CN107468617A - A kind of Essence of crease-resistant moisturizing and preparation method thereof - Google Patents
A kind of Essence of crease-resistant moisturizing and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
The invention discloses a kind of Essence of crease-resistant moisturizing, it is made up of the raw material below according to parts by weight：36 parts of polygonin, 12 16 parts of FOLIUM HIBISCI MUTABILIS extract solution, 18 22 parts of felwort extract solution, 13 17 parts of tuber of pinellia extract solution, 25 parts of VC ethylethers, 12 parts of IPM, 23 parts of trehalose, 0.3 0.7 parts of tetrahydro curcumin, 12 parts of alcohol of triolefin fertility, 1.5 2.0 parts of glycerine, 34 parts of hyaluronic acid, 23 parts of oat beta glucan, 23 parts of sorbitan monostearate, 90 95 parts of deionized water.The invention also discloses the preparation method of the Essence of the crease-resistant moisturizing.Essence prepared by the present invention can Glycerin, reduce skin wrinkle, to skin carry out continue moisturizing, improve the coarse situation of scaly dry skin, easy to use, positive effect.
Description
Technical field
The present invention relates to cosmetic technical field, specifically a kind of Essence of crease-resistant moisturizing and preparation method thereof.
Background technology
With age ageing, the visual appearance of Long Term Contact adverse environmental factors or malnutritive skin, physical characteristic and
Physiological function changes, it is considered to be cosmetically undesirable.Clinically often show as pachylosis, drying, sensitivity
Property and fragility increase, cutis laxa, elasticity reduce, wrinkle increase, atrophoderma.These agings all with the age, hypometabolism,
Long Term Contact adverse environmental factors or malnutrition have close relationship.
With the progress and expanding economy and the continuous improvement of living standards of the people of society, people are to beauty and skin care
Cosmetic is increasingly paid attention to.Essence is exactly one kind in beauty and skin care cosmetics.Essence is the superfine product in skin care item, and composition is smart
Cause, effect is powerful, significant effect, any skin or inclined oily skin can be applied to, after toner, face cream it
Before.The species of Essence is various, and effect is also different, and its effect includes anti-aging, crease-resistant, moisturizing, whitening, nti-freckle etc.
Deng.With the development in epoch, consumer proposes higher and higher performance requirement, existing crease-resistant moisturizing essence to Essence
It can not gradually meet the market demand because anti-wrinkle effect is not good enough.
The content of the invention
It is an object of the invention to provide a kind of Essence of crease-resistant moisturizing and preparation method thereof, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：Polygonin 3-6 parts, FOLIUM HIBISCI MUTABILIS extraction
Liquid 12-16 parts, felwort extract solution 18-22 parts, tuber of pinellia extract solution 13-17 parts, VC ethylether 2-5 parts, IPM 1-2
Part, trehalose 2-3 parts, tetrahydro curcumin 0.3-0.7 parts, triolefin fertility alcohol 1-2 parts, glycerine 1.5-2.0 parts, hyaluronic acid 3-4
Part, avenabeta glucosan 2-3 parts, sorbitan monostearate 2-3 parts, deionized water 90-95 parts.
As the further scheme of the present invention：It is made up of the raw material below according to parts by weight：Polygonin 4-5 parts, cotton rose
Leaf extract 13-15 parts, felwort extract solution 19-21 parts, tuber of pinellia extract solution 14-16 parts, VC ethylether 3-4 parts, nutmeg are different
Propyl ester 1.3-1.7 parts, trehalose 2.2-2.8 parts, tetrahydro curcumin 0.4-0.6 parts, triolefin fertility alcohol 1.3-1.8 parts, glycerine
1.6-1.9 parts, hyaluronic acid 3.1-3.7 parts, avenabeta glucosan 2.4-2.8 parts, sorbitan monostearate 2.2-2.5
Part, deionized water 91-94 parts.
As further scheme of the invention：It is made up of the raw material below according to parts by weight：4.3 parts of polygonin, wooden cottonrose hibiscus
14 parts of Rong's leaf extract, 20 parts of felwort extract solution, 15 parts of tuber of pinellia extract solution, 4 parts of VC ethylethers, 1.5 parts of IPM,
2.4 parts of trehalose, 0.5 part of tetrahydro curcumin, 1.6 parts of alcohol of triolefin fertility, 1.7 parts of glycerine, 3.3 parts of hyaluronic acid, oat β-Portugal
2.6 parts of glycan, 2.4 parts of sorbitan monostearate, 93 parts of deionized water.
As further scheme of the invention：The FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：Weigh cotton rose
Leaf, chopping, be sent into percolator, diacolation processing carried out using the ethanol water of 12-15 times of weight, obtain percolate and
Diacolation residue, diacolation residue is added to the water of 8-10 times of weight, soak 1-2h, infusion 1-2h, obtain infusion extract solution and infusion
Residue, percolate and infusion extract solution are merged, are concentrated by evaporation the 18-22% for original volume, obtain FOLIUM HIBISCI MUTABILIS extraction
Liquid.
As further scheme of the invention：The felwort extract solution is made by following methods：Felwort is weighed, is cut
It is broken, add the ethanol water of 8-10 times of weight, soak 2-3h, heating and refluxing extraction 1-2h, obtain reflux extracting liquid and
Refluxing extraction residue, the ethanol water of 6-7 times of weight is added into a reflux extracting liquid, soak 1-2h, heat back
Stream extraction 40-50min, secondary back extract solution and secondary back extraction residue are obtained, by a reflux extracting liquid and secondary returning
Flow extract solution to merge, be concentrated by evaporation the 25-30% for original volume, obtain felwort extract solution.
As further scheme of the invention：The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded,
The ethanol water of 5-6 times of weight is added, soaks 4-5h, ultrasonic extraction 50-60min, obtains ultrasonic extraction liquid and ultrasonic extraction
Residue, ultrasonic extraction residue is sent into autoclave, the water of 6-8 times of weight is added, at 0.18-0.20Mpa, 110-115 DEG C
Boiling 50-60min, cooking liquor and boiling residue are obtained, ultrasonic extraction liquid and cooking liquor are merged, are concentrated by evaporation as original volume
20-25%, obtain tuber of pinellia extract solution.
As further scheme of the invention：The extraction frequency of the ultrasonic extraction is 40-60KHz.
As further scheme of the invention：The concentration of alcohol of the ethanol water is 50-60%.
The preparation method of the Essence of the crease-resistant moisturizing, step are as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
30-35min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 40-50min,
Discharging, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
15-20min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 35-40min, is discharged,
Obtain the 4th mixture；
5）Second mixture and the 4th mixture are merged, glycerine and hyaluronic acid is added, ultrasonication 40-50min, obtains
5th mixture；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, the homogeneous at 50-55 DEG C
Handle 15-20min, you can.
As further scheme of the invention：Step 5）In, ultrasonication frequency is 80-100KHz.
Compared with prior art, the beneficial effects of the invention are as follows：
Essence prepared by the present invention can Glycerin, reduce skin wrinkle, recover elasticity of skin, to skin carry out continue guarantor
It is wet, improve the coarse situation of scaly dry skin, easy to use, positive effect, there is important market value and social value.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：3 parts of polygonin, FOLIUM HIBISCI MUTABILIS extract solution
12 parts, 18 parts of felwort extract solution, 13 parts of tuber of pinellia extract solution, 2 parts of VC ethylethers, 1 part of IPM, 2 parts of trehalose, four
0.3 part of hydrogen curcumin, 1 part of alcohol of triolefin fertility, 1.5 parts of glycerine, 3 parts of hyaluronic acid, 2 parts of avenabeta glucosan, anhydrous sorbitol
2 parts of monostearate, 90 parts of deionized water.
Wherein, the FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator,
Diacolation processing is carried out using the ethanol water of 12 times of weight, obtains percolate and diacolation residue, diacolation residue is added 8
The water of times weight, 1h, infusion 1h are soaked, obtain infusion extract solution and infusion residue, percolate and infusion extract solution are closed
And be concentrated by evaporation as the 18% of original volume, obtain FOLIUM HIBISCI MUTABILIS extract solution；
The felwort extract solution is made by following methods：Felwort is weighed, is shredded, adds the ethanol water of 8 times of weight, leaching
2h, heating and refluxing extraction 1h are steeped, obtains a reflux extracting liquid and a refluxing extraction residue, is added into a reflux extracting liquid
Enter the ethanol water of 6 times of weight, soak 1h, heating and refluxing extraction 40min, obtain secondary back extract solution and secondary back carries
Residue is taken, a reflux extracting liquid and secondary back extract solution are merged, is concentrated by evaporation as the 25% of original volume, obtains felwort
Extract solution；
The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 5 times of weight, immersion
4h, ultrasonic extraction 50min, ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is sent into autoclave, added
The water of 6 times of weight, the boiling 50min at 0.18Mpa, 110 DEG C, cooking liquor and boiling residue are obtained, by ultrasonic extraction liquid and steaming
Boil liquid merges, and is concentrated by evaporation as the 20% of original volume, obtains tuber of pinellia extract solution, the extraction frequency of the ultrasonic extraction is 40KHz.
The concentration of alcohol of above-mentioned ethanol water is 50%.
In the present embodiment, the preparation method of the Essence of the crease-resistant moisturizing, step is as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
30min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 40min, goes out
Material, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
15min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 35min, is discharged, is obtained
4th mixture；
5）Second mixture and the 4th mixture are merged, add glycerine and hyaluronic acid, ultrasonication 40min, obtains the
Five mixtures, wherein, ultrasonication frequency is 80KHz；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, at 50 DEG C at homogeneous
Manage 15min, you can.
Embodiment 2
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：4 parts of polygonin, FOLIUM HIBISCI MUTABILIS extract solution
13 parts, 21 parts of felwort extract solution, 16 parts of tuber of pinellia extract solution, 3 parts of VC ethylethers, 1.3 parts of IPM, trehalose 2.2
Part, 0.6 part of tetrahydro curcumin, triolefin fertility 1.8 parts of alcohol, 1.9 parts of glycerine, 3.1 parts of hyaluronic acid, 2.4 parts of avenabeta glucosan,
2.5 parts of sorbitan monostearate, 94 parts of deionized water.
Wherein, the FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator,
Diacolation processing is carried out using the ethanol water of 13 times of weight, obtains percolate and diacolation residue, diacolation residue is added 8
The water of times weight, 1.5h, infusion 1h are soaked, infusion extract solution and infusion residue are obtained, by percolate and infusion extract solution
Merge, be concentrated by evaporation as the 20% of original volume, obtain FOLIUM HIBISCI MUTABILIS extract solution；
The felwort extract solution is made by following methods：Felwort is weighed, is shredded, adds the ethanol water of 8.5 times of weight,
2.5h, heating and refluxing extraction 1h are soaked, a reflux extracting liquid and a refluxing extraction residue are obtained, to a reflux extracting liquid
The middle ethanol water for adding 6 times of weight, soaks 1h, heating and refluxing extraction 45min, obtains secondary back extract solution and secondary returning
Stream extraction residue, a reflux extracting liquid and secondary back extract solution are merged, and are concentrated by evaporation as the 26% of original volume, are obtained dragon
Courage grass extract solution；
The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 5 times of weight, immersion
4.5h, ultrasonic extraction 52min, ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is sent into autoclave, added
Enter the water of 6 times of weight, the boiling 55min at 0.20Mpa, 112 DEG C, obtain cooking liquor and boiling residue, by ultrasonic extraction liquid and
Cooking liquor merges, and is concentrated by evaporation as the 20% of original volume, obtains tuber of pinellia extract solution, and the extraction frequency of the ultrasonic extraction is
50KHz。
The concentration of alcohol of above-mentioned ethanol water is 50%.
In the present embodiment, the preparation method of the Essence of the crease-resistant moisturizing, step is as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
30min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 42min, goes out
Material, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
16min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 38min, is discharged, is obtained
4th mixture；
5）Second mixture and the 4th mixture are merged, add glycerine and hyaluronic acid, ultrasonication 45min, obtains the
Five mixtures, wherein, ultrasonication frequency is 80KHz；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, at 52 DEG C at homogeneous
Manage 16min, you can.
Embodiment 3
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：4.3 parts of polygonin, FOLIUM HIBISCI MUTABILIS extraction
14 parts of liquid, 20 parts of felwort extract solution, 15 parts of tuber of pinellia extract solution, 4 parts of VC ethylethers, 1.5 parts of IPM, trehalose
2.4 parts, 0.5 part of tetrahydro curcumin, triolefin fertility 1.6 parts of alcohol, 1.7 parts of glycerine, 3.3 parts of hyaluronic acid, avenabeta glucosan 2.6
Part, 2.4 parts of sorbitan monostearate, 93 parts of deionized water.
Wherein, the FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator,
Diacolation processing is carried out using the ethanol water of 13 times of weight, obtains percolate and diacolation residue, diacolation residue is added 9
The water of times weight, 1.5h, infusion 1.5h are soaked, obtain infusion extract solution and infusion residue, percolate and infusion are extracted
Liquid merges, and is concentrated by evaporation as the 20% of original volume, obtains FOLIUM HIBISCI MUTABILIS extract solution；
The felwort extract solution is made by following methods：Felwort is weighed, is shredded, adds the ethanol water of 9 times of weight, leaching
2.5h, heating and refluxing extraction 1.5h are steeped, a reflux extracting liquid and a refluxing extraction residue are obtained, to a reflux extracting liquid
The middle ethanol water for adding 7 times of weight, soaks 1.5h, heating and refluxing extraction 45min, obtains secondary back extract solution and secondary
Refluxing extraction residue, a reflux extracting liquid and secondary back extract solution are merged, are concentrated by evaporation as the 27% of original volume, obtain
Felwort extract solution；
The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 5.5 times of weight, immersion
4.5h, ultrasonic extraction 55min, ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is sent into autoclave, added
Enter the water of 7 times of weight, the boiling 55min at 0.19Mpa, 112 DEG C, obtain cooking liquor and boiling residue, by ultrasonic extraction liquid and
Cooking liquor merges, and is concentrated by evaporation as the 23% of original volume, obtains tuber of pinellia extract solution, and the extraction frequency of the ultrasonic extraction is
50KHz。
The concentration of alcohol of above-mentioned ethanol water is 55%.
In the present embodiment, the preparation method of the Essence of the crease-resistant moisturizing, step is as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
32min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 45min, goes out
Material, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
17min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 37min, is discharged, is obtained
4th mixture；
5）Second mixture and the 4th mixture are merged, add glycerine and hyaluronic acid, ultrasonication 45min, obtains the
Five mixtures, wherein, ultrasonication frequency is 90KHz；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, at 52 DEG C at homogeneous
Manage 18min, you can.
Embodiment 4
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：5 parts of polygonin, FOLIUM HIBISCI MUTABILIS extract solution
15 parts, 19 parts of felwort extract solution, 14 parts of tuber of pinellia extract solution, 4 parts of VC ethylethers, 1.7 parts of IPM, trehalose 2.8
Part, 0.4 part of tetrahydro curcumin, triolefin fertility 1.3 parts of alcohol, 1.6 parts of glycerine, 3.7 parts of hyaluronic acid, 2.8 parts of avenabeta glucosan,
2.2 parts of sorbitan monostearate, 91 parts of deionized water.
Wherein, the FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator,
Diacolation processing is carried out using the ethanol water of 14 times of weight, obtains percolate and diacolation residue, diacolation residue is added 9
The water of times weight, 2h, infusion 1.5h are soaked, infusion extract solution and infusion residue are obtained, by percolate and infusion extract solution
Merge, be concentrated by evaporation as the 22% of original volume, obtain FOLIUM HIBISCI MUTABILIS extract solution；
The felwort extract solution is made by following methods：Felwort is weighed, is shredded, adds the ethanol water of 9 times of weight, leaching
3h, heating and refluxing extraction 1.5h are steeped, a reflux extracting liquid and a refluxing extraction residue are obtained, into a reflux extracting liquid
The ethanol water of 7 times of weight is added, soaks 2h, heating and refluxing extraction 45min, obtains secondary back extract solution and secondary back
Residue is extracted, a reflux extracting liquid and secondary back extract solution are merged, is concentrated by evaporation as the 30% of original volume, obtains rough gentian
Careless extract solution；
The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 6 times of weight, immersion
5h, ultrasonic extraction 60min, ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is sent into autoclave, added
The water of 7 times of weight, the boiling 58min at 0.20Mpa, 115 DEG C, cooking liquor and boiling residue are obtained, by ultrasonic extraction liquid and steaming
Boil liquid merges, and is concentrated by evaporation as the 25% of original volume, obtains tuber of pinellia extract solution, the extraction frequency of the ultrasonic extraction is 60KHz.
The concentration of alcohol of above-mentioned ethanol water is 60%.
In the present embodiment, the preparation method of the Essence of the crease-resistant moisturizing, step is as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
32min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 50min, goes out
Material, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
18min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 40min, is discharged, is obtained
4th mixture；
5）Second mixture and the 4th mixture are merged, add glycerine and hyaluronic acid, ultrasonication 45min, obtains the
Five mixtures, wherein, ultrasonication frequency is 90KHz；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, at 55 DEG C at homogeneous
Manage 19min, you can.
Embodiment 5
A kind of Essence of crease-resistant moisturizing, is made up of the raw material below according to parts by weight：6 parts of polygonin, FOLIUM HIBISCI MUTABILIS extract solution
16 parts, 22 parts of felwort extract solution, 17 parts of tuber of pinellia extract solution, 5 parts of VC ethylethers, 2 parts of IPM, 3 parts of trehalose, four
0.7 part of hydrogen curcumin, 2 parts of alcohol of triolefin fertility, 2.0 parts of glycerine, 4 parts of hyaluronic acid, 3 parts of avenabeta glucosan, anhydrous sorbitol
3 parts of monostearate, 95 parts of deionized water.
Wherein, the FOLIUM HIBISCI MUTABILIS extract solution is made by following methods：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator,
Diacolation processing is carried out using the ethanol water of 15 times of weight, percolate and diacolation residue is obtained, diacolation residue is added
The water of 10 times of weight, 2h, infusion 2h are soaked, infusion extract solution and infusion residue are obtained, by percolate and infusion extract solution
Merge, be concentrated by evaporation as the 22% of original volume, obtain FOLIUM HIBISCI MUTABILIS extract solution；
The felwort extract solution is made by following methods：Felwort is weighed, is shredded, adds the ethanol water of 10 times of weight,
3h, heating and refluxing extraction 2h are soaked, a reflux extracting liquid and a refluxing extraction residue are obtained, into a reflux extracting liquid
The ethanol water of 7 times of weight is added, soaks 2h, heating and refluxing extraction 50min, obtains secondary back extract solution and secondary back
Residue is extracted, a reflux extracting liquid and secondary back extract solution are merged, is concentrated by evaporation as the 30% of original volume, obtains rough gentian
Careless extract solution；
The tuber of pinellia extract solution is made by following methods：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 6 times of weight, immersion
5h, ultrasonic extraction 60min, ultrasonic extraction liquid and ultrasonic extraction residue are obtained, ultrasonic extraction residue is sent into autoclave, added
The water of 8 times of weight, the boiling 60min at 0.20Mpa, 115 DEG C, cooking liquor and boiling residue are obtained, by ultrasonic extraction liquid and steaming
Boil liquid merges, and is concentrated by evaporation as the 25% of original volume, obtains tuber of pinellia extract solution, the extraction frequency of the ultrasonic extraction is 60KHz.
The concentration of alcohol of above-mentioned ethanol water is 60%.
In the present embodiment, the preparation method of the Essence of the crease-resistant moisturizing, step is as follows：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
35min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 50min, goes out
Material, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
20min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 40min, is discharged, is obtained
4th mixture；
5）Second mixture and the 4th mixture are merged, add glycerine and hyaluronic acid, ultrasonication 50min, obtains the
Five mixtures, wherein, ultrasonication frequency is 100KHz；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, at 55 DEG C at homogeneous
Manage 20min, you can.
In order to which the Essence prepared to the present invention carries out compliance test result, tests below is carried out：
The coarse experimenter of 100 cutis laxa, scaly dry skin is selected, the age is between 35-52 year.
Application method：After thorough clean skin, the Essence prepared by embodiment 3 is uniformly smeared on skin, gently patted,
Once in the morning and once at night, 30 days courses for the treatment of, 3 courses for the treatment of are used.
Curative effect determinate standard：
It is effective：User feels very satisfied, and the flexible more consolidation children of skin is sliding, and water profit is glossy, and wrinkle substantially subtracts
It is few；Dermatoglyph density significantly reduces under microscope.
Effectively：User feels general satisfaction, and skin elasticity gloss lubricity increased；Wrinkle has been reduced；
Dermatoglyph density has been reduced under microscope.
It is invalid：User feels dissatisfied, and the coarse dry sensation of skin is not improved, and wrinkle is without reduction, skin bullet
Property gloss lubricity is without increase；Dermatoglyph density is not improved under microscope.
After use by 3 courses for the treatment of, this 100 experimenters are paid a return visit and recorded, effective 65, effective 31,
Invalid 4, total effective rate 96%.Experimenter is without allergy or other toxicities.
Essence prepared by the present invention can Glycerin, reduce skin wrinkle, recover elasticity of skin, skin is held
Continue insurance wet, improve the coarse situation of scaly dry skin, easy to use, positive effect, there is important market value and social value.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula, can also be on the premise of present inventive concept not be departed from one skilled in the relevant art's possessed knowledge
Various changes can be made.
Claims (10)
1. a kind of Essence of crease-resistant moisturizing, it is characterised in that be made up of the raw material below according to parts by weight：Polygonin 3-6 parts,
FOLIUM HIBISCI MUTABILIS extract solution 12-16 parts, felwort extract solution 18-22 parts, tuber of pinellia extract solution 13-17 parts, VC ethylether 2-5 parts, meat
Cardamom isopropyl ester 1-2 parts, trehalose 2-3 parts, tetrahydro curcumin 0.3-0.7 parts, triolefin fertility alcohol 1-2 parts, glycerine 1.5-2.0
Part, hyaluronic acid 3-4 parts, avenabeta glucosan 2-3 parts, sorbitan monostearate 2-3 parts, deionized water 90-95 parts.
2. the Essence of crease-resistant moisturizing according to claim 1, it is characterised in that by below according to the raw material system of parts by weight
Into：Polygonin 4-5 parts, FOLIUM HIBISCI MUTABILIS extract solution 13-15 parts, felwort extract solution 19-21 parts, tuber of pinellia extract solution 14-16 parts, VC
Ethylether 3-4 parts, IPM 1.3-1.7 parts, trehalose 2.2-2.8 parts, tetrahydro curcumin 0.4-0.6 parts, triolefin life
Educate alcohol 1.3-1.8 parts, glycerine 1.6-1.9 parts, hyaluronic acid 3.1-3.7 parts, avenabeta glucosan 2.4-2.8 parts, Sorbitan
Alcohol monostearate 2.2-2.5 parts, deionized water 91-94 parts.
3. the Essence of crease-resistant moisturizing according to claim 2, it is characterised in that by below according to the raw material system of parts by weight
Into：4.3 parts of polygonin, 14 parts of FOLIUM HIBISCI MUTABILIS extract solution, 20 parts of felwort extract solution, 15 parts of tuber of pinellia extract solution, VC ethylethers 4
Part, 1.5 parts of IPM, 2.4 parts of trehalose, 0.5 part of tetrahydro curcumin, triolefin fertility 1.6 parts of alcohol, 1.7 parts of glycerine, thoroughly
Bright 3.3 parts of matter acid, 2.6 parts of avenabeta glucosan, 2.4 parts of sorbitan monostearate, 93 parts of deionized water.
4. the Essence of crease-resistant moisturizing according to claim 1, it is characterised in that the FOLIUM HIBISCI MUTABILIS extract solution is by following
Method is made：FOLIUM HIBISCI MUTABILIS is weighed, is shredded, is sent into percolator, is carried out using the ethanol water of 12-15 times of weight at diacolation
Reason, percolate and diacolation residue are obtained, diacolation residue is added to the water of 8-10 times of weight, soaked 1-2h, infusion 1-2h, obtain
Infusion extract solution and infusion residue are obtained, percolate and infusion extract solution are merged, are concentrated by evaporation the 18-22% for original volume,
Obtain FOLIUM HIBISCI MUTABILIS extract solution.
5. the Essence of crease-resistant moisturizing according to claim 1, it is characterised in that the felwort extract solution is by with lower section
Method is made：Felwort is weighed, is shredded, adds the ethanol water of 8-10 times of weight, soaks 2-3h, heating and refluxing extraction 1-2h,
A reflux extracting liquid and a refluxing extraction residue are obtained, the ethanol water of 6-7 times of weight is added into a reflux extracting liquid
Solution, 1-2h, heating and refluxing extraction 40-50min are soaked, secondary back extract solution and secondary back extraction residue are obtained, by one
Secondary reflux extracting liquid and secondary back extract solution merges, and is concentrated by evaporation the 25-30% for original volume, obtains felwort extract solution.
6. the Essence of crease-resistant moisturizing according to claim 1, it is characterised in that the tuber of pinellia extract solution is by following methods
It is made：The tuber of pinellia is weighed, is shredded, adds the ethanol water of 5-6 times of weight, 4-5h is soaked, ultrasonic extraction 50-60min, is surpassed
Sound extract solution and ultrasonic extraction residue, ultrasonic extraction residue is sent into autoclave, the water of 6-8 times of weight is added, in 0.18-
Boiling 50-60min at 0.20Mpa, 110-115 DEG C, cooking liquor and boiling residue are obtained, ultrasonic extraction liquid and cooking liquor are closed
And the 20-25% for original volume is concentrated by evaporation, obtain tuber of pinellia extract solution.
7. the Essence of crease-resistant moisturizing according to claim 6, it is characterised in that the extraction frequency of the ultrasonic extraction is
40-60KHz。
8. the Essence of the crease-resistant moisturizing according to claim 4 or 5 or 6, it is characterised in that the second of the ethanol water
Determining alcohol is 50-60%.
9. the preparation method of the Essence of a kind of crease-resistant moisturizing as described in claim 1-8 is any, it is characterised in that step is such as
Under：
1）Polygonin, FOLIUM HIBISCI MUTABILIS extract solution and IPM are weighed, is put into magnetic stirrer, magnetic agitation mixing
30-35min, obtain the first mixture；
2）Tetrahydro curcumin and triolefin fertility alcohol are weighed, is added into the first mixture, continues magnetic agitation mixing 40-50min,
Discharging, obtain the second mixture；
3）Felwort extract solution, tuber of pinellia extract solution and VC ethylethers are weighed, is put into magnetic stirrer, magnetic agitation mixing
15-20min, obtain the 3rd mixture；
4）Trehalose and avenabeta glucosan are weighed, is added into the 3rd mixture, continues magnetic agitation 35-40min, is discharged,
Obtain the 4th mixture；
5）Second mixture and the 4th mixture are merged, glycerine and hyaluronic acid is added, ultrasonication 40-50min, obtains
5th mixture；
6）5th mixture, sorbitan monostearate and deionized water are sent into emulsification pot, the homogeneous at 50-55 DEG C
Handle 15-20min, you can.
10. the preparation method of the Essence of crease-resistant moisturizing according to claim 9, it is characterised in that step 5）In, ultrasound
Ripple processing frequency is 80-100KHz.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710824042.0A CN107468617A (en) | 2017-09-13 | 2017-09-13 | A kind of Essence of crease-resistant moisturizing and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114632046A (en) * | 2022-04-18 | 2022-06-17 | 成都花荟缘文化发展有限公司 | Uvioresistant hibiscus perfume and preparation method thereof |
| AU2019249392B2 (en) * | 2018-04-03 | 2022-10-20 | Sami Labs Limited | Skin care compositions and their applications |
-
2017
- 2017-09-13 CN CN201710824042.0A patent/CN107468617A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2019249392B2 (en) * | 2018-04-03 | 2022-10-20 | Sami Labs Limited | Skin care compositions and their applications |
| CN114632046A (en) * | 2022-04-18 | 2022-06-17 | 成都花荟缘文化发展有限公司 | Uvioresistant hibiscus perfume and preparation method thereof |
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Application publication date: 20171215 |