CN107519112B - Pure natural fresh-keeping shampoo with mulberry leaf health care function and preparation method thereof - Google Patents
Pure natural fresh-keeping shampoo with mulberry leaf health care function and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention relates to a pure natural fresh-keeping shampoo with a mulberry leaf health-care function and a preparation method thereof, wherein the pure natural fresh-keeping shampoo with the mulberry leaf health-care function is prepared by fermenting 30-60 wt% of mulberry leaves, 15-30 wt% of ginger and 15-40 wt% of black glutinous rice serving as main raw materials, and the sum of the mass percentages of the raw material components is 100 wt%. The pure natural fresh-keeping shampoo prepared by the technology has long preservation time, is rich in various trace elements beneficial to human bodies, is usually used for washing hair, can make the hair black and beautiful, can prevent white hair and alopecia, has the effects of resisting bacteria, relieving itching and nourishing scalp, and has great economic and social benefits.
Description
Technical Field
The invention relates to a pure natural shampoo with health care function and a preparation method thereof, wherein mulberry leaves are taken as main raw materials.
Background
The shampoo is also called shampoo, is used for basic care of hair and scalp, and is one of essential daily necessities in daily life of people. The shampoo in the current market is mostly chemical shampoo, generally contains mixed salt of triethanolamine of fatty alcohol sulfate and ammonium hydroxide, lauric acid isopropanolamide, methyl chloroisothiazolinone, zinc pyrithione, pyridone acetate, p-hydroxy phenyl acid, and chemical preparations such as silicone glycol distearate, spice, pigment and the like, has certain effects on removing dirt, dandruff and moistening hair, but can damage scalp and hair roots after long-term use, generate dandruff and itching phenomena, and greatly damage the hair.
With the continuous improvement of the health consciousness of people, the pure natural personal care product is pursued by people, and the pure natural shampoo which is pure natural, integrates the functions of moistening hair, blackening hair, resisting bacteria, relieving itching, preventing white hair and is rich in various vitamins and trace elements has huge market potential.
Disclosure of Invention
On one hand, the invention provides a preparation method of a pure natural fresh-keeping shampoo with a mulberry leaf health-care function, which is prepared by fermenting 30-60 wt% of mulberry leaves, 15-30 wt% of ginger and 15-40 wt% of black glutinous rice serving as main raw materials, wherein the sum of the mass percentages of the raw material components is 100 wt%.
The invention takes mulberry leaves, ginger, black glutinous rice and the like as main raw materials, and adopts a fermentation process to prepare the pure natural shampoo. The method of the invention can fully reserve and biologically extract the main active ingredients of mulberry leaves and the like, and adopts the processes of filtration, sterilization and the like to ensure that the shampoo can be preserved for a long time and is convenient for commercial production aiming at the defects of more mixed bacteria, short preservation time, easy aging, incapability of commercial production and the like of pure natural fermentation liquor.
The mulberry leaves are dry leaves of mulberry of the family Moraceae, also known as mulberry of family, yellow mulberry leaves and the like, are widely planted in various places in south and north China, are rich in yield and are main food of silkworms. The mulberry leaves contain various phenols, organic acids, alkalis, esters, vitamin B1, B2 and the like, have broad-spectrum antibacterial effect, promote hair growth to a certain extent by hair washing, resist bacteria and relieve itching, and also can make the hair black and bright.
The ginger can stimulate hair follicles, accelerate blood circulation of scalp and play a certain role in hair growth. The ginger can also sterilize and deoil, and can effectively clean garbage and grease accumulated on the scalp.
The black glutinous rice has high nutritive value, contains rich calcium, phosphorus, iron, vitamin B1, vitamin B2 and the like besides protein, fat and carbohydrate, and has the effects of enriching blood and nourishing qi. It is especially suitable for juvenile canities, puerperal asthenia, asthenia after illness, anemia, and kidney essence deficiency.
Preferably, the mulberry leaves are dehydrated to reduce the water content to 8-10 wt%, and then are crushed and sieved by a 150-180-mesh sieve to obtain the mulberry leaf powder.
Preferably, the ginger powder is obtained by dehydrating the ginger until the water content is as low as 8-10 wt%, then crushing and sieving with a 20-50 mesh sieve.
Preferably, the soaked black glutinous rice prepared by soaking the black glutinous rice is steamed into cooked black glutinous rice by steam, and finally water is added for crushing to obtain the black glutinous rice paste.
Preferably, the soaking is to soak the black glutinous rice in water at 20 to 30 ℃ for 12 to 18 hours, and then to dry the soaked black glutinous rice by filtration to obtain the soaked black glutinous rice.
Preferably, the steam pressure of the steam steaming is controlled to be 0.1-0.12Mp, and the time is 15-20 minutes, so that the rice yield of the soaked black glutinous rice is 160-180%, and the cooked black glutinous rice is obtained.
Preferably, the cooked black glutinous rice is showered with cold water to make the central temperature of the cooked black glutinous rice be 25-35 ℃, then water is added, and the black glutinous rice paste is obtained after crushing.
Preferably, the black glutinous rice paste, the mulberry leaf powder and the ginger powder are mixed and added with a fermentation strain, and the mixture is fermented for 48 to 72 hours at a temperature of between 30 and 35 ℃. The fermentation is carried out to separate out the active ingredients such as organic acid, ester, vitamin B1, B2 and the like in the mulberry leaves, the ginger and the glutinous rice, and simultaneously, a small amount of bioethanol in the fermentation liquor enables the fermentation liquor to be easy to store, thus obtaining the pure natural fresh-keeping shampoo.
Preferably, the fermentation strain is a composite fermentation strain of yeast and aspergillus. Preferably, the addition amount of the fermentation strain is 2-3 wt% of the total mass of the black glutinous rice paste, the mulberry leaf powder and the ginger powder.
Preferably, the pure natural fresh-keeping shampoo is sterilized at a constant temperature of 65-68 ℃ for 35-40 minutes after being filtered.
On the other hand, the invention also provides the pure natural fresh-keeping shampoo prepared by the method.
The pure natural fresh-keeping shampoo prepared by the technology has long preservation time, is rich in various trace elements beneficial to human bodies, is usually used for washing hair, can make the hair black and beautiful, can prevent white hair and alopecia, has the effects of resisting bacteria, relieving itching and nourishing scalp, and has great economic and social benefits.
Detailed Description
The present invention is further illustrated by the following examples, which are to be understood as merely illustrative and not restrictive.
The invention takes mulberry leaves, ginger and black glutinous rice as main raw materials to prepare pure natural fresh-keeping shampoo. Wherein the method steps may comprise: soaking black glutinous rice, steaming with steam, fermenting, filtering, bottling, sterilizing and the like. The preparation method of the pure natural fresh-keeping shampoo provided by the invention is exemplarily described below.
Weighing the raw materials according to the mass ratio of the raw materials. Wherein 30-60 wt% of mulberry leaves (preferably 50-60 wt%), 15-30 wt% of ginger (preferably 15-20 wt%), 15-40 wt% of black glutinous rice (preferably 15-25 wt%) are used as main raw materials, and the sum of the mass percentages of the raw materials is 100 wt%. For example, each main raw material is (by mass fraction): 35% of mulberry leaves, 30% of ginger and 35% of black glutinous rice.
Collecting and processing mulberry leaves. Collecting mulberry leaf materials, drying and dehydrating the materials to ensure that the water content of the materials is reduced to 8-10%, and then crushing the materials until the materials can pass through 150-180 meshes for later use (obtaining mulberry leaf powder).
Collecting and processing ginger: collecting ginger materials, drying and dehydrating the ginger materials to enable the water content of the materials to be 8% -10%, and then crushing the ginger materials until the ginger materials can pass through 20-50 meshes for later use (obtaining ginger powder).
Soaking black glutinous rice. Specifically, the black glutinous rice is placed in water, soaked for 12-18 hours at 20-30 ℃, and then filtered to be dry, so that the soaked black glutinous rice is obtained. As an example, the soaked black glutinous rice is prepared by soaking cleaned black glutinous rice in water at room temperature (25 ℃) for 12-18 hours to make the black glutinous rice swell by absorbing water without white core, and filtering to dry.
Preparing cooked black glutinous rice. And steaming the soaked black glutinous rice by adopting a steam steaming mode. Specifically, the steam pressure of steam steaming can be controlled to be 0.1-0.12Mp, the time is 15-20 minutes, the rice yield of the soaked black glutinous rice is 160-180%, and finally the cooked black glutinous rice is obtained.
And (4) preparing the black glutinous rice paste. And spraying cold water on the cooked black glutinous rice to quickly cool the cooked black glutinous rice, and controlling the central temperature of the cooked black glutinous rice to be 25-35 ℃ after cooling. Then adding a small amount of water, and grinding to obtain the black glutinous rice paste. Wherein the adding amount of water is that the mass ratio of cooked black glutinous rice is 1: (0.1-0.2). For example, a small amount of deionized water is added to the cooled cooked black glutinous rice and pulverized with a refiner to obtain a black glutinous rice paste.
And (5) fermenting. Mixing the black glutinous rice paste, the mulberry leaf powder and the ginger powder, adding a fermentation strain, and fermenting at 30-35 ℃ for 48-72 hours to obtain the pure natural fresh-keeping shampoo. The fermentation strain can be composite fermentation strain of yeast and aspergillus. The addition amount of the fermentation strain can be 2-3 wt% of the total mass of the black glutinous rice paste, the mulberry leaf powder and the ginger powder. As an example, adding a composite fermentation strain of microzyme and aspergillus into the obtained black glutinous rice paste, uniformly stirring the obtained mulberry leaf powder and ginger powder together, placing the mixture into a fermentation tank for heat preservation and fermentation, wherein the adding amount of the composite fermentation strain powder is 2-3% of the total mass of fed materials, and controlling the fermentation time to be 48-72 hours to obtain fermentation liquor, namely the pure natural shampoo.
And (5) filtering. And (3) carrying out rough filtration and ultrafiltration filtration on the fermented pure natural shampoo to obtain filtrate, namely the filtered pure natural shampoo. Wherein the rough filtration is completed by adopting plate-and-frame filtration with the aperture of 2-4 microns, the ultrafiltration is completed by adopting an inorganic ceramic membrane with the aperture of 30nm, and the membrane feeding pressure is controlled to be 0.1-0.2 MPa.
Bottling and sterilizing. And bottling the filtered pure natural shampoo, and sterilizing at the constant temperature of 65-68 ℃ for 35-40 minutes to obtain the fresh-keeping pure natural shampoo.
The present invention will be described in detail by way of examples. It is also to be understood that the following examples are illustrative of the present invention and are not to be construed as limiting the scope of the invention, and that certain insubstantial modifications and adaptations of the invention by those skilled in the art may be made in light of the above teachings. The specific process parameters and the like of the following examples are also only one example of suitable ranges, i.e., those skilled in the art can select the appropriate ranges through the description herein, and are not limited to the specific values exemplified below.
Example 1:
in the following embodiments of the present invention, each of the raw materials is commercially available. The raw materials used in the invention are as follows: 35kg of mulberry leaves, 30kg of ginger and 35kg of black glutinous rice, and the used water is deionized water. The specific method for preparing the fresh-keeping pure natural shampoo comprises the following steps:
(1) collecting and processing mulberry leaves: collecting materials, drying and dehydrating until the water content of the materials is lower than 8% -10%, and crushing to powder which can pass through 150-180 meshes for later use;
(2) collecting and processing ginger: collecting materials, drying and dehydrating until the water content of the materials is lower than 8% -10%, and crushing to 20-50 meshes for later use;
(3) soaking black glutinous rice. Firstly, cleaning black glutinous rice, soaking the black glutinous rice in clear water for 12 to 18 hours, controlling the temperature of the soaking water to be within the range of 10 to 15 ℃, and filtering the black glutinous rice to be dry by a natural method, wherein the filtering time for soaking the black glutinous rice is controlled to be about 30 minutes, generally 25 minutes, so as to soak the black glutinous rice;
(4) soaking the black glutinous rice in the previous step, placing the black glutinous rice in a steamer, steaming for 10-15 minutes by steam, controlling the steam pressure to be 0.1-0.12Mpa, controlling the cooking degree of the steamed black glutinous rice to be about eighty percent, namely controlling the rice yield to be 160% -180%, obtaining cooked glutinous rice, thoroughly spraying cold water on the cooked black glutinous rice which is cooked to be about eighty percent, rapidly cooling the central temperature of the cooked black glutinous rice to 25-35 ℃, adding water, and grinding the mixture into black glutinous rice paste;
(5) fermenting, namely adding the mulberry leaf powder and the ginger powder obtained in the steps (1) and (2) into the black sticky rice paste, adding a composite fermentation strain of saccharomycetes and aspergillus, wherein the addition amount is 2-3% of the total feeding amount, uniformly stirring the materials together, placing the materials in a fermentation tank for heat preservation and fermentation, and controlling the fermentation time to be 48-72 hours to obtain fermentation liquor, namely pure natural shampoo;
(6) filtering to obtain pure natural shampoo, and coarse filtering and ultrafiltering the fermented pure natural shampoo to obtain filtrate as pure natural shampoo; wherein the rough filtration is completed by adopting plate-and-frame filtration with the aperture of 2-4 microns, the ultrafiltration is completed by adopting an inorganic ceramic membrane with the aperture of 30nm, and the membrane feeding pressure is controlled to be 0.1-0.2 MPa;
(7) bottling, sterilizing, bottling, and sterilizing at 65-68 deg.C for 35-40 min to obtain the final product.
Example 2:
in the following embodiments of the present invention, each of the raw materials is commercially available. The raw materials used in the invention are as follows: 55kg of mulberry leaves, 20kg of ginger and 25kg of black glutinous rice, and the used water is deionized water. The specific method for preparing the fresh-keeping pure natural shampoo comprises the following steps:
(1) collecting and processing mulberry leaves: collecting materials, drying and dehydrating until the water content of the materials is lower than 8% -10%, and crushing to powder which can pass through 150-180 meshes for later use;
(2) collecting and processing ginger: collecting materials, drying and dehydrating until the water content of the materials is lower than 8% -10%, and crushing to 20-50 meshes for later use;
(3) soaking black glutinous rice. Firstly, cleaning black glutinous rice, soaking the black glutinous rice in clear water for 12 to 18 hours, controlling the temperature of the soaking water to be within the range of 10 to 15 ℃, and filtering the black glutinous rice to be dry by a natural method, wherein the filtering time for soaking the black glutinous rice is controlled to be about 30 minutes, generally 25 minutes, so as to soak the black glutinous rice;
(4) soaking the black glutinous rice in the previous step, placing the black glutinous rice in a steamer, steaming for 10-15 minutes by steam, controlling the steam pressure to be 0.1-0.12Mpa, controlling the cooking degree of the steamed black glutinous rice to be about eighty percent, namely controlling the rice yield to be 160% -180%, obtaining cooked glutinous rice, thoroughly spraying cold water on the cooked black glutinous rice which is cooked to be about eighty percent, rapidly cooling the central temperature of the cooked black glutinous rice to 25-35 ℃, adding water, and grinding the mixture into black glutinous rice paste;
(5) fermenting, namely adding the mulberry leaf powder and the ginger powder obtained in the steps (1) and (2) into the black sticky rice paste, adding a composite fermentation strain of saccharomycetes and aspergillus, wherein the addition amount is 2-3% of the total feeding amount, uniformly stirring the materials together, placing the materials in a fermentation tank for heat preservation and fermentation, and controlling the fermentation time to be 48-72 hours to obtain fermentation liquor, namely pure natural shampoo;
(6) filtering to obtain pure natural shampoo, and coarse filtering and ultrafiltering the fermented pure natural shampoo to obtain filtrate as pure natural shampoo; wherein the rough filtration is completed by adopting plate-and-frame filtration with the aperture of 2-4 microns, the ultrafiltration is completed by adopting an inorganic ceramic membrane with the aperture of 30nm, and the membrane feeding pressure is controlled to be 0.1-0.2 MPa;
(7) bottling, sterilizing, bottling, and sterilizing at 65-68 deg.C for 35-40 min to obtain the final product.
Table of specific ingredient analysis (nutrient content/per 100g) of the fresh-keeping all natural shampoos prepared in examples 1 and 2, as follows:
because the fresh-keeping pure natural shampoo prepared in the above examples 1 and 2 contains the glutinous rice fermented component, namely the natural alcohol, the fresh-keeping pure natural shampoo has good bacteriostatic effect under the sealing condition, and is sampled and evaluated under the normal temperature condition (20 ℃, dark) at 1.5, 3, 4.5, 6 and 6.5 months respectively; under accelerated conditions (temperature 70 ℃, humidity 60%), samples were taken for evaluation at 1.5, 3, 4.5, 6, 6.5 months. The appearance, color and nutrient components of the fresh-keeping shampoo are not obviously changed, and the preservation time is much longer than that of the common pure natural self-made shampoo (2-3 weeks).
The effect examples of preventing hair loss were carried out using the fresh-keeping pure natural shampoos prepared in examples 1 and 2. Wherein the experimental population used in each example is 20, 10 men and 10 women, all have pathological alopecia symptoms, and the age is 18-45 years old;
the using method comprises the following steps: the fresh pure natural shampoo prepared in the examples 1 and 2 is used for cleaning hair 1 time a day, one month is taken as a treatment course continuously, and three treatment courses are taken as the observation of curative effect;
the experimental results are as follows: the therapeutic criteria are classified as significant (no apparent hair loss, with a large amount of new hair growth), effective (hair loss controlled, with a small amount of new hair growth), and ineffective (no change before and after treatment);
the efficacy of the fresh pure natural shampoo prepared in this example is shown in the following table:
the above description is only for the preferred embodiment of the present invention, and the scope of the present invention is not limited thereby. The shampoo prepared by the method is used for washing hair, lasts for 1-3 months, and has remarkable effects of blackening hair and improving hair quality. However, sang Ye is cold in nature and should be used with cautions during the menstrual period or pregnancy.
Claims (1)
1. A preparation method of a pure natural fresh-keeping shampoo is characterized by being prepared by fermenting 30-60 wt% of mulberry leaves, 15-30 wt% of ginger and 15-40 wt% of black glutinous rice which are used as main raw materials, wherein the sum of the mass percentages of the raw material components is 100 wt%;
the preparation method of the pure natural fresh-keeping shampoo comprises the following steps:
(1) dehydrating mulberry leaves until the water content is 8-10 wt%, crushing and sieving with a 150-180-mesh sieve to obtain mulberry leaf powder;
(2) dehydrating ginger until the water content is 8-10 wt%, then crushing and sieving with a 20-50 mesh sieve to obtain ginger powder;
(3) putting black glutinous rice into water, soaking for 12-18 hours at 20-30 ℃, filtering to obtain soaked black glutinous rice, steaming the soaked black glutinous rice prepared by soaking into steam to obtain cooked black glutinous rice, spraying cold water to the cooked black glutinous rice so that the central temperature of the cooked black glutinous rice is 25-35 ℃, adding water, and crushing to obtain black glutinous rice paste, wherein the steam pressure of steam steaming is controlled to be 0.1-0.12MPa for 15-20 minutes, so that the rice output rate of the soaked black glutinous rice is 160-180%;
(4) mixing the black glutinous rice paste, the mulberry leaf powder and the ginger powder, adding a fermentation strain, fermenting for 48-72 hours at 30-35 ℃ to separate out organic acids and esters, vitamins B1 and B2 from the black glutinous rice paste, the mulberry leaf powder and the ginger powder, filtering, and sterilizing at the constant temperature of 65-68 ℃ for 35-40 minutes to obtain the pure natural fresh-keeping shampoo;
the fermentation strain is a composite fermentation strain of saccharomycetes and aspergillus, and the addition amount of the composite fermentation strain is 2-3 wt% of the total mass of the black glutinous rice paste, the mulberry leaf powder and the ginger powder.
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| CN108338948A (en) * | 2018-03-15 | 2018-07-31 | 佛山实瑞先导材料研究院（普通合伙） | The hair cream of blackening hair containing various trace elements |
| TWI732113B (en) * | 2018-04-09 | 2021-07-01 | 陳耀寬 | Nourishing hair nourishing agent |
| CN108721170A (en) * | 2018-07-31 | 2018-11-02 | 广西容县顺芯茶麸制品厂 | A kind of pure plant Yang Fa treatment oil powder |
| CN110151622A (en) * | 2019-05-29 | 2019-08-23 | 山东腾贵医药有限公司 | A kind of phalacrosis prevention and hair generation compound formulation and preparation method thereof |
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