CN107467639A - A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder - Google Patents

A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder Download PDF

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Publication number
CN107467639A
CN107467639A CN201610400851.4A CN201610400851A CN107467639A CN 107467639 A CN107467639 A CN 107467639A CN 201610400851 A CN201610400851 A CN 201610400851A CN 107467639 A CN107467639 A CN 107467639A
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oat bran
powder
dietary fiber
filtrate
oat
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朱明达
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention relates to a kind of oat bran method of comprehensive utilization.This method carries out intensive processing to oat bran using biological enzyme and Crushing of Ultrafine method, Joint Production beta glucan nutrient powder, dietary fiber micro powder and avenin, a kind of new production method is provided for oat bran comprehensive utilization.This method first crushes oat bran, first carry out microwave deactivating enzyme, filtered after hot water stirs' extraction, the supernatant enzymolysis of separation, isoelectric point are concentrated in vacuo after being separated off albumen, concentrate is spray-dried to be prepared into oat beta glucan nutrient powder, ultramicro grinding after the drying precipitate that waste residue after being extracted to oat bran centrifuges out, is prepared into dietary fiber micro powder.

Description

A kind of coproduction prepares avenabeta glucosan nutrient powder and the method for dietary fiber micro powder
Technical field
The invention belongs to technical field of food biotechnology, is related to a kind of oat bran intensive processing technology, specifically with oat Wheat bran is raw material, utilizes the skill of biological enzyme Joint Production avenabeta glucosan nutrient powder, dietary fiber micro powder and avenin Art.
Background technology
Oat has higher nutritive value, compared with other cereal, in protein, dimension life as a kind of rain fed crops The nutrient index contents such as element, mineral element and dietary fiber are high, and nutrition equilibrium modern studies show, protein content in oat It is abundant, occupy the first in cereal, and the essential amino acid Compositional balance in avenin, its amino acid pattern is close to FAO/ The provisional pattern of amino acids that WHO is promulgated is in addition, be rich in soluble dietary fiber beta glucan and insoluble meals in oat bran Fiber.Its chemical name of beta glucan is(1-3)(1-4)- callose, it is a kind of non-starch linear polysaccharide, it is raw at present The general physiological action for thinking beta glucan of thing medical field and nutrition educational circles mainly have gut purge effect, reconcile blood glucose, reduce cholesterol, Improve immunity.And insoluble dietary fiber plays important life to fat-reducing, diabetes mellitus prevention, promotion function of intestinal canal improvement etc. Manage adjustment effect.
In existing patented technology, existing some reports on extracting beta glucan from oat, such as patent 200710018232 provide a kind of method for separating glucan from cereal bran using membrane separation technique, and this method utilizes egg White matter solubility in alkalescence, normal temperature is maximum, and the principle that can be separated out in acid condition, extracts cereal with ethanol and water respectively Albumen in seed, extract solution are centrifuged, and after acid is heavy after filtrate is enriched with using membrane separation technique, then carry out alcohol precipitation, Centrifuge, and membrane filtration is used after precipitation is carried out into precipitation, obtain refined beta glucan.But due in alcohol precipitation process Middle to use ethanol, ethanol is not high to the selectivity of the beta glucan in solution, causes the beta glucan purity of preparation not high, yield It is low.In addition, ethanol belongs to inflammable explosive article, there can be many requirements to the environment and safety of production plant, increase production cost.
A kind of method for extraction avenabeta glucosan that patent 200610089486.6 is recorded, comprises the following steps:1st, will Oat bran is at 50-60 DEG C plus water stirs, and adjusts PH8-10;2nd, add protease and hydrolysis oat bran is handled at 45-60 DEG C Albumen in skin adds;3rd, amylase is handled at 80 DEG C, filtering, obtains supernatant liquid;4th, use molecular cut off for 30000-50000Da ultrafiltration membrance filter, obtains beta glucan solution, and freeze-drying obtains beta glucan product, has purity 85% effect.
The preparation method step that patent 200610097431.X describes a kind of avenabeta glucosan is, using oat bran as original Material, through crushing, microwave radiation exaraction plus amylase and saccharification ferment treatment, isoelectric precipitation, centrifugation, supernatant concentration, second Alcohol precipitation, centrifuge and collect precipitation plus water redissolutions, beta glucan enzyme hydrolysis, obtained with significant after spray-drying process Promote enteron aisle and faecal bifidobacteria, the high-purity avenabeta glucosan product of Bacillus acidi lactici increment effect.
Patent is that a kind of preparation method of 03147786.0 avenabeta glucosan recorded comprises the following steps 1, oat system It is standby into oat bran, enzyme deactivation;2nd, under the conditions of 45-60 DEG C, add water to stir, be adjusted to PH9-11;3rd, filtrate is collected after separating, is added Enter ɑ-starch ferment treatment, 70-90 DEG C of holding 1-2 hour;4th, 10-30 DEG C is cooled to, 4.5-5 is adjusted to, is stood after stirring, is sunk Shallow lake protein;5th, supernatant is centrifuged to obtain, is concentrated by ultrafiltration, isopropanol is added in concentrate, obtains beta glucan gelatinous precipitate; 6th, beta glucan gelatinous precipitate is centrifuged, vacuum drying, obtains beta glucan product.
The method that above-mentioned technical proposal prepares beta glucan using oat or oat bran, mostly chemical method, Enzymatic Extraction, Extracted using organic solvent, gentle alkali extraction method and saturation sulfuric acid be by precipitation.These methods are required for introducing organic solvent, separation Product afterwards has chemical residual, and water consumption is larger, and wastewater treatment capacity is big.Also the technical scheme having using gel chromatography separation and The methods of ultrafiltration membrance filter, but all because cost height is only applicable to laboratory operation, industrialized production can not be carried out.Utilizing swallow There is starch, protein and insoluble diedairy fiber during wheat bran skin extraction beta glucan to discard with waste material, causes The loss of nutrient in oat.Oat starch, oat egg white matter and insoluble diedairy fiber also have excellent nutrition and processing Characteristic.If using starch, protein and dietary fiber only as the accessory substance in avenabeta glucosan extraction process without being subject to Make full use of, not only cause actual production inefficiencies, high expensive, can also bring serious environmental pollution.Therefore, it is of the invention Nutrient synthesis in oat is used the angle extracted and produced from full constituent.
The content of the invention
The present invention is a kind of from oat bran so as to provide in order to solve the comprehensive utilization development problem for improving oat bran The method that middle extraction prepares avenabeta glucosan nutrient powder, dietary fiber micro powder and avenin.
A kind of coproduction of the present invention makes avenabeta glucosan nutrient powder and the method for dietary fiber micro powder, its technical scheme bag Include following steps:
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, adjust pH value 9 or so, are extracted 2 hours at 40-50 DEG C, with 100 Mesh filter-cloth filtering, collect filtrate;
3rd, filtrate is regathered after above-mentioned filtrate is centrifuged with 4000rpm, filtrate is collected and is cooled to 20-30 DEG C, use diatomite Plate-frame filtering obtains filtrate, and adjustment pH value is 4.0, stands 2 hours after stirring, then centrifuges to obtain oat again with 10000rpm Protein solid and separating liquid;
4th, add in filtrate isolated in low temperature ɑ-amylase to step 3, adjust by the 1%-1.5% mass of oat bran raw material PH value to neutrality, stir process is concentrated in vacuo after 1 hour, and concentrate is spray-dried to be prepared into avenabeta glucosan nutrient powder;
5th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, that isolates is upper Clear liquid is returned in the filtrate of step 3, ultramicro grinding after the drying precipitate centrifuged out, is prepared into dietary fiber micro powder.
The present invention has the beneficial effect that:
1st, the oat bran after oat processing flour is used to obtain avenabeta glucosan nutrition simultaneously by joint production process for raw material Three kinds of powder, dietary fiber micro powder and avenin products, accomplish that the nutrient in oat bran utilizes comprehensively, greatly improve main product The added value of product and byproduct;
2nd, the present invention uses microwave deactivating enzyme technology, is passivated the activity of enzyme in wheat bran, extends shelf life of products, is gone out with conventional vapor Enzyme, have the advantages that it is quick, efficiently, low energy consumption and easily controllable;
3rd, the present invention uses biological enzymolysis technology, compared with conventional chemical methods extract, is more conducive to environmental protection, and produced in enterprise Cheng Zhong, industrial water is saved, reduce the processing cost of trade effluent;
4th, in present invention process using microwave deactivating enzyme, biological enzymolysis, etc. the technology such as electrically separated and ultramicro grinding realize oat resource The reasonable utilization of exploitation, realizes the high added value complete utilization of waste resource, reduces production cost.
Embodiment
Embodiment 1
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, use edible soda ash(Sodium carbonate)PH value 9 or so is adjusted, in 40- 50 DEG C are extracted 2 hours, with 100 mesh filter-cloth filterings, collect filtrate;
3rd, filtrate is regathered after filtrate is centrifuged with 4000rpm, is cooled to 20-30 DEG C, is obtained with diatomite plate-frame filtering Filtrate, food-grade acetic acid or citric acid adjustment pH value are 4.0, stand 2 hours after stirring, are then centrifuged again with 10000rpm Obtain avenin solid and filtrate;
4th, add in filtrate isolated in low temperature ɑ-amylase to step 3, use by the 1%-1.5% mass of oat bran raw material Edible soda ash adjusts pH value to neutrality, and it is 40% that stir process, which is concentrated in vacuo to material concentration for 1 hour, the spray-dried system of concentrate It is standby into avenabeta glucosan nutrient powder;
5th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, the supernatant isolated Return in the filtrate of step 3, the oat slag sediment isolated, ultramicro grinding after drying, be prepared into dietary fiber micro powder.
This embodiment can produce major product avenabeta glucosan nutrient powder and byproduct dietary fiber micro powder and oat egg In vain.
Embodiment 2
1st, oat bran is crushed into oat bran powder, microwave deactivating enzyme is carried out to oat bran powder;
2nd, by oat bran powder and deionized water with 1:10 mixing, by the 1%-1.5% mass of oat bran raw material add low temperature ɑ- Amylase, extracted 2 hours at 40-50 DEG C, with 100 mesh filter-cloth filterings, collect filtrate;
3rd, for filtrate through being concentrated in vacuo to material concentration 40%, concentrate is spray-dried to be prepared into avenabeta glucosan nutrient powder;
4th, the waste residue after oat bran extraction in step 2 is separated using Horizontal spiral discharging centrifuge, the supernatant isolated Return in the filtrate of step 3, the oat slag sediment isolated, ultramicro grinding after drying, be prepared into dietary fiber micro powder.
This embodiment can produce major product avenabeta glucosan nutrient powder(Include avenin)And byproduct meals are fine Tie up micro mist.

Claims (4)

1. a kind of coproduction prepares avenabeta glucosan nutrient powder and the method for dietary fiber micro powder, comprise the following steps:
1., by after crushing oat bran powder carry out microwave deactivating enzyme;
2., by oat bran powder and deionized water with 1:10 mixing, adjust pH value 9 or so, are extracted 2 hours at 40-50 DEG C, use 100 mesh filter-cloth filterings, collect filtrate;
3., the filtrate of step 2. is centrifuged with 4000rpm after regather filtrate, using being centrifuged after isoelectric point deproteinized Obtain avenin solid and centrate;
4., add low temperature ɑ-amylase to step 3. by the 1%-1.5% mass of oat bran raw material in isolated separating liquid In, adjust pH value to neutrality, stir process to be concentrated in vacuo for 1 hour, concentrate is spray-dried to be prepared into avenabeta glucosan nutrition Powder;
5., ultramicro grinding after the drying precipitate that is centrifuged out to the waste residue after the step 2. extraction of middle oat bran, be prepared into Dietary fiber micro powder.
2. according to the method for claim 1, it is characterised in that the oat bran is adopted by the cereal kernel of removal endosperm Mechanically it is ground into 60-100 mesh.
3. according to the method for claim 1, it is characterised in that step 2. it is described 4000rpm is centrifuged after regather Filtrate is cooled to 20-30 DEG C, obtains filtrate with diatomite plate-frame filtering, adjustment pH value is 4.0, stands 2 hours after stirring, then Avenin solid and separating liquid are centrifuged to obtain with 10000rpm again.
4. according to the method for claim 1, it is characterised in that step 5. it is described to oat bran extract after waste residue, adopt Separated with horizontal spiral discharge sedimentation centrifuge, the supernatant isolated is returned in the filtrate of step 3., is centrifuged Ultramicro grinding after the drying precipitate gone out, is prepared into dietary fiber micro powder.
CN201610400851.4A 2016-06-08 2016-06-08 A kind of coproduction prepares oat beta glucan nutrient powder and the method for dietary fiber micro powder Pending CN107467639A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113519859A (en) * 2021-07-21 2021-10-22 内蒙古阴山优麦食品有限公司 Preparation process of high-content oat beta-glucan dietary fiber powder
WO2023126058A1 (en) * 2021-12-30 2023-07-06 Oatly Ab A continuous process and system for preparing a liquid oat base or drink from an oat derived material

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CN1966531A (en) * 2006-11-08 2007-05-23 江南大学 Process for preparing oat beta-glucans
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CN101828668A (en) * 2010-04-13 2010-09-15 山东轻工业学院 Method for preparing dietary fiber by combining enzymatic alkaline method and wet ultra-micro pulverization
CN101857646A (en) * 2010-05-27 2010-10-13 山西金绿禾燕麦研究所 Method for extracting high-purity beta-glucan and whole oat flour from oat bran
CN102835616A (en) * 2011-06-23 2012-12-26 庞兵 Oat bran nutrition powder and dietary fibers
CN103772527A (en) * 2014-02-24 2014-05-07 常州毅博生物科技有限公司 Method for extracting high-purity beta-glucosan from oat bran

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CN102835616A (en) * 2011-06-23 2012-12-26 庞兵 Oat bran nutrition powder and dietary fibers
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113519859A (en) * 2021-07-21 2021-10-22 内蒙古阴山优麦食品有限公司 Preparation process of high-content oat beta-glucan dietary fiber powder
WO2023126058A1 (en) * 2021-12-30 2023-07-06 Oatly Ab A continuous process and system for preparing a liquid oat base or drink from an oat derived material

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