CN107582432A - A kind of anti-dandruff shampoo composition for improving effective particle over-deposit - Google Patents
A kind of anti-dandruff shampoo composition for improving effective particle over-deposit Download PDFInfo
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- CN107582432A CN107582432A CN201710629699.1A CN201710629699A CN107582432A CN 107582432 A CN107582432 A CN 107582432A CN 201710629699 A CN201710629699 A CN 201710629699A CN 107582432 A CN107582432 A CN 107582432A
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Abstract
The invention belongs to field of daily chemicals, are related to a kind of hair-washing composition.A kind of anti-dandruff shampoo composition for improving effective particle over-deposit, contains following raw material：Anion surfactant, amphoteric surfactant, cationic cellulose derivative 0.05 3%, anti-dandruff agent, non-volatile conditioning agent, the pure water of suspending agent and surplus.The present invention provides a kind of anti-dandruff shampoo composition that can improve effective particle over-deposit, the problem of making still will not to feel greasy after user is long-term use of, harden etc. uncomfortable；Said composition by composition framework rationally build, the limitation of the Synergistic between raw material, raw material key parameter, on the premise of reaching good flocculating strength and carrying effective particulate matter, flocculate selective deposition can be accomplished, will not cause to build up deposition.Composition composition is gentle, all kinds of hair qualitys is applicable, significant effect, cost is cheap, and application is simple and direct.
Description
Technical field
The invention belongs to field of daily chemicals, are related to a kind of hair-washing composition.
Background technology
In two-in-one dandruff control shampoo containing at this stage, particularly with flocculation carry polysiloxane particle and anti-dandruff particle so as to
Deposit to hair or scalp brings conditioning and anti-dandruff effect, there is obviously two-in-one and anti-dandruff effect in a short time
Fruit, this is effect that is art-recognized and can realizing.And this effect is realized, largely pass through Cationic polysaccharide polymer
To achieve the goal.Such as wide variety of formed using cation melon gum derivative and anion surfactant is wadded a quilt with cotton on the market
Solidifying Two-in-one shampoo, the effect of fairly obvious instant conditioning can be brought.
Similar, there is provided the dandruff control shampoo for nursing one's health effect is also known in the field.Such as Chinese Patent Application No.
00809131.5 and Chinese Patent Application No. 00808517.X discloses one kind by anion surfactant and cation Guar
The flocculate that gum derivative is formed carries silicone oil particle and zpt particles, by for cationic guar derivative parameter
Preferred implementation carries the ability of effective particulate matter；Chinese Patent Application No. 201480045888.9 also disclose it is a kind of by the moon from
Sub- surfactant, amphoteric surfactant and cationic guar derivative carry selenium disulfide, ZPT and silicon
Oxygen alkane realizes the effect of anti-dandruff conditioning.
But although these utilize cation melon gum derivative and the flocculation effect ten of anion surfactant formation
It is clearly demarcated aobvious, but due to this flocculation deposition not optionally, therefore in most cases, with this type hair washing group
The wash number of compound increases, and effective particle such as polysiloxane particle etc. can be deposited progressively without being cleaned, with
The passage of time, the discomforts such as user will feel greasy, harden.
However, there is another solution at this stage, the cation-modified cellulose derivative of traditional scheme is utilized
To replace cation melon gum derivative to be flocculated, although this scheme can be effectively improved the disadvantage of working substance over-deposit
End, but often in many shampoo systems, it is difficult to accomplish its flocculating strength and carry the ability and sun of effective particulate matter
Ion melon gum derivative is matched, and therefore, the carrying capacity Shortcomings of its effective particulate matter, hair washing impact sense is also insufficient.
If it has been found that match somebody with somebody by the optimizely select for system, limit the use of some raw materials, at the same preferred sun from
The molecular weight and charge density of subbundle element derivative, it can accomplish in terms of flocculating strength and the ability of the effective particulate matter of carrying
It can approach and be better than cation melon gum derivative, its instant two-in-one effect brought is no less than cation melon glue
Derivative, and have surprisingly found that and pass through confirmation, even if flocculating strength and the ability of the effective particulate matter of carrying are equal to together
Cation melon gum derivative, by the undiscovered phenomenon for having over-deposit after long-term cleaning.
It is an object of the invention to provide a kind of anti-dandruff shampoo composition, passes through rationally building for composition system framework
And the limitation to raw material key parameter so that said composition has outstanding flocculating strength and carries the energy of effective particulate matter
Power, and the effect of effective particulate matter over-deposit can be improved, user caused by long-term overclean deposition will not be caused
Bad experience.
The content of the invention
The problem of it is an object of the invention to overcome effective particulate matter over-deposit in the prior art, with hair-washing composition
Wash number increase, effective particle such as polysiloxane particle etc. can progressively accumulation deposition and can not be by with a hair washing
Composition cleans up, over time, user will feel greasy, harden etc. it is uncomfortable the problem of, in order to overcome this
Kind technological deficiency, the present invention provide a kind of anti-dandruff shampoo composition that can improve effective particle over-deposit, make user long-term
Still the problem of will not feeling greasy, harden etc. uncomfortable after use；Said composition passes through rationally the building of composition framework, former
The limitation of Synergistic, raw material key parameter between material, reaching good flocculating strength and carrying the premise of effective particulate matter
Under, flocculate selective deposition can be accomplished, will not cause to build up deposition.Composition composition is gentle, and all kinds of hair qualitys are fitted
With significant effect, cost is cheap, and application is simple and direct.
The invention discloses a kind of anti-dandruff shampoo composition for improving effective particle over-deposit, the hair-washing composition contains
The raw material of composition weight percentage proportioning are accounted for below：
(A) anion surfactant 5-20%；
(B) amphoteric surfactant 0.3-30%；
(C) cationic cellulose derivative 0.05-3%, the viscosity of its 2% pure water solution is 75-40000cps；And nitrogen content
For 0.5-2.5%；
（D）Anti-dandruff agent 0.1-3%；
（E）Non-volatile conditioning agent 0.05-5%；
（F）Suspending agent 0.01-10%；And surplus
（G）Pure water.
Described anion surfactant is selected from ethoxylated dodecyl alcohol sulfate, glycerine monofatty ester sulphur
Hydrochlorate, fatty alcohol ether sulfosuccinate ester salt, N- fatty acyl amino-acid salts, fatty acyl methyl tauride, monoalkyl sulfate,
Monoalkyl carboxylate, the one or more in alkylphosphonate.Wherein preferably at least contain N- fatty acyl amino-acid salts, fat
One or both of fat acyl methyl taurine salt, is found through experiments that, containing such as amino acid surfactant structure, and
And the surfactant with larger Packing parameter, help to reduce integral system excitant, while anion table can be strengthened
Face activating agent, amphoteric surfactant and flocculating strength caused by cationic cellulose derivative and flocculation persistence.
Described amphoteric surfactant is selected from fatty acyl both sexes acetate, fatty acyl CAB, fatty acid amide hydroxyl
One or more in propylsultaine glycine betaine.Preferred fat acyl both sexes acetate and one kind in fatty acyl CAB or
Two kinds, particularly preferred fatty acyl CAB.The addition of amphoteric surfactant so that flocculating strength and flocculation persistence are entered
One step is strengthened, meanwhile, if anionic surfactant portion has the addition of the high surfactant of preferred Packing parameter, both sexes table
Face activating agent is advantageous to increase the easy modulability of composition viscosity, and it is known in the art that the addition of amphoteric surfactant, right
Performance can be achieved in foaming properties, gentle performance and technique all to have greatly improved.
Wherein, R1It is glucoside residue；
Wherein R2Selected from hydroxy alkylidene, alkylene oxide alkylidene, polyoxalkylene, and combinations thereof；
Wherein, R3、R4And R5Independently selected from long alkyl chain, each group contains up to 20 carbon atoms；
Wherein, X-Selected from least one of halogen family anion, sulfate ion, methyl sulfate；
Preferably, the preferred nitrogen content of the cationic cellulose derivative is about 1.1% to about 3.0%, while its pure water solution
Viscosity is about 500 cps to about 38000cps.More preferably nitrogen content is about 1.5% to about 2.9%, while its 2% pure water solution is viscous
Degree is about 1000 cps to about 35000 cps；Most preferably nitrogen content is about 2.5% to about 2.9%, while its 2% pure water solution
Viscosity is about 10000 cps to about 30000 cps；Cationic cellulose derivative is the important original that flocculation is formed in the present invention
Material, applicants experimentally found that, in the case of most preferably formula framework, its flocculating strength is no less than institute in the prior art
The flocculating strength that the cationic guar derivative stated is reached, and it has surprisingly been found that while flocculating degree is suitable, it is excellent
The cationic cellulose derivative of choosing has very broad dilution flocculation scope in the system of the present invention.Also test simultaneously
It was found that although cationic cellulose derivative can reach the flocculating strength that cationic guar derivative is reached, not
Over-deposit can be caused in long-term and multiple cleaning process as cationic guar derivative, it is applicant's understanding that this
The depositional mode and the depositional mode of cationic guar derivative flocculated in itself with cationic cellulose derivative are different
Caused by result.
In flocculation mode, in the composition framework finally protected of the present invention, its pure water dilution range 5 times -20 times it
Between there are the visible solid flocculate that can carry active principle, and in 20 to 60 times of dilution range, largely only have
The flocculate become cloudy, dilution flocculation scope is extremely wide, the dilution of cationic cellulose derivative used in general prior art
Process, although the flocculation that can be become cloudy in wider dilution range can be accomplished, it is difficult in the case of low power number
There is the appearance of solid floccules；And cationic guar derivative is then on the contrary, it can accomplish there is stronger solid wadding in low power number
Condensate occurs, and can not but accomplish to flocculate in wider dilution range.It is actual, when hair-washing composition is acted on hair, be from
Low extension rate to high extension rate is carried out, and dilution range is wider, represents that it has hair conditioning in a very long time.Due to
Adsorption mechanism of the flocculate of cationic cellulose derivative on hair is " solid floccules deposition " and " flocculation become cloudy
Thing Electrostatic Absorption ", this make it that the deposition of cationic cellulose derivative is selective, when flocculate relies on Coulomb force electrostatic
After being adsorbed onto on hair, the negative electrical charge on hair reduces, and those flocculates adsorbed by Coulomb force just do not adsorb, so as to
Control the absorption of flocculate.And the sedimentation mechanism of cationic guar derivative flocculate is " solid floccules deposition ",
That is no matter how many flocculate are deposited on hair, it is all without being selectively adsorbed.
Described anti-dandruff agent is selected from ZPT, hexamidine two（Isethionic acid）In salt, Octopirox
It is one or more of.It is considered as effective particle if anti-dandruff agent is to be present in the form of granules among hair-washing composition
One kind, can be by Cationic polysaccharide polymer（Cationic cellulose derivative and cationic guar derivative）With anion table
The solid-state flocculate parcel that face activating agent is formed is adsorbed and carried to scalp, reaches anti-dandruff purpose.
Described non-volatile conditioning agent is one or both of scattered polysiloxanes, ammonia end dimethyl silicone polymer
Compounding, and polysiloxanes described preferably wherein and ammonia end dimethyl silicone polymer are micro- using particle diameter as about 0.05 micron to about 50
The size of rice is present in composition.This is also considered one kind of effective particulate matter, has opsonic action for hair, can quilt
Cationic polysaccharide polymer（Cationic cellulose derivative and cationic guar derivative）With anion surfactant shape
Into solid-state flocculate parcel adsorb and carry to hair, can realize two-in-one effect, improve hair-washing composition
Use feel.
Described suspending agent is selected from acyl derivative and long chain amine oxide.Wherein, described acyl derivative is included but not
It is limited to the ethylene glycol fatty acid containing 16-22 carbon atom, long chain hydrocarbons, the long-chain ester of long chain fatty acids, long chain alkanol amides
Long-chain ester.Wherein described long chain amine oxide includes but is not limited to the dimethyl amine of 16-22 carbon atom.Preferably comprise
The fatty acid ethylene glycol diester of 18 carbon atoms.Applicant experiments prove that, flocculating degree of this suspending agent for system
Influence very little, and suspending power is very sufficient, and suspending power is provided not against yield value.
A kind of above-mentioned anti-dandruff shampoo composition for improving effective particulate matter over-deposit, except it is above-mentioned it is necessary into point it
Outside, at least one also containing following component：
Aid in suspending agent：0.01-5%；
Nonionic surfactant：0.01-5%;
Organic conditioning oil：0.01-2%
Higher aliphatic：0.01-5%
Preservative：0.01-1%；
Essence：0.01-3%；
Viscosity modifier：0.01-4%；
Chelating agent：0.005-0.2%；
Ultra-violet absorber：0.01-2%；
Plant extracts and its derivative：0.0001-5%；
Wherein, described auxiliary suspending agent is selected from hydroxypropyl methyl cellulose, hydroxyethyl cellulose, melon gum derivative, starch
Derivative, hydroxypropyl starch phosphate, the one or more in xanthan gum；And acrylic polymer and its derivative, card ripple
Nurse polymer, acrylic acid（Ester）Class/C10 ~ C30 alkylol acrylamide acid ester copolymers, acrylates/C10 ~ C30 alkylol acrylamide acid esters
Cross-linked copolymer emulsifying agent, acrylic acid（Ester）Analog copolymer, the cross-linked polymer of polyacrylate -1, acrylic acid（Ester）Class/tristearin
Alcohol polyethers（20）Methacrylate copolymer is not then in the range of selection.Follow-up this kind of suspending agent why is not selected, is
Applicant experiments prove that, although such suspending agent can provide good stability and yield value, for hair washing group
The flocculating strength of compound has a great impact, in order to ensure the carrying capacity of the effect of hair-washing composition and effective particulate matter, because
This does not do preferably.
Described shampoo can be combined in the personal care articles of different dosage forms with arbitrary proportion.
A kind of above-mentioned anti-dandruff shampoo composition for improving effective particulate matter over-deposit, can arbitrary proportion and conventional base-material system
Into in hair class cosmetics, State of cosmetics can be one kind in solution, suspension, emulsion, paste, solid-like.
A kind of above-mentioned anti-dandruff shampoo composition for improving effective particulate matter over-deposit, its collocation method are conventional configuration
And hybrid technology, do not elaborate herein.
1st, the flocculating strength of care composition of the invention is strong, there is notable flocculating effect in wider dilution range,
Effective particle can be effectively carried, and can plays good conditioning effect.The present invention has selected high nitrogen content and HMW
Cationic cellulose derivative, and arrange in pairs or groups and do not influence the suspension stabilizer of flocculating strength, preferably anion surfactant
With the collocation of amphoteric surfactant so that can be flocculated visible solid floccules in low extension rate, this contributes to
Imitate the carrying of particulate matter；And can realize has significantly flocculation phenomenon in broader dilution range, and this causes hair washing group
The conditioning effect of compound becomes more preferably.In the composition framework that the present invention finally protects, its pure water dilution range is at 5 times -20 times
Between there are the visible solid flocculate that can carry active principle, and in 20 to 60 times of dilution range, it is most of only
There is the flocculate become cloudy, dilution flocculation scope is extremely wide, and cationic cellulose derivative is dilute used in general prior art
Process is released, although the flocculation that can be become cloudy in wider dilution range can be accomplished, is difficult to do in the case of low power number
To the appearance for having solid floccules；And cationic guar derivative is then on the contrary, it can accomplish there is stronger solid in low power number
Flocculate occurs, and can not but accomplish to flocculate in wider dilution range.
2nd, the flocculate of hair-washing composition of the invention can be adsorbed optionally on hair and on scalp, and improvement has
Imitate the over-deposit of particulate matter.It is known in the art that the effectively particulate matter such as anti-dandruff agent or silicone oil emulsification particle in shampoo can
Wrap up and carry to be flocculated thing, if the deposition of flocculate or absorption are uncontrolled, can cause in long-term use process
In have the over-deposit of effective particulate matter.It is applicant's understanding that suction of the flocculate of cationic cellulose derivative on hair
Random reason is " solid floccules deposition " and " the flocculate Electrostatic Absorption become cloudy ", and this causes cationic cellulose derivative
Deposition is selective, and after flocculate is by Coulomb force Electrostatic Absorption to hair, the negative electrical charge on hair reduces, and relies on
Those flocculates of Coulomb force absorption, which just adsorb, no longer to be adsorbed, so as to control the absorption of flocculate.And cation guar gum spreads out
The sedimentation mechanism of biological floc is " solid floccules deposition ", that is to say, that no matter how many flocculate are deposited on hair, its
It will be deposited on scalp.And these solid floccules are required, because this solid floccules can carry hair washing group
On effective particle to scalp or hair among compound, reach anti-dandruff function, also realize two-in-one hair washing experience
3rd, the compounding synergy between hair-washing composition of the invention is obvious, passes through the synergy between raw material so that wash
The flocculating degree and flocculation scope for sending out composition are strengthened, while reduce the difficulty of technique, reduce the excitant of system, improve
Thickening efficiency.
Therefore, the present invention can accomplish to improve effective particle over-deposit, at the same can reach good anti-dandruff effect and
Two-in-one effect, improve deficiency of the prior art.
Brief description of the drawings
Fig. 1 is the silicone oil deposition test data of embodiment and comparative example.
Fig. 2 is the zpt depositions that embodiment and comparative example are once cleaned.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, below in conjunction with the accompanying drawings to the present invention
Embodiment be described in detail.
Table 1 below is 3 preferred embodiments of the present invention and 3 comparative examples.Wherein, comparative example 4 is from one kind on the market
Sell the measured dandruff control shampoo containing made with cationic guar derivative.
Wherein, the key parameter of the cationic cellulose derivative in table 1 is as shown in table 2 below：
After topknot is cleaned multiple times, measure topknot on silicone oil, with this come characterize silicone oil particulate matter with cleaning time
Several deposition conditions；The arm of employment simultaneously replaces scalp, carries out the cleaning test of arm, and measures the zpt contents on arm,
The Carriage of anti-dandruff agent is characterized with this.Test comparison is carried out to above-mentioned 3 groups of embodiments and 4 groups of comparative examples, obtained such as the institute of table 3
The test result shown.
Plot analysis is carried out to above-mentioned experimental result.
Silicone oil deposition is analyzed first, by carrying out drawing arrangement to data, obtains the column diagram of silicone oil deposition, such as
Shown in Fig. 1.Secondly, drawing arrangement is carried out to zpt deposition, obtains Fig. 2.
From upper two map analysis, preferable cationic cellulose can be seen that by the contrast of embodiment 1-3 and comparative example 2
Derivative contributes to silicone oil and zpt deposition；By the contrast of embodiment 1 and embodiment 2, it has also been discovered that amino acid surface is lived
Property agent addition, to flocculation have synergistic effect；Analysis embodiment 1-3 and comparative example 1, the silicone oil deposition of comparative example 4 can be sent out
Existing, embodiment 1-3 silicone oil deposition is with the increase of wash number, and it does not have an apparent growth trend, and the He of comparative example 1
Comparative example 4 then rises appreciably trend, that is to say, that the embodiment that the present invention protects has and improves effective particulate matter such as silicone oil
The effect of grain thing；By embodiment 1 and comparative example 3 it can be found that using suspending agent instead after, the deposition of its silicone oil and zpt's
Deposition has all been reduced, therefore the technical goal to be realized to reach this patent, then should not select what this patent was enumerated
The suspending agent of non-choosing.
Claims (9)
1. a kind of anti-dandruff shampoo composition for improving effective particle over-deposit, it is characterised in that contain following percetage by weight
The raw material of proportioning：
(A) anion surfactant 5-20%；
(B) amphoteric surfactant 0.3-30%；
(C) cationic cellulose derivative 0.05-3%, the viscosity of its 2% pure water solution is 75-40000cps；And nitrogen content
For 0.5-2.5%；
（D）Anti-dandruff agent 0.1-3%；
（E）Non-volatile conditioning agent 0.05-5%；
（F）Suspending agent 0.01-10%；And surplus
（G）Pure water.
2. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Anion surfactant be selected from ethoxylated dodecyl alcohol sulfate, glycerine monofatty ester sulfate, fatty alcohol ether sulphur
Base succinate salt, N- fatty acyl amino-acid salts, fatty acyl methyl tauride, monoalkyl sulfate, monoalkyl carboxylate are single
At least one of alkyl phosphate salt.
3. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Anion surfactant contain at least one of N- fatty acyl amino-acid salts, fatty acyl methyl tauride.
4. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Amphoteric surfactant be selected from fatty acyl both sexes acetate, fatty acyl CAB, fatty acid amide hydroxypropyl sulfobetaines
At least one of alkali.
5. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
The preferred Polyquaternium-10 of cationic cellulose derivative.
6. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Anti-dandruff agent be selected from ZPT, hexamidine two（Isethionic acid）One or more in salt, Octopirox.
7. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Non-volatile conditioning agent be one or both of scattered polysiloxanes, ammonia end dimethyl silicone polymer compounding.
8. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：It is described
Suspending agent be selected from acyl derivative and long chain amine oxide.
9. the anti-dandruff shampoo composition according to claim 1 for improving effective particle over-deposit, it is characterised in that：Also contain
There is at least one of following component：
Aid in suspending agent：0.01-5%；
Nonionic surfactant：0.01-5%；
Organic conditioning oil：0.01-2%；
Higher aliphatic：0.01-5%；
Preservative：0.01-1%；
Essence：0.01-3%；
Viscosity modifier：0.01-4%；
Chelating agent：0.005-0.2%；
Ultra-violet absorber：0.01-2%；
Plant extracts and its derivative：0.0001-5%.
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| CN201710629699.1A CN107582432B (en) | 2017-07-28 | 2017-07-28 | Dandruff removing shampoo composition for improving excessive deposition of effective particles |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109498499A (en) * | 2018-11-26 | 2019-03-22 | 澳宝化妆品（惠州）有限公司 | A kind of composition for maintenance hair scalp before having one's hair wash |
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| CN1204255A (en) * | 1995-10-16 | 1999-01-06 | 普罗克特和甘保尔公司 | Conditioning shampoo compositions having improved stability |
| CN1238680A (en) * | 1996-10-25 | 1999-12-15 | 普罗克特和甘保尔公司 | Conditioning shampoo composition |
| CN1353601A (en) * | 1999-05-03 | 2002-06-12 | 宝洁公司 | Anti-dandruff and conditioning shampoos containing polyalkylene glycols and cationic polymers |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
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2017
- 2017-07-28 CN CN201710629699.1A patent/CN107582432B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1204255A (en) * | 1995-10-16 | 1999-01-06 | 普罗克特和甘保尔公司 | Conditioning shampoo compositions having improved stability |
| CN1238680A (en) * | 1996-10-25 | 1999-12-15 | 普罗克特和甘保尔公司 | Conditioning shampoo composition |
| CN1353601A (en) * | 1999-05-03 | 2002-06-12 | 宝洁公司 | Anti-dandruff and conditioning shampoos containing polyalkylene glycols and cationic polymers |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109498499A (en) * | 2018-11-26 | 2019-03-22 | 澳宝化妆品（惠州）有限公司 | A kind of composition for maintenance hair scalp before having one's hair wash |
| CN109498499B (en) * | 2018-11-26 | 2022-01-28 | 澳宝化妆品（惠州）有限公司 | Composition for caring hair and scalp before washing hair |
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| CN107582432B (en) | 2020-07-10 |
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