CN107467639A - A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder - Google Patents
A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder Download PDFInfo
- Publication number
- CN107467639A CN107467639A CN201610400851.4A CN201610400851A CN107467639A CN 107467639 A CN107467639 A CN 107467639A CN 201610400851 A CN201610400851 A CN 201610400851A CN 107467639 A CN107467639 A CN 107467639A
- Authority
- CN
- China
- Prior art keywords
- oat bran
- powder
- dietary fiber
- filtrate
- oat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000843 powder Substances 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 25
- 235000013325 dietary fiber Nutrition 0.000 title claims abstract description 19
- 235000015097 nutrients Nutrition 0.000 title claims abstract description 17
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 title abstract description 18
- 229920002498 Beta-glucan Polymers 0.000 title abstract description 18
- 229940038580 oat bran Drugs 0.000 claims abstract description 40
- 102000004190 Enzymes Human genes 0.000 claims abstract description 13
- 108090000790 Enzymes Proteins 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- XXRYFVCIMARHRS-UHFFFAOYSA-N propan-2-yl n-dimethoxyphosphorylcarbamate Chemical compound COP(=O)(OC)NC(=O)OC(C)C XXRYFVCIMARHRS-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002699 waste material Substances 0.000 claims abstract description 8
- 238000000227 grinding Methods 0.000 claims abstract description 7
- 239000006228 supernatant Substances 0.000 claims abstract description 7
- 239000012141 concentrate Substances 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000002244 precipitate Substances 0.000 claims abstract description 6
- 239000000706 filtrate Substances 0.000 claims description 25
- 229920001503 Glucan Polymers 0.000 claims description 18
- TWNIBLMWSKIRAT-VFUOTHLCSA-N levoglucosan Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@H]2CO[C@@H]1O2 TWNIBLMWSKIRAT-VFUOTHLCSA-N 0.000 claims description 17
- 238000001914 filtration Methods 0.000 claims description 8
- 239000004382 Amylase Substances 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 235000013339 cereals Nutrition 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 235000016709 nutrition Nutrition 0.000 claims description 5
- 230000035764 nutrition Effects 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000000284 extract Substances 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 238000004062 sedimentation Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 238000000926 separation method Methods 0.000 abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 11
- 239000000047 product Substances 0.000 description 10
- 238000001556 precipitation Methods 0.000 description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 229920002472 Starch Polymers 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 235000018102 proteins Nutrition 0.000 description 5
- 102000004169 proteins and genes Human genes 0.000 description 5
- 108090000623 proteins and genes Proteins 0.000 description 5
- 239000008107 starch Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 235000019698 starch Nutrition 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 102000013142 Amylases Human genes 0.000 description 3
- 108010065511 Amylases Proteins 0.000 description 3
- 235000019418 amylase Nutrition 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 235000017550 sodium carbonate Nutrition 0.000 description 3
- 238000000108 ultra-filtration Methods 0.000 description 3
- 235000015099 wheat brans Nutrition 0.000 description 3
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 2
- 102000002322 Egg Proteins Human genes 0.000 description 2
- 108010000912 Egg Proteins Proteins 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 235000014103 egg white Nutrition 0.000 description 2
- 210000000969 egg white Anatomy 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000186000 Bifidobacterium Species 0.000 description 1
- 229920000018 Callose Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 238000005227 gel permeation chromatography Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000008235 industrial water Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000005374 membrane filtration Methods 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of oat bran method of comprehensive utilization.This method carries out intensive processing to oat bran using biological enzyme and Crushing of Ultrafine method, Joint Production beta glucan nutrient powder, dietary fiber micro powder and avenin, a kind of new production method is provided for oat bran comprehensive utilization.This method first crushes oat bran, first carry out microwave deactivating enzyme, filtered after hot water stirs' extraction, the supernatant enzymolysis of separation, isoelectric point are concentrated in vacuo after being separated off albumen, concentrate is spray-dried to be prepared into oat beta glucan nutrient powder, ultramicro grinding after the drying precipitate that waste residue after being extracted to oat bran centrifuges out, is prepared into dietary fiber micro powder.
Description
Technical field
The invention belongs to technical field of food biotechnology, is related to a kind of oat bran intensive processing technology, specifically with oat
Wheat bran is raw material, utilizes the skill of biological enzyme Joint Production avenabeta glucosan nutrient powder, dietary fiber micro powder and avenin
Art.
Background technology
Oat has higher nutritive value, compared with other cereal, in protein, dimension life as a kind of rain fed crops
The nutrient index contents such as element, mineral element and dietary fiber are high, and nutrition equilibrium modern studies show, protein content in oat
It is abundant, occupy the first in cereal, and the essential amino acid Compositional balance in avenin, its amino acid pattern is close to FAO/
The provisional pattern of amino acids that WHO is promulgated is in addition, be rich in soluble dietary fiber beta glucan and insoluble meals in oat bran
Fiber.Its chemical name of beta glucan is(1-3)(1-4)- callose, it is a kind of non-starch linear polysaccharide, it is raw at present
The general physiological action for thinking beta glucan of thing medical field and nutrition educational circles mainly have gut purge effect, reconcile blood glucose, reduce cholesterol,
Improve immunity.And insoluble dietary fiber plays important life to fat-reducing, diabetes mellitus prevention, promotion function of intestinal canal improvement etc.
Manage adjustment effect.
In existing patented technology, existing some reports on extracting beta glucan from oat, such as patent
200710018232 provide a kind of method for separating glucan from cereal bran using membrane separation technique, and this method utilizes egg
White matter solubility in alkalescence, normal temperature is maximum, and the principle that can be separated out in acid condition, extracts cereal with ethanol and water respectively
Albumen in seed, extract solution are centrifuged, and after acid is heavy after filtrate is enriched with using membrane separation technique, then carry out alcohol precipitation,
Centrifuge, and membrane filtration is used after precipitation is carried out into precipitation, obtain refined beta glucan.But due in alcohol precipitation process
Middle to use ethanol, ethanol is not high to the selectivity of the beta glucan in solution, causes the beta glucan purity of preparation not high, yield
It is low.In addition, ethanol belongs to inflammable explosive article, there can be many requirements to the environment and safety of production plant, increase production cost.
A kind of method for extraction avenabeta glucosan that patent 200610089486.6 is recorded, comprises the following steps:1st, will
Oat bran is at 50-60 DEG C plus water stirs, and adjusts PH8-10;2nd, add protease and hydrolysis oat bran is handled at 45-60 DEG C
Albumen in skin adds;3rd, amylase is handled at 80 DEG C, filtering, obtains supernatant liquid;4th, use molecular cut off for
30000-50000Da ultrafiltration membrance filter, obtains beta glucan solution, and freeze-drying obtains beta glucan product, has purity
85% effect.
The preparation method step that patent 200610097431.X describes a kind of avenabeta glucosan is, using oat bran as original
Material, through crushing, microwave radiation exaraction plus amylase and saccharification ferment treatment, isoelectric precipitation, centrifugation, supernatant concentration, second
Alcohol precipitation, centrifuge and collect precipitation plus water redissolutions, beta glucan enzyme hydrolysis, obtained with significant after spray-drying process
Promote enteron aisle and faecal bifidobacteria, the high-purity avenabeta glucosan product of Bacillus acidi lactici increment effect.
Patent is that a kind of preparation method of 03147786.0 avenabeta glucosan recorded comprises the following steps 1, oat system
It is standby into oat bran, enzyme deactivation;2nd, under the conditions of 45-60 DEG C, add water to stir, be adjusted to PH9-11;3rd, filtrate is collected after separating, is added
Enter ɑ-starch ferment treatment, 70-90 DEG C of holding 1-2 hour;4th, 10-30 DEG C is cooled to, 4.5-5 is adjusted to, is stood after stirring, is sunk
Shallow lake protein;5th, supernatant is centrifuged to obtain, is concentrated by ultrafiltration, isopropanol is added in concentrate, obtains beta glucan gelatinous precipitate;
6th, beta glucan gelatinous precipitate is centrifuged, vacuum drying, obtains beta glucan product.
The method that above-mentioned technical proposal prepares beta glucan using oat or oat bran, mostly chemical method, Enzymatic Extraction,
Extracted using organic solvent, gentle alkali extraction method and saturation sulfuric acid be by precipitation.These methods are required for introducing organic solvent, separation
Product afterwards has chemical residual, and water consumption is larger, and wastewater treatment capacity is big.Also the technical scheme having using gel chromatography separation and
The methods of ultrafiltration membrance filter, but all because cost height is only applicable to laboratory operation, industrialized production can not be carried out.Utilizing swallow
There is starch, protein and insoluble diedairy fiber during wheat bran skin extraction beta glucan to discard with waste material, causes
The loss of nutrient in oat.Oat starch, oat egg white matter and insoluble diedairy fiber also have excellent nutrition and processing
Characteristic.If using starch, protein and dietary fiber only as the accessory substance in avenabeta glucosan extraction process without being subject to
Make full use of, not only cause actual production inefficiencies, high expensive, can also bring serious environmental pollution.Therefore, it is of the invention
Nutrient synthesis in oat is used the angle extracted and produced from full constituent.
The content of the invention
The present invention is a kind of from oat bran so as to provide in order to solve the comprehensive utilization development problem for improving oat bran
The method that middle extraction prepares avenabeta glucosan nutrient powder, dietary fiber micro powder and avenin.
A kind of coproduction of the present invention makes avenabeta glucosan nutrient powder and the method for dietary fiber micro powder, its technical scheme bag
Include following steps:
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, adjust pH value 9 or so, are extracted 2 hours at 40-50 DEG C, with 100
Mesh filter-cloth filtering, collect filtrate;
3rd, filtrate is regathered after above-mentioned filtrate is centrifuged with 4000rpm, filtrate is collected and is cooled to 20-30 DEG C, use diatomite
Plate-frame filtering obtains filtrate, and adjustment pH value is 4.0, stands 2 hours after stirring, then centrifuges to obtain oat again with 10000rpm
Protein solid and separating liquid;
4th, add in filtrate isolated in low temperature ɑ-amylase to step 3, adjust by the 1%-1.5% mass of oat bran raw material
PH value to neutrality, stir process is concentrated in vacuo after 1 hour, and concentrate is spray-dried to be prepared into avenabeta glucosan nutrient powder;
5th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, that isolates is upper
Clear liquid is returned in the filtrate of step 3, ultramicro grinding after the drying precipitate centrifuged out, is prepared into dietary fiber micro powder.
The present invention has the beneficial effect that:
1st, the oat bran after oat processing flour is used to obtain avenabeta glucosan nutrition simultaneously by joint production process for raw material
Three kinds of powder, dietary fiber micro powder and avenin products, accomplish that the nutrient in oat bran utilizes comprehensively, greatly improve main product
The added value of product and byproduct;
2nd, the present invention uses microwave deactivating enzyme technology, is passivated the activity of enzyme in wheat bran, extends shelf life of products, is gone out with conventional vapor
Enzyme, have the advantages that it is quick, efficiently, low energy consumption and easily controllable;
3rd, the present invention uses biological enzymolysis technology, compared with conventional chemical methods extract, is more conducive to environmental protection, and produced in enterprise
Cheng Zhong, industrial water is saved, reduce the processing cost of trade effluent;
4th, in present invention process using microwave deactivating enzyme, biological enzymolysis, etc. the technology such as electrically separated and ultramicro grinding realize oat resource
The reasonable utilization of exploitation, realizes the high added value complete utilization of waste resource, reduces production cost.
Embodiment
Embodiment 1
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, use edible soda ash(Sodium carbonate)PH value 9 or so is adjusted, in 40-
50 DEG C are extracted 2 hours, with 100 mesh filter-cloth filterings, collect filtrate;
3rd, filtrate is regathered after filtrate is centrifuged with 4000rpm, is cooled to 20-30 DEG C, is obtained with diatomite plate-frame filtering
Filtrate, food-grade acetic acid or citric acid adjustment pH value are 4.0, stand 2 hours after stirring, are then centrifuged again with 10000rpm
Obtain avenin solid and filtrate;
4th, add in filtrate isolated in low temperature ɑ-amylase to step 3, use by the 1%-1.5% mass of oat bran raw material
Edible soda ash adjusts pH value to neutrality, and it is 40% that stir process, which is concentrated in vacuo to material concentration for 1 hour, the spray-dried system of concentrate
It is standby into avenabeta glucosan nutrient powder;
5th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, the supernatant isolated
Return in the filtrate of step 3, the oat slag sediment isolated, ultramicro grinding after drying, be prepared into dietary fiber micro powder.
This embodiment can produce major product avenabeta glucosan nutrient powder and byproduct dietary fiber micro powder and oat egg
In vain.
Embodiment 2
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, by the 1%-1.5% mass of oat bran raw material add low temperature ɑ-
Amylase, extracted 2 hours at 40-50 DEG C, with 100 mesh filter-cloth filterings, collect filtrate;
3rd, for filtrate through being concentrated in vacuo to material concentration 40%, concentrate is spray-dried to be prepared into avenabeta glucosan nutrient powder;
4th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, the supernatant isolated
Return in the filtrate of step 3, the oat slag sediment isolated, ultramicro grinding after drying, be prepared into dietary fiber micro powder.
This embodiment can produce major product avenabeta glucosan nutrient powder(Include avenin)And byproduct meals are fine
Tie up micro mist.
Claims (4)
1. a kind of coproduction prepares avenabeta glucosan nutrient powder and the method for dietary fiber micro powder, comprise the following steps:
1., by after crushing oat bran powder carry out microwave deactivating enzyme;
2., by oat bran powder and deionized water with 1:10 mixing, adjust pH value 9 or so, are extracted 2 hours at 40-50 DEG C, use
100 mesh filter-cloth filterings, collect filtrate;
3., the filtrate of step 2. is centrifuged with 4000rpm after regather filtrate, using being centrifuged after isoelectric point deproteinized
Obtain avenin solid and centrate;
4., add low temperature ɑ-amylase to step 3. by the 1%-1.5% mass of oat bran raw material in isolated separating liquid
In, adjust pH value to neutrality, stir process to be concentrated in vacuo for 1 hour, concentrate is spray-dried to be prepared into avenabeta glucosan nutrition
Powder;
5., ultramicro grinding after the drying precipitate that is centrifuged out to the waste residue after the step 2. extraction of middle oat bran, be prepared into
Dietary fiber micro powder.
2. according to the method for claim 1, it is characterised in that the oat bran is adopted by the cereal kernel of removal endosperm
Mechanically it is ground into 60-100 mesh.
3. according to the method for claim 1, it is characterised in that step 2. it is described 4000rpm is centrifuged after regather
Filtrate is cooled to 20-30 DEG C, obtains filtrate with diatomite plate-frame filtering, adjustment pH value is 4.0, stands 2 hours after stirring, then
Avenin solid and separating liquid are centrifuged to obtain with 10000rpm again.
4. according to the method for claim 1, it is characterised in that step 5. it is described to oat bran extract after waste residue, adopt
Separated with horizontal spiral discharge sedimentation centrifuge, the supernatant isolated is returned in the filtrate of step 3., is centrifuged
Ultramicro grinding after the drying precipitate gone out, is prepared into dietary fiber micro powder.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610400851.4A CN107467639A (en) | 2016-06-08 | 2016-06-08 | A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610400851.4A CN107467639A (en) | 2016-06-08 | 2016-06-08 | A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder |
Publications (1)
Publication Number | Publication Date |
---|---|
CN107467639A true CN107467639A (en) | 2017-12-15 |
Family
ID=60593486
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610400851.4A Pending CN107467639A (en) | 2016-06-08 | 2016-06-08 | A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107467639A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113519859A (en) * | 2021-07-21 | 2021-10-22 | 内蒙古阴山优麦食品有限公司 | Preparation process of high-content oat beta-glucan dietary fiber powder |
WO2023126058A1 (en) * | 2021-12-30 | 2023-07-06 | Oatly Ab | A continuous process and system for preparing a liquid oat base or drink from an oat derived material |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1566161A (en) * | 2003-06-26 | 2005-01-19 | 中国农业科学院农产品加工研究所 | Process for preparing oat-beta glucan |
CN1966531A (en) * | 2006-11-08 | 2007-05-23 | 江南大学 | Process for preparing oat beta-glucans |
CN1973681A (en) * | 2006-12-13 | 2007-06-06 | 山西金绿禾燕麦研究所 | Technological process of producing oat diet fiber and nutritious powder with oat bran |
CN101805774A (en) * | 2010-03-12 | 2010-08-18 | 南通康麦生物科技有限公司 | Method for comprehensively extracting oat polypeptide and oat glucan |
CN101828668A (en) * | 2010-04-13 | 2010-09-15 | 山东轻工业学院 | Method for preparing dietary fiber by combining enzymatic alkaline method and wet ultra-micro pulverization |
CN101857646A (en) * | 2010-05-27 | 2010-10-13 | 山西金绿禾燕麦研究所 | Method for extracting high-purity beta-glucan and whole oat flour from oat bran |
CN102835616A (en) * | 2011-06-23 | 2012-12-26 | 庞兵 | Oat bran nutrition powder and dietary fibers |
CN103772527A (en) * | 2014-02-24 | 2014-05-07 | 常州毅博生物科技有限公司 | Method for extracting high-purity beta-glucosan from oat bran |
-
2016
- 2016-06-08 CN CN201610400851.4A patent/CN107467639A/en active Pending
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1566161A (en) * | 2003-06-26 | 2005-01-19 | 中国农业科学院农产品加工研究所 | Process for preparing oat-beta glucan |
CN1966531A (en) * | 2006-11-08 | 2007-05-23 | 江南大学 | Process for preparing oat beta-glucans |
CN1973681A (en) * | 2006-12-13 | 2007-06-06 | 山西金绿禾燕麦研究所 | Technological process of producing oat diet fiber and nutritious powder with oat bran |
CN101805774A (en) * | 2010-03-12 | 2010-08-18 | 南通康麦生物科技有限公司 | Method for comprehensively extracting oat polypeptide and oat glucan |
CN101828668A (en) * | 2010-04-13 | 2010-09-15 | 山东轻工业学院 | Method for preparing dietary fiber by combining enzymatic alkaline method and wet ultra-micro pulverization |
CN101857646A (en) * | 2010-05-27 | 2010-10-13 | 山西金绿禾燕麦研究所 | Method for extracting high-purity beta-glucan and whole oat flour from oat bran |
CN102835616A (en) * | 2011-06-23 | 2012-12-26 | 庞兵 | Oat bran nutrition powder and dietary fibers |
CN103772527A (en) * | 2014-02-24 | 2014-05-07 | 常州毅博生物科技有限公司 | Method for extracting high-purity beta-glucosan from oat bran |
Non-Patent Citations (1)
Title |
---|
祝钧 等主编: "《化妆品植物学》", 31 July 2009, 中国农业大学出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113519859A (en) * | 2021-07-21 | 2021-10-22 | 内蒙古阴山优麦食品有限公司 | Preparation process of high-content oat beta-glucan dietary fiber powder |
WO2023126058A1 (en) * | 2021-12-30 | 2023-07-06 | Oatly Ab | A continuous process and system for preparing a liquid oat base or drink from an oat derived material |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Tang et al. | Recovery of protein from brewer's spent grain by ultrafiltration | |
US20220080333A1 (en) | Ultrasonic composite acidic water extraction method for cordyceps polysaccharide and cordycepin in cordyceps militaris | |
CN101948897B (en) | Method for extracting shinyleaf yellowhorn oil, shinyleaf yellowhorn polysaccharide and shinyleaf yellowhorn protolysate peptide from shinyleaf yellowhorn | |
CN106333193B (en) | Full-resource utilization method of sweet potato starch processing wastewater | |
CN101766282B (en) | Process method for simultaneously extracting soybean function factor and therapeutic factor from bean pulp | |
WO2018196476A1 (en) | Process for preparing decolored concentrated fresh momordica grosvenori juice | |
CN101805774B (en) | Method for comprehensively extracting oat polypeptide and oat glucan | |
CN109608559A (en) | A method of extracting active polysaccharide from seaweed | |
CN1489923A (en) | Method for producing soya protein bioactive peptide | |
CN107858393A (en) | A kind of method that polypeptide is extracted from walnut dregs | |
CN108112728B (en) | Process for extracting active ingredients from tea | |
CN106213523A (en) | A kind of extracting method of Salicornia Bigelovii Torr. dietary fiber | |
CN101120776A (en) | Method for extracting beta-glucan from cereal bran using membrane separation technology | |
CN101455398A (en) | Soya-dregs water soluble diet fiber preparation method using nano filtration and spray-drying method | |
CN104757564A (en) | Method for preparing dietary fibers by means of peanut shells | |
CN110746515A (en) | Lycium barbarum polysaccharide, lycium barbarum red element and lycium barbarum polypeptide prepared by synchronous separation and preparation method thereof | |
KR101170685B1 (en) | Method for producing a water-soluble dietary fiber from a rice by-products | |
CN107467639A (en) | A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder | |
CN101884361A (en) | Separated oat protein preparation process | |
CN114457132A (en) | Method for preparing starch and non-thermal denatured protein powder by using rice as raw material | |
CN103436577A (en) | Integrated method for directly producing modified soybean protein from soybean meal | |
CN101095454B (en) | Method of separating protein from cereal kernel by adopting membrane separation technique | |
CN1709141A (en) | Method for producing water-soluble pollen | |
CN117186264A (en) | Green and efficient highland barley beta-glucan extraction method | |
CN104830927B (en) | A kind of method that forulic acid oligosaccharide syrup is prepared using wheat bran |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171215 |
|
RJ01 | Rejection of invention patent application after publication |