CN107446692A - Utilize the integrated approach of melon seeds edible health oil in August - Google Patents
Utilize the integrated approach of melon seeds edible health oil in August Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/42—Treatment of water, waste water, or sewage by ion-exchange
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
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Abstract
The present invention provides the process using melon seeds liquefaction in August, and August, melon seeds was ground, adds water, adjusts material liquid pH value, adds amylase, acid protease and cellulase hydrolysis, centrifuges to obtain Fructus Akebiae oil and waste water；Waste water obtains efflux, carries oily circulation step into enzymolysis next time, efflux circulates 3~5 uses through 732 cationic exchange resin adsorptions；The method for stating the wastewater produced production beverage of circulation liquefaction, specific steps include as follows：It is raw material that it is wastewater produced, which to circulate liquefaction, add wet slag, water content is reached 15~35%, add 10~25% Fructus Akebiae pulp mud, add 10~25% pineapple juice, add final concentration of 300U~600U/L pectase, 20~30 DEG C of 7~12h of hydrolysis, obtain hydrolyzate, filtering, 1~3% nisin is added, 5~10s instantaneous sterilizings obtain Fructus Akebiae beverage products at 110~120 DEG C.
Description
Technical field
The invention belongs to food processing technology field, relates to the use of the integrated approach of melon seeds edible health oil in August, has
Body is related to a kind of normal temperature and produces melon seeds oil in August and its functional components extraction process method.
Background technology
Threeleaf akebia, a kind of Wild liana fruit tree of Lardizabalaceae Akebia are commonly called as that September is fried, Fructus Akebiae.It is a kind of important
Medicinal plant, its root, rattan, fruit, seed can be used as medicine.China and Japan are originated in, distribution in China is in Shandong, Hebei, Shanxi
Taihang Mountain, Funiu Shan Mountain, Dabie Mountain and Tongbai Shan Mountain are originated in areas to the south, Henan, are grown on the area of 250 meters to 2500 meters of height above sea level,
It is grown in mountain region cheuch side sparse woods or hills shrubbery more.Threeleaf akebia pulp is containing abundant nutriment, rich in protein, fat
Fat, starch and various soluble sugars, calcium, phosphorus, iron, organic acid, vitamin B l, BZ, B6 etc., it can eat raw, make wine, beverage processed.Wood
Grease type composition is rich in logical seed, nutritive value is high, has good medical value, and ornamental value.
Fat content enriches in August melon seeds, and in terms of oil extraction, Xie little Xia et al. utilizes supercritical CO2Extraction equipment
The good oil of Fructus Akebiae is extracted, obtained grease color is shallow, no precipitation, fragrant taste, using gas chromatograph-mass spectrometer (GC-MS) to its fat
Fat acid constituents content is analyzed, and as a result finds that unrighted acid relative amount accounts for 72.43% in grease, growth in humans is required
Oleic acid, linoleic acid content respectively reach 43.52% and 28.54%, it is seen that its nutritive value is high, in face of domestic edible oil and fat
Add the severe situation of king's quality and quantity, Fructus Akebiae is ingeniously highly suitable as a kind of new edible health-care oil fatty oil material source.
Grease type composition is rich in akebi seed, is also demonstrate,proved through test center of Inst. of Oil Crops, Chinese Academy of Agriculture
It is real：Akebi seed oil content is up to 43%, mainly based on oleic acid, linoleic acid, palmitic acid, and contains a small amount of acetic acid and flax
Contain 10 kinds of aliphatic acid in the akebia trifoliata varaustralis seed such as acid, arachidic acid, account for the 99.75% of recognizate total mass number, wherein saturated fat
5 kinds of acid, account for total mass fraction 23.39% [including palm fibre puts sour (20.14%), 16- methyl-Heptadecanoic acide (3.03%), Pork and beans
Plant sour (0.10%), capric acid (0.08%) and 15- methyl-brown eleostearic acid (0.04%)]；5 kinds of unrighted acid, accounts for total content
76.36% includes 11- oleic acid (47.63%), linoleic acid (27.05%), 8- oleic acid (l.07%), 11- eicosenoic acids
(0.29%) and 13- docosenoic acids (0.32%)].Akebi seed oil contains abundant vitamin E, vitamin C and Wei Sheng
Plain B.Unrighted acid, the generation of some diseases or moist skin quality with strengthen immunity function, can be prevented or reduced, delays to decline
Always.Linoleic acid is unrighted acid needed by human, it is impossible to synthesized, can only be absorbed from food or medicine by human body itself, its
Arachidonic acid and leukotrienes can be converted into human body, arachidonic acid is the premise material of prostaglandin, and prostaglandin
The important function being metabolized with wide regulation mechanism.In addition, Ve contents are 23mg/100g in the seed oil squeezed out, also have
Vc, VB, and contain acetic acid class composition, acetic acid class composition often has fruit delicate fragrance, and the presence of these compositions is akebi seed oil tool
Fruity reason.
Ou Yangyu wish et al. the extraction of Fructus Akebiae fruit seed oil functional component with antioxidation activity research, with petroleum ether ultrasound
The oil yield of extraction, content of fatty acid and unrighted acid relative amount are all higher.Using GC-MS, Atomic absorption and often
The functional component of analytic approach research Fructus Akebiae fruit seed oil is advised, melon and fruit in August is investigated by determining peroxide value and free radical scavenging activity
The antioxidation activity of seed oil.As a result show, acid number (KOH), saponification number (KOH) and the iodine number (I) of Fructus Akebiae fruit seed oil are respectively
1.23rd, 260mg/g and 83.02g/100g.Fructus Akebiae fruit seed fatty acid oil composition is mainly palmitic acid (30.08%) and oleic acid
(48.93%), in its oil potassium, sodium, calcium, magnesium, Zn content be respectively 2.57,5.12,3.15,0.23,0.21mg/g.In sesame oil
Middle addition Fructus Akebiae fruit seed oil, heats 60min, sesame oil peroxidating with 235nm ultraviolet lights 450min and at 80 DEG C respectively
It is worth the reduction respectively 11.46% and 16.81% than adding BHT；Compare Fructus Akebiae fruit seed oil with sesame oil, VE, different VC-Na and
BHT radical scavenging activity, as a result find reducing power, ultra-oxygen anion free radical and the H of Fructus Akebiae fruit seed oil2O2Remove
Ability is most strong.
Melon seeds oil colours in August pool is in orange yellow, and compared with level Four sunflower oil national standard, acid number and peroxide value are low, oil
Lipid oxidation degree is low, and Nature comparison is stable, easily preserves, is a kind of preferable vegetable fat of quality, meets national edible oil and fat
Standard, bribery value content is relatively low, and it is a kind of non-drying grease to illustrate grease, and saponification number content is somewhat higher, shows fatty in grease
Acid molecule amount is small, if edible be easier to be absorbed by the body.
The content of the invention
Due to, containing abundant vitamin E, vitamin C and vitamin B, eight being pressed using conventional high-temperature oil in August melon seeds
Month melon seeds oil, wherein can be aoxidized containing a large amount of functional components.Organic solvent extraction melon seeds oil method in August easily makes chemical substance
Remained in August melon seeds oil, cause edible risk.And Ou Yangyuzhu et al. Fructus Akebiae fruit seed oil functional component extraction with
In antioxidation activity research, it is indicated that from fatty acid species, oil yield, grease outward appearance (color and white depositions) integrated survey 4
The grease of kind solvent extraction, the grease outward appearance of ethanol extraction is limpid transparent, and color is fresher, and fatty acid species are more, best in quality；Its
Secondary is the grease of ethyl acetate extraction, and oil yield is high, and fatty acid species are more, but have sediment in oil；Remaining two kinds of solvent extraction
Oil fatty acid species it is less, have that sediment or color are deeper, and oil quality is poor.Market is more willing to carry using normal temperature aqueous enzymatic method
Melon seeds oil tech products obtained therefrom in August is taken, edible the problems such as risk is not present, August, melon seeds oil quality was higher.But in aqueous enzymatic method system
Can produce a large amount of industrial wastewaters during August melon seeds oil, due in waste water containing substantial amounts of water-soluble functional components, using biography
System method of wastewater treatment can cause functional components to lose, and also add business processes waste water cost.It is existing in order to make up
The defects of technology, the present invention provide a whole set of in August melon seeds oil-producing technique method, the method further comprises liquefaction, and to form waste water sharp again
With handling process process, prepared than traditional melon seeds in August oil and aqueous enzymatic method oil-producing technique possesses more perfect preparation technology, it is made
August, melon seeds oil was more with health role, produced more preferable environment-protecting clean, compensate for existing melon seeds in August oil defective workmanship processed, and
The extensive market demand for preparing high-quality melon seeds in August oil can be met.
First purpose of the invention is to provide the process using melon seeds liquefaction in August, and it is comprised the following steps that：
(1) melon seeds in August is weighed, is ground 1~3 time on common grinding machine, is added to the normal-temperature water that water temperature is 20~30 DEG C
In, feed liquid is obtained after stirring；
(2) it is 5~6.5 to adjust material liquid pH, adds amylase and cellulase respectively to final concentration of 55~130U/L, enzyme
Certain time is solved, obtains enzymolysis liquid；
(3) acid protease of temperature sensitivity is added again into enzymolysis liquid to final concentration of 45~150U/L, is digested
Certain time, 20~35min is incubated more than 55 DEG C, the acid protease of the temperature sensitivity refers to more than 45 DEG C quickly
Inactivation characteristics.
(4) feed liquid I is centrifugally separating to obtain liquid and wet slag on sedimentation centrifuge, liquid is directly entered dish-style separation
Machine, isolate melon seeds oil in August and waste water I.
(5) gained melon seeds in August oil is dried under vacuum, filtered after standing, obtain finished product melon seeds in August oil, and
Examine product oil.
(6) waste water I obtains efflux I, 732 cationic ion-exchange resins are used after absorption through 732 cationic exchange resin adsorptions
0.3~3mol/L hydrochloric acid is eluted, and obtains eluent.
The reagent of above-mentioned regulation pH value of solution is 0.5moL/L hydrochloric acid or 0.5moL/L sodium hydrate aqueous solutions.
Above-mentioned enzymolysis time is 0.5~4h.
In a specific embodiment, step (1) the volume L for adding water and melon seeds in August weight kg ratios are 1
~4：1.
In a specific embodiment, step (6) eluent, neutralized with 1mol/L sodium hydroxides, high temperature evaporation
Concentration, obtains aminoacids solution, can adjust pH and be refining to obtain various amino acid sterlings, can also be directly used in Plant leaf fertilizer or feeding
Feed additives use.
Second purpose of the invention is to provide the method that waste water material caused by above-mentioned liquefaction recycles, its specific steps
It is as follows：
(a) melon seeds in August is weighed, is ground 1~3 time on common grinding machine, efflux I is added, is heated to 30~40 DEG C of left sides
The right side, feed liquid II is obtained after stirring；
(b) it is 5.5~6.5 to adjust the pH of feed liquid II, adds amylase and cellulase respectively to final concentration of 55~130U/
L, certain time is digested, obtains enzymolysis liquid I；
(c) acid protease of temperature sensitivity is added again into enzymolysis liquid I to final concentration of 45~150U/L, is digested
Certain time, 20~35min is incubated more than 55 DEG C, obtains feed liquid III, the acid protease of the temperature sensitivity refers to 45
The characteristic of rapid deactivation more than DEG C.
(d) feed liquid III is centrifugally separating to obtain liquid and wet slag on sedimentation centrifuge, liquid is directly entered dish-style separation
Machine, isolate melon seeds oil in August and waste water II.
(e) gained melon seeds in August oil is dried under vacuum, filtered after standing, obtain finished product melon seeds in August oil, and
Examine product oil.
(h) gained waste water II is obtained into efflux II through 732 cationic exchange resin adsorptions.
(I) by gained efflux II and melon seeds in August after grinding, 30~40 DEG C or so are heated to, into enzymolysis next time
Oily circulation step is carried, efflux circulates 3~5 uses, and the wherein volume L of efflux II and melon seeds seed in August weight kg ratios are
10~15：1.
The reagent of above-mentioned regulation pH value of solution is 0.5moL/L hydrochloric acid or 0.5moL/L sodium hydrate aqueous solutions.
Above-mentioned enzymolysis time is 0.5~4h.
In a specific embodiment, step (a) the volume L for adding efflux I and melon seeds in August weight kg
Than for 6~10：1.
3rd purpose of the invention is to provide the method for the wastewater produced production beverage of above-mentioned circulation liquefaction, specific steps bag
Include as follows：It is raw material that it is wastewater produced, which to circulate liquefaction, adds wet slag, water content is reached 15~35%, add 10~25%
Fructus Akebiae pulp mud, adds 10~25% pineapple juice, adds final concentration of 300U~600U/L pectase, 20~30 DEG C
7~12h is hydrolyzed, hydrolyzate is obtained, filtering, adds 1~3% nisin, 5~10s is instantaneous at 110~120 DEG C
Sterilize to obtain Fructus Akebiae beverage products.
The wet slag refers to the wet slag that step (4) or step (d) are obtained, and the % refers to mass ratio.
The Fructus Akebiae pulp mud refers to melon and fruit peeling in August, removes seed, directly with after smashing to pieces.
The pineapple juice refers to that pineapple peel smashs filtrates obtained by rear three layers of filtered through gauze to pieces.
Technique effect
1st, emulsification of the protein during melon seeds oil separation in August is avoided, enables melon seeds oil in August quickly and water
Separation, also makes anti-oxidation function composition in melon seeds oil in August at utmost retain, and can improves amino acid and list in waste water
The content of sugar, also allows for the exploitation of beverage.
2nd, due to reducing protein content during extraction August melon seeds oil, emulsification is made substantially to weaken, it is more sharp
Used in the circulating repetition of water, reduce the discharge capacity of waste water.
3rd, due to directly using fruit beverage product is produced based on waste water, the wind of contaminated wastewater environment can be greatly reduced
Danger, while also improve the value of active ingredient in waste water.
Embodiment
Embodiment 1
Melon seeds seed 100kg in August is weighed, is ground 1~3 time on common grinding machine, is added to the temperature that water temperature is 30~40 DEG C
In water 300L, feed liquid is obtained after stirring；It is with 0.5moL/L hydrochloric acid or 0.5moL/L sodium hydrate aqueous solutions regulation material liquid pH
6, amylase and cellulase are added respectively to final concentration of 60U/L, digests 4h, then add temperature sensitivity again into enzymolysis liquid
Property acid protease to final concentration of 80U/L, digest 3h, 35min be incubated more than 55 DEG C, obtains feed liquid I.By feed liquid I heavy
Liquid and wet slag are centrifugally separating to obtain on drop centrifuge, liquid is directly entered disk centrifuge, and it is oily and useless to isolate August melon seeds
Water I.Gained melon seeds in August oil is dried under vacuum, filtered after standing, obtains finished product melon seeds in August oil, and examine finished product
Oil.Waste water I obtains efflux I, 732 cationic ion-exchange resins, 0.3~3mol/ after absorption through 732 cationic exchange resin adsorptions
L hydrochloric acid is eluted, and obtains eluent.
Embodiment 2
Melon seeds seed 200kg in August is weighed, is ground 3 times on common grinding machine, adds 1500L effluxes I, it is heated to 30~
40 DEG C or so, feed liquid II is obtained after stirring；With 0.5moL/L hydrochloric acid or 0.5moL/L sodium hydrate aqueous solutions regulation feed liquid II
PH is 5.5, adds amylase and cellulase respectively to final concentration of 50U/L, digests 3h, obtain enzymolysis liquid I.Into enzymolysis liquid I
The acid protease of temperature sensitivity is added again to final concentration of 80U/L, is digested 3h, is incubated 35min more than 55 DEG C, must expect
Liquid III.Feed liquid III is centrifugally separating to obtain liquid and wet slag on sedimentation centrifuge, liquid is directly entered disk centrifuge, separation
Go out melon seeds oil in August and waste water II.Will gained melon seeds in August oil dry under vacuum, stand after filter, obtain finished product August
Melon seeds oil, and examine product oil.By gained waste water II through 732 cationic exchange resin adsorptions, efflux II is obtained.Gained is flowed out
The 2500L of liquid II and melon seeds seed 200kg in August after grinding, is heated to 30~40 DEG C or so, oily circulation is proposed into enzymolysis next time
Step, efflux circulate 3~5 uses.
Embodiment 3
It is raw material to take circulation liquefaction wastewater produced, and adding 15% bacillus subtilis bacterium solution (can produce neutral proteinase
Bacterial strain), 37 DEG C of culture 12h, final concentration of 420U/L pectase is added, this mixed liquor is obtained as degumming liquid, to what is won
The mulberry skin circulation wastewater produced 100kg of liquefaction is raw material, adds 700kg wet slags, water content is reached 20% or so, add
120kg (15%) Fructus Akebiae pulp mud, 180kg (20% or so) pineapple juice is added, add final concentration of 450U/L fruit
Glue enzyme, 28 DEG C of hydrolysis 8h, obtains hydrolyzate, filters to obtain about 400kg, 6kg (1.5%) nisin is added, at 120 DEG C
Lower 6s instantaneous sterilizings obtain Fructus Akebiae beverage products.
Claims (7)
1. using the process of melon seeds liquefaction in August, it is comprised the following steps that：
(1) melon seeds in August is weighed, is ground 1~3 time on common grinding machine, is added in the normal-temperature water that water temperature is 20~30 DEG C,
Feed liquid is obtained after stirring；
(2) it is 5~6.5 to adjust material liquid pH, adds amylase and cellulase respectively to final concentration of 55~130U/L, enzymolysis one
Fix time, obtain enzymolysis liquid；
(3) acid protease for adding temperature sensitivity again into enzymolysis liquid is certain to final concentration of 45~150U/L, enzymolysis
Time, 20~35min is incubated more than 55 DEG C, the acid protease of the temperature sensitivity refers to the rapid deactivation more than 45 DEG C
Characteristic；
(4) feed liquid I being centrifugally separating to obtain liquid and wet slag on sedimentation centrifuge, liquid is directly entered disk centrifuge, point
Separate out melon seeds oil in August and waste water I；
(5) gained melon seeds in August oil is dried under vacuum, filtered after standing, obtain finished product melon seeds in August oil, and examine
Product oil；
(6) waste water I obtains efflux I through 732 cationic exchange resin adsorptions, after absorption 732 cationic ion-exchange resins with 0.3~
3mol/L hydrochloric acid is eluted, and obtains eluent.
2. method according to claim 1, wherein enzymolysis time are 0.5~4h.
3. method according to claim 1, wherein step (1) the volume L for adding water and melon seeds in August weight kg ratios are 1
~4：1.
4. according to the method for claims 1 to 3, wherein the method that waste water material caused by the liquefaction recycles, its is specific
Step is as follows：
(a) melon seeds in August is weighed, is ground 1~3 time on common grinding machine, efflux I is added, is heated to 30~40 DEG C or so,
Feed liquid II is obtained after stirring；
(b) it is 5.5~6.5 to adjust the pH of feed liquid II, adds amylase and cellulase respectively to final concentration of 55~130U/L, enzyme
Certain time is solved, obtains enzymolysis liquid I；
(c) acid protease for adding temperature sensitivity again into enzymolysis liquid I is certain to final concentration of 45~150U/L, enzymolysis
Time, 20~35min is incubated more than 55 DEG C, obtains feed liquid III, the acid protease of the temperature sensitivity refer to 45 DEG C with
Upper rapid deactivation characteristic；
(d) feed liquid III being centrifugally separating to obtain liquid and wet slag on sedimentation centrifuge, liquid is directly entered disk centrifuge, point
Separate out melon seeds oil in August and waste water II；
(e) gained melon seeds in August oil is dried under vacuum, filtered after standing, obtain finished product melon seeds in August oil, and examine
Product oil；
(h) gained waste water II is obtained into efflux II through 732 cationic exchange resin adsorptions；
(I) by gained efflux II and melon seeds in August after grinding, 30~40 DEG C or so is heated to, oil is carried into enzymolysis next time
Circulation step, efflux circulate 3~5 uses, the weight kg ratios of the wherein volume L of efflux II and melon seeds seed in August for 10~
15：1.
5. method according to claim 4, wherein enzymolysis time are 0.5~4h.
6. method according to claim 4, wherein step (a) the volume L for adding efflux I and melon seeds in August weight kg
Than for 6~10：1.
7. according to the method for claim 1~6, wherein the method for the wastewater produced production beverage of circulation liquefaction, specific step
Suddenly include as follows：It is raw material that it is wastewater produced, which to circulate liquefaction, addition wet slag, water content is reached 15~35%, add 10~
25% Fructus Akebiae pulp mud, adds 10~25% pineapple juice, adds final concentration of 300U~600U/L pectase, 20~
30 DEG C of 7~12h of hydrolysis, obtain hydrolyzate, filtering, add 1~3% nisin, 5~10s at 110~120 DEG C
Instantaneous sterilizing obtains Fructus Akebiae beverage products.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108432891A (en) * | 2018-05-07 | 2018-08-24 | 董秦林 | Plant blend oil composition |
| CN108936180A (en) * | 2018-08-15 | 2018-12-07 | 黄清华 | Sour mew-open country banana compound solid beverage and wild banana extract production method |
| CN110055129A (en) * | 2019-05-20 | 2019-07-26 | 贵州师范大学 | A kind of method that aqua method extracts melon seeds in August oil |
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| CN110055129A (en) * | 2019-05-20 | 2019-07-26 | 贵州师范大学 | A kind of method that aqua method extracts melon seeds in August oil |
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