to chrysanthemum in ancient myth legend.
The flos Chrysanthemi is dry capitula of Compositae. Mainly produced in Zhejiang, Anhui, Henan, etc. Harvesting when 9-11 month flowers are full, drying in the shade or baking, or fumigating and steaming, and drying in the sun. Unprocessed. The herbs are classified into Bo Ju, Chu Ju, Gong Ju and Hang Ju according to the producing area and processing method. Since the flowers have different colors, they are divided into yellow chrysanthemum and white chrysanthemum.
Chrysanthemum is indicated for wind-heat type common cold, headache, vertigo, red and swollen eyes, blurred vision, sores and abscess.
Mint, name of traditional Chinese medicine. The soil is named 'Yindancao', is a labiate plant, namely other dry whole plants of the same genus, mostly grows beside a mountain wetland river, and roots and stems transversely grow underground, and is an aromatic crop with special economic value. It is a sweating and antipyretic, and can be used for treating influenza, headache, conjunctival congestion, fever, sore throat, and gum swelling. The mint picked in the bright greenhouse is also a fresh vegetable on a dining table in spring festival, and is fresh, cool and delicious. Herba Menthae is usually used instead of tea for clearing away heart-fire and improving eyesight. In China, the yield of mint is the greatest mainly in Jiangsu province and Anhui province.
Mint, pungent in flavor and cool in flavor can dispel heat, so it is specially used for dispelling wind and dissipating heat. So it is the key herb for headache, wind syndrome of head, eye, throat and mouth, infantile convulsions, scrofula, sores and scabies.
Preferably, in step B, the volume ratio of ethanol to water is 1: (8-20).
Preferably, the long-acting mosquito-repelling children mosquito-repelling flower water comprises the following components in percentage by weight: 4.8 to 10 percent of ethanol, 2 to 5 percent of mixed essential oil, 0.5 to 2 percent of plant essence, 0.1 to 0.3 percent of brevibacillus laterosporus agent and the balance of water.
Preferably, the Brevibacillus laterosporus agent contains (2-5) × 107CFU of Brevibacillus laterosporus SNB 10.
The invention has the advantages that: the children mosquito-repellent flower water capable of repelling mosquitoes for a long time comprises the following components: water, mixed essential oil, plant essence, a bacillus brevis inoculum and the balance. According to the invention, the brevibacillus laterosporus microbial inoculum with a good insecticidal effect is added on the basis of the original floral water, and the brevibacillus laterosporus is matched with chrysanthemum and mint in the traditional Chinese medicine essential oil, so that the long-acting mosquito repelling effect can be achieved, the mosquito repelling time can reach 12-16 hours, and the overnight requirement can be met.
Detailed Description
Example 1:
a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time comprises the following steps:
A. mixing essential oils of flos Chrysanthemi, folium Eucalypti Globueli, herba Menthae, Borneolum Syntheticum, flos Caryophylli, flos Rosae Rugosae, and Glycyrrhrizae radix, and stirring to obtain mixed essential oil;
B. mixing ethanol and water, adding mixed essential oil and plant essence, stirring, and sterilizing;
C. adding the Brevibacillus laterosporus agent into the solution, homogenizing and filtering to obtain the product.
The long-acting mosquito-repelling children mosquito-repelling flower dew comprises the following components in percentage by weight: 6% of ethanol, 3% of mixed essential oil, 1% of plant essence, 0.2% of a brevibacillus laterosporus agent and the balance of water.
The brevibacillus laterosporus agent contains 4 x 107CFU of Brevibacillus laterosporus SNB 10.
Example 2:
a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time comprises the following steps:
A. mixing essential oils of flos Chrysanthemi, folium Eucalypti Globueli, herba Menthae, Borneolum Syntheticum, flos Caryophylli, flos Rosae Rugosae, and Glycyrrhrizae radix, and stirring to obtain mixed essential oil;
B. mixing ethanol and water, adding mixed essential oil and plant essence, stirring, and sterilizing;
C. adding the Brevibacillus laterosporus agent into the solution, homogenizing and filtering to obtain the product.
The long-acting mosquito-repelling children mosquito-repelling flower dew comprises the following components in percentage by weight: 4.8% of ethanol, 5% of mixed essential oil, 0.5% of plant essence, 0.3% of brevibacillus laterosporus agent and the balance of water.
The brevibacillus laterosporus agent contains 2 x 107CFU of Brevibacillus laterosporus SNB 10.
Example 3:
a preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time comprises the following steps:
A. mixing essential oils of flos Chrysanthemi, folium Eucalypti Globueli, herba Menthae, Borneolum Syntheticum, flos Caryophylli, flos Rosae Rugosae, and Glycyrrhrizae radix, and stirring to obtain mixed essential oil;
B. mixing ethanol and water, adding mixed essential oil and plant essence, stirring, and sterilizing;
C. adding the Brevibacillus laterosporus agent into the solution, homogenizing and filtering to obtain the product.
The long-acting mosquito-repelling children mosquito-repelling flower dew comprises the following components in percentage by weight: 10% of ethanol, 2% of mixed essential oil, 2% of plant essence, 0.1% of brevibacillus laterosporus agent and the balance of water.
The brevibacillus laterosporus agent contains 5 x 107CFU of Brevibacillus laterosporus SNB 10.
The mosquito-repellent toilet water for children for long-acting mosquito repelling has the mosquito repelling time of 12-16 hours, and the mosquito repelling time is shortened to 5-7 hours under the condition of not adding the brevibacillus laterosporus agent.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (1)

1. A preparation method of children mosquito-repellent floral water capable of repelling mosquitoes for a long time is characterized by comprising the following steps:
A. mixing essential oils of flos Chrysanthemi, folium Eucalypti Globueli, herba Menthae, Borneolum Syntheticum, flos Caryophylli, flos Rosae Rugosae, and Glycyrrhrizae radix, and stirring to obtain mixed essential oil;
B. mixing ethanol and water, adding mixed essential oil and plant essence, stirring, and sterilizing;
C. adding the brevibacillus laterosporus agent into the solution, homogenizing and filtering to obtain the product;
in the step B, the volume ratio of the ethanol to the water is 1: (8-20);
the long-acting mosquito-repelling children mosquito-repelling flower dew comprises the following components in percentage by weight: 4.8-10% of ethanol, 2-5% of mixed essential oil, 0.5-2% of plant essence, 0.1-0.3% of brevibacillus laterosporus agent and the balance of water;
the Brevibacillus laterosporus preparation contains (2-5) × 107CFU of Brevibacillus laterosporus SNB 10.
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* Cited by examiner, † Cited by third party
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CN107691494A (en) * 2017-11-08 2018-02-16 李倩 A kind of preparation method of children's mosquito repellent incense liquid of long-acting mosquito-driving
WO2023220508A1 (en) * 2022-05-13 2023-11-16 Nutrition & Biosciences USA 4, Inc. Compositions comprising brevibacilla multifunctional fermentates and methods of use
WO2024191710A2 (en) * 2023-03-16 2024-09-19 Nutrition & Biosciences USA 4, Inc. Personal care compositions for malodor control and methods thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1548028A (en) * 2003-05-13 2004-11-24 上海家化联合股份有限公司 Mosquito-repellent toilet water
CN101695469A (en) * 2009-10-26 2010-04-21 张发明 Mosquito dispelling liquid
WO2014045131A1 (en) * 2012-09-24 2014-03-27 Lincoln University Biocontrol compositions
CN105232416A (en) * 2015-11-23 2016-01-13 梁秀萍 Rose essential oil floral water and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1548028A (en) * 2003-05-13 2004-11-24 上海家化联合股份有限公司 Mosquito-repellent toilet water
CN101695469A (en) * 2009-10-26 2010-04-21 张发明 Mosquito dispelling liquid
WO2014045131A1 (en) * 2012-09-24 2014-03-27 Lincoln University Biocontrol compositions
CN105232416A (en) * 2015-11-23 2016-01-13 梁秀萍 Rose essential oil floral water and preparation method thereof

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