CN107549165B - Gel for preventing and treating trunk-boring pests and application thereof - Google Patents
Gel for preventing and treating trunk-boring pests and application thereof Download PDFInfo
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- CN107549165B CN107549165B CN201710796911.3A CN201710796911A CN107549165B CN 107549165 B CN107549165 B CN 107549165B CN 201710796911 A CN201710796911 A CN 201710796911A CN 107549165 B CN107549165 B CN 107549165B
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Abstract
The invention relates to a gel for preventing and treating stem borers, which comprises the following components: 20-30 g of agent A, 40-60 mL of agent B, 10-20 mL of agent C, 30-50 mL of agent D, 1-1.5 g of agent E and water for supplementing the total volume to 1000 mL. The agent A is one or more of xanthan gum, sodium alginate and locust bean gum; the agent B is one of 1.3-propylene glycol or sorbitol; the agent C is absolute ethyl alcohol; the D agent is one of a 25% chlorbenzuron suspending agent, 1.2% nicotine-matrine missible oil, 1% celastrus angulatus aqueous emulsion or 0.5% veratrine soluble solution; the E agent is one of 50% carbendazim wettable powder or 70% thiophanate methyl wettable powder. The invention also relates to the application of the gel in preventing and treating the stem borers, which has good prevention and treatment effect on the stem borers, is nontoxic and tasteless, and is safe to natural enemies and environment of the stem borers.
Description
Technical Field
The invention relates to a gel for preventing and treating stem borers and application thereof.
Background
Trunk borers mainly eat main trunks, branches and other parts of trees, and live in hidden life with larvae in the trees for a long time, so that the trees are sore and have holes, the conducting and transporting tissues are damaged, the transportation of nutrients and water is blocked, the trees are poor in growth, leaves are yellow, branches are withered, the wood quality and the fruit yield are affected, the ornamental value is reduced, the trees die in severe cases, and the damaged branches and trunks of the trees are easy to break and hurt pedestrians and vehicles.
The trunk borers mainly comprise longicorn, bark beetle, sulcus orbital elephant and the like, eggs are laid in bark of adults, and larvae gradually enter phloem, cambium and xylem after hatching to cause harm. Because the insect population is slightly influenced by environmental conditions in a tree body, the insect population is less, the insect population density is relatively stable, and the prevention difficulty is higher. The method for controlling the stem borers by utilizing natural enemies such as scleroderma guani, beauveria bassiana, pathogenic nematodes and the like is the most environment-friendly method, but the production, transportation, storage, multiplication and release of the natural enemies all need certain environmental conditions, the technical difficulty is high, and the application effect is not ideal. Tests show that the prevention and control effects of trunk borers are not ideal when the roots are filled with or buried with drugs, the trunks are punched and filled with drugs or bags are hung on the trunks, and the drug bottles are inserted. The liquid medicine is filled into the moth holes or the excrement discharge holes, so that the pesticide has a good effect of preventing trunk borers which are damaged by eating downwards; for the trunk borers eating upwards or having a plurality of defecation holes, the liquid medicine is easy to run off, and the control effect is obviously reduced.
The Qiaojian is equal to that of 2010, the paste for preventing and treating the stem borers is published, patent invention authorization is obtained in 2013, the paste is ZL 201010592873.8, the paste has certain fluidity and moderate viscosity, the problem that liquid medicine is easy to run off is solved, and the paste has good prevention and treatment effects on the stem borers of one insect, such as anoplophora glabripennis, anoplophora chinensis, rust-colored anoplophora glabripennis, longicorn, mulberry longicorn and the like, but the paste has a relatively quick volatilization, so that the prevention effect on the species with more insects and more excretory holes, such as the small linear horn moth.
Disclosure of Invention
The invention aims to provide a gel which has good control effect on stem borers, is nontoxic and tasteless, and is safe to natural enemies of the stem borers and the environment.
The invention adopts the following technical scheme:
a gel for controlling stem-boring insects, which comprises the following components: 20-30 g of agent A, 40-60 mL of agent B, 10-20 mL of agent C, 30-50 mL of agent D, 1-1.5 g of agent E and water for supplementing the total volume to 1000 mL.
The agent A is one or more of xanthan gum, sodium alginate and locust bean gum.
The agent B is one of 1, 3-propylene glycol or sorbitol, and sorbitol is preferred.
The agent C is absolute ethyl alcohol.
The D agent is one of 25% chlorbenzuron suspending agent, 1.2% nicotine-matrine missible oil, 1% celastrine aqueous emulsion or 0.5% veratrine soluble solution, and 25% chlorbenzuron suspending agent is preferred.
The E agent is one of 50% carbendazim wettable powder or 70% thiophanate methyl wettable powder.
Further, the agent A is xanthan gum 20-25 g.
Further, the agent A is 23-27 g of locust bean gum.
Further, the agent A is 25-30 g of sodium alginate.
Further, the agent A is 27g and comprises 15-20 g of xanthan gum and 12-7 g of locust bean gum.
Further, the agent A is 28g and comprises 10-15 g of xanthan gum and 18-13 g of locust bean gum.
Further, the D agent is a 25% chlorbenzuron suspending agent.
A method for preparing the gel, which comprises the following steps:
(1) weighing the components according to the mixture ratio of the components;
(2) dissolving the agent A with 800mL of 700-800 water, uniformly stirring, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), adding water to a constant volume of 1000mL, and uniformly stirring to obtain gel.
An application of the gel in preventing and treating stem borers is disclosed. The application comprises the following steps: cleaning up the insect dung in the dung discharge hole, and then extruding the gel into the dung discharge hole.
The invention has the beneficial effects that:
(1) the gel of the invention is in a stable viscous state and has poor fluidity, and compared with the existing paste for preventing and treating stem borers, the gel has stronger moisture retention and slower volatilization, the lasting period can reach more than 10 days, and the control effect on the small linear angle codling moth can reach more than 95 percent.
(2) The gel of the invention can also be used for preventing and controlling other trunk borers such as longicorn, orbital elephant and the like.
(3) The gel is non-toxic, tasteless and safe to natural enemies and environment.
Detailed Description
For the purpose of enhancing understanding of the present invention, the following detailed description is given in conjunction with examples, which are given by way of illustration only and are not intended to limit the scope of the present invention.
Example 1
(1) Weighing the components according to the mixture ratio of the components; 20g of xanthan gum as an agent A, 40mL of 1.3-propylene glycol as an agent B, 10mL of absolute ethanol as an agent C, 50mL of 1.2% nicotine-matrine emulsifiable concentrate as an agent D, and 1g of 70% thiophanate-methyl wettable powder as an agent E;
(2) dissolving the agent A with 800mL of 700-800 water, uniformly stirring, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), adding water to a constant volume of 1000mL, and uniformly stirring to obtain gel.
When the device is used, the insect dung in the dung discharging hole is cleaned, and then the gel is squeezed into the dung discharging hole.
Example 2
(1) Weighing the components according to the mixture ratio of the components; 22g of xanthan gum serving as an agent A, 60mL of sorbitol serving as an agent B, 20mL of absolute ethanol serving as an agent C, 30mL of 25% chlorbenzuron suspending agent serving as an agent D, and 1.5g of 50% carbendazim wettable powder serving as an agent E;
(2) dissolving the agent A with 700-800mL of water, stirring with force, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), diluting to 1000mL with water, and forcibly stirring to obtain gel.
When the device is used, the insect dung in the dung discharging hole is cleaned, and then the gel is squeezed into the dung discharging hole.
Example 3
(1) Weighing the components according to the mixture ratio of the components; 25g of xanthan gum serving as an agent A, 50mL of sorbitol serving as an agent B, 15mL of absolute ethanol serving as an agent C, 40mL of 1% celastrus angulatus aqueous emulsion serving as an agent D, and 1.2g of 70% thiophanate methyl wettable powder serving as an agent E;
(2) dissolving the agent A with 700-800mL of water, stirring with force, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), diluting to 1000mL with water, and forcibly stirring to obtain gel.
When the device is used, the insect dung in the dung discharging hole is cleaned, and then the gel is squeezed into the dung discharging hole.
Example 4
(1) Weighing the components according to the mixture ratio of the components; the preparation A is 22g of xanthan gum, the preparation B is 60mL of sorbitol, the preparation C is 20mL of absolute ethyl alcohol, the preparation D is 30mL of 0.5% veratrine soluble solution, and the preparation E is 1.5g of 50% carbendazim wettable powder;
(2) dissolving the agent A with 700-800mL of water, stirring with force, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), diluting to 1000mL with water, and forcibly stirring to obtain gel.
When the device is used, the insect dung in the dung discharging hole is cleaned, and then the gel is squeezed into the dung discharging hole.
Example 5
The same as example 1, except that the agent A was locust bean gum 23 g.
Example 6
The same as example 2 except that the agent A was locust bean gum 27 g.
Example 7
The same as example 3, except that the agent A was locust bean gum 25 g.
Example 8
The difference is that the agent A is 25g of sodium alginate as in example 1.
Example 9
The difference is 30g of sodium alginate as agent A, just as in example 3.
Example 10
The difference is that 27g of sodium alginate is used as the agent A, as in example 4.
Example 11
The only difference from example 1 is that agent a comprises xanthan gum 15g and locust bean gum 12 g.
Example 12
The only difference from example 2 is that the agent A comprises xanthan gum 17g and locust bean gum 10 g.
Example 13
The difference from example 3 is only that the agent A includes xanthan gum 20g and locust bean gum 7 g.
Example 14
The only difference from example 1 is that agent a comprises xanthan gum 10g and locust bean gum 18 g.
Example 15
The difference from example 3 is only that the agent A includes xanthan gum 15g and locust bean gum 13 g.
Example 16
The only difference from example 4 is that the agent A comprises xanthan gum 13g and locust bean gum 15 g.
Effect example 1 drying time
Materials: the paste obtained in patent No. ZL 201010592873.8 and the gels obtained in examples 1 to 16 were used.
The method comprises the following steps: and (3) taking the paste and the gel with equal mass, and simultaneously placing the paste and the gel in a vacuum freeze dryer for drying, wherein the drying time is compared.
The results show that the drying time of the gel prepared in the embodiments 1 to 16 of the invention is 3 to 5 times of that of the paste. Has stronger moisture retention, slower evaporation and longer lasting period than the paste.
Effect example 2 controlling Effect
Materials: gels obtained according to examples 1, 2, 3, 4, 7, 10, 13 and 16 of the present invention.
Comparative materials: the paste obtained in example 1 of patent No. ZL 201010592873.8. Namely 4kg of 1.2 percent nicotine-matrine missible oil, 4kg of kaolin, 1kg of glycerol, 1kg of thickening agent and 10kg of water.
The method comprises the following steps: injecting the gel or paste into the cleaned wormholes by a pressure medicine gun. Clear water is used as a control, the number of worm holes without fresh worm excrement is counted after 15 days to serve as the number of dead worms, 30 worm holes are counted to serve as a group, the corrected mortality rate is calculated, three groups of parallel experiments are carried out, and the average value is taken. The results are shown in Table 1.
TABLE 1 comparison of the controlling effects of gels and pastes on trunk-boring pests
As can be seen from Table 1, the examples of the invention have good control effect on both orbital elephant and Monochamus mori, and the corrected mortality rate reaches more than 97%, which is about 10% higher than that of the paste of the comparative material. The gel has better moisture retention and longer lasting period, does not influence the pesticide effect due to loss and volatilization, simultaneously combines the excellent mixture ratio of each medicament, has excellent control effect on the small linear horned beetles with clustering property and multiple wormholes, and has corrected mortality rate of not less than 97 percent, thereby showing the excellent performance of the gel on the prevention and control of wormhole pests.
The above-mentioned embodiments are merely illustrative of the preferred embodiments of the present invention, but not restrictive, and those skilled in the art can easily understand the spirit of the present invention from the above-mentioned embodiments and make various extensions and changes, but they are within the scope of the present invention without departing from the spirit of the present invention.
Claims (9)
1. A gel for controlling stem-borer pests by injecting into a moth channel, which is used for controlling the small angle bark beetle and comprises the following components: 20-30 g of agent A, 40-60 mL of agent B, 10-20 mL of agent C, 30-50 mL of agent D, 1-1.5 g of agent E and water for complementing the total volume to 1000 mL;
the agent A is one or more of xanthan gum, sodium alginate and locust bean gum;
the agent B is one of 1.3-propylene glycol or sorbitol;
the agent C is absolute ethyl alcohol;
the D agent is one of a 25% chlorbenzuron suspending agent, 1.2% nicotine-matrine missible oil, 1% celastrus angulatus aqueous emulsion or 0.5% veratrine soluble solution;
the E agent is one of 50% carbendazim wettable powder or 70% thiophanate methyl wettable powder;
when the agent A is xanthan gum, the using amount of the xanthan gum is 20-25 g.
2. The gel for controlling stem-boring insects according to claim 1, wherein the agent A is locust bean gum 23-27 g.
3. The gel for preventing and treating stem borers according to claim 1, wherein the dose A of sodium alginate is 25-30 g.
4. The gel for controlling stem-boring insects according to claim 1, wherein the agent A is 27g, and comprises 15-20 g of xanthan gum and 12-7 g of locust bean gum.
5. The gel for controlling stem-boring insects according to claim 1, wherein the agent A is 28g and comprises 10-15 g of xanthan gum and 18-13 g of locust bean gum.
6. The gel of claim 1, wherein said D agent is a 25% chlorbenzuron suspension.
7. A process for preparing a gel according to any one of claims 1 to 6, comprising the steps of:
(1) weighing the components according to the mixture ratio of the components;
(2) dissolving the agent A with 800mL of 700-800 water, uniformly stirring, and standing for 1-2 hours until the agent A is completely dissolved;
(3) dissolving the agent E in water, sequentially adding the agent E, the agent B, the agent C and the agent D into the agent A prepared in the step (2), adding water to a constant volume of 1000mL, and uniformly stirring to obtain gel.
8. Use of a gel according to any one of claims 1 to 6 for controlling stem-boring pests.
9. Use according to claim 8, characterized in that it comprises the following steps: cleaning up the insect dung in the dung discharge hole, and then extruding the gel into the dung discharge hole.
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PT774896E (en) * | 1994-08-03 | 2001-12-28 | Syngenta Ltd | GEL FORMULATION |
CN102125028B (en) * | 2010-12-17 | 2013-10-30 | 乔建国 | Paste for preventing and curing stem borer |
CN103609557A (en) * | 2013-12-05 | 2014-03-05 | 南京农业大学 | Preparation of water-soluble gel for preventing and treating pear rot |
CN105028439B (en) * | 2015-06-25 | 2017-09-19 | 青岛中达农业科技有限公司 | It is a kind of to be used to prevent and treat gel of apple fruit diseases and preparation method thereof |
CN105284864B (en) * | 2015-12-04 | 2017-03-15 | 李开森 | Woods fruit notes dry insecticide and its preparation method and application |
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小线角木蠹蛾综合防治技术规程;白瑞霞等;《河北农业科学》;20191231;第23卷(第1期);第51-53页 * |
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