CN107501992A - A kind of madder haematochrome preparation method and application - Google Patents
A kind of madder haematochrome preparation method and application Download PDFInfo
- Publication number
- CN107501992A CN107501992A CN201710706150.8A CN201710706150A CN107501992A CN 107501992 A CN107501992 A CN 107501992A CN 201710706150 A CN201710706150 A CN 201710706150A CN 107501992 A CN107501992 A CN 107501992A
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- CN
- China
- Prior art keywords
- madder
- solution
- fabric
- haematochrome
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of madder haematochrome preparation method and application.The technical scheme is that：Madder after clean dry is crushed with medicinal herb grinder；Obtained madder powder is added to be extracted using 25% ethanol solution, is obtained filter residue and solution, is repeated twice；Obtained solution is mixed again, using sedimentator to the clarification dye liquor positioned at upper strata；Obtained clarification dye liquor carries out being concentrated to give dye concentrated solution using vacuum decompressioning and concentrating tank；Obtained dye concentrated solution is dried to obtain dyestuff pulvis by vacuum constant temperature drying box.A kind of application of madder haematochrome, the madder red-brown pigment, in field of textiles, dyes as natural dyeing agent to fabric, the madder red-brown pigment is ecological decoration method to the colouring method of fabric, and described fabric is cotton, hair, silk, the natural fabric of crudefiber crop.Scheme preparation method provided by the invention is reasonable, and production efficiency is high, pollution-free, has a wide range of application.
Description
Technical field
The present invention relates to natural dye extractive technique field, more particularly to a kind of madder haematochrome preparation method is with answering
With.
Background technology
Madder contains a variety of gunlock anthraquinone derivatives, such as rubican, purpuroxanthin, purpurin, pseudo- hydroxyl madder
Careless element, munjistin and Physcion etc., again can be with the white active component of isolated liter.Madder is during Ancient Times in China document is recorded
One of vegetable colour occurred earliest, and the red plants dyestuff that the mankind use earliest.Madder can be used in hair, cotton, silk, fiber crops
Deng the dyeing of fiber, using the method for first coal after stain in conventional art.The dyestuff of madder extraction is used in clothes dyeing have
The effect of environmental protection, therefore the research to madder has a very big significance.The extracting method of madder generally uses water-bath
Method direct extraction method, but this method is less efficient.
The content of the invention
In view of the deficienciess of the prior art, raw material raising effect can be saved it is a primary object of the present invention to provide one kind
The madder haematochrome preparation method of rate.
To achieve the above object, the invention provides following technical scheme：A kind of preparation method of madder haematochrome, bag
Include following steps,
1）, the madder after clean dry crushed with medicinal herb grinder；
2）, by step 1）In obtained madder powder be added to and extracted using 25% ethanol solution, obtain filter residue and molten
Liquid；；
3）, by step 2）In filter residue be added to again in 25% ethanol solution, repeat extract, obtain solution again；
4）, by step 2）Obtained solution and step 3）Obtained solution is mixed, using sedimentator to positioned at the clear of upper strata
Clear dye liquor；
5）, clarification dye liquor that step 4 obtains carried out using vacuum decompressioning and concentrating tank to be concentrated to give dye concentrated solution；
6）, by step 5）In obtained dye concentrated solution be dried to obtain dyestuff pulvis by vacuum constant temperature drying box.
Preferably, the step 1）In, it is 30 ~ 70 mesh to crush the particle that madder obtains.
Preferably, the step 2）In with step 3）In, during extraction carried out in thermostat water bath, temperature is 80 DEG C.
Preferably, during the extraction, filtered after 2 hours using vavuum pump.
Preferably, the step 2）With step 3）Extraction process in add have lanthanum chloride solution.
A kind of application of madder haematochrome, it is characterised in that：Madder red-brown pigment is being weaved as natural dyeing agent
Field, fabric is dyed.
Preferably, the madder red-brown pigment is ecological decoration method to the colouring method of fabric.
Preferably, described fabric is cotton, hair, silk, the natural fabric of crudefiber crop.
The present invention has the following advantages that raw material sources of the present invention are convenient, simple production process relative to prior art;System
Standby powdering dyestuff, is highly convenient for transporting, store and producing, and production efficiency is high.
Embodiment
The invention will be further described below.Raw material sources of the present invention are convenient, simple production process;Prepare powdering
Dyestuff, it is highly convenient for transporting, store and producing, production efficiency is high.
A kind of preparation method of madder haematochrome, comprises the following steps,
1）, the madder after clean dry crushed with medicinal herb grinder；
2）, by step 1）In obtained madder powder be added to and extracted using 25% ethanol solution, obtain filter residue and molten
Liquid；；
3）, by step 2）In filter residue be added to again in 25% ethanol solution, repeat extract, obtain solution again；
4）, by step 2）Obtained solution and step 3）Obtained solution is mixed, using sedimentator to positioned at the clear of upper strata
Clear dye liquor；
5）, clarification dye liquor that step 4 obtains carried out using vacuum decompressioning and concentrating tank to be concentrated to give dye concentrated solution；
6）, by step 5）In obtained dye concentrated solution be dried to obtain dyestuff pulvis by vacuum constant temperature drying box.
Above-mentioned steps can directly obtain dyestuff pulvis, and madder is easily obtained, and production equipment is setting for prior art
It is standby, be not in pollution in process, very environmentally friendly, production efficiency is high.
Preferably, the step 1）In, it is 30 ~ 70 mesh to crush the particle that madder obtains.So it is easy to the suitable of haematochrome
Profit extraction.
Preferably, the step 2）In with step 3）In, during extraction carried out in thermostat water bath, temperature is 80 DEG C.
Preferably, during the extraction, filtered after 2 hours using vavuum pump.
Preferably, the step 2）With step 3）Extraction process in add have lanthanum chloride solution.
A kind of application of madder haematochrome, it is characterised in that：Madder red-brown pigment is being weaved as natural dyeing agent
Field, fabric is dyed.
Preferably, the madder red-brown pigment is ecological decoration method to the colouring method of fabric.
Preferably, described fabric is cotton, hair, silk, the natural fabric of crudefiber crop.
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
Those of ordinary skill for, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (8)
- A kind of 1. preparation method of madder haematochrome, it is characterised in that：Comprise the following steps,1）, the madder after clean dry crushed with medicinal herb grinder；2）, by step 1）In obtained madder powder be added to and extracted using 25% ethanol solution, obtain filter residue and molten Liquid；；3）, by step 2）In filter residue be added to again in 25% ethanol solution, repeat extract, obtain solution again；4）, by step 2）Obtained solution and step 3）Obtained solution is mixed, using sedimentator to positioned at the clear of upper strata Clear dye liquor；5）, clarification dye liquor that step 4 obtains carried out using vacuum decompressioning and concentrating tank to be concentrated to give dye concentrated solution；6）, by step 5）In obtained dye concentrated solution be dried to obtain dyestuff pulvis by vacuum constant temperature drying box.
- A kind of 2. preparation method of the red poison of madder according to claim 1, it is characterised in that：The step 1）In, It is 30 ~ 70 mesh to crush the particle that madder obtains.
- A kind of 3. preparation method of madder haematochrome according to claim 1, it is characterised in that：The step 2）In with Step 3）In, during extraction carried out in thermostat water bath, temperature is 80 DEG C.
- A kind of 4. preparation method of the red poison of madder according to claim 3, it is characterised in that：During the extraction, warp Filtered after spending 2 hours using vavuum pump.
- A kind of 5. preparation method of the red poison of madder according to claim 1, it is characterised in that：The step 2）With step Rapid 3）Extraction process in add have lanthanum chloride solution.
- A kind of 6. application of madder haematochrome, it is characterised in that：The madder red-brown pigment is being spun as natural dyeing agent Field is knitted, fabric is dyed.
- A kind of 7. application of madder haematochrome according to claim 6, it is characterised in that：The madder red-brown pigment Colouring method to fabric is ecological decoration method.
- A kind of 8. application of the red poison of madder according to claim 6, it is characterised in that：Described fabric be cotton, hair, Silk, the natural fabric of crudefiber crop.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710706150.8A CN107501992A (en) | 2017-08-17 | 2017-08-17 | A kind of madder haematochrome preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710706150.8A CN107501992A (en) | 2017-08-17 | 2017-08-17 | A kind of madder haematochrome preparation method and application |
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| Publication Number | Publication Date |
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| CN107501992A true CN107501992A (en) | 2017-12-22 |
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| CN201710706150.8A Pending CN107501992A (en) | 2017-08-17 | 2017-08-17 | A kind of madder haematochrome preparation method and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108997775A (en) * | 2018-06-20 | 2018-12-14 | 马鞍山中粮生物化学有限公司 | A kind of extracting method of natural madder red edible pigment |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1730564A (en) * | 2005-08-11 | 2006-02-08 | 上海交通大学 | Preparation method of gamene vegetable dye |
| CN1844257A (en) * | 2006-03-21 | 2006-10-11 | 宁波大学 | Method for preparing alizarin red rare-earth chromium dye |
| CN101580647A (en) * | 2009-06-11 | 2009-11-18 | 五邑大学 | Preparation method of liquid plant dye |
| CN105178067A (en) * | 2015-09-28 | 2015-12-23 | 江苏丹毛纺织股份有限公司 | Technology method for wool tops dyed with madder plant dye |
-
2017
- 2017-08-17 CN CN201710706150.8A patent/CN107501992A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1730564A (en) * | 2005-08-11 | 2006-02-08 | 上海交通大学 | Preparation method of gamene vegetable dye |
| CN1844257A (en) * | 2006-03-21 | 2006-10-11 | 宁波大学 | Method for preparing alizarin red rare-earth chromium dye |
| CN101580647A (en) * | 2009-06-11 | 2009-11-18 | 五邑大学 | Preparation method of liquid plant dye |
| CN105178067A (en) * | 2015-09-28 | 2015-12-23 | 江苏丹毛纺织股份有限公司 | Technology method for wool tops dyed with madder plant dye |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108997775A (en) * | 2018-06-20 | 2018-12-14 | 马鞍山中粮生物化学有限公司 | A kind of extracting method of natural madder red edible pigment |
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Application publication date: 20171222 |
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