CN107637693A - A kind of gel combination of glycerol monobutyralte - Google Patents

A kind of gel combination of glycerol monobutyralte Download PDF

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Publication number
CN107637693A
CN107637693A CN201711111693.1A CN201711111693A CN107637693A CN 107637693 A CN107637693 A CN 107637693A CN 201711111693 A CN201711111693 A CN 201711111693A CN 107637693 A CN107637693 A CN 107637693A
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CN
China
Prior art keywords
glycerol monobutyralte
glycerol
monobutyralte
gel
gel combination
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711111693.1A
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Chinese (zh)
Inventor
张磊
白桦
顾丹
袁锐
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Jiangnan University
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Jiangnan University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Jiangnan University filed Critical Jiangnan University
Priority to CN201711111693.1A priority Critical patent/CN107637693A/en
Publication of CN107637693A publication Critical patent/CN107637693A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of gel combination of glycerol monobutyralte, it is related to the solidification of glycerol monobutyralte, belongs to animal feed additive field.Said composition is formed by the configuration of following part by weight, 10~80 parts of glycerol monobutyralte, 10~60 parts of glycerin monostearate, 1~30 part of edible wax, 1~30 part of sorbitan monostearate.Gel agent molecule is self-assembly of stable three-dimensional net structure in the present invention, and the three-dimensional net structure is readily able to the glycerol monobutyralte parcel of flowing wherein, it is lost flowability, turn into a kind of gel solid state, so as to effectively solidify tributyrin.The present invention has the advantages of preparation method green non-pollution, zero-emission, production cost is low, glycerol monobutyralte content is high, feeding facilitates, thus has good promotional value.

Description

A kind of gel combination of glycerol monobutyralte
Technical field
The present invention relates to a kind of gel combination of glycerol monobutyralte, it is related to the solidification of glycerol monobutyralte, belongs to animal feeding Feed additives field.
Background technology
Glycerol monobutyralte is a kind of green safe feed addictive, not decomposed under one's belt, dynamic as butanoic acid derivative Butyric acid and glycerine are resolved into thing enteron aisle, butyric acid energy part substitute antibiotics, alleviates the inflammatory reaction of enteron aisle, improves exempting from for body Epidemic disease power, keep intestinal health.But glycerol monobutyralte has the phenomenon of Difficulty in actual production and application, it is main former Because being that glycerol monobutyralte exists in liquid form, use is very inconvenient.In addition, glycerol monobutyralte easily becomes sour, the smell is awful, sternly Ghost image rings the appetite of feeding personnel health and animal.
Existing disclosed glycerol monobutyralte curing mode, inorganic adsorbent white carbon silica gel adsorption (CN201410298903.2) tributyrin can not be largely adsorbed, and adsorbent surface is more moist, commodity form is bad. Tannin cladding process (CN201110219669.6) equipment investment is big, and production cost is high, complex process and the too high tannin pair of content Animal has very strong anti-oxidant action.Fatty acid calcium is low for microcapsule method (CN201510012138.8) covering amount of membrane material In 50%, and the discharge capacity of waste water is big.
The content of the invention
It is an object of the invention to provide a kind of gel combination of glycerol monobutyralte, in said composition gel agent molecule from Assembling forms stable three-dimensional net structure, and the three-dimensional net structure is readily able to the glycerol monobutyralte parcel of flowing wherein, made It loses flowability, and turns into a kind of gel solid state, so as to effectively solidify tributyrin.
To achieve the above object, the present invention can take following technical proposals:
The present invention is using glycerol monobutyralte as primary raw material, keeping temperature glycerol monobutyralte 50 DEG C~100 under stirring DEG C, add the additives such as glycerin monostearate, edible wax, sorbitan monostearate and be well mixed, be then cooled to Type.The glycerol monobutyralte gel combination is formed by the configuration of following part by weight:
Material name Constituent content (part)
Glycerol monobutyralte 10~80
Glycerin monostearate 10~60
Edible wax 1~30
Sorbitan monostearate 1~30
The glycerol monobutyralte be only son's acid glyceride, two glycerol monobutyraltes, tributyrin one or more and It is combined.
The edible wax is the one or more and its any combination of palm wax, rice bran wax, beeswax.
Advantages of the present invention is as follows:The present invention has that preparation method green non-pollution, zero-emission, production cost be low, butyric acid The advantages of glyceride content is high, feeding facilitates, thus there is good promotional value.
Embodiment
Following embodiment is used for illustrating the present invention.
Embodiment 1
A kind of glycerol monobutyralte gel combination, the glycerol monobutyralte gel combination by following part by weight configure and Into:
Material name Constituent content (part)
Tributyrin 55
Glycerin monostearate 10
Palm wax 5
Sorbitan monostearate 30
Tributyrin temperature 70 C is kept, glycerin monostearate, palm wax, sorbierite are added under stirring The additives such as acid anhydride monostearate are simultaneously well mixed, and are then cooled and shaped.The gel combination is protected in the temperature less than 45 DEG C Gel stability is held, not oil spilling.
Embodiment 2
A kind of glycerol monobutyralte gel combination, the glycerol monobutyralte gel combination by following part by weight configure and Into:
Material name Constituent content (part)
Only son's acid glyceride 15
Tributyrin 65
Glycerin monostearate 10
Rice bran wax 9
Sorbitan monostearate 1
Only son's acid glyceride, tributyrin are well mixed, 70 DEG C of keeping temperature, added under stirring single hard The additives such as glycerol, rice bran wax, sorbitan monostearate are simultaneously well mixed, and are then cooled and shaped.The gel group Compound keeps gel stability in the temperature less than 45 DEG C, not oil spilling.
Embodiment 3
A kind of glycerol monobutyralte gel combination, the glycerol monobutyralte gel combination by following part by weight configure and Into:
Material name Constituent content (part)
Only son's acid glyceride 15
Two glycerol monobutyraltes 25
Tributyrin 40
Glycerin monostearate 10
Beeswax 1
Sorbitan monostearate 9
Only son's acid glyceride, two glycerol monobutyraltes, tributyrin are well mixed, 70 DEG C of keeping temperature, stirred The additives such as glycerin monostearate, beeswax, sorbitan monostearate are added under state and are well mixed, are then cooled to Type.The gel combination keeps gel stability in the temperature less than 45 DEG C, not oil spilling.
Embodiment 4
A kind of glycerol monobutyralte gel combination, the glycerol monobutyralte gel combination by following part by weight configure and Into:
Material name Constituent content (part)
Only son's acid glyceride 2
Two glycerol monobutyraltes 2
Tributyrin 6
Glycerin monostearate 60
Rice bran wax 20
Sorbitan monostearate 10
Only son's acid glyceride, two glycerol monobutyraltes, tributyrin are well mixed, keep 70 DEG C of glycerol monobutyralte, Add the additives such as glycerin monostearate, rice bran wax, sorbitan monostearate and be well mixed, be then cooled and shaped. The gel combination keeps gel stability in the temperature less than 45 DEG C, not oil spilling.
Embodiment 5
A kind of glycerol monobutyralte gel combination, the glycerol monobutyralte gel combination by following part by weight configure and Into:
Material name Constituent content (part)
Only son's acid glyceride 5
Two glycerol monobutyraltes 10
Tributyrin 30
Glycerin monostearate 15
Rice bran wax 30
Sorbitan monostearate 10
Only son's acid glyceride, two glycerol monobutyraltes, tributyrin are well mixed, keep 70 DEG C of glycerol monobutyralte, Add the additives such as glycerin monostearate, rice bran wax, sorbitan monostearate and be well mixed, be then cooled and shaped. The gel combination keeps gel stability in the temperature less than 45 DEG C, not oil spilling.
Above-described is only embodiments of the present invention, but is never limited the scope of the present invention, and the present invention is unlimited In above example.It is appreciated that those skilled in the art directly lead without departing from the spirit and concept in the present invention The oher improvements and changes for going out or associating, it is considered as being included within protection scope of the present invention.

Claims (3)

1. a kind of glycerol monobutyralte gel combination, it is characterised in that the glycerol monobutyralte gel combination presses following weight ratio Example configuration forms:
2. glycerol monobutyralte gel combination according to claim 1, it is characterised in that the glycerol monobutyralte is only son's acid One or more in glyceride, two glycerol monobutyraltes, tributyrin.
3. glycerol monobutyralte gel combination according to claim 1, it is characterised in that the edible wax is palm wax, rice bran Wax, beeswax, one or more.
CN201711111693.1A 2017-11-13 2017-11-13 A kind of gel combination of glycerol monobutyralte Pending CN107637693A (en)

Priority Applications (1)

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Applications Claiming Priority (1)

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CN201711111693.1A CN107637693A (en) 2017-11-13 2017-11-13 A kind of gel combination of glycerol monobutyralte

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CN107637693A true CN107637693A (en) 2018-01-30

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111149919A (en) * 2020-01-14 2020-05-15 湖南泰丰动物药业有限公司 Glycerol butyrate compound for poultry as well as preparation method and application thereof
CN112189762A (en) * 2019-07-08 2021-01-08 龙岩新奥生物科技有限公司 Feeding composition and preparation method and application thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102510725A (en) * 2009-06-12 2012-06-20 玛尔斯有限公司 Polymer gelation of oils
CN106172879A (en) * 2016-07-18 2016-12-07 马鞍山市黄池食品(集团)有限公司 A kind of luteolin Semen Sesami gel oil and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102510725A (en) * 2009-06-12 2012-06-20 玛尔斯有限公司 Polymer gelation of oils
CN106172879A (en) * 2016-07-18 2016-12-07 马鞍山市黄池食品(集团)有限公司 A kind of luteolin Semen Sesami gel oil and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
牛丽亚等: "米糠蜡与单甘酯复配制备菜籽油基凝胶油", 《中国油脂》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112189762A (en) * 2019-07-08 2021-01-08 龙岩新奥生物科技有限公司 Feeding composition and preparation method and application thereof
CN111149919A (en) * 2020-01-14 2020-05-15 湖南泰丰动物药业有限公司 Glycerol butyrate compound for poultry as well as preparation method and application thereof

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