CN107602103A - A kind of Chinese jade porcelain material prescription and manufacture craft - Google Patents

A kind of Chinese jade porcelain material prescription and manufacture craft Download PDF

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Publication number
CN107602103A
CN107602103A CN201710785591.1A CN201710785591A CN107602103A CN 107602103 A CN107602103 A CN 107602103A CN 201710785591 A CN201710785591 A CN 201710785591A CN 107602103 A CN107602103 A CN 107602103A
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China
Prior art keywords
raw material
mud
sand
porcelain
potassium sodium
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CN201710785591.1A
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Chinese (zh)
Inventor
帅建
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Liling Xiang Hao Ceramic Technology Co Ltd
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Liling Xiang Hao Ceramic Technology Co Ltd
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Priority to CN201710785591.1A priority Critical patent/CN107602103A/en
Publication of CN107602103A publication Critical patent/CN107602103A/en
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Abstract

The invention discloses a kind of Chinese jade porcelain material prescription and its manufacture craft, including raw material:Quartz sand 22%, potassium sodium sand 32%, Datong District's soil 18%, wash mud 28%;By raw material, ball milling is into product mud in ball mill, then successively by sieving, pugging, base, repaired biscuit, the technological forming such as low-firing;Its raw material 54% caused ettle in washup; by being reused to the tailings in washup; 22% quartz sand in tailings and 32% potassium sodium sand are used as porcelain raw material; material property is stable; effectively solves the problems, such as the waste discharge of washup company; solve porcelain thermal stability problems during firing ceramics, and not desulphurization, environmental protection, steady quality, effectively reduce cost.

Description

A kind of Chinese jade porcelain material prescription and manufacture craft
Technical field
The present invention relates to porcelain preparing technical field, specially a kind of Chinese jade porcelain material prescription and manufacture craft.
Background technology
In existing porcelain preparation process, magnesia porcelain sintering procedure desulphurization more than 1%, and thermal stability is bad, after finished product Phase is easy to crack.And imitative china is high to quality requirements of raw materials, what existing imitative china raw material used is all that new ore deposit is native, quality It is unstable, price is high, not environmentally, all cost height be present using new ore deposit, efficiency is low, the problems such as time-consuming.And present mineral products Resource is nervous, and mining environment is destroyed greatly, and many washup companies tailings can not reuse, and pollutes environment, threatens people property people Raw safety.
The content of the invention
It is an object of the invention to provide a kind of Chinese jade porcelain material prescription and manufacture craft, tailings 54% can be utilized to have Effect solves the problems, such as the waste discharge of washup company, solves porcelain thermal stability problems, but also not desulphurization, guarantor during firing ceramics Retaining ring border, steady quality, cost is effectively reduced, to solve the problems mentioned in the above background technology.
To achieve the above object, the present invention provides following technical scheme:A kind of Chinese jade porcelain material prescription, including following matter Measure the raw material of fraction proportioning:Quartz sand 21-23%, potassium sodium sand 31-33%, Datong District soil 17-19%, wash mud 27-29%.
Preferably, the raw material quartz sand and potassium sodium sand account for both from the recycling to the tailings in washup, tailings The 54% of raw material total amount.
Preferably, including raw material:Quartz sand 21%, potassium sodium sand 33%, Datong District's soil 17%, wash mud 29%.
Preferably, including raw material:Quartz sand 23%, potassium sodium sand 31%, Datong District's soil 19%, wash mud 27%.
Preferably, including raw material:Quartz sand 22%, potassium sodium sand 32%, Datong District's soil 18%, wash mud 28%.
The present invention provides another technical solution:A kind of manufacture craft of Chinese jade porcelain, comprises the following steps:
S1:Selected raw material, removal of impurities;
S2:The raw material for standby of above-mentioned mass fraction proportioning is weighed successively;
S3:By quartz sand, potassium sodium sand, Datong District's soil, wash mud and be added in proportion in ball mill, and press total raw material:Ballstone:Water=1: 2:0.5 ratio addition water, 12 hours of mixing and ball milling, is made product mud;
S4:By product mud 325 mesh of sieving, iron removaling to less than 0.2, squeeze to aqueous 22%;
S5:Mud after S4 is handled is added on vacuum deairing machine and carries out vacuum pugging twice;
S6:Pugging after S5 is handled is placed on Blank drawing machine carries out throwing shaping, and repaired biscuit by porcelain model;
S7:By after the body drying trimmed at 800-850 DEG C, low temperature biscuiting in the CO gases containing 3-5%, and biscuit is beaten Ground smooth;
S8:To biscuit glazing, then by 1240-1280 DEG C, in the CO gases containing 6-8% low-firing be molded, obtain porcelain into Product.
Preferably, the Contents of Main Components of manufactured product mud has silica 65%, alchlor 22%, three in the S3 Iron oxide 0.19%, calcium oxide 0.27%, magnesia 0.29%, potassium oxide 0.93%, sodium oxide molybdena 3.5%, titanium dioxide 0.12%, burning subtract Amount 7%.
Preferably, low temperature biscuiting temperature is 800 DEG C -820 DEG C in the S7, and CO content is 4%.
Preferably, it is 1240-1260 DEG C to the firing temperature of biscuit in the S8, CO content is 7%.
Compared with prior art, the beneficial effects of the invention are as follows:
This Chinese jade porcelain material prescription and its manufacture craft, by being reused to the tailings in washup, by 22% in tailings Quartz sand and 32% potassium sodium sand are used as porcelain raw material, and material property is stable, effectively solves the problems, such as the waste discharge of washup company, solve Porcelain thermal stability problems during firing ceramics of having determined, but also not desulphurization, environmental protection, steady quality, are effectively reduced Cost.
Embodiment
The embodiment of the present invention is will be detailed below, however, the embodiment of the present invention is not limited thereto.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, Belong to the scope of protection of the invention.
In the embodiment of the present invention:A kind of Chinese jade porcelain material prescription, include the raw material of following mass fraction proportioning:Quartz sand 21-23%, potassium sodium sand 31-33%, Datong District soil 17-19%, wash mud 27-29%;Wherein, raw material quartz sand and potassium sodium sand are both from right The recycling of tailings in washup, low cost materials, stable performance are reduced by making full use of tailings rational proportion, tailings accounts for The 54% of raw material total amount.
Embodiment one:
Take raw material:Quartz sand 21%, potassium sodium sand 33%, Datong District's soil 17%, wash mud 29%.
Matched based on above-mentioned raw materials, there is provided a kind of manufacture craft of Chinese jade porcelain, comprise the following steps:
The first step:Selected raw material, removal of impurities;
Second step:Quartz sand 21% is weighed successively, potassium sodium sand 33%, Datong District's soil 17%, it is standby to wash mud 29%;
3rd step:By quartz sand, potassium sodium sand, Datong District's soil, wash mud and be added in proportion in ball mill, and press total raw material:Ballstone:Water =1:2:0.5 ratio addition water, 12 hours of mixing and ball milling, is made product mud;The Contents of Main Components of product mud reaches titanium dioxide Silicon 60%, alchlor 20%, ferric oxide 0.10%, calcium oxide 0.25%, magnesia 0.20%, potassium oxide 0.90%, sodium oxide molybdena 3.5%th, titanium dioxide 0.1%, burning decrement 5%;
4th step:By product mud 325 mesh of sieving, iron removaling to less than 0.2, squeeze to aqueous 22%;
5th step:Mud after step 4 is handled is added on vacuum deairing machine and carries out vacuum pugging twice;
6th step:Pugging after step 5 is handled is placed on Blank drawing machine carries out throwing shaping, and repaired biscuit by porcelain model;
7th step:By after the body drying trimmed at 800-850 DEG C, low temperature biscuiting in the CO gases containing 3-5%, and by biscuiting Base polishes smooth;Low temperature biscuiting actual temp is 800 DEG C -820 DEG C, and CO content is 4%;
8th step:To biscuit glazing, then by 1240-1280 DEG C, low-firing is molded in the CO gases containing 6-8%, obtains porcelain Finished product;At 1240-1260 DEG C, CO content is 7% for actual temp control.
Embodiment two:
Take raw material:Quartz sand 23%, potassium sodium sand 31%, Datong District's soil 19%, wash mud 27%.
Being matched based on above-mentioned raw materials, there is provided a kind of manufacture craft of Chinese jade porcelain, its making step is identical with embodiment one, Burdensome elaboration is not made herein;Its in the third step obtained product mud Contents of Main Components up to silica 66%, alchlor 24%th, ferric oxide 0.3%, calcium oxide 0.3%, magnesia 0.3%, potassium oxide 0.95%, sodium oxide molybdena 1.7%, titanium dioxide 0.15%, Burn decrement 7.5%.
Embodiment three:
Take raw material:Quartz sand 22%, potassium sodium sand 32%, Datong District's soil 18%, wash mud 28%.
Matched based on above-mentioned raw materials, there is provided a kind of manufacture craft of Chinese jade porcelain, its making step and embodiment one, two-phase Together, burdensome elaboration is not made herein;Its in the third step obtained product mud Contents of Main Components up to silica 65%, three oxygen Change aluminium 22%, ferric oxide 0.19%, calcium oxide 0.27%, magnesia 0.29%, potassium oxide 0.93%, sodium oxide molybdena 3.5%, titanium dioxide 0.12%th, decrement 7% is burnt.
Comparative example one, two, three, it can be obtained from the composition of the product mud of preparation, the finished product cement content in embodiment three is most To approach existing porcelain composition, therefore material content quartz sand 22%, potassium sodium sand 32%, Datong District's soil 18%, it is porcelain material to wash mud 28% The optimum proportioning of material formula.
In summary:This Chinese jade porcelain material prescription and its manufacture craft, will by being reused to the tailings in washup 22% quartz sand and 32% potassium sodium sand in tailings are used as porcelain raw material, and material property is stable, effective to solve washup public affairs Waste discharge problem is taken charge of, solves porcelain thermal stability problems during firing ceramics, but also not desulphurization, environmental protection, quality are steady It is fixed, effectively reduce cost.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (9)

1. a kind of Chinese jade porcelain material prescription, it is characterised in that include the raw material of following mass fraction proportioning:Quartz sand 21- 23%, potassium sodium sand 31-33%, Datong District soil 17-19%, wash mud 27-29%.
2. a kind of Chinese jade porcelain material prescription according to claim 1, it is characterised in that the raw material quartz sand and potassium sodium For sand both from the recycling to the tailings in washup, tailings accounts for the 54% of raw material total amount.
3. a kind of Chinese jade porcelain material prescription according to claim 1, it is characterised in that including raw material:Quartz sand 21%, Potassium sodium sand 33%, Datong District's soil 17%, wash mud 29%.
4. a kind of Chinese jade porcelain material prescription according to claim 1, it is characterised in that including raw material:Quartz sand 23%, Potassium sodium sand 31%, Datong District's soil 19%, wash mud 27%.
5. a kind of Chinese jade porcelain material prescription according to claim 1, it is characterised in that including raw material:Quartz sand 22%, Potassium sodium sand 32%, Datong District's soil 18%, wash mud 28%.
6. a kind of manufacture craft of Chinese jade porcelain according to claim 1, it is characterised in that comprise the following steps:
S1:Selected raw material, removal of impurities;
S2:The raw material for standby of above-mentioned mass fraction proportioning is weighed successively;
S3:By quartz sand, potassium sodium sand, Datong District's soil, wash mud and be added in proportion in ball mill, and press total raw material:Ballstone:Water=1: 2:0.5 ratio addition water, 12 hours of mixing and ball milling, is made product mud;
S4:By product mud 325 mesh of sieving, iron removaling to less than 0.2, squeeze to aqueous 22%;
S5:Mud after S4 is handled is added on vacuum deairing machine and carries out vacuum pugging twice;
S6:Pugging after S5 is handled is placed on Blank drawing machine carries out throwing shaping, and repaired biscuit by porcelain model;
S7:By after the body drying trimmed at 800-850 DEG C, low temperature biscuiting in the CO gases containing 3-5%, and biscuit is beaten Ground smooth;
S8:To biscuit glazing, then by 1240-1280 DEG C, in the CO gases containing 6-8% low-firing be molded, obtain porcelain into Product.
A kind of 7. manufacture craft of Chinese jade porcelain according to claim 6, it is characterised in that manufactured finished product in the S3 The Contents of Main Components of mud has silica 65%, alchlor 22%, ferric oxide 0.19%, calcium oxide 0.27%, magnesia 0.29%th, potassium oxide 0.93%, sodium oxide molybdena 3.5%, titanium dioxide 0.12%, burning decrement 7%.
A kind of 8. manufacture craft of Chinese jade porcelain according to claim 6, it is characterised in that low temperature biscuiting temperature in the S7 Spend for 800 DEG C -820 DEG C, CO content is 4%.
9. the manufacture craft of a kind of Chinese jade porcelain according to claim 6, it is characterised in that to biscuit in the S8 Firing temperature is 1240-1260 DEG C, and CO content is 7%.
CN201710785591.1A 2017-09-04 2017-09-04 A kind of Chinese jade porcelain material prescription and manufacture craft Pending CN107602103A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101928132A (en) * 2010-06-23 2010-12-29 平定莹玉陶瓷有限公司 Ordinary fine procelain
CN102924048A (en) * 2012-11-14 2013-02-13 陈启军 Moderate-strength electric porcelain product and manufacturing method thereof
CN106673445A (en) * 2016-12-05 2017-05-17 钦州市钦南区生产力促进中心 Heat-resistant tableware material and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101928132A (en) * 2010-06-23 2010-12-29 平定莹玉陶瓷有限公司 Ordinary fine procelain
CN102924048A (en) * 2012-11-14 2013-02-13 陈启军 Moderate-strength electric porcelain product and manufacturing method thereof
CN106673445A (en) * 2016-12-05 2017-05-17 钦州市钦南区生产力促进中心 Heat-resistant tableware material and preparation method thereof

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Application publication date: 20180119