CN107434293A - A kind of preparation technology of rich iodine drinking water - Google Patents

A kind of preparation technology of rich iodine drinking water Download PDF

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Publication number
CN107434293A
CN107434293A CN201710707112.4A CN201710707112A CN107434293A CN 107434293 A CN107434293 A CN 107434293A CN 201710707112 A CN201710707112 A CN 201710707112A CN 107434293 A CN107434293 A CN 107434293A
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powder
drinking water
iodine
preparation technology
raw material
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CN201710707112.4A
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CN107434293B (en
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付全贵
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Weifang Kanglong Biotechnology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/68Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/683Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of complex-forming compounds

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The present invention provides a kind of preparation technology of rich iodine drinking water, and described preparation technology prepares, grinds, seals and prepared rich iodine drinking water step including raw material.Described raw material prepares:Using following raw material components:Medical stone, zeolite and Potassiumiodate powder.Described raw material prepares:Also include following raw material components:Lithium carbonate powder, diatomite in powder, wooden fish stone powder, quartz sand powder.Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%.Content of iodine is 0.2 0.39 mg/L in described drinking water.

Description

A kind of preparation technology of rich iodine drinking water
Technical field
The present invention relates to a kind of preparation technology of rich iodine drinking water, belong to drinking water technical field.
Background technology
Iodine deficiency is a kind of extremely extensive endemic disease of distribution, except a few countries such as Norway, Iceland.Countries in the world are not With degree threatened by iodine deficiency.Iodine deficiency is its basic reason in food and drinking-water, and purpose major function is synthetic thyroid Element, iodine deficiency make thyroxine dyssynthesis, so as to influence to grow.The weight of clinical manifestation depends on the degree of iodine deficiency, held Continuous time and the age of illness.Foetal period iodine deficiency can lethal tire, premature labor and congenital malformation;Neonatal period, then shows as thyroid gland Hypofunction;Children and puberty then cause endemicgoiter, region Hypothyroidism and pure deaf It is mute.It is long then to may occur in which Subclinical Hypothyroidism with slight iodine deficiency, show as slight mental retardation, or slight hearing Obstacle, it is often accompanied by Physique growth backwardness.
The addition of iodine at present be mostly by salt compounded of iodine, but iodine be heated it is volatile, so, be lost in during culinary art etc. serious.
The trace element such as iodine is not easy to store in human body, if short-term or interim supplement, it is difficult to realize its effect;If By tonic or if building up one's health by taking tonic, not only it is difficult to select, it is also difficult to it is long-term to maintain to take, and people will drink largely daily Water, if carrying out supplement mineral element by drinking-water, chronicity and continuity can ensure.
If added in water, as direct drinking, not only the retention rate of iodine will greatly increase;Moreover, the amount that people drink water It is much higher than the amount eaten salt or supplement medicine;If it is possible to iodine is added in water, the effect that enriches the iodine will be greatly improved Fruit;However, Potassiumiodate is soluble in water, and can excessively be poisoned;Therefore, iodine rational content in water how is controlled, obtains rich iodine Drinking water, it is the Important Problems of current field concern.
The content of the invention
The present invention for solve the shortcomings of the prior art, there is provided a kind of preparation technology of rich iodine drinking water, with realize with Lower goal of the invention:It is simple and effective that common drinking water is prepared into rich iodine drinking water, while the content of iodine is controlled rational In the range of.
In order to solve the above technical problems, using following technical scheme:
A kind of preparation technology of rich iodine drinking water, it is characterised in that:Described preparation technology includes raw material and prepares, grinds, seals And prepare rich iodine drinking water step.
Described raw material prepares:Using following raw material components:Medical stone, zeolite and Potassiumiodate powder.
Described raw material prepares:Also include following raw material components:Lithium carbonate powder, diatomite in powder, wooden fish stone powder, quartz sand Powder.
Described raw material prepares:Using the raw material components of following parts by weight:Medical stone 70-75 parts, zeolite 15-16 parts, Potassiumiodate powder 15-17 parts, lithium carbonate powder 30-32 parts, diatomite in powder 20-22 parts, wooden fish stone powder 30-33 parts, quartz sand powder 20-21 parts.
Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%;
Described zeolite:Voidage is 50%, density 2.3g/cm3
Described lithium carbonate powder:Purity is 99.9%, and fineness is 150 mesh, relative density 2.11;
Described diatomite in powder:Fineness is 100 mesh, water absorption rate 60%, density 2.1g/cm3
Described limonite:Fineness is 200 mesh, density 3g/cm3, porosity 1%;
Described quartz sand powder:Fineness is 150 mesh, dioxide-containing silica 99.4%, density 2.52g/cm3
Described grinding:Medical stone is ground to 150 targeted fine powders, zeolite is ground to 300 targeted fine powders.
Described technique also includes preparing lithium addition block;It is described to prepare lithium addition block:
Lithium carbonate powder, diatomite in powder, wooden fish stone powder and quartz sand powder are well mixed, suitable quantity of water is added, stirs into pasty state;Make Frustillatum, and it is incubated 3 hours under the conditions of 100 DEG C.
Described sealing:Potassiumiodate powder, medical stone powder, well mixed be positioned in ceramic vessel of zeolite powder are sealed;Institute The micro-pore diameter for the ceramic vessel stated is less than 0.0001mm.
Content of iodine is 0.2-0.39 mg/L in described drinking water.
Compared with prior art, the beneficial effects of the invention are as follows:
(1)Common drinking water fast and effectively can be prepared into rich iodine drinking water by the present invention, and the element prepared addition body is put Enter in water, immersion more than 2min can obtain content of iodine 0.2-0.39mg/L, lithium content 0.9-2.2 mg/L rich iodine drinking water.
(2)Element prepared by present invention addition body can Reusability more than 1000 times, through experiment, 1000 are used in immersion After secondary, it still can be put in 2min in common drinking water and obtain content of iodine 0.2-0.36mg/L, lithium content 0.9-2.0mg/L richness Iodine drinking water.
Embodiment
A kind of preparation technology of rich iodine drinking water of embodiment 1
Comprise the steps:
Step 1, raw material prepare
Prepare according to following weight and weigh raw material:70 parts of medical stone, 15 parts of zeolite, 15 parts of Potassiumiodate powder;
Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%;
Described zeolite:Voidage is 50%, density 2.3g/cm3
Described Potassiumiodate powder:Using national standard supplementation of iodine salt Potassiumiodate powder.
Step 2, grinding
Medical stone is ground to 150 targeted fine powders, zeolite is ground to 300 targeted fine powders.
Step 3, sealing
Potassiumiodate powder, medical stone powder, the well mixed iodine that obtains of zeolite powder are added into powder, is positioned in ceramic vessel and seals;Institute The ceramic vessel stated is the salable ceramic vessel that micro-pore diameter made of sintering process is less than 0.0001.
Step 4, prepare rich iodine drinking water
Ceramic vessel is put into common drinking water, the iodine addition powder usage amount of every liter of water is 25g;More than 2min is soaked, i.e., Rich iodine drinking water is can obtain, with the extension of soak time, the content of iodine in water increased.
A kind of preparation technology of rich iodine drinking water of embodiment 2
Comprise the steps:
Step 1, raw material prepare
Prepare according to following weight and weigh raw material:70 parts of medical stone, 15 parts of zeolite, 15 parts of Potassiumiodate powder, carbonic acid 30 parts of lithium powder, 20 parts of diatomite in powder, 30 parts of wooden fish stone powder, 20 parts of quartz sand powder;
Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%;
Described zeolite:Voidage is 50%, density 2.3g/cm3
Described Potassiumiodate powder:Using national standard supplementation of iodine salt Potassiumiodate powder;
Described lithium carbonate powder:Purity is 99.9%, and fineness is 150 mesh, relative density 2.11;
Described diatomite in powder:Fineness is 100 mesh, water absorption rate 60%, density 2.1g/cm3
Described limonite:Fineness is 200 mesh, density 3g/cm3, porosity 1%;
Described quartz sand powder:Fineness is 150 mesh, dioxide-containing silica 99.4%, density 2.52g/cm3
Step 2, grinding
Medical stone is ground to 150 targeted fine powders, zeolite is ground to 300 targeted fine powders.
Step 3, prepare lithium addition block
Lithium carbonate powder, diatomite in powder, wooden fish stone powder and quartz sand powder are well mixed, suitable quantity of water is added, stirs into pasty state;Make Frustillatum, and 3 hours are incubated under the conditions of 100 DEG C, lithium addition block is obtained after cooling.
Step 4, sealing
Potassiumiodate powder, medical stone powder, the well mixed iodine that obtains of zeolite powder are added into powder, is positioned in ceramic vessel and seals;Institute The ceramic vessel stated is the salable ceramic vessel that micro-pore diameter made of sintering process is less than 0.0001mm.
Step 4, prepare rich iodine drinking water
Ceramic vessel and lithium addition block are put into common drinking water, the iodine addition powder usage amount of every liter of water is 25g, and lithium adds The usage amount of block is 20g;Soak more than 2min, you can rich iodine drinking water is obtained, wherein rich in iodine and lithium;With soak time Extend, the iodine, lithium content in water increased.
A kind of preparation technology of rich iodine drinking water of embodiment 3
Comprise the steps:
Step 1, raw material prepare
Prepare according to following weight and weigh raw material:75 parts of medical stone, 16 parts of zeolite, 17 parts of Potassiumiodate powder, carbonic acid 32 parts of lithium powder, 22 parts of diatomite in powder, 33 parts of wooden fish stone powder, 21 parts of quartz sand powder;
Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%;
Described zeolite:Voidage is 50%, density 2.3g/cm3
Described Potassiumiodate powder:Using national standard supplementation of iodine salt Potassiumiodate powder;
Described lithium carbonate powder:Purity is 99.9%, and fineness is 150 mesh, relative density 2.11;
Described diatomite in powder:Fineness is 100 mesh, water absorption rate 60%, density 2.1g/cm3
Described limonite:Fineness is 200 mesh, density 3g/cm3, porosity 1%;
Described quartz sand powder:Fineness is 150 mesh, dioxide-containing silica 99.4%, density 2.52g/cm3
Step 2, grinding
Medical stone is ground to 150 targeted fine powders, zeolite is ground to 300 targeted fine powders.
Step 3, prepare lithium addition block
Lithium carbonate powder, diatomite in powder, wooden fish stone powder and quartz sand powder are well mixed, suitable quantity of water is added, stirs into pasty state;Make Frustillatum, and 3 hours are incubated under the conditions of 100 DEG C, lithium addition block is obtained after cooling.
Step 4, sealing
Potassiumiodate powder, medical stone powder, the well mixed iodine that obtains of zeolite powder are added into powder, is positioned in ceramic vessel and seals;Institute The ceramic vessel stated is the salable ceramic vessel that micro-pore diameter made of sintering process is less than 0.0001.
Step 4, prepare rich iodine drinking water
Ceramic vessel and lithium addition block are put into common drinking water, the iodine addition powder usage amount of every liter of water is 25g, and lithium adds The usage amount of block is 20g;Soak more than 2min, you can rich iodine drinking water is obtained, wherein rich in iodine and lithium;With soak time Extend, the iodine, lithium content in water increased.
Experiment:
It is control group to take common drinking water 1L, respectively the content micro- with embodiment 1-3 rich iodine drinking water contrast;Rich iodine Element adds body in drinking water(Ceramic vessel and lithium addition block)After addition, fetched water respectively detection in following soak time point: 2min, 10min, 1 hours and 20 hours;Above water is 25 DEG C;Concrete outcome is shown in Table 1;
Table 1
As seen from the above table, the content of iodine significantly improves than common drinking water in embodiment 1-3 water, and element addition body soaks in water When steeping 2min, iodine has been added to 0.2-0.23mg/L in embodiment 1-3 water, and lithium content increases in embodiment 2-3 water 0.9-1.3 mg/L;When element addition body soaks 10min in water, iodine has been added to 0.25- in embodiment 1-3 water 0.29mg/L, lithium content increases to 1.2-1.6mg/L in embodiment 2-3 water;After 1 hour, the trace element in water contains Measure basicly stable, the obvious increase of nothing.
In addition to specified otherwise, ratio of the present invention is mass ratio, and described percentage is mass percent.
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still can be with Technical scheme described in foregoing embodiments is modified, or equivalent substitution is carried out to which part technical characteristic.It is all Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc., it should be included in the guarantor of the present invention Within the scope of shield.Citing described above for best mode for carrying out the invention, wherein the part do not addressed in detail is this area The common knowledge of those of ordinary skill;Protection scope of the present invention is defined by the content of claim, any based on the present invention's Technical inspiration and the equivalent transformation carried out, also within protection scope of the present invention.

Claims (10)

  1. A kind of 1. preparation technology of rich iodine drinking water, it is characterised in that:Described preparation technology includes raw material and prepares, grind, be close Seal and prepare rich iodine drinking water step.
  2. A kind of 2. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:Described raw material prepares: Using following raw material components:Medical stone, zeolite and Potassiumiodate powder.
  3. A kind of 3. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:Described raw material prepares: Also include following raw material components:Lithium carbonate powder, diatomite in powder, wooden fish stone powder, quartz sand powder.
  4. A kind of 4. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:Described raw material prepares: Using the raw material components of following parts by weight:Medical stone 70-75 parts, zeolite 15-16 parts, Potassiumiodate powder 15-17 parts, lithium carbonate Powder 30-32 parts, diatomite in powder 20-22 parts, wooden fish stone powder 30-33 parts, quartz sand powder 20-21 parts.
  5. A kind of 5. preparation technology of rich iodine drinking water according to claim 2, it is characterised in that:
    Described medical stone:Density is 1.3 g/cm3, dioxide-containing silica 70%, alundum (Al2O3) content is 9.8%;
    Described zeolite:Voidage is 50%, density 2.3g/cm3
  6. A kind of 6. preparation technology of rich iodine drinking water according to claim 3, it is characterised in that:
    Described lithium carbonate powder:Purity is 99.9%, and fineness is 150 mesh, relative density 2.11;
    Described diatomite in powder:Fineness is 100 mesh, water absorption rate 60%, density 2.1g/cm3
    Described limonite:Fineness is 200 mesh, density 3g/cm3, porosity 1%;
    Described quartz sand powder:Fineness is 150 mesh, dioxide-containing silica 99.4%, density 2.52g/cm3
  7. A kind of 7. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:
    Described grinding:Medical stone is ground to 150 targeted fine powders, zeolite is ground to 300 targeted fine powders.
  8. A kind of 8. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:
    Described technique also includes preparing lithium addition block;It is described to prepare lithium addition block:
    Lithium carbonate powder, diatomite in powder, wooden fish stone powder and quartz sand powder are well mixed, suitable quantity of water is added, stirs into pasty state;Make Frustillatum, and it is incubated 3 hours under the conditions of 100 DEG C.
  9. A kind of 9. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:
    Described sealing:Potassiumiodate powder, medical stone powder, well mixed be positioned in ceramic vessel of zeolite powder are sealed;Described The micro-pore diameter of ceramic vessel is less than 0.0001mm.
  10. A kind of 10. preparation technology of rich iodine drinking water according to claim 1, it is characterised in that:In described drinking water Content of iodine is 0.2-0.39 mg/L.
CN201710707112.4A 2017-08-17 2017-08-17 Preparation process of iodine-rich drinking water Active CN107434293B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1100616A (en) * 1994-05-26 1995-03-29 卢永鑫 Filter core containing iodine for mineral water pot
CN1715203A (en) * 2005-07-18 2006-01-04 王发 Calcium sulfite water quality duplex ball and manufacturing method thereof
CN103301666A (en) * 2013-07-04 2013-09-18 姚力芝 Multifunctional water purifier
US20150151987A1 (en) * 2010-03-22 2015-06-04 Water Security Corporation, Inc. Water treatment system and filter
CN105622067A (en) * 2016-02-17 2016-06-01 广西大学 Negative-ion water purification ceramic ball and method for preparing same
CN106938872A (en) * 2017-05-15 2017-07-11 福州润君山泉水有限公司 Bag-pack drinking water multistage purification mineralization device
CN107311290A (en) * 2017-08-17 2017-11-03 付全贵 A kind of preparation technology of rich trace elements drinking water

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1100616A (en) * 1994-05-26 1995-03-29 卢永鑫 Filter core containing iodine for mineral water pot
CN1715203A (en) * 2005-07-18 2006-01-04 王发 Calcium sulfite water quality duplex ball and manufacturing method thereof
US20150151987A1 (en) * 2010-03-22 2015-06-04 Water Security Corporation, Inc. Water treatment system and filter
CN103301666A (en) * 2013-07-04 2013-09-18 姚力芝 Multifunctional water purifier
CN105622067A (en) * 2016-02-17 2016-06-01 广西大学 Negative-ion water purification ceramic ball and method for preparing same
CN106938872A (en) * 2017-05-15 2017-07-11 福州润君山泉水有限公司 Bag-pack drinking water multistage purification mineralization device
CN107311290A (en) * 2017-08-17 2017-11-03 付全贵 A kind of preparation technology of rich trace elements drinking water

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* Cited by examiner, † Cited by third party
Title
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龙图天下主编: "《七彩神仙鱼饲养指南》", 31 March 2010, 长春:吉林科学技术出版社 *

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Address after: 261000 north of Beigong East Street and west of Jinma Road, high tech Zone, Weifang City, Shandong Province

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Patentee before: Quan Quan Fu

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