CN107523213A - A kind of preparation method of decoration thermal insulation coatings - Google Patents
A kind of preparation method of decoration thermal insulation coatings Download PDFInfo
- Publication number
- CN107523213A CN107523213A CN201710770392.3A CN201710770392A CN107523213A CN 107523213 A CN107523213 A CN 107523213A CN 201710770392 A CN201710770392 A CN 201710770392A CN 107523213 A CN107523213 A CN 107523213A
- Authority
- CN
- China
- Prior art keywords
- parts
- thermal insulation
- insulation coatings
- dicyandiamide
- diatomite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/085—Copper
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Building Environments (AREA)
Abstract
This application discloses a kind of preparation method of decoration thermal insulation coatings, deionized water, sodium hydroxide, diatomite, octanol, hydrochloric acid, Firebrake ZB, dicyandiamide, copper powder, scale graphite, ethanol, polyvinyl alcohol, urea, butanone, t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene are weighed；Preparation method is simple, high insulating effect, 15 25 μm of fineness, good flame retardation effect, and resistance to 400 600 DEG C of high temperature is not fallen off, and resistance to moisture is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, wall, metal, timber and plastics is not corroded, paint film is smooth, scrubbing resistance 2,000 2200 times, hardness 5H；Do not peel in the 8d of water resistance 4, not dry linting, fast drying, surface drying 80 100min, pliability 1mm, glossiness is good；Soak that 3 7d are non-foaming, do not ftracture in sodium chloride solution, low-temperature stability is good, does not condense, does not lump, does not separate.
Description
Technical field
The application belongs to decoration material field, more particularly to a kind of preparation method of decoration thermal insulation coatings.
Background technology
Insulation material generally refers to the material that thermal conductivity factor is less than or equal to 0.12.Insulation material have developed rapidly, in industry
With good heat preservation technology and material are used in building, can often play a multiplier effect.One ton is often used in building
Mineral wool insulating product, one ton of oil can be saved within 1 year.
Developed Background：Traditional heat preserving and insulating material is to improve gas phase voidage, reduces thermal conductivity factor and the coefficient of conductivity
Based on.In use environment convection heat transfer' heat-transfer by convection and radiant heat transfer will raise fiber-like insulation material, it is necessary to have thicker coating；
And section bar class inorganic heat insulation material will carry out assembling construction, there is that seam is more, damages attractive in appearance, water proofing property is poor, service life is short etc.
Defect.Therefore, people are seeking with studying a kind of new material that can greatly improve insulation material heat insulating reflecting performance always.
The organic hard aluminium foil froth pulp of phenolic foam material category macromolecule, formed by thermosetting phenolic resin foaming,
There is lightweight, fire prevention, chance naked light not to burn, be smokeless, be nontoxic, without dripping off for it, and temperature in use is enclosed extensively（- 196~+200 DEG C）Low temperature
Do not shunk under environment, be not brittle, being the preferable heat-insulating material of HVAC Refrigeration Engineering, because phenol formaldehyde foam rate of closed hole is high, then heat conduction
Coefficient is low, and heat-proof quality is good, and has a water resisting property and water vapour permeability, is preferable heat insulating energy saving material.Because phenolic aldehyde has
There is benzene ring structure, so dimensionally stable, rate of change<1%.And chemical composition stability, anti-corrosion is anti-aging, is particularly resistant to organic molten
Liquid, strong acid, weak base corrosion.Foaming agent is made without freon meet International Environmental Protection standard, and its molecule in production technology foaming
Containing hydrogen, oxygen, carbon in structure, during pyrolytic, the gas of spilling is nontoxic, tasteless, harmless to human body, environment, meets
National green environmental requirement.So the super composite plate of phenolic aldehyde is optimal fire prevention, adiabatic, energy-conservation, environment-friendly and green attractive in appearance guarantor
Adiabator.
Phenol formaldehyde foam is known as the laudatory title of " king of insulation material ", is insulated fire acoustic material of new generation.In developed country
Pnenolic aldehyde foam material is quickly grown, and is widely used to the fields such as building, national defence, foreign trade, storage, the energy.U.S.'s construction industry
In sound-insulating foamed plastics used, phenolic materials have accounted for 40%；Japan has also set up phenol formaldehyde foam popularization association to promote this
Kind new material.
Most promising a kind of heat insulating material in the building ranks that phenol formaldehyde foam is still generally acknowledged in the world.Cause
For the material that this new material obtains with common macromolecule resin by addition fire retardant has the difference of essence, in fire not
Burning, it is non-fusible, toxic smog will not be also distributed, and it is excellent with light, nontoxic, corrosion-free, insulation, energy-conservation, sound insulation, inexpensive etc.
Point, and being foamed without freon, non-environmental-pollution, processability are good, easy for construction, its combination property be various insulation materials without
Method analogy.Being common to advanced and central air-conditioning system of high-rise building the insulation such as hotel, apartment, hospital, (the advanced of Hong Kong is built
Building central air conditioner system, majority uses phenolic foam material instead).To refrigeration, the cold insulation of freezer and for industry such as petrochemical industries
The insulation of pipeline and equipment, building partition, outer wall composite board, suspended ceiling, abatvoix etc. have incontrovertible comprehensive advantage,
It is undesirable to solve other organic material fire protecting performances, and inorganic material water absorption rate it is big, easily " condensation ", construction when skin thorn
The problems such as itching, it is air-conditioning system, the optimal insulation material of the third generation of various electrical equipment.
The content of the invention
The technical problem of solution：
The application is directed to above-mentioned technical problem, there is provided a kind of preparation method of decoration thermal insulation coatings, solves existing decoration and protects
The technical problems such as thermo-paint poor water resistance, heat insulation effect difference and corrosion-resistant.
Technical scheme：
A kind of preparation method of decoration thermal insulation coatings, comprises the following steps：
The first step：100 parts of deionized water, sodium hydroxide 0.1-0.5 parts, diatomite 2-6 parts, pungent is weighed according to parts by weight proportioning
Alcohol 1.5-1.9 parts, hydrochloric acid 1-1.4 parts, Firebrake ZB 1-5 parts, dicyandiamide 1.1-1.5 parts, copper powder 1-20 parts, scale graphite 5-25
Part, ethanol 10-30 parts, polyvinyl alcohol 10-30 parts, urea 2-6 parts, butanone 11-15 parts, t etram-ethyltetravinylcyclotetrasiloxane
20-40 parts and silicone oil dimethylbenzene 0.4-0.8 parts；
Second step：Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5-25min, adds salt
Acid, Firebrake ZB, dicyandiamide and copper powder, stir 60-80min under 65-75 DEG C of condition of water bath heating, then with scale graphite, ethanol
Put into together in reactor with polyvinyl alcohol, open mixer mixing, be warming up to 80-100 DEG C, mixing velocity 350-450r/
Min, mix 20-40min；
3rd step：Surplus stock is added, regulation mixing velocity to 800-1000 r/min, mixes 2-4h, finally will be well mixed
Product input sand mill in, be sanded 30-40min produce.
As a preferred technical solution of the present invention：The raw material of decoration thermal insulation coatings is by weight in the first step
Number proportioning is as follows：100 parts of deionized water, 0.1 part of sodium hydroxide, 2 parts of diatomite, 1.5 parts of octanol, 1 part of hydrochloric acid, 1 part of Firebrake ZB,
1.1 parts of dicyandiamide, 1 part of copper powder, 5 parts of scale graphite, 10 parts of ethanol, 10 parts of polyvinyl alcohol, 2 parts of urea, 11 parts of butanone, tetramethyl
0.4 part of 20 parts of tetravinyl cyclotetrasiloxane and silicone oil dimethylbenzene.
As a preferred technical solution of the present invention：The raw material of decoration thermal insulation coatings is by weight in the first step
Number proportioning is as follows：100 parts of deionized water, 0.5 part of sodium hydroxide, 6 parts of diatomite, 1.9 parts of octanol, 1.4 parts of hydrochloric acid, Firebrake ZB 5
Part, 1.5 parts of dicyandiamide, 20 parts of copper powder, 25 parts of scale graphite, 30 parts of ethanol, 30 parts of polyvinyl alcohol, 6 parts of urea, 15 parts of butanone,
0.8 part of 40 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
As a preferred technical solution of the present invention：The raw material of decoration thermal insulation coatings is by weight in the first step
Number proportioning is as follows：100 parts of deionized water, 0.2 part of sodium hydroxide, 3 parts of diatomite, 1.6 parts of octanol, 1.1 parts of hydrochloric acid, Firebrake ZB 2
Part, 1.2 parts of dicyandiamide, 5 parts of copper powder, 10 parts of scale graphite, 15 parts of ethanol, 15 parts of polyvinyl alcohol, 3 parts of urea, 12 parts of butanone, four
0.5 part of 25 parts of methyl tetravinyl cyclotetrasiloxane and silicone oil dimethylbenzene.
As a preferred technical solution of the present invention：The raw material of decoration thermal insulation coatings is by weight in the first step
Number proportioning is as follows：100 parts of deionized water, 0.4 part of sodium hydroxide, 5 parts of diatomite, 1.8 parts of octanol, 1.3 parts of hydrochloric acid, Firebrake ZB 4
Part, 1.4 parts of dicyandiamide, 15 parts of copper powder, 20 parts of scale graphite, 25 parts of ethanol, 25 parts of polyvinyl alcohol, 5 parts of urea, 14 parts of butanone,
0.7 part of 35 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
As a preferred technical solution of the present invention：The raw material of decoration thermal insulation coatings is by weight in the first step
Number proportioning is as follows：100 parts of deionized water, 0.3 part of sodium hydroxide, 4 parts of diatomite, 1.7 parts of octanol, 1.2 parts of hydrochloric acid, Firebrake ZB 3
Part, 1.3 parts of dicyandiamide, 10 parts of copper powder, 15 parts of scale graphite, 20 parts of ethanol, 20 parts of polyvinyl alcohol, 4 parts of urea, 13 parts of butanone,
0.6 part of 30 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
Beneficial effect：
A kind of preparation method of decoration thermal insulation coatings of the present invention compared with prior art, is had using above technical scheme
Following technique effect：1st, preparation method is simple, high insulating effect, 15-25 μm of fineness, good flame retardation effect, resistance to 400-600 DEG C of high temperature
Do not fall off, resistance to moisture is excellent；2nd, intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, to wall, metal, timber
Do not corrode with plastics, paint film is smooth, scrubbing resistance 2000-2200 times, hardness 5H；3rd, do not peel in water resistance 4-8d, not dry linting,
Fast drying, surface drying 80-100min, pliability 1mm, glossiness are good；4th, immersion 3-7d is non-foaming in sodium chloride solution, does not open
Split, low-temperature stability is good, does not condense, does not lump, does not separate, and can extensively produce and constantly replace current material.
Embodiment
Embodiment 1:
100 parts of deionized water, 0.1 part of sodium hydroxide, 2 parts of diatomite, 1.5 parts of octanol, hydrochloric acid 1 are weighed according to parts by weight proportioning
Part, 1 part of Firebrake ZB, 1.1 parts of dicyandiamide, 1 part of copper powder, 5 parts of scale graphite, 10 parts of ethanol, 10 parts of polyvinyl alcohol, 2 parts of urea, fourth
0.4 part of 11 parts of ketone, 20 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5min, adds hydrochloric acid, boric acid
Zinc, dicyandiamide and copper powder, 60min is stirred under 65 DEG C of condition of water bath heating, then together with scale graphite, ethanol and polyvinyl alcohol
Put into reactor, open mixer mixing, be warming up to 80 DEG C, mixing velocity 350r/min, mix 20min.
Surplus stock is added, regulation mixing velocity to 800 r/min, mixes 2h, finally puts into well mixed product
In sand mill, 30min is sanded and produces.
Preparation method is simple, high insulating effect, 25 μm of fineness, good flame retardation effect, and resistance to 400 DEG C of high temperature is not fallen off, resistance to moisture
Property is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, wall, metal, timber and plastics is not corroded,
Paint film is smooth, scrubbing resistance 2000 times, hardness 5H；Do not peel in water resistance 4d, not dry linting, fast drying, surface drying 100min, pliability
1mm, glossiness are good；Immersion 3d is non-foaming in sodium chloride solution, does not ftracture, and low-temperature stability is good, does not condense, does not lump, no
Separation.
Embodiment 2:
100 parts of deionized water, 0.5 part of sodium hydroxide, 6 parts of diatomite, 1.9 parts of octanol, hydrochloric acid are weighed according to parts by weight proportioning
1.4 parts, 5 parts of Firebrake ZB, 1.5 parts of dicyandiamide, 20 parts of copper powder, 25 parts of scale graphite, 30 parts of ethanol, 30 parts of polyvinyl alcohol, urea 6
Part, 15 parts of butanone, 40 parts of t etram-ethyltetravinylcyclotetrasiloxane and 0.8 part of silicone oil dimethylbenzene.
Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5-25min, adds hydrochloric acid, boron
Sour zinc, dicyandiamide and copper powder, stir 60-80min under 65-75 DEG C of condition of water bath heating, then with scale graphite, ethanol and poly- second
Enol is put into reactor together, is opened mixer mixing, is warming up to 80-100 DEG C, mixing velocity 350-450r/min, mixes
Close 20-40min.
Surplus stock is added, regulation mixing velocity to 800-1000 r/min, mixes 2-4h, finally by well mixed production
In thing input sand mill, 30-40min is sanded and produces.
Preparation method is simple, high insulating effect, 15-25 μm of fineness, good flame retardation effect, and resistance to 400-600 DEG C of high temperature is not fallen off,
Resistance to moisture is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, to wall, metal, timber and plastics not
Corrosion, paint film is smooth, scrubbing resistance 2000-2200 times, hardness 5H；Do not peel in water resistance 4-8d, not dry linting, fast drying, surface drying
80-100min, pliability 1mm, glossiness are good；Immersion 3-7d is non-foaming in sodium chloride solution, does not ftracture, low-temperature stability
It is good, do not condense, do not lump, do not separate.
Embodiment 3:
100 parts of deionized water, 0.2 part of sodium hydroxide, 3 parts of diatomite, 1.6 parts of octanol, hydrochloric acid are weighed according to parts by weight proportioning
1.1 parts, 2 parts of Firebrake ZB, 1.2 parts of dicyandiamide, 5 parts of copper powder, 10 parts of scale graphite, 15 parts of ethanol, 15 parts of polyvinyl alcohol, urea 3
Part, 12 parts of butanone, 25 parts of t etram-ethyltetravinylcyclotetrasiloxane and 0.5 part of silicone oil dimethylbenzene.
Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5-25min, adds hydrochloric acid, boron
Sour zinc, dicyandiamide and copper powder, stir 60-80min under 65-75 DEG C of condition of water bath heating, then with scale graphite, ethanol and poly- second
Enol is put into reactor together, is opened mixer mixing, is warming up to 80-100 DEG C, mixing velocity 350-450r/min, mixes
Close 20-40min.
Surplus stock is added, regulation mixing velocity to 800-1000 r/min, mixes 2-4h, finally by well mixed production
In thing input sand mill, 30-40min is sanded and produces.
Preparation method is simple, high insulating effect, 15-25 μm of fineness, good flame retardation effect, and resistance to 400-600 DEG C of high temperature is not fallen off,
Resistance to moisture is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, to wall, metal, timber and plastics not
Corrosion, paint film is smooth, scrubbing resistance 2000-2200 times, hardness 5H；Do not peel in water resistance 4-8d, not dry linting, fast drying, surface drying
80-100min, pliability 1mm, glossiness are good；Immersion 3-7d is non-foaming in sodium chloride solution, does not ftracture, low-temperature stability
It is good, do not condense, do not lump, do not separate.
Embodiment 4:
100 parts of deionized water, 0.4 part of sodium hydroxide, 5 parts of diatomite, 1.8 parts of octanol, hydrochloric acid are weighed according to parts by weight proportioning
1.3 parts, 4 parts of Firebrake ZB, 1.4 parts of dicyandiamide, 15 parts of copper powder, 20 parts of scale graphite, 25 parts of ethanol, 25 parts of polyvinyl alcohol, urea 5
Part, 14 parts of butanone, 35 parts of t etram-ethyltetravinylcyclotetrasiloxane and 0.7 part of silicone oil dimethylbenzene.
Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5-25min, adds hydrochloric acid, boron
Sour zinc, dicyandiamide and copper powder, stir 60-80min under 65-75 DEG C of condition of water bath heating, then with scale graphite, ethanol and poly- second
Enol is put into reactor together, is opened mixer mixing, is warming up to 80-100 DEG C, mixing velocity 350-450r/min, mixes
Close 20-40min.
Surplus stock is added, regulation mixing velocity to 800-1000 r/min, mixes 2-4h, finally by well mixed production
In thing input sand mill, 30-40min is sanded and produces.
Preparation method is simple, high insulating effect, 15-25 μm of fineness, good flame retardation effect, and resistance to 400-600 DEG C of high temperature is not fallen off,
Resistance to moisture is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, to wall, metal, timber and plastics not
Corrosion, paint film is smooth, scrubbing resistance 2000-2200 times, hardness 5H；Do not peel in water resistance 4-8d, not dry linting, fast drying, surface drying
80-100min, pliability 1mm, glossiness are good；Immersion 3-7d is non-foaming in sodium chloride solution, does not ftracture, low-temperature stability
It is good, do not condense, do not lump, do not separate.
Embodiment 5:
100 parts of deionized water, 0.3 part of sodium hydroxide, 4 parts of diatomite, 1.7 parts of octanol, hydrochloric acid are weighed according to parts by weight proportioning
1.2 parts, 3 parts of Firebrake ZB, 1.3 parts of dicyandiamide, 10 parts of copper powder, 15 parts of scale graphite, 20 parts of ethanol, 20 parts of polyvinyl alcohol, urea 4
Part, 13 parts of butanone, 30 parts of t etram-ethyltetravinylcyclotetrasiloxane and 0.6 part of silicone oil dimethylbenzene.
Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 15min, adds hydrochloric acid, boric acid
Zinc, dicyandiamide and copper powder, 70min is stirred under 70 DEG C of condition of water bath heating, then together with scale graphite, ethanol and polyvinyl alcohol
Put into reactor, open mixer mixing, be warming up to 90 DEG C, mixing velocity 400r/min, mix 30min.
Surplus stock is added, regulation mixing velocity to 900 r/min, mixes 3h, finally puts into well mixed product
In sand mill, 35min is sanded and produces.
Preparation method is simple, high insulating effect, 15 μm of fineness, good flame retardation effect, and resistance to 600 DEG C of high temperature is not fallen off, resistance to moisture
Property is excellent；Intensity is high after product film forming, adhesion 1 grade, good corrosion resistance, wall, metal, timber and plastics is not corroded,
Paint film is smooth, scrubbing resistance 2200 times, hardness 5H；Do not peel in water resistance 8d, not dry linting, fast drying, surface drying 80min, pliability
1mm, glossiness are good；Immersion 7d is non-foaming in sodium chloride solution, does not ftracture, and low-temperature stability is good, does not condense, does not lump, no
Separation.
Composition all components in above example can be with commercially available.
The above embodiments are intended to illustrate the present invention, rather than limitation, therefore with the present invention's
Any change in claims suitable implication and scope, all it is considered as being included within the scope of the claims.
Claims (6)
1. a kind of preparation method of decoration thermal insulation coatings, it is characterised in that comprise the following steps：
The first step：100 parts of deionized water, sodium hydroxide 0.1-0.5 parts, diatomite 2-6 parts, pungent is weighed according to parts by weight proportioning
Alcohol 1.5-1.9 parts, hydrochloric acid 1-1.4 parts, Firebrake ZB 1-5 parts, dicyandiamide 1.1-1.5 parts, copper powder 1-20 parts, scale graphite 5-25
Part, ethanol 10-30 parts, polyvinyl alcohol 10-30 parts, urea 2-6 parts, butanone 11-15 parts, t etram-ethyltetravinylcyclotetrasiloxane
20-40 parts and silicone oil dimethylbenzene 0.4-0.8 parts；
Second step：Deionized water, sodium hydroxide, diatomite and octanol are put into grinder and grind 5-25min, adds salt
Acid, Firebrake ZB, dicyandiamide and copper powder, stir 60-80min under 65-75 DEG C of condition of water bath heating, then with scale graphite, ethanol
Put into together in reactor with polyvinyl alcohol, open mixer mixing, be warming up to 80-100 DEG C, mixing velocity 350-450r/
Min, mix 20-40min；
3rd step：Surplus stock is added, regulation mixing velocity to 800-1000 r/min, mixes 2-4h, finally will be well mixed
Product input sand mill in, be sanded 30-40min produce.
A kind of 2. preparation method of decoration thermal insulation coatings according to claim 1, it is characterised in that：In the first step
The raw materials by weight portion proportioning of decoration thermal insulation coatings is as follows：100 parts of deionized water, 0.1 part of sodium hydroxide, 2 parts of diatomite,
1.5 parts of octanol, 1 part of hydrochloric acid, 1 part of Firebrake ZB, 1.1 parts of dicyandiamide, 1 part of copper powder, 5 parts of scale graphite, 10 parts of ethanol, polyvinyl alcohol
0.4 part of 10 parts, 2 parts of urea, 11 parts of butanone, 20 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
A kind of 3. preparation method of decoration thermal insulation coatings according to claim 1, it is characterised in that：In the first step
The raw materials by weight portion proportioning of decoration thermal insulation coatings is as follows：100 parts of deionized water, 0.5 part of sodium hydroxide, 6 parts of diatomite,
1.9 parts of octanol, 1.4 parts of hydrochloric acid, 5 parts of Firebrake ZB, 1.5 parts of dicyandiamide, 20 parts of copper powder, 25 parts of scale graphite, 30 parts of ethanol, poly- second
0.8 part of 30 parts of enol, 6 parts of urea, 15 parts of butanone, 40 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
A kind of 4. preparation method of decoration thermal insulation coatings according to claim 1, it is characterised in that：In the first step
The raw materials by weight portion proportioning of decoration thermal insulation coatings is as follows：100 parts of deionized water, 0.2 part of sodium hydroxide, 3 parts of diatomite,
1.6 parts of octanol, 1.1 parts of hydrochloric acid, 2 parts of Firebrake ZB, 1.2 parts of dicyandiamide, 5 parts of copper powder, 10 parts of scale graphite, 15 parts of ethanol, poly- second
0.5 part of 15 parts of enol, 3 parts of urea, 12 parts of butanone, 25 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
A kind of 5. preparation method of decoration thermal insulation coatings according to claim 1, it is characterised in that：In the first step
The raw materials by weight portion proportioning of decoration thermal insulation coatings is as follows：100 parts of deionized water, 0.4 part of sodium hydroxide, 5 parts of diatomite,
1.8 parts of octanol, 1.3 parts of hydrochloric acid, 4 parts of Firebrake ZB, 1.4 parts of dicyandiamide, 15 parts of copper powder, 20 parts of scale graphite, 25 parts of ethanol, poly- second
0.7 part of 25 parts of enol, 5 parts of urea, 14 parts of butanone, 35 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
A kind of 6. preparation method of decoration thermal insulation coatings according to claim 1, it is characterised in that：In the first step
The raw materials by weight portion proportioning of decoration thermal insulation coatings is as follows：100 parts of deionized water, 0.3 part of sodium hydroxide, 4 parts of diatomite,
1.7 parts of octanol, 1.2 parts of hydrochloric acid, 3 parts of Firebrake ZB, 1.3 parts of dicyandiamide, 10 parts of copper powder, 15 parts of scale graphite, 20 parts of ethanol, poly- second
0.6 part of 20 parts of enol, 4 parts of urea, 13 parts of butanone, 30 parts of t etram-ethyltetravinylcyclotetrasiloxane and silicone oil dimethylbenzene.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710770392.3A CN107523213A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of decoration thermal insulation coatings |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710770392.3A CN107523213A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of decoration thermal insulation coatings |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107523213A true CN107523213A (en) | 2017-12-29 |
Family
ID=60682931
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710770392.3A Pending CN107523213A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of decoration thermal insulation coatings |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107523213A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023033770A1 (en) * | 2021-09-06 | 2023-03-09 | Mugla Sitki Kocman Universitesi Strateji Gelistirme Daire Baskanligi | A novel non-environmentally hazardous insulating material |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103755270A (en) * | 2013-12-10 | 2014-04-30 | 青岛优维奥信息技术有限公司 | Biological compound coating for buildings |
| CN104559371A (en) * | 2014-12-27 | 2015-04-29 | 青岛佳尚创意文化有限公司 | Flame retardant and heat insulation building coating |
-
2017
- 2017-08-31 CN CN201710770392.3A patent/CN107523213A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103755270A (en) * | 2013-12-10 | 2014-04-30 | 青岛优维奥信息技术有限公司 | Biological compound coating for buildings |
| CN104559371A (en) * | 2014-12-27 | 2015-04-29 | 青岛佳尚创意文化有限公司 | Flame retardant and heat insulation building coating |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023033770A1 (en) * | 2021-09-06 | 2023-03-09 | Mugla Sitki Kocman Universitesi Strateji Gelistirme Daire Baskanligi | A novel non-environmentally hazardous insulating material |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103130478A (en) | Environmentally-friendly building heat insulation material | |
| CN101139200A (en) | Novel wall lightweight heat-insulating material and method for preparing same | |
| CN101628801A (en) | Inorganic light-weight aggregate thermal insulation mortar | |
| CN101503591B (en) | Aqueous low smoke low toxicity fire-resisting paint for thin section steel structure and preparation thereof | |
| CN105086723A (en) | Building fireproof coating | |
| CN106046671B (en) | Phenol-formaldehyde resin modified compound insulating material and preparation method thereof | |
| CN102942331B (en) | External wall heat-insulation and fire-retardant material and preparation method thereof | |
| CN103740049A (en) | Composite heat insulation plate | |
| CN108586965A (en) | Thermosetting property aeroge modified polyphenyl plate and preparation method thereof and construction wall | |
| CN107523213A (en) | A kind of preparation method of decoration thermal insulation coatings | |
| CN103172345B (en) | Light refractory sound-insulation insulation board and preparation method thereof | |
| CN105220846A (en) | A kind of coating process of building fireproof paint | |
| CN1868969A (en) | High carbon high strength fireproof board | |
| CN102953446A (en) | Phenolic foam heat-insulating board made of composite flame-retardant material | |
| CN105061985B (en) | A kind of preparation method of modified phenolic foam warming plate | |
| CN213418315U (en) | Panel for suspended ceiling | |
| CN112196176B (en) | Multilayer composite corrosion-resistant heat-insulating material and preparation method thereof | |
| CN201095842Y (en) | Metal composite board with fireproofing sandwich layer | |
| CN203320719U (en) | Metal interlayer fireproof plate | |
| CN107459766A (en) | Phenol formaldehyde foam thermal insulating composite panel and preparation method thereof | |
| CN107573769A (en) | A kind of preparation method of organosilicon thermal insulation coatings for building | |
| CN113563772A (en) | Fireproof, environment-friendly and weather-resistant organic insulation board fireproof slurry and preparation method thereof | |
| CN203022145U (en) | Phenolic foam insulation board of composite inflaming retarding material | |
| CN106517984B (en) | A kind of building decoration fire proofing material and its preparation method and application | |
| CN105504672B (en) | Non-ignitable level exterior-wall heat insulation and decoration integrated board |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171229 |
|
| RJ01 | Rejection of invention patent application after publication |