CN107536928A - A kind of habitat processing method of the fresh tuber of pinellia - Google Patents
A kind of habitat processing method of the fresh tuber of pinellia Download PDFInfo
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- CN107536928A CN107536928A CN201710798222.6A CN201710798222A CN107536928A CN 107536928 A CN107536928 A CN 107536928A CN 201710798222 A CN201710798222 A CN 201710798222A CN 107536928 A CN107536928 A CN 107536928A
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Abstract
The invention discloses a kind of habitat processing method of the fresh tuber of pinellia, belong to toxic traditional Chinese medicine material processing technique field.In order to strengthen the tuber of pinellia kobadrin drug effect while solving the problems, such as that toxic component remains in the tuber of pinellia, the invention provides a kind of habitat processing method of the fresh tuber of pinellia, the present invention makes full use of the physiological property of tuber of pinellia plant cell, by pricking the steps such as hole, stifling, hypertonic solution immersion, the vexed system of penetrating fluid and HIGH PRESSURE TREATMENT, so that the tuber of pinellia thin slice moderate stimulation toxic component calcium oxalate crystal content prepared reduces, aspartate content increase with Antitussive and Expectorant Effect, the medical value of the tuber of pinellia is improved, ensure that the pharmaceutical safety of the tuber of pinellia.
Description
Technical field
The invention belongs to toxic traditional Chinese medicine material processing technique field, specifically a kind of habitat processing method of the fresh tuber of pinellia.
Background technology
The tuber of pinellia is aroid the tuber of pinellia Pinellia ternata (Thunb.) Breit. dry tuber.Its stem tuber
There is eliminating dampness and eliminating phlegm, stopping nausea and vomiting by lowering the adverse flow of QI, dissolving lump and resolving mass.Cure mainly vomiting, gastric disorder causing nausea, cough and phlegm, fullness in chest, dizziness and sleepless
Deng disease.Tuber of pinellia health product taste fiber crops tongue and pierce larynx, its toxicity is mainly shown as excitant toxicity, and clinic does not typically have to health product, it is necessary to big gun
It can be applied after system.
At present, the processing method for the fresh tuber of pinellia is divided into fermentation, peeling, the step dried, and the wherein tuber of pinellia place of production is dried
Conventional method dried, it is necessary to be continuously exposed to the sun on the threshing ground that Yanguan Pass is sufficient, ventilation condition is good, and will anti-fog
Influence, had a great influence by external condition；The tuber of pinellia dry when due to the time it is longer, and easily by external condition influenceed and it is tacky,
Fermentation is even rotted, and sodium pyrosulfite chemicals is spilt in the place of production for the ease of storage through smoking method frequently with sulphur or directly mixing
It is handled to ensure that its surface is pure white, while can also play desinsection, antisepsis.But sulphur or sodium pyrosulfite are being processed
During can produce the chemical compositions such as sulfur dioxide, easy penetration cell wall is attached on amylum body, gos deep into medicinal material organization internal, with
Some compositions therein react, and then influence medical material quanlity.
In the prior art, number of patent application discloses " a kind of tuber of pinellia and its processing method ", the hair for 2011101470284
It is bright to clean the fresh tuber of pinellia, decortication, it is placed in the acid solution that pH is 1-6 and soaks 2-30min, take out, rinses surface remaining
Acid solution, dry, produce, the invention makes tuber of pinellia surface keep pure white, has no side effect, and can substitute existing stove drying technique；
Number of patent application 2014102022912 disclose a kind of " method of the Habitat producing tuber of pinellia " invention by light-coloured vinegar and white alum solution with
It is placed in after fresh tuber of pinellia mixing in hyperbaric environment and boils 30-60min, the invention had both avoided sulfur dioxide toxic component residual, again
Reduce the content of poisonous stimulation component calcium oxalate in the health product tuber of pinellia.
Research shows, amino acid, alkaloid, organic acid, choline, trace volatile oil, protocatechualdehyde, β-paddy are contained in the tuber of pinellia
The active ingredient such as sterol and its glucoside, the content of amino acid have large effect to drug effect, and wherein aspartic acid has town
Cough goes phlegm to act on, and its content height affects the power of tuber of pinellia effect, can effectively improve the tuber of pinellia for tuber of pinellia processing method at present
Middle amino acid content and the report of function are simultaneously few.
The content of the invention
For the above situation, to overcome the defect of prior art, the purpose of the present invention is just to provide a kind of production of the fresh tuber of pinellia
Ground processing method, can effectively solve the problems, such as to strengthen the tuber of pinellia kobadrin drug effect while toxic component remains in the tuber of pinellia.
The particular content of the present invention is as follows：
A kind of habitat processing method of the fresh tuber of pinellia, it comprises the following steps：
1., take the fresh tuber of pinellia, decortication is cleaned, and is cut into the thick pieces of 5-6mm, is uniformly pricked first in tuber of pinellia sheet surface with pin
Aperture, small hole number 4-5, hole diameter 1.5-2mm；
2., 1. step is handled after 120-150 DEG C of water vapour of tuber of pinellia thin slice fumigate 30-60s, then by tuber of pinellia thin slice
Immerse in the glucose solution that concentration is 40%, soak 40-60min, take out tuber of pinellia thin slice infra-red drying 5-10min, glucose
Solution filtering is standby；
3., in parts by weight, take step 2. middle glucose solution 2-5 parts for soaking tuber of pinellia thin slice, 15-20 part ethylenediamines
Tetraacethyl disodium, 5-7 parts aspartic acid, the mixing of 30-50 parts water, stir to solution is transparent and penetrating fluid are made；
4., penetrating fluid is placed in sprayer, uniformly spray dried tuber of pinellia thin slice, be sprayed onto tuber of pinellia thin slice and moisten completely
Thoroughly, then the tuber of pinellia thin slice of wetting is piled up in transparent porcelain jar, sealing is placed on the place that natural light is transmitted to, and stands 24-
36 hours, then penetrating fluid that tuber of pinellia thin slice is equipped with to 0.1-0.5 times of its weight was placed in pressure vessel, was 0.16- in pressure
20-30min is suppressed under 0.18MPa, thin slice is taken out and carries out infra-red drying again to tuber of pinellia thin slice water content≤8%, you can.
Further, it is preferable that 1. middle hole diameter is 1.5mm to step.
Further, it is preferable that step 3. in penetrating fluid in each parts by weight of raw material be：Soaked the Portugal of tuber of pinellia thin slice
4 parts of grape sugar juice, 16.5 parts of disodium ethylene diamine tetraacetates, 6 parts of aspartic acids, 40 parts of water.
The beneficial effects of the present invention are：The tuber of pinellia processing method of the present invention makes full use of the physiology of tuber of pinellia plant cell special
Property, by pricking the steps such as hole, stifling, hypertonic solution immersion, the vexed system of penetrating fluid and HIGH PRESSURE TREATMENT so that in the tuber of pinellia thin slice of preparation
Stimulate toxic component calcium oxalate crystal content to reduce, the aspartate content increase with Antitussive and Expectorant Effect, improve the tuber of pinellia
Medical value, ensure that the pharmaceutical safety of the tuber of pinellia.
Embodiment
Embodiment 1
A kind of habitat processing method of the fresh tuber of pinellia, it comprises the following steps：
1., take the fresh tuber of pinellia, decortication is cleaned, and cuts into the thick pieces of 5mm, is uniformly pricked first in tuber of pinellia sheet surface with pin small
Hole, small hole number 4, hole diameter 1.5mm；
2., 1. step is handled after tuber of pinellia thin slice with 120 DEG C of water vapours fumigate 30s, then by tuber of pinellia thin slice immerse it is dense
Spend in the glucose solution for 40%, soak 40min, take out tuber of pinellia thin slice infra-red drying 5min, glucose solution filtering is standby；
3., in parts by weight, take step 2. middle 2 parts of the glucose solution for soaking tuber of pinellia thin slice, 15 parts of ethylenediamine tetrems
Acid disodium, 5 parts of aspartic acids, 30 parts of water mixing, stir to solution is transparent and penetrating fluid are made；
4., penetrating fluid is placed in sprayer, uniformly spray dried tuber of pinellia thin slice, be sprayed onto tuber of pinellia thin slice and moisten completely
Thoroughly, then the tuber of pinellia thin slice of wetting is piled up in transparent porcelain jar, sealing is placed on the place that natural light is transmitted to, and it is small to stand 24
When, then penetrating fluid that tuber of pinellia thin slice is equipped with to 0.1 times of its weight is placed in pressure vessel, is suppressed in the case where pressure is 0.16MPa
20min, it is 6%% to take out thin slice and carry out infra-red drying to tuber of pinellia thin slice water content again, you can.
Embodiment 2
A kind of habitat processing method of the fresh tuber of pinellia, it comprises the following steps：
1., take the fresh tuber of pinellia, decortication is cleaned, and cuts into the thick pieces of 6mm, is uniformly pricked first in tuber of pinellia sheet surface with pin small
Hole, small hole number 5, hole diameter 2mm；
2., 1. step is handled after tuber of pinellia thin slice with 150 DEG C of water vapours fumigate 60s, then by tuber of pinellia thin slice immerse it is dense
Spend in the glucose solution for 40%, soak 60min, take out tuber of pinellia thin slice infra-red drying 10min, glucose solution filtering is standby
With；
3., in parts by weight, take step 2. middle 5 parts of the glucose solution for soaking tuber of pinellia thin slice, 20 parts of ethylenediamine tetrems
Acid disodium, 7 parts of aspartic acids, 50 parts of water mixing, stir to solution is transparent and penetrating fluid are made；
4., penetrating fluid is placed in sprayer, uniformly spray dried tuber of pinellia thin slice, be sprayed onto tuber of pinellia thin slice and moisten completely
Thoroughly, then the tuber of pinellia thin slice of wetting is piled up in transparent porcelain jar, sealing is placed on the place that natural light is transmitted to, and stands 24-
36 hours, then penetrating fluid that tuber of pinellia thin slice is equipped with to 0.5 times of its weight was placed in pressure vessel, in the case where pressure is 0.18MPa
30min is suppressed, thin slice is taken out and carries out infra-red drying again to tuber of pinellia thin slice water content 8%, you can.
Embodiment 3
A kind of habitat processing method of the fresh tuber of pinellia, it comprises the following steps：
1., take the fresh tuber of pinellia, decortication is cleaned, and is cut into the thick pieces of 5.5mm, is uniformly pricked first in tuber of pinellia sheet surface with pin
Aperture, small hole number 4, hole diameter 1.8mm；
2., 1. step is handled after tuber of pinellia thin slice with 140 DEG C of water vapours fumigate 45s, then by tuber of pinellia thin slice immerse it is dense
Spend in the glucose solution for 40%, soak 50min, take out tuber of pinellia thin slice infra-red drying 8min, glucose solution filtering is standby；
3., in parts by weight, take step 2. middle 4 parts of the glucose solution for soaking tuber of pinellia thin slice, 16.5 parts of ethylenediamine tetraacetics
Acetic acid disodium, 6 parts of aspartic acids, 40 parts of water mixing, stir to solution is transparent and penetrating fluid are made；
4., penetrating fluid is placed in sprayer, uniformly spray dried tuber of pinellia thin slice, be sprayed onto tuber of pinellia thin slice and moisten completely
Thoroughly, then the tuber of pinellia thin slice of wetting is piled up in transparent porcelain jar, sealing is placed on the place that natural light is transmitted to, and it is small to stand 30
When, then penetrating fluid that tuber of pinellia thin slice is equipped with to 0.3 times of its weight is placed in pressure vessel, is suppressed in the case where pressure is 0.17MPa
25min, take out thin slice and carry out infra-red drying again to tuber of pinellia thin slice water content 4%, you can.
Test example 1
Influence of the tuber of pinellia surface hole diameter to aspartate content and calcium oxalate crystal content
For reagent material：Pick up from the Gansu Province Longnan City Xihe County tuber of pinellia [Pinelliaternatat (Thunb.) Breit.]
Dry tuber is the primary tuber of pinellia.
Test method：The fresh tuber of pinellia is taken, decortication is cleaned, and is cut into the thick pieces of 5.5mm, is taken 10, numbering 1-10
Respectively 10 tuber of pinellia sheet surfaces uniformly with pin prick aperture, small hole number 4, hole diameter be respectively 1mm,
1.1mm, 1.2,1.3mm, 1.4mm, 1.5mm, 1.6mm, 1.7mm, 1.8mm, 1.9mm, 2.0mm, then by above-mentioned 10 tablets of tuber of pinellia
3. thin slice is handled by the step of embodiment 3, the content of the aspartic acid in tuber of pinellia thin slice is determined after processing.
Method for measuring：
1st, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, is extracted by 75% ethanol water bath refluxing extraction, ether
Remove the operations such as miscellaneous, hydrochloric acid constant volume and obtain sample detection liquid, aspartic acid detection is carried out using automatic amino acid analyzer, passed through
The content for determining aspartic acid in the tuber of pinellia of primary crude drug is 22.45 μ g/100g
2nd, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, using high performance liquid chromatography, with 0.5% phosphoric acid water
Solution is mobile phase, using oxalic acid as reference substance, is measured.
Measurement result is as shown in table 1
Table 1
As it can be seen from table 1 generally, tuber of pinellia surface hole diameter is stepped up from 1.0mm-2.0mm so that in the tuber of pinellia
The spill-out of aspartic acid be stepped up, calcium oxalate crystal content is gradually reducing, when aperture is 1.5mm tuber of pinellia asparagus fern ammonia
The spill-out of acid and the tuber of pinellia spill-out in 1-1.4mm apertures are without larger difference, but calcium oxalate crystal content substantially reduces, for
Although tuber of pinellia thin slice calcium oxalate crystal spilling of the aperture more than 1.5mm is more, the aspartic acid in tuber of pinellia cell contains simultaneously
Amount is greatly reduced, therefore, it can be deduced that when aperture is 1.5mm, the aspartic acid in the tuber of pinellia overflows less, and calcium oxalate crystal contains
Amount substantially reduces, and the stimulation toxicity of the tuber of pinellia reduces.
Test example 2
Different glucose solution is for the brilliant influence with aspartate content of tuber of pinellia calcium oxalate crystal growth in healthy
For reagent material：Pick up from the Gansu Province Longnan City Xihe County tuber of pinellia [Pinelliaternatat (Thunb.) Breit.]
Dry tuber is the primary tuber of pinellia.
Test method：The fresh tuber of pinellia is taken, decortication is cleaned, and cuts into the thick pieces of 5.5mm, takes 5, numbering 1-5 distinguishes 5 half
Summer sheet surface uniformly with pin prick aperture, small hole number 4, hole diameter 1.5mm, respectively select 20%, 30%, 40%,
50%th, 2. the glucose solution of 60% concentration is operated by the step of embodiment 3, detects the calcium oxalate crystal in tuber of pinellia thin slice
With the content of aspartic acid.
Assay method
Method for measuring：
1st, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, is extracted by 75% ethanol water bath refluxing extraction, ether
Remove the operations such as miscellaneous, hydrochloric acid constant volume and obtain sample detection liquid, aspartic acid detection is carried out using automatic amino acid analyzer, passed through
The content for determining aspartic acid in the tuber of pinellia of primary crude drug is 22.38 μ g/100g
2nd, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, using high performance liquid chromatography, with 0.5% phosphoric acid water
Solution is mobile phase, using oxalic acid as reference substance, is measured.
Measurement result is shown in Table 2
Influence of the different glucose solution of table 2 to tuber of pinellia Calcium Oxalate and aspartic acid
As known from Table 2, with the increase of concentration of glucose, the content of calcium oxalate crystal and aspartic acid in tuber of pinellia cell
Gradually reducing, because the concentration increase of glucose solution forms hypertonic solution, immersion causes moisture in tuber of pinellia cell and each
Amino acid and other chemical compositions in kind cell constantly ooze out, and then cell is shunk, and are less than 40% in concentration of glucose
When glucose solution concentration be not up to hypertonic solution, so tuber of pinellia cell does not shrink, cell various composition is not sent out
Changing, when glucose concentration is more than 40%, tuber of pinellia cell not only seriously shrinks, and the various chemical substances in cell are lost in
Seriously, hence it is evident that learning, when glucose concentration is 40%, the oxalic acid calcium content in cell substantially reduces, asparagus fern ammonia
Sour number of dropouts is also smaller.
Test example 3
Different penetrating fluids match the influence to tuber of pinellia Calcium Oxalate and aspartate content
For reagent material：Pick up from the Gansu Province Longnan City Xihe County tuber of pinellia [Pinelliaternatat (Thunb.) Breit.]
Dry tuber is the primary tuber of pinellia.
Influence of the penetrating fluid of the different ratio of table 3 (parts by weight) to tuber of pinellia Calcium Oxalate and aspartate content
Test method：The fresh tuber of pinellia is taken, decortication is cleaned, and is cut into the thick pieces of 5.5mm, is taken 5, numbering 1-5
5 tuber of pinellia sheet surfaces uniformly prick aperture, small hole number 4, hole diameter 1.5mm, by the tuber of pinellia with pin respectively
Handled according to the processing step described in embodiment 3, different disposal is that the proportioning of penetrating fluid is different.
Method for measuring：
1st, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, is extracted by 75% ethanol water bath refluxing extraction, ether
Remove the operations such as miscellaneous, hydrochloric acid constant volume and obtain sample detection liquid, aspartic acid detection is carried out using automatic amino acid analyzer, passed through
The content for determining aspartic acid in the tuber of pinellia of primary crude drug is 22.33 μ g/100g
2nd, it is raw material by the tuber of pinellia thin slice after above-mentioned 10 processing, using high performance liquid chromatography, with 0.5% phosphoric acid water
Solution is mobile phase, using oxalic acid as reference substance, is measured.
Measurement result is as shown in table 4 below
Influence of the penetrating fluid solubility of the different ratio of table 4 to tuber of pinellia calcium oxalate crystal and aspartate content
As known from Table 4, the proportioning difference of penetrating fluid result in containing for calcium oxalate crystal in tuber of pinellia finished product and aspartic acid
Measure it is different, when 4 parts of 6 parts of 16.5 parts of disodium ethylene diamine tetraacetate, aspartic acid, glucose solution, the water 40 in penetrating fluid
Aspartate content highest during part in tuber of pinellia finished product, while calcium oxalate crystal content is relatively low.
Claims (3)
- A kind of 1. habitat processing method of the fresh tuber of pinellia, it is characterised in that：Comprise the following steps：1., take the fresh tuber of pinellia, decortication is cleaned, and cuts into the thick pieces of 5-6mm, is uniformly pricked first in tuber of pinellia sheet surface with pin small Hole, small hole number 4-5, hole diameter 1.5-2mm；2., 1. step is handled after 120-150 DEG C of water vapour of tuber of pinellia thin slice fumigate 30-60s, then tuber of pinellia thin slice is immersed Concentration is in 40% glucose solution, soaks 40-60min, takes out tuber of pinellia thin slice infra-red drying 5-10min, glucose solution Filter standby；3., in parts by weight, take step 2. middle glucose solution 2-5 parts for soaking tuber of pinellia thin slice, 15-20 part ethylenediamine tetrems Acid disodium, 5-7 parts aspartic acid, the mixing of 30-50 parts water, stir to solution is transparent and penetrating fluid are made；4., penetrating fluid is placed in sprayer, uniformly spray dried tuber of pinellia thin slice, be sprayed onto tuber of pinellia thin slice and run through completely, Then the tuber of pinellia thin slice of wetting is piled up in transparent porcelain jar, sealing is placed on the place that natural light is transmitted to, and it is small to stand 24-36 When, then tuber of pinellia thin slice is equipped with to the penetrating fluid of 0.1-0.5 times of its weightIt is placed in pressure vessel, 20-30min is suppressed in the case where pressure is 0.16-0.18MPa, takes out thin slice and carry out infrared do again It is dry to tuber of pinellia thin slice water content≤8%, you can.
- A kind of 2. habitat processing method of fresh tuber of pinellia according to claim 1, it is characterised in that：Step 1. middle hole diameter For 1.5mm.
- A kind of 3. habitat processing method of fresh tuber of pinellia according to claim 1, it is characterised in that：Step 3. in penetrating fluid In each parts by weight of raw material be：Soaked 4 parts of the glucose solution of tuber of pinellia thin slice, 16.5 parts of disodium ethylene diamine tetraacetates, 6 parts Aspartic acid, 40 parts of water.
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Application publication date: 20180105 |