CN107629824A - A kind of vehicle lead-free synthetic fuel - Google Patents
A kind of vehicle lead-free synthetic fuel Download PDFInfo
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Abstract
A kind of vehicle lead-free synthetic fuel, is consisted of the following composition：The methanol of 40~60 parts by weight；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；The butane of 6.5~17 parts by weight；The aliphatic acid ammonium of 1~5 part of parts by weight；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8 1.5 parts by weight；The parts by weight of the parts by weight of peracetic acid spy butyl ester 2~3, the parts by weight of oleic acid 5~7, MTBE5~7, the parts by weight of paraffin 3~6；The phosphate of 0.2~1 part of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight of phosphoric acid sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5 0.9 parts by weight, the 2 of 0.5 0.9 parts by weight, 6 BHTs, the compound additive of 1.2~2 parts by weight, the temperature range of preparation is+20 DEG C~20 DEG C.
Description
Technical field
The invention discloses a kind of liquid fuel, specifically a kind of vehicle lead-free synthetic fuel.
Background technology
Conventional gasoline process technology is fractionated using the different boiling of heterogeneity in crude oil, fractionates out different productions
Product, such as：Natural gas, gasoline, diesel oil, heavy oil and pitch etc., or be catalyzed, cracking, the technique productions such as reformation require higher
Fuel oil, such as aviation kerosine.But conventionally produced out different boiling, the product oil of different proportion tend not to meet
The substantial amounts of demand in market simultaneously expends crude oil significantly, increases the cost of cost crude, therefore, gasoline is developed according to this market demand
Additive technology, it is added directly into product oil, generates the label gasoline of daily need, so as to reduces the usage amount of crude oil.
In addition, with the raising of people's environmental protection consciousness, vehicle emission pollution problem is increasingly taken seriously.Europe, the United States,
Japan and China in succession proposes this country new gasoline standard, its to sulfur content, benzene content, arene content, olefin(e) centent and
Oxygen content is proposed strict regulation and limitation.Because motor vehicle emission is one of atmosphere pollution main source, vehicular emission
Contaminant capacity to account for atmosphere pollution ratio in rising trend always, as China's automobile production amount and recoverable amount constantly increase, discharge
Regulation is increasingly strict, and society is to improving fuel oil quality, more and more high using the cry of clean fuel.
In order to further reduce the tail gas pollution brought due to incomplete combustion, people gradually make oxygen containing clean fuel
For the important directions of the research of fuel from now on, it is concentrated mainly on using alcohols and ethers and is used as gasoline addO-on therapy.Because of the methanol amount of being
The industrial chemicals being easy to get greatly, so, methanol turns into main research direction as the utilization of motor vehicle fuel, but a large amount of real
Verify bright：Methanol directly can not be used for automobile engine fuel instead of gasoline, because the lower boiling influence of methanol, directly
Have influence on the startup and acceleration of automobile.Therefore, it is often miscible using methanol and gasoline in the research of high-clean gasoline, and add
Associated additives.
Chinese patent 200410054960.2 discloses a kind of blended gasoline containing methanol, and its component includes：Naphtha,
Mixed xylenes, toluene, methanol, isopropanol, C9+ petroleum hydrocarbons, isopentane, methyl tertiary butyl ether(MTBE) or and tertbutyl ether.It is this
The shortcomings that blended gasoline, is, higher as the content of the naphtha of raw material using oil, is so reducing oil consumption, is reducing to oil
Dependence in terms of effect be not it is obvious that in addition, methyl tertiary butyl ether(MTBE) selected in component, because the characteristic of itself causes
It easily enters underground water through soil, and just has strong peculiar smell containing a small amount of methyl tertiary butyl ether(MTBE) in drinking water, if
Human body, which sucks a small amount of methyl tertiary butyl ether(MTBE), will produce stimulation nose and throat, cause headache, nausea and dizziness.So from
Methyl tertiary butyl ether(MTBE) is very undesirable as the environment protecting of blend component.
Further, since methanol gasoline is usually present immiscible, lamination in configuration, part evaporation when in use causes
Vapour lock makes engine operating intermittency occur, is short of power, and methanol and the mixing of other gasoline it is immiscible, layering etc. is existing
As, it is difficult to produce and promote on a large scale.
The purpose of the present invention is aiming at disadvantage mentioned above, there is provided a kind of methanol usage is big, and production cost is low, not stratified, property
Can be stable, octane number is high, no vapour lock, and the high-clean gasoline that can be used in mixed way with other conventional gasoline arbitrary proportions.
The content of the invention
The purpose of invention be to provide for it is a kind of based on regenerated resources, reduce atmosphere pollution, save national foreign exchange and disappear
Alcohol synthetic fuel consume, used ethanol to be prepared for primary raw material and preparation method thereof.
The object of the present invention is achieved like this, a kind of vehicle lead-free synthetic fuel, consists of the following composition：40~60 weights
Measure the methanol of part；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；The butane of 6.5~17 parts by weight；1~5 part of parts by weight
Aliphatic acid ammonium；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8-1.5 parts by weight；The weight of peracetic acid spy butyl ester 2~3
Measure part, the parts by weight of oleic acid 5~7, the parts by weight of MTBE5~7, the parts by weight of paraffin 3~6；The phosphate of 0.2~1 part of parts by weight；0.2
The vulcanization butylene of~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight of phosphoric acid sodium；The parts by weight of ethylene glycol 1,
The hydrogen peroxide of 0.5-0.9 parts by weight, the BHT of 0.5-0.9 parts by weight, 1.2~2 parts by weight it is compound
Additive, the temperature range of preparation are+20 DEG C~-20 DEG C, described compound additive, with the gross weight meter of compound additive,
It is made up of following components by proportioning：The complexing agent 0.5% of 15%~20% benzene-like compounds of multiple-effect energizer 30%~41%~
The higher alcohols 16%~19% of 24% ether compound, 8%~24% detergent-dispersant additive 0.7%~1.2%, its summation are 100%.
Described multiple-effect energizer is dimethoxymethane, cyclopentadiene tricarbonyl manganese, ferrocene, nitric acid lipoid substance
In two or more mixture.
Described benzene-like compounds are toluene, dimethylbenzene, any one in ortho-xylene or two kinds of mixtures.
Described complexing agent is the sub- bigcatkin willow propane diamine of N, N ' two, 4,4- methylene bis-phenols, dimeric dibasic acid, fatty acid ester, carbonic acid
Two or more mixture in fat.
Described ether compound is the mixture of isopropyl ether or methyl tertiary butyl ether(MTBE) or both.
Described detergent-dispersant additive is alkyl sodium salicylate, dichloroethanes, METHYLPYRROLIDONE, gasoline detergent point
Any two kinds of mixtures in powder, the alkyl in described alkyl sodium salicylate are methyl, ethyl, propyl group, appointing in butyl
Meaning is a kind of.
Described more charcoal alcohol are isopropyl acetone, n-butanol, isobutanol, two or more any mixture in acetone.
The preparation method for the synthetic fuel stated, step are as follows：
1st step, by weight, by fat methanol；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；6.5~17 weights
Measure the butane of part；The aliphatic acid ammonium of 1~5 part of parts by weight；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8-1.5 parts by weight；
The parts by weight of the parts by weight of peracetic acid spy butyl ester 2~3, the parts by weight of oleic acid 5~7, MTBE5~7, the parts by weight of paraffin 3~6；0.2~
The phosphate of 1 part of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight phosphorus
Sour sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5-0.9 parts by weight, the BHT of 0.5-0.9 parts by weight,
After well mixed, 30~40 DEG C of dissolvings are heated to, are stirred；
2nd step, following components are by proportioning：The complexing agent of 15%~20% benzene-like compounds of multiple-effect energizer 30%~41%
The higher alcohols 16%~19% of 0.5%~24% ether compound, 8%~24% detergent-dispersant additive 0.7%~1.2%, its summation are
100%, it is well mixed, is warming up to 40~50 DEG C, 1~3h is incubated under agitation, after letting cool, you can；The use of described additive
Amount is the 0.5%~1% of biodiesel weight；The material of the 1st step of mixed material and mediation is sufficiently mixed uniformly.
Institute's Pass through above-mentioned technical proposal of the present invention, because the main component in raw material employs reproducible methanol and second
Alcohol, and be incorporated a small amount of industrial chemicals, then synthesis is simply made by science, produced thing fuel after testing, its fuel value
1.1 ten thousand kilocalories are can reach, hydrocarbon and a discharge capacity aoxidized are extremely low, and calorific value is suitable with current gasoline, can directly apply
Used in existing automobile engine as power fuel, raw material needed for the present invention easily obtains, and manufacturing process is simple, has fabulous
Popularizing application prospect.
Using the present invention of as above technical scheme, had the advantages that relative to prior art：
1. the product belongs to universal high-cleanness fuel oil, do not need to adjust engine, can be random as regular gasoline
Use.I.e. operation is easy, easy to use.
2. explosive force is strong, octane number is high, the capability of antidetonance is good, so as to improve the power performance of engine.
3. energy-conserving and environment-protective, methanol oxygen content are up to 50%, promote full combustion of fuel complete, make motor vehicle exhaust emission has
Evil material reduces by 20 " --- -50%, atmosphere pollution can be reduced, is advantageous to energy-conserving and environment-protective.
4. good economy performance, methanol fuel are lower than oil-fired cost, the alternative 1 ton of common gasoline product of 1.5 tons of methanol,
Its efficiency ratio improves about 5-8 times using coal, than reducing 20-----'50% using the cost of regular gasoline.
5. the raw material used are mostly cheap twice laid, very objective with waste becoming treasure, economic benefit！
6. intersolubility is good, capability and performance is stable, holding time length, is adapted to long-distance transport.
Embodiment
It is as follows for the more detailed elaboration present invention, the one embodiment of the invention：
Embodiment 1
A kind of vehicle lead-free synthetic fuel, is consisted of the following composition：The methanol of 60 parts by weight；The fatty alcohol of 30 parts of parts by weight
Polyethenoxy ether；The butane of 17 parts by weight；The aliphatic acid ammonium of 5 parts of parts by weight；The barium sulfonate of 1 parts by weight；The stabilization of 1.5 parts by weight
Agent；The parts by weight of peracetic acid spy butyl ester 3, the parts by weight of oleic acid 7, MTBE7 parts by weight, the parts by weight of paraffin 6；The phosphorus of 1 part of parts by weight
Acid esters；The vulcanization butylene of 1 parts by weight；The methyl-silicone oil of 2 parts by weight；5 parts by weight of phosphoric acid sodium；The parts by weight of ethylene glycol 1,0.9 weight
The hydrogen peroxide of part, the BHT of 0.9 parts by weight, the compound additive of 2 parts by weight, the temperature range of preparation
For+20 DEG C~-20 DEG C, described compound additive, with the gross weight meter of compound additive, it is made up of following components by proportioning：
The ether compound 8%~24% of 15%~20% benzene-like compounds of multiple-effect energizer, 30%~41% complexing agent 0.5%~24%
The higher alcohols 16%~19% of detergent-dispersant additive 0.7%~1.2%, its summation are 100%.
Described multiple-effect energizer is dimethoxymethane, cyclopentadiene tricarbonyl manganese, ferrocene, nitric acid lipoid substance
In two or more mixture.
Described benzene-like compounds are toluene, dimethylbenzene, any one in ortho-xylene or two kinds of mixtures.
Described complexing agent is the sub- bigcatkin willow propane diamine of N, N ' two, 4,4- methylene bis-phenols, dimeric dibasic acid, fatty acid ester, carbonic acid
Two or more mixture in fat.
Described ether compound is the mixture of isopropyl ether or methyl tertiary butyl ether(MTBE) or both.
Described detergent-dispersant additive is alkyl sodium salicylate, dichloroethanes, METHYLPYRROLIDONE, gasoline detergent point
Any two kinds of mixtures in powder, the alkyl in described alkyl sodium salicylate are methyl, ethyl, propyl group, appointing in butyl
Meaning is a kind of.
Described more charcoal alcohol are isopropyl acetone, n-butanol, isobutanol, two or more any mixture in acetone.
The preparation method for the synthetic fuel stated, step are as follows：
1st step, by weight, by fat methanol；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；6.5~17 weights
Measure the butane of part；The aliphatic acid ammonium of 1~5 part of parts by weight；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8-1.5 parts by weight；
The parts by weight of the parts by weight of peracetic acid spy butyl ester 2~3, the parts by weight of oleic acid 5~7, MTBE5~7, the parts by weight of paraffin 3~6；0.2~
The phosphate of 1 part of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight phosphorus
Sour sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5-0.9 parts by weight, the BHT of 0.5-0.9 parts by weight,
After well mixed, 30~40 DEG C of dissolvings are heated to, are stirred；
2nd step, following components are by proportioning：The complexing agent of 15%~20% benzene-like compounds of multiple-effect energizer 30%~41%
The higher alcohols 16%~19% of 0.5%~24% ether compound, 8%~24% detergent-dispersant additive 0.7%~1.2%, its summation are
100%, it is well mixed, is warming up to 40~50 DEG C, 1~3h is incubated under agitation, after letting cool, you can；The use of described additive
Amount is the 0.5%~1% of biodiesel weight；The material of the 1st step of mixed material and mediation is sufficiently mixed uniformly.
Embodiment 2
A kind of vehicle lead-free synthetic fuel, is consisted of the following composition：The methanol of 40 parts by weight；The fatty alcohol of 10 parts of parts by weight
Polyethenoxy ether；6.5 the butane of parts by weight；The aliphatic acid ammonium of 1 part of parts by weight；The barium sulfonate of 0.2 parts by weight；0.8 parts by weight
Stabilizer；The parts by weight of peracetic acid spy butyl ester 2, the parts by weight of oleic acid 5, MTBE5 parts by weight, the parts by weight of paraffin 3；0.2 part of weight
The phosphate of part；The vulcanization butylene of 0.2 parts by weight；The methyl-silicone oil of 1.2 parts by weight；1 parts by weight of phosphoric acid sodium；The weight of ethylene glycol 1
Part, the hydrogen peroxide of 0.5 parts by weight, the BHT of 0.5 parts by weight, the compound additive of 1.2 parts by weight, match somebody with somebody
The temperature range of system is+20 DEG C~-20 DEG C, described compound additive, with the gross weight meter of compound additive, by following components
Formed by proportioning：The ethers chemical combination of 15%~20% benzene-like compounds of multiple-effect energizer, 30%~41% complexing agent 0.5%~24%
The higher alcohols 16%~19% of 8%~24% detergent-dispersant additive of thing 0.7%~1.2%, its summation are 100%.
Described multiple-effect energizer is dimethoxymethane, cyclopentadiene tricarbonyl manganese, ferrocene, nitric acid lipoid substance
In two or more mixture.
Described benzene-like compounds are toluene, dimethylbenzene, any one in ortho-xylene or two kinds of mixtures.
Described complexing agent is the sub- bigcatkin willow propane diamine of N, N ' two, 4,4- methylene bis-phenols, dimeric dibasic acid, fatty acid ester, carbonic acid
Two or more mixture in fat.
Described ether compound is the mixture of isopropyl ether or methyl tertiary butyl ether(MTBE) or both.
Described detergent-dispersant additive is alkyl sodium salicylate, dichloroethanes, METHYLPYRROLIDONE, gasoline detergent point
Any two kinds of mixtures in powder, the alkyl in described alkyl sodium salicylate are methyl, ethyl, propyl group, appointing in butyl
Meaning is a kind of.
Described more charcoal alcohol are isopropyl acetone, n-butanol, isobutanol, two or more any mixture in acetone.
The preparation method for the synthetic fuel stated, step are as follows：
1st step, by weight, by fat methanol；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；6.5~17 weights
Measure the butane of part；The aliphatic acid ammonium of 1~5 part of parts by weight；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8-1.5 parts by weight；
The parts by weight of the parts by weight of peracetic acid spy butyl ester 2~3, the parts by weight of oleic acid 5~7, MTBE5~7, the parts by weight of paraffin 3~6；0.2~
The phosphate of 1 part of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight phosphorus
Sour sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5-0.9 parts by weight, the BHT of 0.5-0.9 parts by weight,
After well mixed, 30~40 DEG C of dissolvings are heated to, are stirred；
2nd step, following components are by proportioning：The complexing agent of 15%~20% benzene-like compounds of multiple-effect energizer 30%~41%
The higher alcohols 16%~19% of 0.5%~24% ether compound, 8%~24% detergent-dispersant additive 0.7%~1.2%, its summation are
100%, it is well mixed, is warming up to 40~50 DEG C, 1~3h is incubated under agitation, after letting cool, you can；The use of described additive
Amount is the 0.5%~1% of biodiesel weight；The material of the 1st step of mixed material and mediation is sufficiently mixed uniformly.
The product high-performance clean methanol gasoline of the present invention, raw material are easy to get, and wide material sources, cost is low, and oxygen content is high, calorific value
Height, octane number is high, can fully meet the power demand of automobile, by the high-performance clean methanol vapour of the above-mentioned several embodiments of the present invention
Oil is used as vehicle fuel, can reach the unleaded petrochemical industry gasoline requirements of more than 93#, and compared with gasoline, power improves 8%~12%,
Oil consumption save 3~5%, due to can fully burn, not coking, exhaust emissions carbon monoxide, nitrogen oxides, hydrocarbon compare vapour
Oil reduces 30%~90%, meets environmental requirement.The high-performance methanol gasoline of the present invention not only can be independent as vehicle fuel
Use, can also be used in mixed way, not limited by ratio with gasoline, and using when be not required to refiting engine.
Claims (8)
1. a kind of vehicle lead-free synthetic fuel, is consisted of the following composition：The methanol of 40~60 parts by weight；10~30 parts of parts by weight
Fatty alcohol polyoxypropylene ether；The butane of 6.5~17 parts by weight；The aliphatic acid ammonium of 1~5 part of parts by weight；The sulphur of 0.2~1 parts by weight
Sour barium；The stabilizer of 0.8-1.5 parts by weight；The parts by weight of peracetic acid spy butyl ester 2~3, the parts by weight of oleic acid 5~7, MTBE5~7
Parts by weight, the parts by weight of paraffin 3~6；The phosphate of 0.2~1 part of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；1.2~2 weights
Measure the methyl-silicone oil of part；1~5 parts by weight of phosphoric acid sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5-0.9 parts by weight, 0.5-0.9
The BHT of parts by weight, the compound additive of 1.2~2 parts by weight, the temperature range of preparation for+20 DEG C~-
20 DEG C, described compound additive, with the gross weight meter of compound additive, it is made up of following components by proportioning：Multiple-effect energizer
The detergent-dispersant additive of 15%~20% benzene-like compounds, 30%~41% complexing agent, 0.5%~24% ether compound 8%~24%
0.7%~1.2% higher alcohols 16%~19%, its summation are 100%.
2. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described multiple-effect energizer is dimethoxy
Methylmethane, cyclopentadiene tricarbonyl manganese, ferrocene, two or more mixture in nitric acid lipoid substance.
3. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described benzene-like compounds are toluene,
Dimethylbenzene, any one in ortho-xylene or two kinds of mixtures.
4. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described complexing agent is the sub- water of N, N ' two
Raise propane diamine, 4,4- methylene bis-phenols, dimeric dibasic acid, fatty acid ester, two or more mixture in carbonic ether.
5. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described ether compound is isopropyl ether
Or the mixture of methyl tertiary butyl ether(MTBE) or both.
6. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described detergent-dispersant additive is alkyl water
Poplar acid calcium, dichloroethanes, METHYLPYRROLIDONE, any two kinds of mixtures in cleaning dispersant for gasoline, described alkyl
Alkyl in calcium salicylate is methyl, ethyl, propyl group, any one in butyl.
7. vehicle lead-free synthetic fuel according to claim 1, it is characterised in that described more charcoal alcohol are isopropyl acetone, positive fourth
Alcohol, isobutanol, two or more any mixture in acetone.
8. the preparation method of the synthetic fuel described in claim 1, it is characterised in that step is as follows：
1st step, by weight, by fat methanol；The fatty alcohol polyoxypropylene ether of 10~30 parts of parts by weight；6.5~17 parts by weight
Butane；The aliphatic acid ammonium of 1~5 part of parts by weight；The barium sulfonate of 0.2~1 parts by weight；The stabilizer of 0.8-1.5 parts by weight；Peroxide
Change the parts by weight of tebutate 2~3 parts by weight, the parts by weight of oleic acid 5~7, MTBE5~7, the parts by weight of paraffin 3~6；0.2~1 part
The phosphate of parts by weight；The vulcanization butylene of 0.2~1 parts by weight；The methyl-silicone oil of 1.2~2 parts by weight；1~5 parts by weight of phosphoric acid
Sodium；The parts by weight of ethylene glycol 1, the hydrogen peroxide of 0.5-0.9 parts by weight, the BHT of 0.5-0.9 parts by weight, mix
After closing uniformly, 30~40 DEG C of dissolvings are heated to, are stirred；
2nd step, following components are by proportioning：The complexing agent 0.5% of 15%~20% benzene-like compounds of multiple-effect energizer 30%~41%
The higher alcohols 16%~19% of 8%~24% detergent-dispersant additive of~24% ether compound 0.7%~1.2%, its summation are
100%, it is well mixed, is warming up to 40~50 DEG C, 1~3h is incubated under agitation, after letting cool, you can；The use of described additive
Amount is the 0.5%~1% of biodiesel weight；The material of the 1st step of mixed material and mediation is sufficiently mixed uniformly.
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| CN109609216A (en) * | 2019-01-04 | 2019-04-12 | 顺德职业技术学院 | A kind of additive and manufacturing method granular material discharged for reducing diesel motor exhaust |
| CN109609215A (en) * | 2019-01-04 | 2019-04-12 | 顺德职业技术学院 | A kind of diesel motor exhaust purification additive and manufacturing method |
| CN111732978A (en) * | 2020-06-02 | 2020-10-02 | 上海中太行之光能源有限公司 | Liquid nano combustion material and preparation method thereof |
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