CN107511910A - A kind of soft ceramic manufacture method of graphene - Google Patents
A kind of soft ceramic manufacture method of graphene Download PDFInfo
- Publication number
- CN107511910A CN107511910A CN201710607699.1A CN201710607699A CN107511910A CN 107511910 A CN107511910 A CN 107511910A CN 201710607699 A CN201710607699 A CN 201710607699A CN 107511910 A CN107511910 A CN 107511910A
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- Prior art keywords
- graphene
- attachment
- manufacture method
- lightly
- ceramic manufacture
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B1/00—Producing shaped prefabricated articles from the material
- B28B1/008—Producing shaped prefabricated articles from the material made from two or more materials having different characteristics or properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B17/00—Details of, or accessories for, apparatus for shaping the material; Auxiliary measures taken in connection with such shaping
- B28B17/02—Conditioning the material prior to shaping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B38/00—Ancillary operations in connection with laminating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B38/00—Ancillary operations in connection with laminating processes
- B32B38/0008—Electrical discharge treatment, e.g. corona, plasma treatment; wave energy or particle radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/005—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising one layer of ceramic material, e.g. porcelain, ceramic tile
- B32B9/007—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising one layer of ceramic material, e.g. porcelain, ceramic tile comprising carbon, e.g. graphite, composite carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B9/00—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00
- B32B9/04—Layered products comprising a layer of a particular substance not covered by groups B32B11/00 - B32B29/00 comprising such particular substance as the main or only constituent of a layer, which is next to another layer of the same or of a different material
Abstract
The invention discloses a kind of soft ceramic manufacture method of graphene, by repeatedly folding, prolong pressure, graphene layer is allowed to be arranged at intervals from top to bottom in porcelain tendre, thus equivalent to allowing thick porcelain tendre to be divided into multiple relatively thin porcelain tendres by graphene layer, the addition of graphene improves the bending resistance of porcelain tendre, this reduces the possibility of cracks of porcelain tendre, and during allowing graphite alkene monomer in the electric field or freely being descended slowly and lightly in magnetic field, graphite alkene monomer can be allowed to carry out the posture of self during descending slowly and lightly in the presence of Hall effect to correct, so that most black alkene monomer is descended slowly and lightly onto the upper surface of pre- attachment with the posture of transverse direction, such orientation, graphene layer can be allowed to have given play to the physical property of graphene in itself to greatest extent.The present invention is used for the manufacture of porcelain tendre.
Description
Technical field
The present invention relates to a kind of soft ceramic manufacture method of graphene.
Background technology
Soft ceramics, not real porcelain, nor ceramic tile, it is a kind of new building and ornament materials.By modified soil
(MCM) be primary raw material, with special temperature control moulding system shaping, baking, cross-linking radiation form it is a kind of have it is flexible
Building decoration plane materiel.At the beginning of birth, it has the appearance of ceramic tile, therefore is commonly called as soft ceramics, later, with technology
Development, can develop into imitative stone material, leather texture imitation, imitation wood etc., and every to imagine, soft ceramics can all be realized.
Existing soft ceramic short life, easily there is slight crack, low intensity, thin soft ceramics are flexible high, but thickness is 3mm
Soft ceramics above are flexible relatively low, and thicker soft ceramics are easily cracked after bending, extension.
The content of the invention
The technical problem to be solved in the present invention is：A kind of porcelain tendre is provided and is not easy the soft pottery manufacturer of cracked graphene
Method.
The present invention solve its technical problem solution be：
A kind of soft ceramic manufacture method of graphene, including following making step：
A) soft pottery material, the graphene of moistening mixed is got out；
B) soft pottery material be shaped into the pre- attachment of horizontal smooth upper surface；
C) pre- attachment is set in the electric field or in magnetic field, allows graphene uniformly to be descended slowly and lightly above pre- attachment to pre- attachment
On body, the attachment that upper surface carries graphene layer is formed；The field strength in the electric field or magnetic field at least two position from top to bottom
Field strength it is different；The direction in the electric field or magnetic field is laterally；
D) attachment is subjected to one or many doublings, prolongs pressure so as to form overlapping body so that overlapping is provided with one in vivo
Graphene layer or multiple spaced graphene layers；
E) to overlapping body mould shape, so as to form prebake body；
F) prebake body is baked.
As the further improvement of such scheme, the average time that descends slowly and lightly of the graphene in step c) is more than 10 second.
As the further improvement of such scheme, the pre- attachment in step c) is in air pressure and is less than 0.5 normal atmosphere
In the environment of pressure.
As the further improvement of such scheme, the middle progress doublings of step d), after prolonging pressure, graphene is allowed above overlapping body
Uniformly descend slowly and lightly onto overlapping body.
As the further improvement of such scheme, the field strength in electric field or magnetic field described in step c) continuously becomes from top to bottom
Change.
The beneficial effects of the invention are as follows：A kind of soft ceramic manufacture method of graphene, by repeatedly folding, prolonging pressure, allow stone
Black alkene layer is arranged at intervals from top to bottom in porcelain tendre, thus equivalent to allowing thick porcelain tendre to be divided into multiple phases by graphene layer
To relatively thin porcelain tendre, the addition of graphene improves the bending resistance of porcelain tendre, this reduces the possibility of cracks of porcelain tendre, and
During allowing graphite alkene monomer in the electric field or freely being descended slowly and lightly in magnetic field, graphite alkene monomer can be allowed in the presence of Hall effect
Carry out the posture of self during descending slowly and lightly to correct so that most black alkene monomer is descended slowly and lightly to pre- attachment with the posture of transverse direction
On the upper surface of body, such orientation, graphene layer can be allowed to have given play to graphene physical in itself to greatest extent
Energy.The present invention is used for the manufacture of porcelain tendre.
Embodiment
Design, concrete structure and the caused technique effect of the present invention are carried out below with reference to embodiment clear, complete
Ground describes, to be completely understood by the purpose of the present invention, feature and effect.Obviously, described embodiment is the one of the present invention
Section Example, rather than whole embodiments, based on embodiments of the invention, those skilled in the art is not paying creativeness
The other embodiment obtained on the premise of work, belongs to the scope of protection of the invention.In addition, what is be previously mentioned in text is all
/ annexation is connect, not singly refers to component and directly connects, and refer to can be according to specific implementation situation, by adding or reducing connection
Auxiliary, to form more excellent draw bail.Each technical characteristic in the present invention, can be with the premise of not conflicting conflict
Combination of interactions.
This is embodiments of the invention, specifically：
A kind of soft ceramic manufacture method of graphene, including following making step：
A) soft pottery material, the graphene of moistening mixed is got out；
B) soft pottery material be shaped into the pre- attachment of horizontal smooth upper surface；
C) pre- attachment is set in the electric field or in magnetic field, allows graphene uniformly to be descended slowly and lightly above pre- attachment to pre- attachment
On body, the attachment that upper surface carries graphene layer is formed；The field strength in the electric field or magnetic field at least two position from top to bottom
Field strength it is different；The direction in the electric field or magnetic field is laterally；
D) attachment is subjected to one or many doublings, prolongs pressure so as to form overlapping body so that overlapping is provided with one in vivo
Graphene layer or multiple spaced graphene layers；
E) to overlapping body mould shape, so as to form prebake body；
F) prebake body is baked.
By repeatedly folding, prolonging pressure, graphene layer is allowed to be arranged at intervals from top to bottom in porcelain tendre, thus equivalent to allowing thickness
Thick porcelain tendre is divided into multiple relatively thin porcelain tendres by graphene layer, and the addition of graphene improves the bending resistance of porcelain tendre,
This reduces the possibility of cracks of porcelain tendre, and during allowing graphite alkene monomer in the electric field or freely being descended slowly and lightly in magnetic field, warp
Can produce electric current when crossing the different position of field strength, in graphite alkene monomer so as to allow graphite alkene monomer carried out during descending slowly and lightly from
My pose adjustment so that most black alkene monomer is descended slowly and lightly onto the upper surface of pre- attachment with the posture of level, allows electric field
Or the direction in magnetic field it is parallel with pre- attachment effect it is best, such orientation can allow graphene to greatest extent
Layer has given play to the physical property of graphene in itself.
The average time that descends slowly and lightly of graphene in the step c) of the present embodiment is more than 10 seconds, the time that the present embodiment uses
For 12 seconds, graphite alkene monomer is allowed to have sufficient time to adjust posture.
The consecutive variations from top to bottom of the field strength in electric field or magnetic field described in step c), so can allow graphite alkene monomer to obtain
To the correction of lasting power.
Self carry out the resistance that is subject to during pose adjustment in order to reduce air to graphite alkene monomer, the pre- attachment in step c)
Body is in environment of the air pressure less than 0.5 standard atmospheric pressure.
The middle progress doublings of step d), after prolonging pressure, graphene is allowed uniformly to be descended slowly and lightly above overlapping body onto overlapping body.So have
Beneficial to the density for the possessed graphite alkene monomer for ensureing graphene layer, while the graphene layer of more layers can be obtained as soon as possible.
The better embodiment of the present invention is illustrated above, but the present invention is not limited to the embodiment,
Those skilled in the art can also make a variety of equivalent modifications or replacement on the premise of without prejudice to spirit of the invention, this
Equivalent modification or replacement are all contained in the application claim limited range a bit.
Claims (5)
- A kind of 1. soft ceramic manufacture method of graphene, it is characterised in that：Including following making step：A) soft pottery material, the graphene of moistening mixed is got out；B) soft pottery material be shaped into the pre- attachment of horizontal smooth upper surface；C) pre- attachment is set in the electric field or in magnetic field, allows graphene uniformly to be descended slowly and lightly above pre- attachment to pre- attachment On, form the attachment that upper surface carries graphene layer；The field strength in the electric field or magnetic field at least two positions from top to bottom Field strength is different；The direction in the electric field or magnetic field is laterally；D) attachment is subjected to one or many doublings, prolongs pressure so as to form overlapping body so that overlapping is provided with a graphite in vivo Alkene layer or multiple spaced graphene layers；E) to overlapping body mould shape, so as to form prebake body；F) prebake body is baked.
- A kind of 2. soft ceramic manufacture method of graphene according to claim 1, it is characterised in that：Graphite in step c) The average time that descends slowly and lightly of alkene is more than 10 second.
- A kind of 3. soft ceramic manufacture method of graphene according to claim 1, it is characterised in that：It is pre- attached in step c) Body to be in environment of the air pressure less than 0.5 standard atmospheric pressure.
- A kind of 4. soft ceramic manufacture method of graphene according to claim 1, it is characterised in that：Carried out in step d) pair After rolling over, prolonging pressure, graphene is allowed uniformly to be descended slowly and lightly above overlapping body onto overlapping body.
- A kind of 5. soft ceramic manufacture method of graphene according to claim 1, it is characterised in that：It is electric described in step c) Or magnetic field field strength consecutive variations from top to bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710607699.1A CN107511910A (en) | 2017-07-24 | 2017-07-24 | A kind of soft ceramic manufacture method of graphene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710607699.1A CN107511910A (en) | 2017-07-24 | 2017-07-24 | A kind of soft ceramic manufacture method of graphene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107511910A true CN107511910A (en) | 2017-12-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710607699.1A Pending CN107511910A (en) | 2017-07-24 | 2017-07-24 | A kind of soft ceramic manufacture method of graphene |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006264316A (en) * | 2005-02-25 | 2006-10-05 | Nagaoka Univ Of Technology | Precision orientation polycrystal ceramic sintered compact, its manufacturing process and manufacturing device |
| CN102382606A (en) * | 2011-09-19 | 2012-03-21 | 常州合润新材料科技有限公司 | Graphene filling isotropic high-performance conducting adhesive and preparation method thereof |
| CN102706219A (en) * | 2012-06-06 | 2012-10-03 | 中国科学院化学研究所 | Micron and nano material-enhancing bionic layered composite material and manufacturing method thereof |
| CN104829237A (en) * | 2015-04-01 | 2015-08-12 | 苏州第一元素纳米技术有限公司 | Preparation method of nanocarbon toughened ceramic |
| CN105469914A (en) * | 2015-11-18 | 2016-04-06 | 中国电力科学研究院 | Device utilizing electric field force to drive orientation of nano particles in thin film materials |
| CN106458602A (en) * | 2014-06-20 | 2017-02-22 | 加利福尼亚大学校董会 | Method for fabrication and transfer of graphene |
-
2017
- 2017-07-24 CN CN201710607699.1A patent/CN107511910A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006264316A (en) * | 2005-02-25 | 2006-10-05 | Nagaoka Univ Of Technology | Precision orientation polycrystal ceramic sintered compact, its manufacturing process and manufacturing device |
| CN102382606A (en) * | 2011-09-19 | 2012-03-21 | 常州合润新材料科技有限公司 | Graphene filling isotropic high-performance conducting adhesive and preparation method thereof |
| CN102706219A (en) * | 2012-06-06 | 2012-10-03 | 中国科学院化学研究所 | Micron and nano material-enhancing bionic layered composite material and manufacturing method thereof |
| CN106458602A (en) * | 2014-06-20 | 2017-02-22 | 加利福尼亚大学校董会 | Method for fabrication and transfer of graphene |
| CN104829237A (en) * | 2015-04-01 | 2015-08-12 | 苏州第一元素纳米技术有限公司 | Preparation method of nanocarbon toughened ceramic |
| CN105469914A (en) * | 2015-11-18 | 2016-04-06 | 中国电力科学研究院 | Device utilizing electric field force to drive orientation of nano particles in thin film materials |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171226 |
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| RJ01 | Rejection of invention patent application after publication |