CN107602654A - A kind of tree peony saponin reparation technology - Google Patents
A kind of tree peony saponin reparation technology Download PDFInfo
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- CN107602654A CN107602654A CN201710746115.9A CN201710746115A CN107602654A CN 107602654 A CN107602654 A CN 107602654A CN 201710746115 A CN201710746115 A CN 201710746115A CN 107602654 A CN107602654 A CN 107602654A
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- saponin
- filtrate
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- tree peony
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Abstract
The present invention relates to peony seeds agricultural byproducts processing field, specifically a kind of tree peony saponin reparation technology, it is comprised the following steps that：(1) soak；(2) lime is added；(3) moisture is adjusted；(4) grind；(5) boil；(6) filter；(7) multiple times of filtration；(8) stand；(9) reclaim；(10) alum is added；(11) secondary filter；(12) decolourize；(13) ethanol is added；(14) refuel；(15) distill；(16) dry, relative to traditional water seaoning, first grind to boil again and possess recovery rate height, the characteristics of low is lost；Filter repeatedly for three times, the tree peony saponin in filter residue is fully extracted, remaining filter residue is natural organic feed and fertilizer, is extended；Use ball milling miniaturization make it that peony seeds dregs of rice powder is uniformly tiny, be easy to following process；Edible oil is added, is prevented to being injured caused by saponin during distillation, while be easy to separate out the post-production of saponin and saponin；Unsaturated fat salt can be removed by adding lime.
Description
Technical field
The present invention relates to peony seeds agricultural byproducts processing field, specifically a kind of tree peony saponin reparation technology.
Background technology
Tree peony saponin belongs to three glucoside terpene saponins, is a kind of natural surfactant, have efficient emulsification, it is scattered,
Wetting etc. surface-active, purposes is quite varied, can directly exported European ＆ American Market as Organic Chemicals, can also be killed as agricultural chemicals
Dead insect in itself, has cheap, widely used advantage without damage crops.
All it is at present to extract tree peony saponin using water seaoning, this method recovery rate is low, and loss is high, it is therefore desirable to a kind of
New method improves recovery rate.
The content of the invention
In order to solve the above problems, the present invention proposes a kind of tree peony saponin reparation technology.
A kind of tree peony saponin reparation technology, it is comprised the following steps that：
(1) soak：The peony seeds dregs of rice are placed in water immersion 12-24 hours；
(2) lime is added：Lime is added while immersion, water temperature is controlled at 15-20 DEG C；
(3) moisture is adjusted：The ventilation of the peony seeds dregs of rice is dried, by water tariff collection 20%；
(4) grind：The peony seeds dregs of rice are crushed repeatedly using mechanical force, wear into 1 mm in size；
(5) boil：Peony seeds dregs of rice powder is placed in boiling water and boils half an hour, is stirred simultaneously；
(6) filter：80 DEG C are cooled to after boiling, is incubated one hour so that ion isolation；It is filtrated to get filtrate and residue；
(7) multiple times of filtration：Residue is placed in boiling water and boils and stirs, residue is collected, filters and go repeatedly for three times residue,
Filtrate three times is merged, and boiled, is concentrated into former filtrate 1/3rd；
(8) stand：At 26-33 DEG C, by filtrate add 200-300 milliliter yeast, and stand a few hours etc. it is to be precipitated and
Float；
(9) reclaim：Using centrifugal process, the nutritional ingredients such as the protein in filter residue are reclaimed, and surveys shallow lake agent using saponin and picks
Except soluble impurities such as inorganic salts；
(10) alum is added：Filtrate adds 0.5-1 grams of alum, stirs and heats, staticly settles；
(11) secondary filter：Filter again, filter residue is reclaimed；
(12) decolourize：Add activated carbon to decolourize to filtrate, clear filtrate is obtained after filtering；
(13) ethanol is added：Filtrate is heated again, and adds ethanol；
(14) refuel：Proper amount of edible oil is added in the solution for adding ethanol；
(15) distill：By filtrate continuous heating, until filtrate crystallisation, separates out tree peony saponin, is thick shape；
(16) dry：Tree peony saponin is placed in thermostatic drying chamber and dried.
Time of repose is to be advisable 4-5 hours during described (8) are stood.
Described tree peony saponin is the amorphous substance of light beige.
The beneficial effects of the invention are as follows：Relative to traditional water seaoning, first grind to boil again and possess recovery rate height, be lost low
Feature；Filter repeatedly for three times, the tree peony saponin in filter residue is fully extracted, remaining filter residue is natural organic feed and fertilizer
Material, extend；Use ball milling miniaturization make it that peony seeds dregs of rice powder is uniformly tiny, be easy to following process；Edible oil is added, prevents from steaming
To injury caused by saponin when evaporating, while it is easy to separate out the post-production of saponin and saponin；Adding lime can be by unsaturated fat
Salt removes.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, below it is right
The present invention is expanded on further.
Embodiment：
A kind of tree peony saponin reparation technology, it is comprised the following steps that：
(1) soak：The peony seeds dregs of rice are placed in water immersion 12-24 hours；
(2) lime is added：Lime is added while immersion, water temperature is controlled at 15-20 DEG C；
(3) moisture is adjusted：The ventilation of the peony seeds dregs of rice is dried, by water tariff collection 20%；
(4) grind：The peony seeds dregs of rice are crushed repeatedly using mechanical force, wear into 1 mm in size；
(5) boil：Peony seeds dregs of rice powder is placed in boiling water and boils half an hour, is stirred simultaneously；
(6) filter：80 DEG C are cooled to after boiling, is incubated one hour so that ion isolation；It is filtrated to get filtrate and residue；
(7) multiple times of filtration：Residue is placed in boiling water and boils and stirs, residue is collected, filters and go repeatedly for three times residue,
Filtrate three times is merged, and boiled, is concentrated into former filtrate 1/3rd；
(8) stand：At 26-33 DEG C, by filtrate add 200-300 milliliter yeast, and stand a few hours etc. it is to be precipitated and
Float；
(9) reclaim：Using centrifugal process, the nutritional ingredients such as the protein in filter residue are reclaimed, and surveys shallow lake agent using saponin and picks
Except soluble impurities such as inorganic salts；
(10) alum is added：Filtrate adds 0.5-1 grams of alum, stirs and heats, staticly settles；
(11) secondary filter：Filter again, filter residue is reclaimed；
(12) decolourize：Add activated carbon to decolourize to filtrate, clear filtrate is obtained after filtering；
(13) ethanol is added：Filtrate is heated again, and adds ethanol；
(14) refuel：Proper amount of edible oil is added in the solution for adding ethanol；
(15) distill：By filtrate continuous heating, until filtrate crystallisation, separates out tree peony saponin, is thick shape；
(16) dry：Tree peony saponin is placed in thermostatic drying chamber and dried.
Time of repose is to be advisable 4-5 hours during described (8) are stood.
Described tree peony saponin is the amorphous substance of light beige.
Relative to traditional water seaoning, first grind to boil again and possess recovery rate height, the characteristics of low is lost.
Filter repeatedly for three times, the tree peony saponin in filter residue fully extracted, remaining filter residue be natural organic feed and
Fertilizer.
Use ball milling miniaturization make it that peony seeds dregs of rice powder is uniformly tiny, be easy to following process.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
For personnel it should be appreciated that the present invention is not limited to the above embodiments, that described in above-described embodiment and specification is the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these change and
Improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claims and its equivalent
Thing defines.
Claims (3)
- A kind of 1. tree peony saponin reparation technology, it is characterised in that：It is comprised the following steps that：(1) soak：The peony seeds dregs of rice are placed in water immersion 12-24 hours；(2) lime is added：Lime is added while immersion, water temperature is controlled at 15-20 DEG C；(3) moisture is adjusted：The ventilation of the peony seeds dregs of rice is dried, by water tariff collection 20%；(4) grind：The peony seeds dregs of rice are crushed repeatedly using mechanical force, wear into 1 mm in size；(5) boil：Peony seeds dregs of rice powder is placed in boiling water and boils half an hour, is stirred simultaneously；(6) filter：80 DEG C are cooled to after boiling, is incubated one hour so that ion isolation；It is filtrated to get filtrate and residue；(7) multiple times of filtration：Residue is placed in boiling water and boils and stirs, residue is collected, residue is filtered and go repeatedly for three times, by three Secondary filtrate merges, and boils, and is concentrated into former filtrate 1/3rd；(8) stand：At 26-33 DEG C, filtrate is added into 200-300 milliliter yeast, and it is to be precipitated and float to stand a few hours etc. Thing；(9) reclaim：Using centrifugal process, the nutritional ingredients such as the protein in filter residue are reclaimed, and surveys shallow lake agent using saponin and rejects nothing The soluble impurities such as machine salt；(10) alum is added：Filtrate adds 0.5-1 grams of alum, stirs and heats, staticly settles；(11) secondary filter：Filter again, filter residue is reclaimed；(12) decolourize：Add activated carbon to decolourize to filtrate, clear filtrate is obtained after filtering；(13) ethanol is added：Filtrate is heated again, and adds ethanol；(14) refuel：Proper amount of edible oil is added in the solution for adding ethanol；(15) distill：By filtrate continuous heating, until filtrate crystallisation, separates out tree peony saponin, is thick shape；(16) dry：Tree peony saponin is placed in thermostatic drying chamber and dried.
- A kind of 2. tree peony saponin reparation technology according to claim 1, it is characterised in that：Stood in described step (8) Time is to be advisable 4-5 hours.
- A kind of 3. tree peony saponin reparation technology according to claim 1, it is characterised in that：Described tree peony saponin is shallow rice The amorphous substance of yellow.
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| CN201710746115.9A CN107602654A (en) | 2017-08-26 | 2017-08-26 | A kind of tree peony saponin reparation technology |
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| CN201710746115.9A CN107602654A (en) | 2017-08-26 | 2017-08-26 | A kind of tree peony saponin reparation technology |
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| CN103087128A (en) * | 2013-02-05 | 2013-05-08 | 菏泽尧舜牡丹生物科技有限公司 | Method for extracting paeoniflorin from peony seed meal |
| CN103045372B (en) * | 2012-12-20 | 2014-04-23 | 菏泽瑞璞牡丹产业科技发展有限公司 | Comprehensive utilization method of peony meal |
| CN103988955A (en) * | 2014-04-09 | 2014-08-20 | 洛阳春魁农业开发有限公司 | Method for preparing scorched aroma peony tea by using peony seed meal |
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| CN104844683A (en) * | 2015-04-15 | 2015-08-19 | 芜湖市丹洋现代农业科技发展有限公司 | Method for extracting peony saponin from peony seed meal |
| CN105532231A (en) * | 2015-12-23 | 2016-05-04 | 李�杰 | Production method and application for selenium-rich peony |
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2017
- 2017-08-26 CN CN201710746115.9A patent/CN107602654A/en active Pending
Patent Citations (6)
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| CN103045372B (en) * | 2012-12-20 | 2014-04-23 | 菏泽瑞璞牡丹产业科技发展有限公司 | Comprehensive utilization method of peony meal |
| CN103087128A (en) * | 2013-02-05 | 2013-05-08 | 菏泽尧舜牡丹生物科技有限公司 | Method for extracting paeoniflorin from peony seed meal |
| CN103988955A (en) * | 2014-04-09 | 2014-08-20 | 洛阳春魁农业开发有限公司 | Method for preparing scorched aroma peony tea by using peony seed meal |
| CN104000196A (en) * | 2014-06-04 | 2014-08-27 | 李�杰 | Compound peony seed oil preparation, and making method and application thereof |
| CN104844683A (en) * | 2015-04-15 | 2015-08-19 | 芜湖市丹洋现代农业科技发展有限公司 | Method for extracting peony saponin from peony seed meal |
| CN105532231A (en) * | 2015-12-23 | 2016-05-04 | 李�杰 | Production method and application for selenium-rich peony |
Non-Patent Citations (7)
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| 刘普等: "紫斑牡丹籽饼粕低聚芪类成分研究", 《中国药学杂志》 * |
| 卢宗元: "牡丹花及牡丹籽饼粕化学成分研究", 《中国优秀硕士学位论文全文数据库（医药卫生科技辑）》 * |
| 史瑞雨等: "牡丹籽油提取技术研究进展", 《内蒙古科技与经济》 * |
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