CN107523226A - A kind of needle felt production is combined with binding agent - Google Patents
A kind of needle felt production is combined with binding agent Download PDFInfo
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- CN107523226A CN107523226A CN201710752059.XA CN201710752059A CN107523226A CN 107523226 A CN107523226 A CN 107523226A CN 201710752059 A CN201710752059 A CN 201710752059A CN 107523226 A CN107523226 A CN 107523226A
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- parts
- binding agent
- needle felt
- combined
- felt production
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
- C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Abstract
The invention discloses a kind of needle felt production to be combined with binding agent, and needle felt production includes the raw material of following parts by weight with binding agent combination：5~10 parts of starch, 5~10 parts of malt extract, 5~8 parts of hydroxyethyl methacrylate, 5~8 parts of hydroxy propyl methacrylate, 10~20 parts of paraffin, 8~13 parts of pine tar, 1~3 part of mould inhibitor, 2~5 parts of nano magnesia, 2~4 parts of nano zine oxide, 50~60 parts of 10~15 parts of rubber oil and glycerine, environment-friendly type material is applied in combination with binding agent in needle felt production of the present invention, the environmentally friendly binding agent of preparation is nontoxic, requirement of the green aspect to product can be met, greatly reduce pollution and the introducing of harmful substance, production technology safety, the construction operation time is short, environment friendly and pollution-free environment, construction technology is simple, it is highly reliable, water resistance is good, application life is grown, binding agent fungus and mildew resistance is good, stability and dispersive property are high, bond properties is good.
Description
Technical field
The present invention relates to binding agent technology field, and in particular to a kind of needle felt production is combined with binding agent.
Background technology
The heat-insulating material industry of China is based on glassy state fibrous material, such as mineral wool, rock mineral wool, aluminium silicate wool
Deng accounting for more than the 80% of national yield, annual estimated output in 2015 reaches 700~8,000,000 tons.By glassy state fibrous material
Manufactured various heat-insulating material products, it is necessary to add binding agent, be coupled to each other with reaching interfibrous.Bonding main at present
Agent is thermosetting resin, such as phenolic resin, Lauxite, acrylic resin, and its content accounts for the 3~5% of heat-insulating material total amount,
About 35~400,000 tons, its value accounts for 1/4 or so of the heat-insulating material gross output value.
There is problems with for existing thermosetting resin：Phenol, formaldehyde, acrylate are its primary raw materials, these things
Matter can cause certain pollution, particularly formaldehyde to environment, be the polluter that country keeps under strict control.Thermosetting resin is in heat-insulating material
Production in, have part volatilize at high temperature, pollute environment, there is no effective control method at present.Heat-insulating material is using process
In, it the harmful substance such as the free formaldehyde of residual, phenol, can be sustained in air, harm is produced to environment, human body.
The content of the invention
To solve the above problems, the present invention proposes that a kind of needle felt production is combined with binding agent.
To realize the object of the invention, the technical scheme of use is：A kind of needle felt production is combined with binding agent, Nomex life
Production includes the raw material of following parts by weight with binding agent combination：5~10 parts of starch, 5~10 parts of malt extract, hydroxyethyl methacrylate
5~8 parts of ethyl ester, 5~8 parts of hydroxy propyl methacrylate, 10~20 parts of paraffin, 8~13 parts of pine tar, 1~3 part of mould inhibitor, receive
50~60 parts of 2~5 parts of magnesia of rice, 2~4 parts of nano zine oxide and glycerine.
Preferably, 10~15 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Preferably, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar, the constant temperature at 50~60 DEG C to convolution internal mixer
Stirring occurs without emulsion to well mixed；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking 30~60min of graft reaction under the conditions of being 30~40 DEG C in temperature, are made mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 50~60 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is done at being 90~100 DEG C in temperature
It is dry, dry to mixed slurry and be changed into sticky paste by liquid condition；
5) paste of step 4 is transferred to 60~100min of high-speed stirred in mixer by, and needle felt production is made and uses and glues
Tie agent combination.
Preferably, the stirring of the mixer that circles round in the production craft step 1 that the needle felt production is combined with binding agent
Speed is arranged to 500~800r/min.
Preferably, the stirring of the mixer that circles round in the production craft step 2 that the needle felt production is combined with binding agent
Speed is arranged to 1000~1500r/min.
Preferably, the stirring of the mixer that circles round in the production craft step 5 that the needle felt production is combined with binding agent
Speed is arranged to 1500~3000r/min.
Beneficial effects of the present invention are：Environment-friendly type material is applied in combination with binding agent in needle felt production of the present invention, preparation
Environmentally friendly binding agent is nontoxic, can meet requirement of the green aspect to product, greatly reduces pollution and harmful substance
Introduce, production technology safety, the construction operation time is short, and environment friendly and pollution-free environment, construction technology is simple, highly reliable, water proofing property
Can be good, application life length, binding agent fungus and mildew resistance is good, stability and dispersive property are high, bond properties is good, mechanicalness after bonding
Firmly it can be not easy to come off.
Brief description of the drawings
Fig. 1 is needle felt production binding agent combination raw materials proportioning table of the present invention.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made
Embodiment, belong to the scope of protection of the invention.
Embodiment 1
A kind of needle felt production is combined with binding agent, and needle felt production includes the original of following parts by weight with binding agent combination
Material：5 parts of starch, 5 parts of malt extract, 5 parts of hydroxyethyl methacrylate, 5 parts of hydroxy propyl methacrylate, 10 parts of paraffin, pine tar 8
Part, 1 part of mould inhibitor, 2 parts of nano magnesia, 2 parts of nano zine oxide and 60 parts of glycerine.
Wherein, 15 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Wherein, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, with 800r/ at 50 DEG C
Min stir speed (S.S.) constant temperature stirs to well mixed and occurs without emulsion；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking graft reaction 60min after stir speed (S.S.) is 1000r/min, system are lifted under the conditions of being 40 DEG C in temperature
Obtain mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 60 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 90 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred in mixer with 3000r/min stir speed (S.S.) high-speed stirred 60min, system by
Needle felt production is obtained to be combined with binding agent.
Embodiment 2
A kind of needle felt production is combined with binding agent, and needle felt production includes the original of following parts by weight with binding agent combination
Material：5 parts of starch, 5 parts of malt extract, 8 parts of hydroxyethyl methacrylate, 8 parts of hydroxy propyl methacrylate, 20 parts of paraffin, pine tar 8
Part, 1 part of mould inhibitor, 2 parts of nano magnesia, 3 parts of nano zine oxide and 60 parts of glycerine.
Wherein, 10 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Wherein, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, with 500r/ at 50 DEG C
Min stir speed (S.S.) constant temperature stirs to well mixed and occurs without emulsion；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking graft reaction 30min after stir speed (S.S.) is 1500r/min, system are lifted under the conditions of being 30 DEG C in temperature
Obtain mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 50 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 100 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred in mixer with 3000r/min stir speed (S.S.) high-speed stirred 100min by,
Needle felt production is made to be combined with binding agent.
Embodiment 3
A kind of needle felt production is combined with binding agent, and needle felt production includes the original of following parts by weight with binding agent combination
Material：5 parts of starch, 10 parts of malt extract, 8 parts of hydroxyethyl methacrylate, 8 parts of hydroxy propyl methacrylate, 10 parts of paraffin, pine are burnt
50 parts of 10 parts of oil, 1 part of mould inhibitor, 35 parts of nano magnesia, 3 parts of nano zine oxide and glycerine.
Wherein, 15 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Wherein, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, with 800r/ at 55 DEG C
Min stir speed (S.S.) constant temperature stirs to well mixed and occurs without emulsion；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking graft reaction 60min after stir speed (S.S.) is 1500r/min, system are lifted under the conditions of being 35 DEG C in temperature
Obtain mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 60 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 100 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred in mixer with 3000r/min stir speed (S.S.) high-speed stirred 80min, system by
Needle felt production is obtained to be combined with binding agent.
Embodiment 4
A kind of needle felt production is combined with binding agent, and needle felt production includes the original of following parts by weight with binding agent combination
Material：8 parts of starch, 8 parts of malt extract, 8 parts of hydroxyethyl methacrylate, 8 parts of hydroxy propyl methacrylate, 15 parts of paraffin, pine tar
55 parts of 12 parts, 2 parts of mould inhibitor, 2 parts of nano magnesia, 2 parts of nano zine oxide and glycerine.
Wherein, 12 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Wherein, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, with 500r/ at 60 DEG C
Min stir speed (S.S.) constant temperature stirs to well mixed and occurs without emulsion；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking graft reaction 50min after stir speed (S.S.) is 1500r/min, system are lifted under the conditions of being 30 DEG C in temperature
Obtain mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 55 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 95 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred in mixer with 2000r/min stir speed (S.S.) high-speed stirred 80min, system by
Needle felt production is obtained to be combined with binding agent.
Embodiment 5
A kind of needle felt production is combined with binding agent, and needle felt production includes the original of following parts by weight with binding agent combination
Material：10 parts of starch, 10 parts of malt extract, 5 parts of hydroxyethyl methacrylate, 5 parts of hydroxy propyl methacrylate, 10 parts of paraffin, pine are burnt
60 parts of 13 parts of oil, 1 part of mould inhibitor, 2 parts of nano magnesia, 2 parts of nano zine oxide and glycerine.
Wherein, 15 parts of rubber oil is also added with during the needle felt production is combined with binding agent.
Wherein, the production technology that the needle felt production is combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, with 600r/ at 60 DEG C
Min stir speed (S.S.) constant temperature stirs to well mixed and occurs without emulsion；
2) starch, malt extract, hydroxyethyl methacrylate, methacrylic acid hydroxypropyl are added in mixing oil bodies of the to step 1
Ester and paraffin, stirring crosslinking graft reaction 50min after stir speed (S.S.) is 1500r/min, system are lifted under the conditions of being 40 DEG C in temperature
Obtain mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, add mould inhibitor,
Nano magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 50 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 95 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred in mixer with 2500r/min stir speed (S.S.) high-speed stirred 100min by,
Needle felt production is made to be combined with binding agent.
In the present invention, environment-friendly type material is applied in combination with binding agent in needle felt production of the present invention, and the environmental protection of preparation bonds
Agent is nontoxic, can meet requirement of the green aspect to product, greatly reduces pollution and the introducing of harmful substance, production
Process safety, the construction operation time is short, and environment friendly and pollution-free environment, construction technology is simple, highly reliable, and water resistance is good, application
Long lifespan, binding agent fungus and mildew resistance is good, stability and dispersive property are high, bond properties is good, after bonding mechanical performance firmly and
Do not allow easy to fall off.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of needle felt production is combined with binding agent, it is characterised in that：Needle felt production binding agent combination includes following heavy
Measure the raw material of number：5~10 parts of starch, 5~10 parts of malt extract, 5~8 parts of hydroxyethyl methacrylate, methacrylic acid hydroxypropyl
5~8 parts of ester, 10~20 parts of paraffin, 8~13 parts of pine tar, 1~3 part of mould inhibitor, 2~5 parts of nano magnesia, nano zine oxide 2
~4 parts and 50~60 parts of glycerine.
2. a kind of needle felt production according to claim 1 is combined with binding agent, it is characterised in that：The needle felt production
10~15 parts of rubber oil is also added with being combined with binding agent.
3. a kind of needle felt production according to claim 1 is combined with binding agent, it is characterised in that：The needle felt production
The production technology combined with binding agent is as follows：
1) adds partial glycerol, whole rubber oil and pine tar to convolution internal mixer, and constant temperature stirs at 50~60 DEG C
Emulsion is occurred without to well mixed；
2) in mixing oil bodies of the to step 1 add starch, malt extract, hydroxyethyl methacrylate, hydroxy propyl methacrylate and
Paraffin, stirring crosslinking 30~60min of graft reaction under the conditions of being 30~40 DEG C in temperature, is made mixed slurry；
3) will add the glycerine of remainder in the mixed slurry of step 2, be uniformly mixed, and add mould inhibitor, nanometer
Magnesia and nano zine oxide, constant temperature is stirred to mixed slurry to micro- sticky state at 50~60 DEG C；
4) mixed slurry of step 3 is delivered in drying machine by carries out pre-gelatinized and is dried at being 90~100 DEG C in temperature, does
It is dry to be changed into sticky paste by liquid condition to mixed slurry；
5) paste of step 4 is transferred to 60~100min of high-speed stirred in mixer, obtained needle felt production binding agent by
Combination.
4. a kind of needle felt production according to claim 3 is combined with binding agent, it is characterised in that：The needle felt production
The stir speed (S.S.) of convolution mixer in the production craft step 1 combined with binding agent is arranged to 500~800r/min.
5. a kind of needle felt production according to claim 3 is combined with binding agent, it is characterised in that：The needle felt production
The stir speed (S.S.) of convolution mixer in the production craft step 2 combined with binding agent is arranged to 1000~1500r/min.
6. a kind of needle felt production according to claim 3 is combined with binding agent, it is characterised in that：The needle felt production
The stir speed (S.S.) of convolution mixer in the production craft step 5 combined with binding agent is arranged to 1500~3000r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710752059.XA CN107523226A (en) | 2017-08-28 | 2017-08-28 | A kind of needle felt production is combined with binding agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710752059.XA CN107523226A (en) | 2017-08-28 | 2017-08-28 | A kind of needle felt production is combined with binding agent |
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| Publication Number | Publication Date |
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| CN107523226A true CN107523226A (en) | 2017-12-29 |
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| CN201710752059.XA Pending CN107523226A (en) | 2017-08-28 | 2017-08-28 | A kind of needle felt production is combined with binding agent |
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Citations (6)
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| CN103857763A (en) * | 2011-07-27 | 2014-06-11 | 圣戈班伊索福公司 | Sizing composition for mineral wool based on maltitol and insulating products obtained |
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2017
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| CN101845113A (en) * | 2003-06-12 | 2010-09-29 | 阿克苏诺贝尔公司 | Glass adhesion promoter |
| CN101130677A (en) * | 2006-08-24 | 2008-02-27 | 罗门哈斯公司 | Curable composition |
| CN102850956A (en) * | 2011-06-30 | 2013-01-02 | 罗门哈斯公司 | Aqueous curable binder composition |
| CN103857763A (en) * | 2011-07-27 | 2014-06-11 | 圣戈班伊索福公司 | Sizing composition for mineral wool based on maltitol and insulating products obtained |
| CN102993988A (en) * | 2012-11-13 | 2013-03-27 | 铜陵国方水暖科技有限责任公司 | Adhesive with strong adhering property |
| CN106928908A (en) * | 2017-02-19 | 2017-07-07 | 广州市芯检康生物科技有限公司 | A kind of new aeroge multifunctional material and preparation method thereof |
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